#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:14:57 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180837 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/68/2016883.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016883_Fobs loop_ _publ_author_name 'Trilleras, Jorge' 'Quiroga, Jairo' 'Cobo, Justo' 'Low, John N.' 'Glidewell, Christopher' _publ_section_title ; Four N^7^-alkoxybenzyl-substituted 4,5,6,7-tetrahydro-1H-pyrazolo[3,4-b]pyridine-5-spiro-1'-cyclohexane-2',6'-diones: hydrogen-bonded supramolecular structures in zero, one, two or three dimensions ; _journal_coeditor_code SK3276 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o665 _journal_page_last o670 _journal_volume 64 _journal_year 2008 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.5770 _cell_length_b 17.4760 _cell_length_c 26.6700 _exptl_crystal_F_000 2539.19 _reflns_d_resolution_high 0.7694 _cod_data_source_file sk3276IVsup5.hkl _cod_data_source_block IV #BEGIN Tags that were not found in dictionaries: _shelx_title ' JTS13' _shelx_refln_list_code 4 _shelx_f_calc_maximum 413.32 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 14082.65 12780.15 492.06 o 6 0 0 23633.55 24759.75 503.95 o 8 0 0 990.55 1059.96 52.90 o 10 0 0 2758.34 2691.84 99.28 o 12 0 0 30.95 51.94 41.82 o 14 0 0 1346.25 1334.38 60.05 o 16 0 0 709.07 677.82 103.15 o 4 1 0 851.94 1164.34 33.66 o 6 1 0 59.62 74.39 53.81 o 8 1 0 2832.63 3106.22 64.45 o 10 1 0 1521.96 1351.55 58.53 o 12 1 0 160.39 256.95 31.50 o 14 1 0 1874.72 1988.39 66.36 o 16 1 0 106.51 220.67 75.74 o 2 2 0 107468.78 93796.74 1374.27 o 4 2 0 49368.19 47321.30 375.42 o 6 2 0 14600.77 13568.94 125.47 o 8 2 0 1002.40 1042.43 29.14 o 10 2 0 210.56 240.57 23.58 o 12 2 0 1026.20 838.61 50.91 o 14 2 0 201.13 195.78 71.59 o 16 2 0 0.23 48.34 52.21 o 2 3 0 22651.95 22599.25 184.64 o 4 3 0 11480.13 12363.01 113.59 o 6 3 0 498.92 965.12 34.87 o 8 3 0 3451.69 3456.08 63.21 o 10 3 0 212.59 294.12 36.89 o 12 3 0 786.04 633.17 53.66 o 14 3 0 1073.25 1094.91 53.00 o 16 3 0 1.42 52.55 76.60 o 0 4 0 38329.38 33970.80 330.95 o 2 4 0 2307.38 1801.60 25.73 o 4 4 0 13147.96 12698.59 146.82 o 6 4 0 4100.11 4015.01 57.58 o 8 4 0 2830.88 2655.17 57.03 o 10 4 0 86.46 176.56 87.30 o 12 4 0 1257.42 1505.73 109.20 o 14 4 0 607.93 536.71 54.50 o 16 4 0 67.78 69.10 58.34 o 2 5 0 3870.23 3978.71 44.98 o 4 5 0 9162.52 8823.70 91.21 o 6 5 0 9363.52 10023.88 107.30 o 8 5 0 4041.39 4239.11 120.30 o 10 5 0 5.14 3.56 73.00 o 12 5 0 282.07 449.46 47.86 o 14 5 0 21.24 88.66 62.13 o 16 5 0 1008.05 950.20 92.98 o 0 6 0 170833.52 166564.81 1805.47 o 2 6 0 936.29 1070.62 21.53 o 4 6 0 4057.88 5161.31 58.73 o 6 6 0 899.35 1235.52 34.58 o 8 6 0 1412.63 1728.71 64.37 o 10 6 0 4070.90 4214.63 107.46 o 12 6 0 445.53 455.11 79.60 o 14 6 0 3.60 15.01 52.61 o 16 6 0 266.72 200.74 121.12 o 2 7 0 2003.38 1848.96 34.14 o 4 7 0 35.24 2.64 10.52 o 6 7 0 5.43 747.81 39.48 o 8 7 0 5447.62 5818.89 104.00 o 10 7 0 612.09 456.17 69.87 o 12 7 0 223.98 181.56 127.27 o 14 7 0 34.08 17.55 63.19 o 16 7 0 6.68 30.04 84.77 o 0 8 0 13986.09 13148.23 184.06 o 2 8 0 232.01 463.55 18.41 o 4 8 0 1572.30 1911.95 31.09 o 6 8 0 18.95 204.34 58.78 o 8 8 0 6294.77 6609.75 115.07 o 10 8 0 4173.98 3887.18 128.33 o 12 8 0 2173.94 2147.02 104.73 o 14 8 0 26.50 169.41 60.74 o 16 8 0 64.90 127.27 68.46 o 2 9 0 1689.32 2237.48 35.39 o 4 9 0 796.34 1266.34 27.50 o 6 9 0 674.32 636.06 39.32 o 8 9 0 12.90 150.99 36.25 o 10 9 0 110.60 376.97 58.88 o 12 9 0 82.02 18.56 77.26 o 14 9 0 62.22 317.78 75.87 o 16 9 0 489.48 507.62 135.03 o 0 10 0 18894.62 18984.76 215.05 o 2 10 0 22.68 34.11 16.00 o 4 10 0 0.02 46.09 38.57 o 6 10 0 386.09 467.78 62.30 o 8 10 0 30.04 98.89 32.06 o 10 10 0 138.34 151.44 54.71 o 12 10 0 1.37 -3.45 61.85 o 14 10 0 158.33 98.24 191.46 o 2 11 0 3515.72 3673.57 57.24 o 4 11 0 429.98 511.39 26.56 o 6 11 0 239.83 276.46 94.67 o 8 11 0 1328.51 1018.40 63.96 o 10 11 0 535.28 802.79 58.97 o 12 11 0 123.43 42.57 53.63 o 14 11 0 3308.40 2939.21 140.13 o 0 12 0 4806.87 6945.20 124.99 o 2 12 0 2275.71 2247.12 46.75 o 4 12 0 2862.60 3193.98 55.84 o 6 12 0 2432.50 2185.68 71.67 o 8 12 0 91.24 48.14 55.41 o 10 12 0 653.91 635.43 52.24 o 12 12 0 16.01 45.77 94.22 o 2 13 0 58.59 83.94 34.43 o 4 13 0 4574.09 4671.29 76.98 o 6 13 0 14035.40 12855.25 242.59 o 8 13 0 114.11 84.53 34.57 o 10 13 0 343.09 343.05 69.95 o 12 13 0 471.44 339.26 71.97 o 14 13 0 347.77 166.33 121.79 o 0 14 0 6712.87 7352.57 135.28 o 2 14 0 1429.53 1385.21 44.57 o 4 14 0 978.72 1175.96 45.88 o 6 14 0 450.21 808.08 61.68 o 8 14 0 597.25 599.76 51.89 o 10 14 0 238.94 195.00 94.13 o 12 14 0 143.04 73.04 92.61 o 2 15 0 1560.74 1409.47 42.62 o 4 15 0 1342.04 1597.10 52.52 o 6 15 0 264.00 473.47 47.15 o 8 15 0 563.05 974.34 80.56 o 10 15 0 1486.68 1729.85 109.74 o 12 15 0 99.16 27.24 72.88 o 0 16 0 43.68 3479.42 149.96 o 2 16 0 1299.20 1252.24 47.85 o 4 16 0 3090.81 2901.19 65.71 o 6 16 0 1595.97 1726.85 73.46 o 8 16 0 1232.84 1298.50 95.19 o 10 16 0 91.41 -106.27 115.21 o 12 16 0 234.63 100.37 107.79 o 2 17 0 44.32 323.24 41.59 o 4 17 0 344.53 567.00 52.66 o 6 17 0 93.48 48.38 47.93 o 8 17 0 501.92 620.54 80.18 o 10 17 0 621.28 663.33 86.95 o 0 18 0 410.03 445.58 75.40 o 2 18 0 0.02 261.51 42.61 o 4 18 0 1459.33 1467.11 91.01 o 6 18 0 16.81 83.88 61.18 o 8 18 0 442.60 531.11 86.23 o 10 18 0 1023.02 988.44 105.01 o 2 19 0 34.30 140.83 53.67 o 4 19 0 285.55 478.12 74.21 o 6 19 0 404.18 328.10 108.63 o 8 19 0 12.26 -40.13 59.78 o 0 20 0 638.30 761.86 74.14 o 2 20 0 146.94 202.82 67.99 o 4 20 0 62.54 -144.73 97.84 o 6 20 0 119.42 104.14 59.85 o 8 20 0 1.08 -12.01 136.38 o 2 21 0 35.85 -15.27 57.23 o 4 21 0 48.49 30.70 96.15 o 6 21 0 494.75 386.57 86.15 o 2 22 0 13.42 76.79 68.65 o 4 22 0 48.91 4.37 61.08 o 2 1 1 5200.79 5336.26 53.91 o 3 1 1 14035.10 13427.23 97.97 o 4 1 1 36405.03 36816.36 249.11 o 5 1 1 14675.19 13900.85 102.72 o 6 1 1 2093.02 2425.42 30.52 o 7 1 1 861.81 1213.10 21.42 o 8 1 1 4037.83 4134.85 47.69 o 9 1 1 971.30 1022.93 28.45 o 10 1 1 3125.41 3177.65 47.61 o 11 1 1 99.37 88.57 17.61 o 12 1 1 107.86 76.88 18.85 o 13 1 1 22.72 29.81 18.79 o 14 1 1 116.86 133.32 30.48 o 15 1 1 150.98 145.15 46.15 o 16 1 1 159.11 159.70 43.58 o 17 1 1 164.96 59.89 45.69 o 1 2 1 13692.57 9454.98 73.28 o 2 2 1 4382.69 3996.75 41.11 o 3 2 1 22005.78 21379.48 129.91 o 4 2 1 27141.79 26819.46 163.90 o 5 2 1 6354.71 6364.47 50.59 o 6 2 1 3697.77 3912.60 46.74 o 7 2 1 1007.05 1177.84 22.92 o 8 2 1 2064.46 2008.01 28.47 o 9 2 1 1741.50 1732.45 32.82 o 10 2 1 21.74 -3.75 15.30 o 11 2 1 44.80 -0.23 15.33 o 12 2 1 1.54 44.37 20.95 o 13 2 1 174.26 166.62 26.76 o 14 2 1 154.62 164.34 28.70 o 15 2 1 53.23 184.80 54.63 o 16 2 1 15.59 14.14 38.28 o 17 2 1 76.46 43.59 47.36 o 1 3 1 14633.11 15909.08 79.90 o 2 3 1 2770.12 3994.09 33.32 o 3 3 1 16.75 341.21 10.25 o 4 3 1 21293.91 21260.91 127.52 o 5 3 1 115.29 72.17 12.50 o 6 3 1 6035.81 6225.62 60.63 o 7 3 1 529.62 779.84 26.44 o 8 3 1 1285.44 1259.60 28.04 o 9 3 1 927.71 1005.03 37.31 o 10 3 1 161.30 211.10 40.12 o 11 3 1 478.19 505.96 36.23 o 12 3 1 210.53 150.78 29.01 o 13 3 1 461.22 597.68 35.51 o 14 3 1 613.74 648.56 39.95 o 15 3 1 48.25 26.22 33.48 o 16 3 1 1116.87 1155.79 66.81 o 17 3 1 117.50 59.85 48.74 o 0 4 1 33560.93 33969.48 232.77 o 1 4 1 24000.27 23710.94 118.14 o 2 4 1 214.95 191.76 8.12 o 3 4 1 13953.80 13666.77 95.31 o 4 4 1 1003.25 1197.30 21.68 o 5 4 1 596.66 648.88 18.60 o 6 4 1 14205.97 15117.49 111.37 o 7 4 1 4900.30 4840.45 49.66 o 8 4 1 522.05 653.51 23.09 o 9 4 1 646.56 641.68 38.12 o 10 4 1 3765.74 3966.32 71.57 o 11 4 1 129.39 144.37 30.23 o 12 4 1 238.11 197.00 37.77 o 13 4 1 137.89 83.93 32.24 o 14 4 1 3.91 37.76 31.18 o 15 4 1 41.62 24.93 31.64 o 16 4 1 7.40 -61.99 41.33 o 17 4 1 113.95 149.42 52.15 o 1 5 1 5343.37 7439.04 44.56 o 2 5 1 3570.21 3708.64 31.24 o 3 5 1 917.72 1025.90 14.54 o 4 5 1 1847.06 2023.29 25.01 o 5 5 1 3925.43 3754.83 38.30 o 6 5 1 4209.28 5061.17 47.85 o 7 5 1 724.07 774.71 24.58 o 8 5 1 1243.50 1638.86 48.66 o 9 5 1 215.13 406.53 34.40 o 10 5 1 35.79 82.74 32.23 o 11 5 1 110.92 182.57 31.91 o 12 5 1 1706.08 1646.92 63.67 o 13 5 1 14.56 130.57 33.75 o 14 5 1 702.04 844.01 45.68 o 15 5 1 9.13 25.66 34.00 o 16 5 1 28.56 138.42 57.61 o 17 5 1 43.53 32.39 59.83 o 0 6 1 29343.89 27630.73 209.18 o 1 6 1 1138.47 1204.04 15.42 o 2 6 1 1766.91 2136.48 20.81 o 3 6 1 569.91 427.17 12.49 o 4 6 1 1212.61 1308.85 21.85 o 5 6 1 98.10 106.75 14.35 o 6 6 1 5072.68 4647.71 46.93 o 7 6 1 468.97 549.25 20.42 o 8 6 1 1434.88 1615.48 41.33 o 9 6 1 747.54 701.03 40.84 o 10 6 1 679.32 759.15 39.58 o 11 6 1 41.99 2.33 31.29 o 12 6 1 405.96 437.85 37.46 o 13 6 1 470.73 489.13 44.02 o 14 6 1 94.81 135.85 36.08 o 15 6 1 9.90 11.73 39.27 o 16 6 1 529.15 607.06 56.71 o 17 6 1 20.97 -12.50 48.42 o 1 7 1 4644.41 4547.26 34.03 o 2 7 1 2044.23 1819.14 20.19 o 3 7 1 75.33 217.18 11.75 o 4 7 1 1072.67 1095.78 17.15 o 5 7 1 8354.43 7948.02 67.10 o 6 7 1 8275.15 8872.93 83.84 o 7 7 1 1009.58 974.07 31.69 o 8 7 1 2493.13 2580.36 51.38 o 9 7 1 416.88 394.80 32.88 o 10 7 1 663.92 785.09 46.33 o 11 7 1 219.67 402.51 55.65 o 12 7 1 204.60 107.03 36.23 o 13 7 1 128.09 201.41 34.90 o 14 7 1 310.51 297.30 46.72 o 15 7 1 124.77 141.30 45.02 o 16 7 1 65.69 -16.08 45.94 o 0 8 1 8781.99 8254.39 80.92 o 1 8 1 16601.98 15562.89 93.84 o 2 8 1 802.91 910.04 15.81 o 3 8 1 354.43 437.29 14.01 o 4 8 1 3494.55 3473.45 33.73 o 5 8 1 474.04 503.13 21.03 o 6 8 1 4200.50 4059.48 44.55 o 7 8 1 3190.36 3291.16 53.35 o 8 8 1 381.44 657.63 41.68 o 9 8 1 5.82 75.70 31.93 o 10 8 1 105.01 503.34 50.28 o 11 8 1 0.11 235.93 67.29 o 12 8 1 1264.03 1426.63 61.22 o 13 8 1 2.38 60.55 36.37 o 14 8 1 558.41 506.21 56.07 o 15 8 1 130.45 72.14 41.30 o 16 8 1 40.32 -24.27 48.47 o 1 9 1 3999.53 4208.95 37.54 o 2 9 1 3052.51 3105.89 30.63 o 3 9 1 1309.67 1354.37 21.74 o 4 9 1 5478.62 5489.24 46.33 o 5 9 1 864.80 832.34 19.63 o 6 9 1 2285.20 2250.65 34.66 o 7 9 1 68.69 43.68 23.00 o 8 9 1 680.75 611.43 36.53 o 9 9 1 373.73 511.57 44.80 o 10 9 1 1590.64 1427.55 50.09 o 11 9 1 8.38 102.28 57.15 o 12 9 1 0.01 61.03 41.62 o 13 9 1 958.33 874.58 57.53 o 14 9 1 749.16 677.47 53.38 o 15 9 1 40.39 84.06 40.90 o 16 9 1 0.06 32.04 51.73 o 0 10 1 4852.02 5373.65 69.15 o 1 10 1 2.49 187.74 14.49 o 2 10 1 0.10 104.09 13.04 o 3 10 1 15.37 37.57 12.93 o 4 10 1 919.84 906.32 22.01 o 5 10 1 12.14 65.52 25.36 o 6 10 1 4262.47 4205.73 47.24 o 7 10 1 1951.22 1833.93 38.05 o 8 10 1 222.81 206.46 24.61 o 9 10 1 2.98 104.66 28.91 o 10 10 1 28.00 104.19 32.49 o 11 10 1 1375.93 1343.94 56.96 o 12 10 1 401.16 323.20 42.49 o 13 10 1 35.97 60.45 47.24 o 14 10 1 302.34 215.10 44.30 o 15 10 1 173.95 45.28 52.53 o 1 11 1 4209.11 4289.42 38.61 o 2 11 1 3911.43 3746.41 41.24 o 3 11 1 1621.02 1554.33 29.08 o 4 11 1 745.78 867.29 23.39 o 5 11 1 1189.52 1315.21 24.75 o 6 11 1 2245.80 2459.86 45.22 o 7 11 1 62.68 199.57 29.49 o 8 11 1 914.65 909.48 35.15 o 9 11 1 3.90 -13.76 25.24 o 10 11 1 3060.29 2806.82 70.74 o 11 11 1 49.06 169.85 40.71 o 12 11 1 18.47 86.37 52.37 o 13 11 1 26.59 53.70 48.17 o 14 11 1 150.94 536.59 123.65 o 15 11 1 68.93 -5.17 66.24 o 0 12 1 12275.18 12256.31 129.82 o 1 12 1 98.39 191.59 17.68 o 2 12 1 160.32 460.04 19.24 o 3 12 1 208.56 210.46 17.21 o 4 12 1 2512.20 2455.68 37.42 o 5 12 1 326.80 394.54 18.75 o 6 12 1 145.54 248.13 52.32 o 7 12 1 850.44 1058.55 30.49 o 8 12 1 70.14 116.11 31.93 o 9 12 1 30.55 1.92 26.58 o 10 12 1 513.90 324.82 40.86 o 11 12 1 0.18 45.68 34.82 o 12 12 1 124.08 -25.27 50.57 o 13 12 1 16.59 -4.81 43.37 o 14 12 1 1678.29 1754.94 84.52 o 1 13 1 126.55 80.67 19.44 o 2 13 1 711.06 619.62 24.17 o 3 13 1 546.30 549.41 21.62 o 4 13 1 270.81 590.77 24.65 o 5 13 1 23.60 110.96 18.31 o 6 13 1 206.60 894.66 52.52 o 7 13 1 525.13 512.10 39.48 o 8 13 1 82.78 40.11 31.20 o 9 13 1 7.21 -25.40 31.16 o 10 13 1 755.64 880.11 57.77 o 11 13 1 578.98 461.61 59.18 o 12 13 1 33.35 95.05 47.88 o 13 13 1 61.06 33.65 54.25 o 14 13 1 361.39 429.21 91.58 o 0 14 1 2588.22 2863.09 56.15 o 1 14 1 965.04 995.69 25.69 o 2 14 1 993.22 1068.17 27.86 o 3 14 1 155.54 213.36 26.06 o 4 14 1 3209.81 3285.75 51.88 o 5 14 1 1.33 32.91 21.60 o 6 14 1 3358.28 3060.49 67.33 o 7 14 1 179.30 219.26 24.99 o 8 14 1 838.58 898.30 40.61 o 9 14 1 141.62 12.93 40.82 o 10 14 1 54.29 52.22 45.55 o 11 14 1 0.42 46.43 40.76 o 12 14 1 265.80 220.69 62.86 o 13 14 1 1.34 144.54 79.72 o 1 15 1 8.42 18.66 12.89 o 2 15 1 51.11 51.69 21.83 o 3 15 1 483.02 458.91 24.73 o 4 15 1 749.04 792.48 32.66 o 5 15 1 48.78 44.97 24.39 o 6 15 1 0.22 45.29 27.51 o 7 15 1 27.81 8.05 34.07 o 8 15 1 1341.97 1438.32 66.08 o 9 15 1 50.98 26.36 43.73 o 10 15 1 714.86 825.15 61.44 o 11 15 1 106.97 98.55 48.42 o 12 15 1 321.06 317.52 208.84 o 13 15 1 42.18 46.08 67.98 o 0 16 1 11884.11 11102.61 144.76 o 1 16 1 67.68 100.24 20.35 o 2 16 1 233.73 583.73 27.26 o 3 16 1 63.99 29.74 26.21 o 4 16 1 892.65 1080.42 38.20 o 5 16 1 0.92 -19.28 28.19 o 6 16 1 171.34 276.51 57.50 o 7 16 1 1.04 -70.55 47.03 o 8 16 1 495.75 537.00 54.33 o 9 16 1 37.45 17.55 42.66 o 10 16 1 4.61 26.31 43.77 o 11 16 1 644.57 625.49 63.48 o 12 16 1 6.89 51.31 58.03 o 1 17 1 572.93 693.11 31.23 o 2 17 1 1360.31 1238.02 35.98 o 3 17 1 98.32 78.84 33.35 o 4 17 1 310.48 213.32 42.45 o 5 17 1 719.50 468.66 49.23 o 6 17 1 7.24 -55.00 36.67 o 7 17 1 57.37 -6.26 38.59 o 8 17 1 0.49 -7.42 65.72 o 9 17 1 226.28 206.23 62.10 o 10 17 1 6.65 31.99 52.07 o 11 17 1 11.90 67.68 58.25 o 0 18 1 141.55 198.06 41.83 o 1 18 1 57.53 44.18 25.00 o 2 18 1 1696.60 1557.95 42.76 o 3 18 1 27.57 21.40 45.82 o 4 18 1 81.33 66.13 78.78 o 5 18 1 75.28 81.66 48.05 o 6 18 1 30.12 15.63 45.07 o 7 18 1 26.15 125.17 44.09 o 8 18 1 258.56 358.85 64.60 o 9 18 1 8.77 51.99 54.88 o 10 18 1 207.46 261.44 69.50 o 1 19 1 241.50 260.69 32.05 o 2 19 1 305.35 227.45 28.99 o 3 19 1 234.33 154.42 37.96 o 4 19 1 335.89 333.11 71.48 o 5 19 1 101.03 88.39 50.08 o 6 19 1 1.21 43.77 48.80 o 7 19 1 45.27 84.60 44.47 o 8 19 1 68.12 41.71 42.14 o 9 19 1 149.15 130.09 80.04 o 0 20 1 183.18 73.73 56.57 o 1 20 1 203.15 265.50 36.10 o 2 20 1 0.51 73.62 36.12 o 3 20 1 33.15 35.13 35.28 o 4 20 1 83.99 66.41 48.28 o 5 20 1 6.66 0.70 41.38 o 6 20 1 75.64 77.51 50.45 o 7 20 1 80.12 46.82 44.42 o 8 20 1 72.81 86.42 59.91 o 1 21 1 5.79 30.41 35.02 o 2 21 1 69.72 110.77 38.50 o 3 21 1 67.91 19.70 42.38 o 4 21 1 101.11 9.93 40.41 o 5 21 1 89.57 118.71 49.41 o 6 21 1 319.61 368.03 80.30 o 0 22 1 91.07 14.97 72.32 o 1 22 1 70.67 62.98 52.03 o 2 22 1 2.86 53.28 47.58 o 3 22 1 121.54 34.12 49.49 o 4 22 1 293.91 281.71 53.90 o 2 0 2 5263.82 4351.84 58.35 o 3 0 2 6845.67 6404.17 56.39 o 4 0 2 40206.68 35419.80 365.21 o 5 0 2 11075.99 10861.26 168.20 o 6 0 2 352.61 439.91 20.78 o 7 0 2 8427.64 8061.98 95.72 o 8 0 2 562.64 566.70 23.49 o 9 0 2 976.04 1088.39 38.24 o 10 0 2 1115.71 1009.20 40.32 o 11 0 2 1580.84 1449.76 46.71 o 12 0 2 2140.08 1770.43 51.70 o 13 0 2 825.87 940.55 39.33 o 14 0 2 112.34 170.70 34.77 o 15 0 2 24.08 86.09 49.82 o 16 0 2 9.36 24.87 72.18 o 17 0 2 1.93 -8.47 56.54 o 2 1 2 5175.16 5560.20 47.72 o 3 1 2 918.61 778.24 16.79 o 4 1 2 20975.32 18951.63 115.56 o 5 1 2 1122.50 1060.40 17.76 o 6 1 2 5312.62 5068.45 45.30 o 7 1 2 3783.75 3715.87 44.25 o 8 1 2 895.35 996.75 25.25 o 9 1 2 73.93 171.57 29.06 o 10 1 2 925.53 894.20 32.80 o 11 1 2 17.91 24.83 31.86 o 12 1 2 129.91 138.18 19.83 o 13 1 2 243.52 328.59 22.95 o 14 1 2 125.75 74.24 27.17 o 15 1 2 14.89 25.67 37.23 o 16 1 2 22.57 59.83 42.62 o 17 1 2 67.27 97.64 62.20 o 1 2 2 32103.31 29017.71 325.76 o 2 2 2 2366.82 2406.53 17.10 o 3 2 2 43875.89 42090.02 235.60 o 4 2 2 23237.74 21390.41 120.78 o 5 2 2 119.39 256.42 12.63 o 6 2 2 1668.64 1870.00 30.40 o 7 2 2 4233.57 3872.54 41.91 o 8 2 2 438.84 424.19 22.50 o 9 2 2 238.72 324.03 24.61 o 10 2 2 852.54 816.01 23.78 o 11 2 2 109.76 111.82 27.78 o 12 2 2 14.91 112.80 22.04 o 13 2 2 333.87 377.93 31.26 o 14 2 2 160.65 288.61 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42.04 o 14 6 2 357.04 395.53 42.50 o 15 6 2 42.00 31.89 46.01 o 16 6 2 207.66 377.78 59.07 o 1 7 2 2552.02 2809.18 25.05 o 2 7 2 513.83 642.20 12.80 o 3 7 2 129.02 196.15 10.61 o 4 7 2 687.55 722.68 15.18 o 5 7 2 740.69 1478.31 26.16 o 6 7 2 327.45 392.28 17.97 o 7 7 2 584.12 714.75 31.65 o 8 7 2 433.34 493.62 37.61 o 9 7 2 49.19 305.94 50.63 o 10 7 2 192.09 122.99 29.45 o 11 7 2 2974.23 2975.27 72.29 o 12 7 2 181.53 97.12 45.25 o 13 7 2 108.14 205.28 41.12 o 14 7 2 153.46 196.58 40.39 o 15 7 2 0.34 53.96 34.32 o 16 7 2 98.86 37.48 55.86 o 0 8 2 774.38 1187.93 24.40 o 1 8 2 584.83 877.27 16.15 o 2 8 2 1533.40 1351.58 18.45 o 3 8 2 257.29 339.77 12.32 o 4 8 2 1080.29 998.45 18.09 o 5 8 2 259.40 340.08 13.44 o 6 8 2 987.65 1051.05 24.64 o 7 8 2 742.85 1144.97 35.08 o 8 8 2 1042.70 985.77 39.05 o 9 8 2 933.56 936.74 42.45 o 10 8 2 2541.80 2456.98 77.50 o 11 8 2 1400.39 1585.46 52.72 o 12 8 2 2128.74 2321.95 70.26 o 13 8 2 183.56 148.72 85.36 o 14 8 2 312.93 305.97 49.45 o 15 8 2 27.52 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609.94 931.61 20.32 o 3 11 2 1157.56 1130.09 25.92 o 4 11 2 1203.58 1139.68 25.95 o 5 11 2 126.64 160.84 18.98 o 6 11 2 2358.26 2429.16 39.77 o 7 11 2 143.56 227.85 19.86 o 8 11 2 98.58 98.25 32.70 o 9 11 2 561.33 392.27 28.86 o 10 11 2 631.11 779.47 57.27 o 11 11 2 401.40 436.44 44.12 o 12 11 2 4.27 -24.75 41.45 o 13 11 2 470.85 409.07 54.00 o 14 11 2 912.62 887.40 68.26 o 15 11 2 0.00 117.90 105.76 o 0 12 2 2312.64 2191.30 46.83 o 1 12 2 111.71 90.79 16.62 o 2 12 2 2382.50 2140.33 32.42 o 3 12 2 38.82 57.55 17.85 o 4 12 2 163.58 343.42 20.45 o 5 12 2 91.65 171.12 20.12 o 6 12 2 119.76 157.40 16.95 o 7 12 2 250.86 312.94 27.85 o 8 12 2 74.01 101.02 25.63 o 9 12 2 0.04 -29.54 26.86 o 10 12 2 6.80 11.14 35.58 o 11 12 2 6.15 6.33 39.77 o 12 12 2 1.12 19.21 37.77 o 13 12 2 90.12 36.68 63.77 o 14 12 2 0.98 37.03 73.59 o 1 13 2 247.46 411.80 20.31 o 2 13 2 2761.79 2718.90 37.49 o 3 13 2 101.06 244.67 18.79 o 4 13 2 1463.93 1450.85 30.72 o 5 13 2 2528.58 2178.55 37.58 o 6 13 2 3168.39 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1 3 3062.23 3103.14 36.91 o 8 1 3 9640.88 9679.28 70.97 o 9 1 3 1847.48 1712.54 32.69 o 10 1 3 3522.75 3471.60 48.67 o 11 1 3 24.39 45.33 22.58 o 12 1 3 1283.18 1286.43 33.06 o 13 1 3 20.84 53.46 20.71 o 14 1 3 2.14 52.53 27.85 o 15 1 3 41.75 44.70 34.22 o 16 1 3 197.76 107.81 48.64 o 17 1 3 276.45 340.60 62.30 o 1 2 3 19627.17 15784.93 320.00 o 2 2 3 2123.86 2429.25 18.42 o 3 2 3 30652.31 27425.86 149.27 o 4 2 3 3028.78 3462.96 27.08 o 5 2 3 3422.68 3601.62 32.16 o 6 2 3 10033.09 10355.44 88.86 o 7 2 3 1050.82 1105.65 20.61 o 8 2 3 4839.14 5078.22 52.75 o 9 2 3 1.03 24.86 23.32 o 10 2 3 2223.65 2300.97 39.31 o 11 2 3 5051.92 5010.98 69.40 o 12 2 3 928.59 824.32 28.00 o 13 2 3 124.06 188.24 32.83 o 14 2 3 237.28 314.23 33.97 o 15 2 3 929.55 916.99 53.91 o 16 2 3 32.98 45.62 37.19 o 17 2 3 10.15 31.76 52.73 o 1 3 3 411.46 448.22 10.49 o 2 3 3 5747.04 5325.84 37.36 o 3 3 3 1495.76 1814.15 20.28 o 4 3 3 7440.47 7113.00 51.73 o 5 3 3 1304.84 1133.08 16.08 o 6 3 3 1499.97 1642.76 22.36 o 7 3 3 204.94 438.29 20.06 o 8 3 3 2023.97 2007.51 29.60 o 9 3 3 803.15 708.59 25.56 o 10 3 3 1091.89 873.87 28.13 o 11 3 3 1938.38 2178.64 47.58 o 12 3 3 227.73 287.05 31.43 o 13 3 3 1192.98 1258.15 44.11 o 14 3 3 236.48 324.88 33.12 o 15 3 3 0.00 -12.13 32.08 o 16 3 3 291.99 481.49 60.95 o 17 3 3 132.04 85.39 52.28 o 0 4 3 106939.82 100520.19 1510.13 o 1 4 3 8.32 210.45 8.28 o 2 4 3 2245.58 2091.42 17.74 o 3 4 3 153.43 270.61 8.54 o 4 4 3 1540.40 1582.48 18.99 o 5 4 3 8598.59 8113.89 73.42 o 6 4 3 8406.69 8480.94 67.21 o 7 4 3 677.35 720.99 20.84 o 8 4 3 137.79 118.86 13.98 o 9 4 3 53.45 293.31 50.78 o 10 4 3 205.24 360.23 24.42 o 11 4 3 1768.95 1853.84 53.30 o 12 4 3 25.88 6.34 25.63 o 13 4 3 257.55 323.98 33.98 o 14 4 3 643.80 641.69 44.44 o 15 4 3 655.05 591.29 45.02 o 16 4 3 318.48 435.54 67.44 o 17 4 3 149.33 86.08 72.90 o 1 5 3 2670.81 3445.25 25.81 o 2 5 3 3422.00 3477.87 26.56 o 3 5 3 2.84 183.10 9.18 o 4 5 3 5676.62 5133.01 40.44 o 5 5 3 0.81 384.99 18.99 o 6 5 3 2040.03 1910.75 28.79 o 7 5 3 1616.29 1646.76 28.35 o 8 5 3 3572.80 3799.56 59.70 o 9 5 3 221.89 393.29 29.78 o 10 5 3 457.91 472.77 32.85 o 11 5 3 703.47 714.00 37.01 o 12 5 3 249.12 250.29 58.15 o 13 5 3 50.88 20.65 45.20 o 14 5 3 0.87 15.79 32.39 o 15 5 3 0.02 -16.83 34.18 o 16 5 3 129.17 133.04 43.91 o 17 5 3 2.77 62.46 48.53 o 0 6 3 2689.14 2739.83 39.47 o 1 6 3 6453.80 6631.98 46.93 o 2 6 3 11784.26 11944.08 72.82 o 3 6 3 886.99 1560.54 18.07 o 4 6 3 2092.14 2120.05 23.67 o 5 6 3 488.97 609.66 16.15 o 6 6 3 92.69 385.38 12.74 o 7 6 3 2.83 17.50 12.91 o 8 6 3 315.08 422.99 30.67 o 9 6 3 468.28 691.97 33.75 o 10 6 3 385.69 315.53 45.32 o 11 6 3 1028.89 1089.36 42.03 o 12 6 3 81.87 382.85 74.93 o 13 6 3 1746.14 1806.00 58.45 o 14 6 3 148.30 231.49 43.48 o 15 6 3 1.79 -5.13 37.06 o 16 6 3 221.64 225.31 65.38 o 1 7 3 1321.46 1032.66 15.37 o 2 7 3 3630.70 3741.98 29.23 o 3 7 3 3933.23 3659.55 32.89 o 4 7 3 574.00 687.17 14.18 o 5 7 3 6067.11 6304.61 49.10 o 6 7 3 23.84 15.31 11.89 o 7 7 3 8.84 69.49 22.72 o 8 7 3 229.75 222.87 46.47 o 9 7 3 2025.18 2089.93 61.24 o 10 7 3 458.81 466.99 35.61 o 11 7 3 619.24 982.85 40.50 o 12 7 3 12.35 85.37 36.70 o 13 7 3 0.56 -14.68 32.69 o 14 7 3 10.86 5.17 43.40 o 15 7 3 80.14 3.22 49.90 o 16 7 3 165.01 102.47 45.11 o 0 8 3 8192.04 6773.16 69.59 o 1 8 3 948.22 1296.45 19.37 o 2 8 3 636.12 966.28 15.84 o 3 8 3 85.12 78.01 12.77 o 4 8 3 141.93 239.81 11.33 o 5 8 3 321.65 312.35 12.89 o 6 8 3 887.55 889.70 20.20 o 7 8 3 666.37 759.79 32.69 o 8 8 3 257.57 208.72 30.29 o 9 8 3 62.28 51.34 33.42 o 10 8 3 136.65 138.62 97.76 o 11 8 3 251.50 307.36 37.54 o 12 8 3 3982.72 4262.78 99.46 o 13 8 3 54.09 7.30 58.19 o 14 8 3 4.76 90.77 47.48 o 15 8 3 1.14 36.10 38.28 o 16 8 3 31.71 122.67 60.47 o 1 9 3 131.38 659.29 14.94 o 2 9 3 3998.53 4353.25 35.01 o 3 9 3 926.50 1015.95 18.48 o 4 9 3 59.96 153.93 14.06 o 5 9 3 231.54 325.94 18.73 o 6 9 3 55.93 35.89 14.06 o 7 9 3 290.41 370.25 19.77 o 8 9 3 922.50 920.47 32.93 o 9 9 3 2474.33 2372.82 59.45 o 10 9 3 574.27 666.15 44.40 o 11 9 3 1966.99 1922.60 70.63 o 12 9 3 668.86 560.90 46.61 o 13 9 3 789.10 658.81 59.25 o 14 9 3 2.85 49.72 38.81 o 15 9 3 52.43 5.40 46.97 o 16 9 3 48.01 39.48 59.42 o 0 10 3 12413.53 12591.00 109.42 o 1 10 3 99.12 161.03 13.13 o 2 10 3 4897.60 4901.05 40.62 o 3 10 3 1717.05 2072.97 26.65 o 4 10 3 551.03 740.79 20.32 o 5 10 3 69.49 201.50 16.99 o 6 10 3 1046.96 1354.86 28.28 o 7 10 3 282.58 341.47 18.92 o 8 10 3 43.50 193.34 29.37 o 9 10 3 86.94 47.96 23.07 o 10 10 3 96.69 120.74 37.34 o 11 10 3 0.77 127.43 39.03 o 12 10 3 569.96 492.93 51.77 o 13 10 3 74.19 323.86 46.29 o 14 10 3 130.34 95.88 47.65 o 15 10 3 289.92 249.69 79.69 o 1 11 3 556.48 561.00 17.25 o 2 11 3 32.00 43.03 18.14 o 3 11 3 218.66 286.90 18.00 o 4 11 3 636.55 674.47 21.94 o 5 11 3 2242.12 2069.06 38.54 o 6 11 3 506.57 536.20 23.28 o 7 11 3 18.06 27.26 15.15 o 8 11 3 1580.28 1622.00 42.25 o 9 11 3 179.13 144.21 30.20 o 10 11 3 1879.16 1599.08 50.77 o 11 11 3 10.92 4.51 52.65 o 12 11 3 18.13 72.01 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8 615.45 511.68 19.81 o 9 6 8 0.01 24.35 19.76 o 10 6 8 2876.37 2737.05 50.65 o 11 6 8 74.56 147.72 32.97 o 12 6 8 14.72 99.45 37.64 o 13 6 8 302.29 312.30 39.12 o 14 6 8 679.12 526.69 52.52 o 15 6 8 15.08 -7.14 63.31 o 16 6 8 1072.30 887.63 72.31 o 1 7 8 328.01 737.65 14.70 o 2 7 8 1288.15 1442.74 19.00 o 3 7 8 4191.33 4324.89 34.80 o 4 7 8 1303.52 1525.35 21.74 o 5 7 8 5.82 39.59 10.87 o 6 7 8 826.85 935.65 15.15 o 7 7 8 1344.29 1389.75 25.99 o 8 7 8 66.55 45.34 15.76 o 9 7 8 285.49 214.53 22.42 o 10 7 8 1091.27 1145.20 33.75 o 11 7 8 316.73 454.88 27.07 o 12 7 8 697.15 700.90 37.48 o 13 7 8 0.90 11.33 36.69 o 14 7 8 97.97 118.03 39.47 o 15 7 8 114.02 104.20 47.49 o 16 7 8 11.54 -25.25 81.64 o 0 8 8 884.77 1025.78 20.38 o 1 8 8 253.96 508.23 13.08 o 2 8 8 539.88 609.39 14.51 o 3 8 8 2727.13 2658.43 29.07 o 4 8 8 3.32 217.71 18.58 o 5 8 8 575.18 613.88 15.43 o 6 8 8 147.97 191.15 10.84 o 7 8 8 1420.86 1372.77 23.58 o 8 8 8 2.72 4.79 16.64 o 9 8 8 1569.68 1404.86 34.99 o 10 8 8 1073.52 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552.34 664.84 15.70 o 3 7 10 114.22 257.88 12.27 o 4 7 10 836.84 806.35 17.10 o 5 7 10 1053.33 1072.51 18.07 o 6 7 10 392.33 422.56 15.48 o 7 7 10 9.23 95.36 24.01 o 8 7 10 572.53 521.62 23.10 o 9 7 10 167.84 299.46 20.51 o 10 7 10 1378.63 1397.22 36.51 o 11 7 10 704.59 742.25 31.71 o 12 7 10 320.99 296.74 38.99 o 13 7 10 17.06 -36.88 35.80 o 14 7 10 60.67 46.15 40.82 o 15 7 10 143.39 90.02 51.25 o 0 8 10 132.08 176.56 14.20 o 1 8 10 6.52 218.47 11.79 o 2 8 10 63.37 81.27 11.47 o 3 8 10 1958.10 1989.75 24.26 o 4 8 10 1832.54 1713.10 22.54 o 5 8 10 1.08 25.13 14.71 o 6 8 10 519.40 578.87 17.11 o 7 8 10 811.59 758.54 20.68 o 8 8 10 242.50 266.85 19.92 o 9 8 10 2793.78 2631.56 57.61 o 10 8 10 107.63 131.00 28.65 o 11 8 10 243.88 239.72 47.45 o 12 8 10 65.28 -16.60 37.72 o 13 8 10 2023.83 2015.34 69.74 o 14 8 10 449.68 450.12 45.35 o 15 8 10 101.38 64.57 44.95 o 1 9 10 497.73 688.71 16.94 o 2 9 10 221.06 233.09 12.80 o 3 9 10 9.06 37.51 12.16 o 4 9 10 137.99 302.97 21.99 o 5 9 10 2946.61 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7 12 215.23 203.02 54.01 o 14 7 12 60.08 34.31 43.65 o 15 7 12 183.93 33.63 132.67 o 0 8 12 3.87 48.72 15.47 o 1 8 12 243.95 344.41 12.43 o 2 8 12 67.56 55.09 13.02 o 3 8 12 1322.81 1237.88 20.42 o 4 8 12 498.59 512.38 16.39 o 5 8 12 83.59 160.82 15.26 o 6 8 12 221.25 280.94 16.48 o 7 8 12 612.31 553.02 25.07 o 8 8 12 469.31 436.05 26.88 o 9 8 12 37.38 113.77 29.90 o 10 8 12 1187.62 1147.73 35.69 o 11 8 12 40.05 43.87 36.37 o 12 8 12 123.81 182.70 40.23 o 13 8 12 315.75 307.74 42.69 o 14 8 12 571.64 649.39 55.90 o 15 8 12 2.47 -40.82 58.39 o 1 9 12 1590.84 1530.36 20.38 o 2 9 12 852.21 871.70 19.23 o 3 9 12 4.09 10.25 12.83 o 4 9 12 261.68 275.73 16.49 o 5 9 12 499.77 621.16 19.73 o 6 9 12 2.02 66.74 19.48 o 7 9 12 993.88 1054.30 35.72 o 8 9 12 903.71 854.82 36.40 o 9 9 12 497.14 458.20 32.34 o 10 9 12 17.44 68.24 26.09 o 11 9 12 824.08 817.18 48.42 o 12 9 12 91.27 88.65 44.04 o 13 9 12 108.24 1.22 40.64 o 14 9 12 5.42 -28.76 50.84 o 15 9 12 355.89 464.90 127.53 o 0 10 12 827.37 692.09 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