#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:14:57 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180837 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/68/2016845.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016845_Fobs loop_ _publ_author_name 'Che, Guang-Bo' 'Wang, Jian' 'Liu, Chun-Bo' 'Li, Xiu-Ying' 'Liu, Bo' _publ_section_title ; A one-dimensional chain structure based on unusual tetranuclear manganese(II) clusters ; _journal_coeditor_code SK3265 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m362 _journal_page_last m364 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 62.126 _cell_angle_beta 70.552 _cell_angle_gamma 82.238 _cell_length_a 11.9926 _cell_length_b 13.5164 _cell_length_c 14.1957 _exptl_crystal_F_000 888.00 _reflns_d_resolution_high 0.7702 _cod_data_source_file sk3265Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' aa in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 254.87 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1896.18 2049.06 49.06 o 3 0 0 6151.84 6410.15 157.53 o 4 0 0 325.22 299.15 39.52 o 5 0 0 2648.92 2554.69 65.76 o 6 0 0 7525.72 7581.14 196.26 o 7 0 0 594.53 524.82 57.98 o 8 0 0 117.45 123.76 26.92 o 9 0 0 0.11 -14.83 29.71 o 10 0 0 135.21 147.44 31.11 o 11 0 0 259.28 234.38 44.83 o 12 0 0 7.43 7.01 60.74 o 13 0 0 16.75 -31.17 31.17 o 14 0 0 176.13 145.03 48.04 o -14 1 0 8.28 10.72 36.69 o -13 1 0 138.85 119.85 46.07 o -12 1 0 69.87 43.92 29.84 o -11 1 0 157.22 142.81 43.95 o -10 1 0 309.76 371.09 69.36 o -9 1 0 549.33 514.43 61.76 o -8 1 0 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