#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/68/2016887.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016887_Fobs loop_ _publ_author_name 'Drebushchak, Tatiana N.' 'Chukanov, Nikita V.' 'Boldyreva, Elena V.' _publ_section_title ; Two polymorphs of chlorpropamide: the \d-form and the high-temperature \e-form ; _journal_coeditor_code TR3050 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o623 _journal_page_last o625 _journal_volume 64 _journal_year 2008 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.3198 _cell_length_b 10.3218 _cell_length_c 26.2663 _exptl_crystal_F_000 1152.00 _reflns_d_resolution_high 0.8400 _[local]_cod_data_source_file tr3050d-formsup2.hkl _[local]_cod_data_source_block d-form #BEGIN Tags that were not found in dictionaries: _shelx_title \d-form _shelx_refln_list_code 4 _shelx_F_calc_maximum 339.69 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10963.35 10516.20 114.42 o 4 0 0 2004.77 1619.54 65.00 o 6 0 0 0.58 -13.13 27.24 o 8 0 0 1306.97 1151.34 76.00 o 10 0 0 893.78 676.45 70.70 o 2 1 0 81255.18 87807.11 1404.82 o 4 1 0 4845.75 5067.45 188.18 o 6 1 0 2998.67 3335.59 77.83 o 8 1 0 2026.29 2066.57 66.24 o 10 1 0 64.43 95.24 53.18 o 0 2 0 378.21 292.91 16.47 o 2 2 0 153.81 146.29 22.20 o 4 2 0 302.00 264.05 37.65 o 6 2 0 913.01 885.62 48.42 o 8 2 0 908.95 704.09 45.77 o 10 2 0 105.09 130.60 53.90 o 2 3 0 11450.47 12361.64 176.21 o 6 3 0 2162.46 1861.90 114.14 o 8 3 0 31.65 50.30 40.90 o 10 3 0 410.03 325.76 54.74 o 0 4 0 4558.09 5219.54 304.34 o 2 4 0 502.48 353.41 75.43 o 4 4 0 5788.57 6481.47 347.68 o 6 4 0 220.40 200.85 25.89 o 8 4 0 46.33 63.50 42.30 o 10 4 0 0.16 23.92 36.72 o 2 5 0 681.69 760.69 141.44 o 4 5 0 504.47 607.46 29.45 o 6 5 0 912.85 959.23 86.03 o 8 5 0 605.91 572.83 50.87 o 0 6 0 221.69 166.09 32.09 o 2 6 0 2806.09 2642.33 50.64 o 4 6 0 1715.90 1888.12 49.81 o 6 6 0 43.31 81.25 64.92 o 8 6 0 636.43 715.65 96.88 o 2 7 0 13.04 -1.91 14.28 o 4 7 0 27.16 24.20 21.85 o 6 7 0 464.38 584.86 95.36 o 8 7 0 6.60 13.91 25.39 o 0 8 0 202.85 166.08 24.98 o 2 8 0 100.29 82.41 17.67 o 4 8 0 225.57 199.99 26.35 o 6 8 0 35.31 35.09 46.91 o 8 8 0 0.69 9.34 28.18 o 2 9 0 433.88 402.79 24.95 o 4 9 0 2.79 11.63 24.15 o 6 9 0 172.58 138.61 39.61 o 0 10 0 162.44 148.02 32.52 o 2 10 0 199.90 174.15 28.23 o 4 10 0 216.22 283.00 62.04 o 6 10 0 72.18 36.74 25.42 o 2 11 0 37.17 27.24 25.15 o 4 11 0 14.12 -0.98 24.54 o 2 12 0 105.88 103.78 36.93 o 1 1 1 2148.88 1998.11 33.34 o 2 1 1 388.58 300.82 15.47 o 3 1 1 539.43 696.96 23.01 o 4 1 1 4137.13 3800.12 48.70 o 5 1 1 0.11 6.40 12.52 o 6 1 1 730.25 776.73 25.72 o 7 1 1 1579.92 1636.34 37.93 o 8 1 1 67.50 65.22 19.14 o 9 1 1 37.11 51.29 23.17 o 10 1 1 132.89 188.05 38.50 o 0 2 1 382.35 415.75 30.46 o 1 2 1 10.52 7.66 11.80 o 2 2 1 6801.93 6206.15 107.46 o 3 2 1 1025.12 1054.97 104.29 o 4 2 1 1748.16 1624.73 102.59 o 5 2 1 1003.23 1059.77 33.88 o 6 2 1 25.18 43.04 11.70 o 7 2 1 192.58 188.13 16.15 o 8 2 1 226.72 299.85 25.80 o 9 2 1 484.11 622.65 59.42 o 10 2 1 23.40 63.81 54.16 o 1 3 1 38.20 21.88 5.94 o 2 3 1 3696.81 4016.37 51.59 o 3 3 1 3016.60 4259.97 129.12 o 4 3 1 697.49 861.29 71.48 o 5 3 1 49.32 69.54 12.32 o 6 3 1 13.78 29.81 12.66 o 7 3 1 223.13 209.78 18.57 o 8 3 1 14.77 18.82 28.94 o 9 3 1 89.33 105.14 39.60 o 10 3 1 5.80 0.21 30.84 o 0 4 1 198.65 223.40 20.13 o 1 4 1 7447.37 8687.59 435.61 o 2 4 1 39.91 71.35 42.63 o 3 4 1 2711.02 3354.38 130.02 o 4 4 1 72.46 108.55 12.09 o 5 4 1 22.48 29.13 9.91 o 6 4 1 222.01 277.29 19.45 o 7 4 1 385.86 322.37 26.13 o 8 4 1 280.65 316.51 34.33 o 9 4 1 205.09 279.49 40.37 o 10 4 1 0.41 19.87 27.63 o 1 5 1 265.95 409.06 94.01 o 2 5 1 114.67 139.66 78.62 o 3 5 1 3182.19 3378.79 43.33 o 4 5 1 88.23 73.91 13.23 o 5 5 1 1448.30 1638.71 70.35 o 6 5 1 334.43 365.98 28.07 o 7 5 1 1372.48 1598.96 39.97 o 8 5 1 33.29 41.86 25.89 o 9 5 1 17.81 41.74 30.71 o 10 5 1 10.16 27.85 23.06 o 0 6 1 30.35 15.95 12.40 o 1 6 1 299.56 280.85 11.89 o 2 6 1 19.86 16.81 9.83 o 3 6 1 1.73 8.42 13.70 o 4 6 1 34.11 31.41 14.26 o 5 6 1 936.64 1161.87 38.26 o 6 6 1 1.39 12.62 24.80 o 7 6 1 38.69 58.82 34.99 o 8 6 1 3.44 -7.81 24.23 o 9 6 1 89.26 65.54 37.96 o 1 7 1 85.24 80.13 10.36 o 2 7 1 298.72 288.98 16.08 o 3 7 1 376.90 314.95 21.40 o 4 7 1 83.86 96.75 16.91 o 5 7 1 231.95 273.81 26.24 o 6 7 1 266.08 251.95 71.18 o 7 7 1 24.43 46.10 23.65 o 8 7 1 40.52 15.91 21.50 o 0 8 1 613.59 649.27 24.77 o 1 8 1 21.96 10.21 10.76 o 2 8 1 147.28 142.70 14.18 o 3 8 1 1548.28 1642.33 70.99 o 4 8 1 473.95 484.92 34.10 o 5 8 1 598.68 678.91 59.75 o 6 8 1 142.78 150.87 40.66 o 7 8 1 25.06 50.91 28.97 o 8 8 1 19.85 3.09 21.70 o 1 9 1 396.63 335.43 17.41 o 2 9 1 99.57 108.70 13.53 o 3 9 1 85.34 76.52 19.30 o 4 9 1 54.96 60.42 17.57 o 5 9 1 17.18 25.14 16.74 o 6 9 1 5.52 6.97 24.84 o 7 9 1 1.69 8.84 19.17 o 0 10 1 237.38 284.03 47.56 o 1 10 1 430.87 453.31 18.40 o 2 10 1 34.20 37.50 14.42 o 3 10 1 9.48 7.71 15.76 o 4 10 1 0.78 14.30 14.89 o 5 10 1 3.05 6.72 22.56 o 6 10 1 3.77 15.08 17.88 o 1 11 1 593.81 682.50 20.91 o 2 11 1 145.50 172.86 19.29 o 3 11 1 107.15 112.26 20.17 o 4 11 1 0.91 13.63 16.01 o 1 12 1 204.74 71.98 30.07 o 2 12 1 0.92 -24.15 24.15 o 1 0 2 22206.40 22062.02 579.29 o 2 0 2 1080.46 694.43 20.33 o 3 0 2 547.96 562.65 23.19 o 4 0 2 290.40 258.97 23.17 o 5 0 2 709.65 645.84 23.33 o 6 0 2 1343.41 1392.85 43.49 o 7 0 2 37.06 31.12 21.00 o 8 0 2 703.29 779.97 53.75 o 9 0 2 1704.20 1820.28 157.66 o 10 0 2 47.88 1.05 49.77 o 1 1 2 3933.76 3970.73 141.66 o 2 1 2 1598.03 1448.00 36.60 o 3 1 2 232.95 265.83 15.07 o 4 1 2 2583.22 2858.84 49.74 o 5 1 2 341.97 351.65 18.83 o 6 1 2 2481.10 2666.35 42.67 o 7 1 2 729.52 798.14 28.66 o 8 1 2 148.61 137.50 33.29 o 9 1 2 41.23 55.14 25.22 o 10 1 2 106.34 83.39 37.80 o 0 2 2 2375.05 2430.90 98.32 o 1 2 2 1681.10 1953.73 39.94 o 2 2 2 7606.11 8039.46 205.94 o 3 2 2 246.61 252.01 22.19 o 4 2 2 287.41 346.50 27.95 o 5 2 2 11.45 5.98 12.64 o 6 2 2 8.68 -7.00 11.18 o 7 2 2 2.58 0.94 13.32 o 8 2 2 580.00 544.61 29.80 o 9 2 2 10.46 27.16 38.72 o 10 2 2 10.83 13.57 36.41 o 1 3 2 287.24 437.13 30.23 o 2 3 2 504.56 459.36 15.10 o 3 3 2 762.68 881.85 36.33 o 4 3 2 837.73 813.71 76.52 o 5 3 2 283.47 265.30 14.08 o 6 3 2 268.28 282.55 19.93 o 7 3 2 854.22 960.23 28.14 o 8 3 2 16.09 9.37 26.49 o 9 3 2 71.14 68.12 39.64 o 10 3 2 290.55 320.16 37.78 o 0 4 2 0.05 31.40 16.26 o 1 4 2 914.73 823.62 41.40 o 2 4 2 1794.83 2168.69 445.95 o 3 4 2 15.48 20.78 40.00 o 4 4 2 1935.28 2182.20 35.88 o 5 4 2 2264.66 2758.39 105.99 o 6 4 2 69.03 119.94 22.54 o 7 4 2 205.30 256.90 23.63 o 8 4 2 5.83 -1.88 30.00 o 9 4 2 19.97 27.81 35.23 o 10 4 2 1.99 5.88 28.52 o 1 5 2 99.10 104.44 25.87 o 2 5 2 773.25 797.81 130.59 o 3 5 2 595.46 749.86 23.56 o 4 5 2 0.44 -2.94 11.40 o 5 5 2 53.55 37.93 12.78 o 6 5 2 1548.03 1749.05 120.87 o 7 5 2 13.87 20.49 24.33 o 8 5 2 574.57 575.57 36.18 o 9 5 2 4.14 22.95 28.65 o 10 5 2 1.80 -20.18 32.69 o 0 6 2 762.92 668.35 21.59 o 1 6 2 250.44 185.11 11.51 o 2 6 2 2920.92 2892.16 37.48 o 3 6 2 41.89 34.42 15.28 o 4 6 2 752.77 813.64 26.40 o 5 6 2 425.80 447.22 24.63 o 6 6 2 200.23 242.94 31.07 o 7 6 2 319.34 381.68 40.34 o 8 6 2 348.98 455.30 31.79 o 9 6 2 34.90 58.86 23.23 o 1 7 2 171.90 125.39 11.01 o 2 7 2 747.93 679.09 32.99 o 3 7 2 682.88 715.03 26.55 o 4 7 2 520.55 574.79 23.54 o 5 7 2 146.67 150.56 21.55 o 6 7 2 195.09 228.99 30.92 o 7 7 2 86.29 62.52 50.99 o 8 7 2 51.44 47.49 22.29 o 9 7 2 63.74 54.72 39.05 o 0 8 2 18.75 19.58 15.03 o 1 8 2 0.22 -6.30 11.60 o 2 8 2 73.69 67.21 12.54 o 3 8 2 1.51 5.07 14.10 o 4 8 2 0.23 6.61 16.51 o 5 8 2 0.98 4.21 17.60 o 6 8 2 76.31 57.70 31.92 o 7 8 2 0.38 -21.09 22.19 o 8 8 2 1.10 -10.85 24.04 o 1 9 2 343.43 301.57 16.64 o 2 9 2 356.31 351.75 19.90 o 3 9 2 273.01 251.60 19.93 o 4 9 2 41.44 51.03 17.15 o 5 9 2 87.36 89.77 21.43 o 6 9 2 61.10 49.90 26.10 o 7 9 2 36.04 36.23 19.70 o 0 10 2 270.00 302.50 26.36 o 1 10 2 199.74 176.80 14.57 o 2 10 2 0.83 0.75 14.29 o 3 10 2 452.74 475.32 35.95 o 4 10 2 99.77 121.76 16.74 o 5 10 2 117.86 157.56 31.16 o 6 10 2 50.35 25.95 21.88 o 1 11 2 67.34 50.25 15.09 o 2 11 2 1.65 13.36 15.14 o 3 11 2 13.62 31.92 13.37 o 4 11 2 0.59 14.64 15.60 o 1 12 2 0.83 -21.19 21.19 o 2 12 2 9.27 17.27 25.18 o 1 1 3 26.11 42.97 9.97 o 2 1 3 66074.73 71926.58 931.29 o 3 1 3 3.13 0.41 11.01 o 4 1 3 219.57 208.82 18.92 o 5 1 3 265.43 295.28 17.21 o 6 1 3 1949.38 1791.67 27.09 o 7 1 3 117.93 114.87 17.18 o 8 1 3 918.38 652.72 35.00 o 9 1 3 1.11 -19.92 27.92 o 10 1 3 228.84 253.51 41.59 o 0 2 3 100272.63 65848.66 1132.22 o 1 2 3 4725.14 4877.96 99.29 o 2 2 3 788.52 991.29 22.91 o 3 2 3 210.47 286.88 21.32 o 4 2 3 7400.44 7442.47 90.76 o 5 2 3 5.36 22.33 11.30 o 6 2 3 113.66 74.80 12.64 o 7 2 3 240.94 226.21 16.19 o 8 2 3 721.81 647.18 39.09 o 9 2 3 12.04 -8.01 36.73 o 10 2 3 127.14 137.93 37.42 o 1 3 3 31.78 6.40 11.98 o 2 3 3 183.31 218.01 18.44 o 3 3 3 775.07 818.34 38.04 o 4 3 3 163.65 186.93 68.04 o 5 3 3 5.99 16.99 15.17 o 6 3 3 155.76 186.33 15.96 o 7 3 3 93.21 111.20 16.67 o 8 3 3 101.66 71.45 28.11 o 9 3 3 55.64 48.08 38.03 o 10 3 3 9.93 0.49 30.69 o 0 4 3 16020.65 16355.03 446.28 o 1 4 3 476.05 609.22 39.11 o 2 4 3 5974.00 7835.09 244.55 o 3 4 3 0.04 -33.69 42.47 o 4 4 3 293.70 315.26 15.97 o 5 4 3 33.97 57.58 21.49 o 6 4 3 55.86 52.35 16.76 o 7 4 3 0.08 -6.39 18.95 o 8 4 3 1006.31 995.13 42.57 o 9 4 3 125.85 91.09 34.81 o 10 4 3 3.84 16.02 27.84 o 1 5 3 16.41 50.02 19.87 o 2 5 3 280.38 246.29 73.77 o 3 5 3 306.36 352.51 18.45 o 4 5 3 113.70 130.56 12.79 o 5 5 3 107.72 102.35 13.99 o 6 5 3 2016.77 2294.41 98.48 o 7 5 3 908.51 899.02 40.55 o 8 5 3 4.83 -9.12 27.60 o 9 5 3 11.23 26.18 29.66 o 10 5 3 134.71 104.20 34.13 o 0 6 3 2624.50 2066.46 62.03 o 1 6 3 932.77 804.93 18.03 o 2 6 3 339.42 302.03 18.47 o 3 6 3 128.68 101.54 16.87 o 4 6 3 107.74 95.36 13.52 o 5 6 3 599.60 638.74 34.11 o 6 6 3 32.99 20.69 16.76 o 7 6 3 28.27 22.24 30.14 o 8 6 3 7.42 33.52 24.08 o 9 6 3 94.63 34.62 39.20 o 1 7 3 39.55 34.71 10.60 o 2 7 3 641.92 584.99 23.39 o 3 7 3 105.76 77.81 17.58 o 4 7 3 77.32 97.85 16.78 o 5 7 3 4.63 3.61 18.13 o 6 7 3 729.56 837.82 49.87 o 7 7 3 308.58 355.74 49.50 o 8 7 3 28.83 38.76 20.40 o 9 7 3 18.25 52.37 39.65 o 0 8 3 1.07 2.33 14.53 o 1 8 3 105.71 85.17 12.90 o 2 8 3 150.61 111.79 15.85 o 3 8 3 240.68 259.56 21.05 o 4 8 3 1124.29 1132.69 53.67 o 5 8 3 3.88 9.98 16.62 o 6 8 3 58.13 71.57 31.82 o 7 8 3 6.54 -19.13 20.49 o 8 8 3 128.75 83.80 23.37 o 1 9 3 11.84 19.84 12.25 o 2 9 3 85.27 84.60 15.56 o 3 9 3 5.35 8.12 13.13 o 4 9 3 0.17 -8.46 16.40 o 5 9 3 40.30 57.05 20.30 o 6 9 3 0.07 -15.65 22.58 o 7 9 3 50.58 59.13 24.01 o 0 10 3 20.29 25.52 20.40 o 1 10 3 32.38 31.46 12.75 o 2 10 3 2.99 0.18 13.31 o 3 10 3 29.24 12.81 14.94 o 4 10 3 56.47 33.57 15.16 o 5 10 3 28.16 8.69 16.89 o 6 10 3 4.56 2.12 21.15 o 1 11 3 51.07 65.75 15.24 o 2 11 3 153.95 136.99 19.28 o 3 11 3 21.32 24.86 17.13 o 4 11 3 1.12 7.52 14.56 o 1 12 3 2.56 25.30 15.42 o 2 12 3 1.39 9.21 35.35 o 0 0 4 4056.73 3592.05 68.52 o 2 0 4 2052.36 2000.99 137.78 o 3 0 4 4.29 18.60 23.89 o 4 0 4 9.77 -14.23 35.84 o 5 0 4 1025.53 1134.19 118.31 o 6 0 4 74.40 54.12 18.38 o 7 0 4 635.51 567.31 34.75 o 8 0 4 1444.52 1411.46 56.83 o 9 0 4 690.31 711.56 49.06 o 10 0 4 17.55 -10.28 43.14 o 1 1 4 1015.92 967.61 27.49 o 2 1 4 36.26 28.86 5.49 o 3 1 4 2747.42 2756.11 60.43 o 4 1 4 1089.00 1104.72 31.29 o 5 1 4 533.88 539.80 17.59 o 6 1 4 2.54 13.50 11.02 o 7 1 4 497.60 470.04 21.42 o 8 1 4 20.49 7.33 19.48 o 9 1 4 176.13 176.36 30.69 o 10 1 4 451.67 428.26 61.74 o 0 2 4 70.83 59.07 17.72 o 1 2 4 5253.61 5520.98 91.95 o 2 2 4 7407.23 6968.58 144.25 o 3 2 4 3.69 12.21 9.37 o 4 2 4 97.90 101.97 17.49 o 5 2 4 1103.04 1182.37 25.54 o 6 2 4 153.22 151.40 13.27 o 7 2 4 52.66 64.71 13.72 o 8 2 4 25.80 -20.68 25.42 o 9 2 4 358.64 339.89 31.78 o 10 2 4 14.96 41.72 32.85 o 1 3 4 3517.83 3620.06 159.46 o 2 3 4 184.65 228.82 18.10 o 3 3 4 515.71 522.83 71.59 o 4 3 4 1600.14 1520.12 100.09 o 5 3 4 704.88 736.09 29.66 o 6 3 4 788.35 874.06 26.68 o 7 3 4 1433.00 1477.64 35.42 o 8 3 4 73.64 60.59 26.05 o 9 3 4 16.92 5.46 35.74 o 10 3 4 1.90 1.71 42.17 o 0 4 4 1372.14 1596.14 53.12 o 1 4 4 14.64 45.70 29.53 o 2 4 4 2442.83 2918.29 173.95 o 3 4 4 1722.01 1860.81 70.91 o 4 4 4 177.21 149.92 15.64 o 5 4 4 1896.69 1872.34 41.84 o 6 4 4 49.56 38.12 17.34 o 7 4 4 258.71 297.58 33.44 o 8 4 4 10.95 -1.58 27.62 o 9 4 4 132.01 194.10 45.47 o 10 4 4 0.75 31.41 25.84 o 1 5 4 88.82 84.83 37.02 o 2 5 4 33.45 47.37 13.87 o 3 5 4 9.63 5.26 11.38 o 4 5 4 527.83 652.79 23.73 o 5 5 4 51.26 16.03 15.52 o 6 5 4 85.36 92.71 18.18 o 7 5 4 116.63 106.70 23.31 o 8 5 4 219.40 391.94 89.11 o 9 5 4 67.66 49.18 31.98 o 10 5 4 0.42 14.66 30.50 o 0 6 4 15.80 20.32 17.15 o 1 6 4 2020.59 1764.48 39.00 o 2 6 4 21.41 45.28 14.11 o 3 6 4 112.98 112.63 14.26 o 4 6 4 232.15 231.59 15.90 o 5 6 4 895.13 939.75 34.68 o 6 6 4 165.56 214.58 27.30 o 7 6 4 247.83 283.99 29.17 o 8 6 4 6.40 16.56 23.71 o 9 6 4 102.72 87.25 42.00 o 1 7 4 477.72 416.84 17.90 o 2 7 4 232.64 240.16 18.34 o 3 7 4 992.48 977.49 53.54 o 4 7 4 28.50 22.97 15.20 o 5 7 4 190.12 239.40 21.81 o 6 7 4 7.98 11.23 24.45 o 7 7 4 221.24 260.00 86.97 o 8 7 4 49.34 57.24 20.33 o 0 8 4 1.57 12.83 14.87 o 1 8 4 283.98 247.14 14.73 o 2 8 4 10.39 3.46 13.96 o 3 8 4 195.62 186.34 16.94 o 4 8 4 97.43 79.54 19.62 o 5 8 4 25.03 42.64 22.13 o 6 8 4 17.87 33.29 21.75 o 7 8 4 24.58 27.78 19.47 o 8 8 4 3.09 -4.97 21.81 o 1 9 4 420.32 418.91 17.83 o 2 9 4 393.98 454.59 26.23 o 3 9 4 410.68 365.59 18.16 o 4 9 4 68.34 70.13 21.51 o 5 9 4 217.03 241.35 23.03 o 6 9 4 16.19 27.80 29.22 o 7 9 4 76.50 63.77 22.62 o 0 10 4 390.44 422.47 28.70 o 1 10 4 290.75 302.16 22.69 o 2 10 4 0.57 -12.36 15.19 o 3 10 4 478.92 541.46 41.25 o 4 10 4 33.88 18.69 16.93 o 5 10 4 176.38 200.62 33.90 o 6 10 4 21.83 45.80 20.56 o 1 11 4 33.54 32.09 15.00 o 2 11 4 18.13 18.89 12.67 o 3 11 4 3.38 0.17 16.20 o 4 11 4 0.85 5.14 14.14 o 1 12 4 39.24 35.66 22.10 o 1 1 5 2046.69 2240.85 59.08 o 2 1 5 2.68 3.14 10.51 o 3 1 5 322.46 377.69 27.33 o 4 1 5 5452.47 5490.27 150.80 o 5 1 5 46.10 50.99 10.54 o 6 1 5 2177.00 2433.40 34.80 o 7 1 5 1130.97 1162.12 30.52 o 8 1 5 254.19 332.60 26.09 o 9 1 5 3.09 14.13 25.56 o 10 1 5 53.89 96.57 48.18 o 0 2 5 8038.01 7867.81 373.37 o 1 2 5 7047.69 6603.05 107.30 o 2 2 5 511.10 512.41 12.00 o 3 2 5 31.69 42.61 10.32 o 4 2 5 140.49 132.60 31.40 o 5 2 5 762.03 870.91 20.59 o 6 2 5 905.96 961.45 22.16 o 7 2 5 84.21 91.49 15.55 o 8 2 5 492.26 573.39 34.54 o 9 2 5 263.46 318.84 31.55 o 10 2 5 37.16 40.29 47.99 o 1 3 5 99.85 99.93 15.56 o 2 3 5 634.39 772.76 45.69 o 3 3 5 4756.44 5243.51 162.64 o 4 3 5 38.15 -9.61 20.04 o 5 3 5 649.18 710.77 23.11 o 6 3 5 34.10 20.74 15.59 o 7 3 5 334.05 322.54 23.36 o 8 3 5 356.38 386.76 36.71 o 9 3 5 55.53 73.70 34.43 o 10 3 5 87.36 67.94 45.46 o 0 4 5 924.03 943.43 68.28 o 1 4 5 1291.43 1440.20 38.64 o 2 4 5 114.76 213.92 39.33 o 3 4 5 81.76 50.98 41.46 o 4 4 5 567.98 622.32 20.47 o 5 4 5 170.73 183.04 16.89 o 6 4 5 205.01 229.99 19.72 o 7 4 5 109.22 116.22 21.60 o 8 4 5 955.68 1033.71 39.10 o 9 4 5 7.43 5.02 33.25 o 10 4 5 66.67 28.25 43.80 o 1 5 5 0.33 -30.14 30.14 o 2 5 5 3119.07 3180.10 228.20 o 3 5 5 638.32 527.49 18.19 o 4 5 5 503.64 595.75 18.37 o 5 5 5 247.19 323.59 35.92 o 6 5 5 1010.15 1101.43 32.63 o 7 5 5 134.67 125.08 22.80 o 8 5 5 111.62 121.65 31.55 o 9 5 5 69.07 36.22 28.88 o 0 6 5 1191.09 1095.59 34.42 o 1 6 5 162.57 143.76 11.91 o 2 6 5 48.75 39.31 12.99 o 3 6 5 312.55 350.32 17.66 o 4 6 5 807.53 900.69 30.09 o 5 6 5 0.02 -16.82 16.82 o 6 6 5 200.14 233.15 27.20 o 7 6 5 20.65 31.68 24.95 o 8 6 5 4.09 -5.09 30.05 o 9 6 5 0.91 -1.16 37.50 o 1 7 5 155.83 122.79 12.89 o 2 7 5 3.70 17.23 15.80 o 3 7 5 146.74 136.21 15.76 o 4 7 5 71.70 65.86 14.45 o 5 7 5 277.96 317.03 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24 0.53 -6.66 17.62 o 5 4 24 155.03 153.92 19.42 o 1 5 24 0.58 5.52 15.68 o 2 5 24 2.28 1.00 18.88 o 3 5 24 53.33 34.54 17.73 o 4 5 24 11.48 19.46 17.03 o 5 5 24 12.99 17.08 14.66 o 0 6 24 130.80 153.20 28.48 o 1 6 24 69.23 66.70 17.86 o 2 6 24 4.31 5.63 16.18 o 3 6 24 45.72 66.95 17.13 o 4 6 24 9.82 -0.22 18.92 o 1 7 24 89.03 126.57 16.84 o 2 7 24 7.78 58.77 20.98 o 3 7 24 142.18 164.39 22.98 o 1 1 25 121.09 107.38 15.44 o 2 1 25 718.24 731.93 55.02 o 3 1 25 86.41 80.57 21.17 o 4 1 25 1.88 2.77 19.51 o 5 1 25 93.79 147.47 27.46 o 6 1 25 151.38 150.69 21.63 o 0 2 25 1142.40 1274.22 56.42 o 1 2 25 0.33 1.85 17.53 o 2 2 25 10.28 2.25 18.38 o 3 2 25 0.32 -23.77 24.13 o 4 2 25 242.80 256.44 30.79 o 5 2 25 55.34 54.56 21.89 o 6 2 25 9.11 18.78 24.76 o 1 3 25 122.99 107.28 15.22 o 2 3 25 4.50 12.67 13.73 o 3 3 25 8.38 27.36 15.06 o 4 3 25 80.65 83.60 19.29 o 5 3 25 6.82 10.23 27.43 o 0 4 25 35.68 54.45 19.58 o 1 4 25 89.66 83.90 13.78 o 2 4 25 0.42 10.97 13.01 o 3 4 25 3.78 5.09 16.99 o 4 4 25 331.58 320.61 21.26 o 5 4 25 1.89 12.72 20.43 o 1 5 25 16.43 24.16 13.95 o 2 5 25 199.22 221.83 20.66 o 3 5 25 3.60 10.02 15.64 o 4 5 25 16.34 15.03 15.57 o 0 6 25 93.41 113.01 22.79 o 1 6 25 7.55 8.10 16.42 o 2 6 25 0.94 9.77 14.40 o 3 6 25 7.65 5.62 13.84 o 0 0 26 49.06 41.65 26.70 o 1 0 26 133.50 130.99 20.32 o 2 0 26 117.88 89.55 26.75 o 3 0 26 23.64 25.61 27.68 o 4 0 26 133.39 123.29 27.62 o 5 0 26 265.07 361.39 37.42 o 1 1 26 0.75 2.81 17.45 o 2 1 26 57.31 49.50 15.14 o 3 1 26 75.75 84.24 19.69 o 4 1 26 5.27 11.75 18.09 o 5 1 26 8.45 9.65 27.70 o 0 2 26 10.81 -15.34 26.51 o 1 2 26 353.70 361.46 35.61 o 2 2 26 120.77 117.98 17.98 o 3 2 26 0.53 1.52 21.27 o 4 2 26 2.47 -11.30 30.65 o 5 2 26 3.69 -10.10 25.02 o 1 3 26 192.99 172.16 17.24 o 2 3 26 125.36 120.37 17.64 o 3 3 26 190.27 193.10 27.36 o 4 3 26 1.93 17.33 26.78 o 5 3 26 17.89 31.26 22.89 o 0 4 26 15.75 14.09 14.40 o 1 4 26 0.49 -0.89 10.89 o 2 4 26 0.87 -2.06 13.64 o 3 4 26 41.67 58.03 16.48 o 4 4 26 81.41 94.40 24.61 o 1 5 26 53.33 77.27 13.96 o 2 5 26 8.04 18.62 15.30 o 3 5 26 84.67 117.44 27.39 o 0 6 26 162.90 150.85 45.24 o 1 6 26 129.93 129.66 27.69 o 2 6 26 61.23 54.03 34.94 o 1 1 27 9.97 19.46 15.88 o 2 1 27 51.38 34.66 19.91 o 3 1 27 2.36 12.88 16.52 o 4 1 27 0.51 -0.79 18.38 o 5 1 27 15.37 23.37 25.67 o 0 2 27 100.61 67.85 22.04 o 1 2 27 17.47 -1.25 14.89 o 2 2 27 2.23 8.88 19.77 o 3 2 27 4.69 17.46 21.87 o 4 2 27 41.99 49.52 26.12 o 5 2 27 68.09 104.06 23.16 o 1 3 27 7.22 12.13 14.86 o 2 3 27 5.35 -1.82 17.90 o 3 3 27 74.56 37.76 18.01 o 4 3 27 26.52 71.14 23.06 o 0 4 27 159.53 134.01 25.16 o 1 4 27 1.37 4.53 14.14 o 2 4 27 56.60 30.65 16.66 o 3 4 27 197.30 240.97 25.07 o 4 4 27 68.06 76.33 20.12 o 1 5 27 128.30 117.11 20.93 o 2 5 27 165.65 155.97 22.19 o 0 0 28 192.36 136.32 45.46 o 1 0 28 47.35 22.32 21.40 o 2 0 28 9.71 24.06 21.77 o 3 0 28 1.38 -4.84 20.25 o 4 0 28 331.23 391.30 31.43 o 1 1 28 27.23 38.63 15.14 o 2 1 28 42.97 66.66 20.77 o 3 1 28 0.03 10.71 16.69 o 0 2 28 46.84 30.91 17.51 o 1 2 28 150.00 144.71 16.32 o 2 2 28 9.24 7.86 16.93 o 3 2 28 10.46 10.14 16.87 o 4 2 28 22.86 11.35 21.80 o 1 3 28 35.16 39.72 11.65 o 2 3 28 181.97 145.70 26.70 o 3 3 28 2.74 0.46 20.48 o 0 4 28 41.26 33.49 24.19 o 1 4 28 33.00 68.29 24.13 o 2 4 28 4.69 9.56 18.83 o 3 4 28 4.80 -0.15 19.50 o 1 5 28 6.14 21.21 17.92 o 1 1 29 43.58 33.25 11.77 o 2 1 29 1.64 0.03 15.90 o 3 1 29 177.38 178.80 40.64 o 0 2 29 2.45 -2.20 16.23 o 1 2 29 2.33 4.09 11.09 o 2 2 29 27.29 16.53 15.23 o 3 2 29 31.09 53.95 20.67 o 1 3 29 51.29 27.00 12.14 o 2 3 29 1.02 -5.12 14.12 o 0 4 29 11.01 30.77 18.00 o 1 4 29 346.65 377.29 25.62 o 0 0 30 619.35 430.93 45.51 o 1 0 30 33.95 12.08 22.18 o 2 0 30 57.31 55.91 32.76 o 1 1 30 3.54 -5.83 15.21 o 2 1 30 96.14 46.29 18.63 o 0 2 30 65.03 27.16 22.31 o 1 2 30 3.36 -1.36 16.22 o 2 2 30 0.51 11.08 19.86 o