#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/69/2016923.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016923_Fobs loop_ _publ_author_name 'Lipstman, Sophia' 'Goldberg, Israel' _publ_section_title ; Hydrogen-bonded assemblies of 5,10,15,20-tetrakis(4-hydroxyphenyl)porphyrin with dimethylformamide, dimethylacetamide and water ; _journal_coeditor_code GD3260 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o3 _journal_page_last o7 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 101.744 _cell_angle_beta 92.479 _cell_angle_gamma 114.916 _cell_length_a 13.6255 _cell_length_b 16.0184 _cell_length_c 26.2466 _exptl_crystal_F_000 2056.00 _reflns_d_resolution_high 0.7602 _[local]_cod_data_source_file gd3260Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Compound so99 (symmetry P-1)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 333.64 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 23.63 23.54 2.83 o 3 0 0 6397.78 6117.46 88.84 o 4 0 0 3044.36 2978.25 46.92 o 5 0 0 1907.19 1701.46 30.40 o 6 0 0 223.07 238.49 9.47 o 7 0 0 317.43 272.33 12.16 o 8 0 0 14.33 13.24 8.27 o 9 0 0 61.83 54.53 10.89 o 10 0 0 8.73 -0.47 12.32 o 11 0 0 343.64 318.19 21.92 o 12 0 0 5.52 30.21 29.69 o 13 0 0 1.75 11.31 34.17 o 14 0 0 7.28 11.50 55.10 o 15 0 0 1.74 -68.98 70.37 o 16 0 0 52.36 104.54 63.09 o -16 1 0 17.13 47.51 75.34 o -15 1 0 133.25 186.24 68.29 o -14 1 0 2.18 -68.98 54.32 o 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15.22 o -6 3 0 3282.02 3032.13 67.63 o -5 3 0 1844.40 1769.23 42.61 o -4 3 0 19871.72 18353.24 440.89 o -3 3 0 3158.75 2695.44 73.31 o -2 3 0 2336.21 2070.33 46.09 o -1 3 0 20288.09 17303.90 286.75 o 0 3 0 95597.66 95768.23 3002.41 o 1 3 0 1528.09 1625.08 32.19 o 2 3 0 570.76 529.53 12.73 o 3 3 0 0.46 35.30 5.66 o 4 3 0 11601.46 12710.09 183.46 o 5 3 0 282.27 295.09 12.65 o 6 3 0 354.41 389.12 15.74 o 7 3 0 2390.61 2621.04 61.29 o 8 3 0 188.55 196.00 20.20 o 9 3 0 435.80 461.89 29.03 o 10 3 0 79.15 52.95 18.31 o 11 3 0 95.96 90.30 27.71 o 12 3 0 461.74 394.59 48.19 o 13 3 0 294.87 185.42 67.30 o 14 3 0 10.99 -31.74 61.93 o -17 4 0 263.77 461.23 110.12 o -16 4 0 84.33 16.31 67.19 o -15 4 0 17.65 6.81 59.76 o -14 4 0 602.56 686.66 80.45 o -13 4 0 12.08 51.40 41.38 o -12 4 0 82.55 61.53 14.94 o -11 4 0 163.03 202.08 18.33 o -10 4 0 100.39 60.82 12.21 o -9 4 0 754.97 840.01 25.80 o -8 4 0 2452.68 2698.65 60.61 o -7 4 0 674.89 582.36 21.49 o -6 4 0 879.70 1237.99 32.40 o -5 4 0 451.22 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o 2 6 0 241.57 226.80 12.94 o 3 6 0 424.82 495.47 19.14 o 4 6 0 1027.77 1191.96 32.85 o 5 6 0 103.02 95.91 14.73 o 6 6 0 139.31 142.27 17.93 o 7 6 0 293.84 254.89 24.01 o 8 6 0 2.33 5.66 16.52 o 9 6 0 115.98 104.54 27.93 o 10 6 0 134.86 109.60 36.64 o 11 6 0 147.53 159.61 36.08 o 12 6 0 2.89 -24.74 29.62 o 13 6 0 124.74 129.05 41.85 o -17 7 0 422.11 271.31 89.50 o -15 7 0 122.17 71.81 58.80 o -14 7 0 403.70 245.18 49.04 o -13 7 0 78.48 72.84 45.34 o -12 7 0 689.29 658.01 35.44 o -11 7 0 80.28 51.40 15.84 o -10 7 0 113.53 155.37 17.98 o -9 7 0 344.43 351.32 19.56 o -8 7 0 4053.58 4264.60 124.31 o -7 7 0 5081.69 5319.29 150.02 o -6 7 0 799.56 831.14 28.33 o -5 7 0 9253.13 10057.94 206.30 o -4 7 0 3913.70 4329.00 94.95 o -3 7 0 575.32 679.45 17.60 o -2 7 0 7278.61 6958.62 143.42 o -1 7 0 947.19 763.53 28.00 o 0 7 0 2235.55 2472.32 67.16 o 1 7 0 229.97 247.58 11.12 o 2 7 0 698.11 669.08 21.44 o 3 7 0 1846.11 1996.95 46.64 o 4 7 0 1605.87 1792.56 49.39 o 5 7 0 492.53 543.03 28.61 o 6 7 0 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