#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/69/2016925.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016925_Fobs loop_ _publ_author_name 'Lipstman, Sophia' 'Goldberg, Israel' _publ_section_title ; Hydrogen-bonded assemblies of 5,10,15,20-tetrakis(4-hydroxyphenyl)porphyrin with dimethylformamide, dimethylacetamide and water ; _journal_coeditor_code GD3260 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o3 _journal_page_last o7 _journal_volume 65 _journal_year 2009 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.271 _cell_angle_gamma 90.000 _cell_length_a 35.5243 _cell_length_b 6.5265 _cell_length_c 29.2172 _exptl_crystal_F_000 2648.00 _reflns_d_resolution_high 0.8255 _[local]_cod_data_source_file gd3260IIIsup4.hkl _[local]_cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' Compound so97 (symmetry C2/c)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 395.08 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 12439.05 10436.13 200.63 o 8 0 0 36660.40 32878.00 571.09 o 10 0 0 92491.64 85362.96 1667.22 o 12 0 0 102.22 204.57 22.79 o 14 0 0 2918.28 3076.86 74.00 o 16 0 0 9628.21 9331.43 193.28 o 18 0 0 19185.81 18882.64 366.59 o 20 0 0 768.33 658.42 32.33 o 22 0 0 10851.69 10341.71 222.32 o 24 0 0 4550.38 4618.11 141.01 o 26 0 0 30.92 80.08 39.13 o 28 0 0 3156.19 3157.56 135.34 o 30 0 0 4022.34 3988.97 180.20 o 32 0 0 1157.56 1162.10 131.36 o 34 0 0 2263.91 2441.48 298.42 o 36 0 0 79.38 206.15 113.85 o 38 0 0 408.35 374.10 112.52 o 40 0 0 197.19 302.64 101.84 o 42 0 0 1079.82 1119.53 185.97 o 3 1 0 69.55 126.90 17.95 o 5 1 0 16424.11 16266.28 269.38 o 7 1 0 83141.71 81658.27 1217.67 o 9 1 0 38443.82 37075.60 492.28 o 11 1 0 1921.83 1614.84 31.27 o 13 1 0 21287.92 20019.44 262.14 o 15 1 0 5232.10 5418.04 81.83 o 17 1 0 12352.23 13614.80 190.23 o 19 1 0 0.86 23.75 14.07 o 21 1 0 6.39 30.27 14.07 o 23 1 0 805.40 751.85 28.46 o 25 1 0 830.21 924.33 38.31 o 27 1 0 43.48 65.25 23.65 o 29 1 0 1175.11 1264.04 60.58 o 31 1 0 7.25 48.02 51.11 o 33 1 0 278.21 375.55 68.20 o 35 1 0 75.46 134.93 53.82 o 37 1 0 1457.19 1815.77 124.74 o 39 1 0 168.04 120.31 60.14 o 41 1 0 38.10 108.81 78.09 o 0 2 0 21141.97 22039.24 577.58 o 2 2 0 7702.37 7244.15 154.53 o 4 2 0 2742.21 2807.62 80.49 o 6 2 0 48044.23 46123.58 923.09 o 8 2 0 26.30 19.29 21.62 o 10 2 0 7057.99 6956.92 148.35 o 12 2 0 819.64 644.24 27.29 o 14 2 0 34883.64 38516.27 567.21 o 16 2 0 8.78 7.52 12.29 o 18 2 0 3961.51 3960.93 83.96 o 20 2 0 734.03 847.13 30.21 o 22 2 0 1166.42 1393.65 42.87 o 24 2 0 1627.42 1637.25 71.98 o 26 2 0 773.53 969.95 54.23 o 28 2 0 2.18 101.19 41.02 o 30 2 0 236.81 303.94 57.49 o 32 2 0 5.35 157.31 61.34 o 34 2 0 42.27 79.74 66.83 o 36 2 0 817.96 548.40 72.01 o 38 2 0 42.19 88.21 55.67 o 40 2 0 301.99 355.02 111.01 o 1 3 0 265.85 167.23 23.48 o 3 3 0 133.84 201.42 27.36 o 5 3 0 6262.84 6675.49 130.19 o 7 3 0 10425.10 12768.01 293.10 o 9 3 0 90.33 126.90 40.06 o 11 3 0 234.45 369.13 37.00 o 13 3 0 68.80 36.49 31.99 o 15 3 0 364.43 360.61 27.43 o 17 3 0 2107.77 2599.58 83.13 o 19 3 0 0.98 26.70 13.42 o 21 3 0 39.74 70.74 43.01 o 23 3 0 4350.86 3905.15 162.08 o 25 3 0 171.64 21.62 57.39 o 27 3 0 216.14 157.79 40.95 o 29 3 0 7.03 23.03 36.45 o 31 3 0 26.81 21.62 51.18 o 33 3 0 244.56 224.65 96.62 o 35 3 0 68.59 289.91 179.17 o 37 3 0 265.47 134.07 148.01 o 0 4 0 8843.90 8495.56 290.32 o 2 4 0 7166.10 7737.98 179.28 o 4 4 0 1286.17 1589.61 69.44 o 6 4 0 357.04 271.89 32.99 o 8 4 0 4.22 0.34 32.30 o 10 4 0 118.80 228.57 60.51 o 12 4 0 5058.99 5505.67 151.23 o 14 4 0 2.53 34.29 26.46 o 16 4 0 8801.62 8945.35 231.31 o 18 4 0 72.55 92.47 22.11 o 20 4 0 116.07 197.23 20.29 o 22 4 0 1688.51 2005.21 225.65 o 24 4 0 52.79 -50.87 134.52 o 26 4 0 20.91 123.16 210.55 o 28 4 0 3.85 -57.43 159.47 o 30 4 0 64.79 355.71 162.84 o 32 4 0 316.26 272.50 176.77 o 34 4 0 11.84 -23.38 172.55 o 36 4 0 341.00 393.70 194.83 o 1 5 0 299.56 445.29 54.75 o 3 5 0 2676.95 2906.65 127.86 o 5 5 0 6468.92 6941.47 231.55 o 7 5 0 349.13 434.41 51.76 o 9 5 0 5880.42 5767.16 180.10 o 11 5 0 12558.03 12969.78 333.36 o 13 5 0 668.15 684.33 44.59 o 15 5 0 1397.98 1160.83 71.94 o 17 5 0 115.03 235.33 130.16 o 19 5 0 30.57 176.94 146.39 o 21 5 0 607.86 695.04 159.23 o 23 5 0 365.35 648.94 159.54 o 25 5 0 97.35 154.08 222.63 o 27 5 0 216.84 191.53 113.85 o 29 5 0 790.78 635.80 148.56 o 31 5 0 301.41 307.82 155.39 o 0 6 0 228.50 198.26 99.64 o 2 6 0 366.34 410.80 60.82 o 4 6 0 7967.85 6990.97 316.03 o 6 6 0 328.31 305.87 60.93 o 8 6 0 1284.34 1157.05 86.98 o 10 6 0 3.50 26.33 59.31 o 12 6 0 216.42 175.98 66.35 o 14 6 0 1479.33 1351.12 93.98 o 16 6 0 47.20 -41.09 63.67 o 18 6 0 90.42 137.99 95.32 o 20 6 0 15.99 20.94 109.87 o 22 6 0 3.78 220.23 144.61 o 24 6 0 22.61 75.82 181.34 o 26 6 0 11.68 189.99 184.91 o 1 7 0 7.26 145.91 73.87 o 3 7 0 690.48 751.85 98.55 o 5 7 0 946.18 898.59 107.75 o 7 7 0 249.45 143.68 67.52 o 9 7 0 111.71 176.94 81.32 o 11 7 0 34.51 219.68 160.91 o 13 7 0 343.45 436.75 140.94 o 15 7 0 94.39 98.99 175.47 o 17 7 0 51.21 303.29 187.14 o 19 7 0 491.90 508.38 222.22 o -41 1 1 176.31 187.96 80.25 o -39 1 1 453.05 512.57 82.21 o -37 1 1 0.02 -12.01 54.16 o -35 1 1 476.25 495.92 65.18 o -33 1 1 284.90 154.53 52.96 o -31 1 1 861.67 960.71 79.26 o -29 1 1 11889.72 12070.23 309.40 o -27 1 1 574.50 654.64 30.34 o -25 1 1 716.20 709.77 30.62 o -23 1 1 104.17 185.42 18.67 o -21 1 1 788.97 1027.30 29.69 o -19 1 1 2689.98 2595.80 50.97 o -17 1 1 318.78 374.83 17.92 o -15 1 1 5946.79 5761.53 87.18 o -13 1 1 479.84 525.24 16.99 o -11 1 1 64.29 179.93 13.42 o -9 1 1 9909.55 8976.93 136.92 o -7 1 1 7224.93 7127.93 109.50 o -5 1 1 8636.07 8064.03 143.07 o -3 1 1 94200.58 85612.13 1409.44 o -1 1 1 6232.20 5355.50 97.62 o 1 1 1 15468.84 14417.52 302.54 o 3 1 1 8244.64 6904.47 157.04 o 7 1 1 103432.70 98964.96 1876.73 o 9 1 1 25994.83 25759.82 374.65 o 11 1 1 6831.62 7124.80 106.34 o 13 1 1 433.46 461.08 15.93 o 15 1 1 23953.78 24300.27 329.24 o 17 1 1 463.64 493.45 19.77 o 19 1 1 2064.95 1839.53 47.68 o 21 1 1 49.76 15.14 14.42 o 23 1 1 2563.86 2359.79 66.59 o 25 1 1 0.01 28.08 22.59 o 27 1 1 7892.90 8160.82 200.83 o 29 1 1 4617.19 4706.66 142.34 o 31 1 1 0.59 27.87 50.49 o 33 1 1 0.03 12.01 49.81 o 35 1 1 1037.28 1493.60 114.58 o 37 1 1 1933.31 1452.34 122.85 o 39 1 1 20.21 -16.17 71.81 o 41 1 1 1228.73 1372.99 135.93 o -40 2 1 195.42 407.06 186.90 o -38 2 1 114.72 141.04 134.66 o -36 2 1 154.98 155.46 59.59 o -34 2 1 3.04 -19.29 45.07 o -32 2 1 349.90 258.60 48.26 o -30 2 1 278.53 272.50 48.95 o -28 2 1 167.47 182.92 34.08 o -26 2 1 3203.70 2999.25 81.18 o -24 2 1 1292.16 1178.57 41.98 o -22 2 1 1979.41 1598.50 48.88 o -20 2 1 893.49 1299.84 40.09 o -18 2 1 13128.16 12659.38 212.61 o -16 2 1 3266.32 3438.37 65.18 o -14 2 1 274.12 258.02 22.62 o -12 2 1 76.49 83.75 15.27 o -10 2 1 18.71 38.75 19.60 o -8 2 1 11887.50 11293.39 196.89 o -6 2 1 2060.08 1697.77 67.17 o -4 2 1 1454.44 1506.51 48.91 o -2 2 1 8.12 138.84 31.44 o 0 2 1 2962.07 2307.85 58.73 o 2 2 1 21272.13 19240.75 411.17 o 4 2 1 21985.40 24184.87 432.18 o 6 2 1 15299.56 15106.28 286.92 o 8 2 1 6245.51 6907.56 144.75 o 10 2 1 4560.05 4873.35 111.21 o 12 2 1 39566.57 42367.64 663.53 o 14 2 1 40048.81 43442.13 617.84 o 16 2 1 4.99 -7.93 21.69 o 18 2 1 2426.90 2368.78 73.94 o 20 2 1 427.24 357.11 36.42 o 22 2 1 3010.88 3517.04 109.87 o 24 2 1 1092.34 975.71 55.57 o 26 2 1 205.64 197.23 44.76 o 28 2 1 635.24 788.88 69.71 o 30 2 1 881.69 727.65 63.98 o 32 2 1 0.34 -56.29 46.99 o 34 2 1 268.06 487.72 77.75 o 36 2 1 563.35 573.84 73.66 o 38 2 1 47.95 137.99 80.53 o 40 2 1 11.11 -156.86 165.20 o -39 3 1 0.95 4.77 101.02 o -37 3 1 122.25 106.10 101.53 o -35 3 1 1.82 195.14 227.23 o -33 3 1 15.35 121.51 165.82 o -31 3 1 1163.05 1463.67 96.38 o -29 3 1 37.15 101.94 56.12 o -27 3 1 801.60 987.31 152.54 o -25 3 1 370.12 300.07 59.69 o -23 3 1 784.31 794.07 37.59 o -21 3 1 205.22 124.80 21.93 o -19 3 1 102.96 65.83 18.64 o -17 3 1 277.07 274.94 24.58 o -15 3 1 2332.15 2731.56 89.07 o -13 3 1 9051.56 9181.71 223.69 o -11 3 1 48.27 37.14 28.90 o -9 3 1 1409.31 1277.22 63.57 o -7 3 1 87.27 161.05 23.51 o -5 3 1 2183.12 2354.40 68.31 o -3 3 1 6406.96 7288.39 186.62 o -1 3 1 311.65 319.63 34.46 o 1 3 1 1340.19 1554.36 52.59 o 3 3 1 19339.96 20845.63 358.45 o 5 3 1 9629.84 9649.07 200.18 o 7 3 1 8288.69 8379.85 173.00 o 9 3 1 462.61 752.88 32.54 o 11 3 1 2.10 38.51 18.64 o 13 3 1 2408.09 2302.53 72.91 o 15 3 1 2995.47 2786.06 70.40 o 17 3 1 66.68 98.24 13.21 o 19 3 1 888.80 798.25 55.47 o 21 3 1 118.71 132.80 44.83 o 23 3 1 3934.70 4426.27 189.82 o 25 3 1 0.97 15.14 46.00 o 27 3 1 6134.84 6049.10 250.74 o 29 3 1 448.65 515.93 81.62 o 31 3 1 1020.77 971.08 88.90 o 33 3 1 201.37 150.41 73.18 o 35 3 1 51.16 80.42 108.33 o 37 3 1 262.60 114.27 113.27 o -36 4 1 128.15 22.65 118.21 o -34 4 1 79.55 5.80 127.96 o -32 4 1 10.48 -83.41 148.90 o -30 4 1 455.52 336.42 179.41 o -28 4 1 1012.00 883.10 187.21 o -26 4 1 555.37 260.39 93.88 o -24 4 1 12.96 124.80 126.66 o -22 4 1 36.13 34.05 24.65 o -20 4 1 1913.13 1978.75 60.99 o -18 4 1 8761.74 8774.44 194.38 o -16 4 1 473.97 550.16 39.10 o -14 4 1 111.16 106.89 33.71 o -12 4 1 3996.35 3967.93 144.71 o -10 4 1 2507.52 2884.71 111.45 o -8 4 1 787.76 1062.04 54.34 o -6 4 1 3250.84 3466.69 106.89 o -4 4 1 1565.16 1525.28 66.56 o -2 4 1 56.14 33.19 27.32 o 0 4 1 1475.97 1190.04 56.26 o 2 4 1 238.84 145.02 29.45 o 4 4 1 661.21 761.01 41.91 o 6 4 1 458.81 548.40 39.92 o 8 4 1 2167.39 2117.93 102.32 o 10 4 1 11159.01 12877.10 365.80 o 12 4 1 1635.59 1635.74 68.92 o 14 4 1 366.24 489.33 42.63 o 16 4 1 1833.17 2048.56 78.81 o 18 4 1 42.94 114.68 21.83 o 20 4 1 1095.88 1123.27 44.69 o 22 4 1 1169.02 1046.39 166.61 o 24 4 1 1522.11 1195.18 148.59 o 26 4 1 924.82 1224.81 146.53 o 28 4 1 114.87 219.68 101.05 o 30 4 1 763.37 583.66 153.09 o 32 4 1 564.45 730.67 200.32 o 34 4 1 133.02 68.58 171.83 o -31 5 1 31.99 410.80 212.54 o -29 5 1 5.46 84.44 188.99 o -27 5 1 739.73 658.42 149.28 o -25 5 1 1542.30 1717.67 297.94 o -23 5 1 471.82 463.45 211.41 o -21 5 1 1696.54 1512.28 191.63 o -19 5 1 2910.57 2704.51 221.60 o -17 5 1 3436.24 3481.96 166.17 o -15 5 1 1023.29 984.98 59.31 o -13 5 1 1406.26 1348.38 58.52 o -11 5 1 11828.62 10906.93 290.25 o -9 5 1 111.91 188.99 46.34 o -7 5 1 1903.49 1740.77 91.20 o -5 5 1 743.47 541.47 68.10 o -3 5 1 2543.62 2567.55 122.06 o -1 5 1 1287.97 1533.97 87.08 o 1 5 1 5575.57 5798.15 208.80 o 3 5 1 6109.81 6557.93 240.07 o 5 5 1 13.25 -22.65 47.81 o 7 5 1 16.63 56.84 39.13 o 9 5 1 1.40 9.92 40.74 o 11 5 1 5.57 139.70 42.49 o 13 5 1 0.01 34.94 33.29 o 15 5 1 726.89 623.71 138.81 o 17 5 1 1695.38 1532.53 171.18 o 19 5 1 1079.33 1141.98 161.53 o 21 5 1 225.43 295.60 157.34 o 23 5 1 900.29 432.87 154.19 o 25 5 1 108.95 48.26 156.79 o 27 5 1 118.30 93.53 160.54 o 29 5 1 601.85 631.13 186.18 o 31 5 1 54.88 -292.19 194.79 o -26 6 1 864.45 1459.42 198.19 o -24 6 1 1356.16 1261.40 190.81 o -22 6 1 530.48 347.37 148.49 o -20 6 1 1017.96 896.39 156.42 o -18 6 1 59.61 212.06 104.69 o -16 6 1 593.52 598.07 137.74 o -14 6 1 3.67 43.49 52.79 o -12 6 1 127.16 192.56 64.77 o -10 6 1 2427.52 2406.81 134.52 o -8 6 1 1386.93 1273.27 122.95 o -6 6 1 77.05 1.37 63.91 o -4 6 1 15347.40 16684.80 507.35 o -2 6 1 6087.81 5866.08 232.72 o 0 6 1 2554.89 2940.70 134.62 o 2 6 1 7338.19 7447.42 249.40 o 4 6 1 1830.14 1771.84 113.85 o 6 6 1 295.35 226.89 76.48 o 8 6 1 24.38 120.69 64.74 o 10 6 1 1109.77 1211.87 96.76 o 12 6 1 1079.80 1347.04 95.18 o 14 6 1 171.28 118.28 67.69 o 16 6 1 238.28 192.56 70.95 o 18 6 1 0.80 -7.93 105.93 o 20 6 1 5.37 1425.64 689.75 o 22 6 1 369.00 149.52 164.00 o 24 6 1 17.33 315.03 195.34 o 26 6 1 1243.04 1360.66 243.29 o -19 7 1 422.00 956.15 232.58 o -17 7 1 300.76 181.41 170.18 o -15 7 1 87.63 311.08 118.28 o -13 7 1 1118.30 1003.69 194.86 o -11 7 1 1588.44 1737.69 213.16 o -9 7 1 1173.11 1404.74 197.20 o -7 7 1 1633.55 1551.44 105.07 o -5 7 1 124.37 141.49 67.45 o -3 7 1 787.76 774.36 100.02 o -1 7 1 278.84 330.34 86.88 o 1 7 1 51.33 21.62 66.86 o 3 7 1 9.74 -53.55 63.71 o 5 7 1 96.39 107.26 86.36 o 7 7 1 238.64 186.45 81.45 o 9 7 1 0.03 78.74 87.15 o 11 7 1 70.09 -198.26 145.06 o 13 7 1 51.35 83.10 121.27 o 15 7 1 12.94 316.99 185.39 o 17 7 1 12.69 239.89 187.10 o 19 7 1 40.07 179.93 147.12 o -42 0 2 0.38 27.49 96.56 o -40 0 2 5.04 74.86 89.14 o -38 0 2 64.69 122.74 96.90 o -36 0 2 12.01 14.00 71.29 o -34 0 2 1236.20 1462.26 145.95 o -32 0 2 3562.47 3578.83 248.27 o -30 0 2 1983.63 1828.44 99.82 o -28 0 2 10811.91 11722.66 300.89 o -26 0 2 893.76 1002.52 52.79 o -24 0 2 7635.90 7822.97 180.24 o -22 0 2 7066.69 7643.76 174.95 o -20 0 2 366.88 400.36 28.18 o -18 0 2 2952.61 3161.71 79.19 o -16 0 2 1114.38 823.59 36.14 o -14 0 2 87.64 103.08 19.57 o -12 0 2 1072.72 1410.30 43.15 o -10 0 2 765.24 726.65 26.98 o -8 0 2 3794.21 3647.89 80.56 o -4 0 2 23454.95 20621.56 521.46 o 4 0 2 41.18 86.50 14.83 o 6 0 2 156087.52 148773.59 4973.64 o 8 0 2 711.98 1674.94 62.16 o 10 0 2 122.40 457.89 61.06 o 12 0 2 9153.61 9026.15 221.77 o 14 0 2 46437.94 43203.06 893.40 o 16 0 2 59.19 126.45 27.49 o 18 0 2 120.57 64.94 33.43 o 20 0 2 3978.54 4744.87 135.27 o 22 0 2 126.60 88.59 30.34 o 24 0 2 4744.21 5143.41 199.29 o 26 0 2 11231.45 10868.25 363.12 o 28 0 2 3639.88 3589.95 148.76 o 30 0 2 1003.18 1011.92 66.01 o 32 0 2 5184.31 5186.04 352.24 o 34 0 2 2.41 33.64 87.25 o 36 0 2 1541.03 1449.53 152.37 o 38 0 2 32.75 80.73 110.53 o 40 0 2 194.87 334.39 121.96 o -41 1 2 463.81 924.33 111.52 o -39 1 2 427.59 260.39 63.98 o -37 1 2 409.59 498.39 71.15 o -35 1 2 10.15 59.11 52.41 o -33 1 2 1841.83 1877.87 122.02 o -31 1 2 253.88 343.93 42.60 o -29 1 2 2042.49 2423.18 76.61 o -27 1 2 234.46 283.62 23.10 o -25 1 2 712.03 605.35 26.43 o -23 1 2 16.58 8.58 17.78 o -21 1 2 4009.25 3390.73 64.74 o -19 1 2 3248.50 3273.10 59.35 o -17 1 2 232.44 261.00 15.55 o -15 1 2 45067.30 46115.61 572.91 o -13 1 2 25.74 62.57 11.43 o -11 1 2 25180.37 24787.89 320.87 o -9 1 2 537.52 526.92 18.71 o -7 1 2 98.14 94.98 9.75 o -5 1 2 1419.57 1140.71 31.27 o -3 1 2 1566.17 1580.75 39.78 o -1 1 2 6830.46 6435.49 127.83 o 1 1 2 1622.52 1480.73 37.07 o 3 1 2 52641.46 51980.43 887.05 o 7 1 2 29917.49 28524.30 707.16 o 9 1 2 2897.42 2837.14 65.15 o 11 1 2 1522.61 1861.84 47.95 o 13 1 2 4000.05 3260.40 63.47 o 15 1 2 16451.40 16627.41 267.56 o 17 1 2 1174.23 1126.98 33.57 o 19 1 2 28330.63 28530.54 444.37 o 21 1 2 44.25 2.71 16.37 o 23 1 2 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