#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/70/2017016.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017016_Fobs loop_ _publ_author_name 'Mu\~noz, Juan Carlos' 'Atria, Ana Mar\'ia' 'Garland, Maria Teresa' 'Baggio, Ricardo' _publ_section_title ; Three lanthanide complexes derived from itaconic acid and 2,2'-bipyridine ; _journal_coeditor_code SK3282 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m121 _journal_page_last m127 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 71.600 _cell_angle_beta 82.315 _cell_angle_gamma 68.392 _cell_length_a 9.5507 _cell_length_b 12.5979 _cell_length_c 17.5824 _exptl_crystal_F_000 1060.00 _reflns_d_resolution_high 0.7632 _[local]_cod_data_source_file sk3282Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' gd in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 316.48 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 55229.46 46151.21 202.60 o 2 0 0 3921.81 4317.71 85.18 o 3 0 0 7230.75 6424.16 116.27 o 4 0 0 2088.54 1688.45 104.75 o 5 0 0 2506.36 2454.41 164.60 o 6 0 0 7472.80 7395.75 293.53 o 7 0 0 433.19 731.90 75.37 o 8 0 0 4304.36 4290.39 300.42 o 10 0 0 3529.05 3458.42 174.96 o 11 0 0 104.30 144.11 145.04 o -11 1 0 4237.01 4382.98 364.89 o -10 1 0 2689.81 2995.91 185.33 o -9 1 0 83.00 70.41 153.10 o -8 1 0 3826.44 3179.88 272.81 o -7 1 0 1402.93 1280.25 95.55 o -5 1 0 679.83 610.70 120.87 o -4 1 0 6661.04 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