#------------------------------------------------------------------------------
#$Date: 2009-05-13 10:52:48 +0300 (Wed, 13 May 2009) $
#$Revision: 717 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2017046.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2017046_Fobs
loop_
_publ_author_name
'Vallat, Olivier'
'Buciumas, Ana-Maria'
'Neier, Reinhard'
'Stoeckli-Evans, Helen'
_publ_section_title
;
 5-Hydroxyalkyl derivatives of <i>tert</i>-butyl
 2-oxo-2,5-dihydro-1<i>H</i>-pyrrole-1-carboxylate:
 diastereoselectivity of the Mukaiyama crossed-aldol-type reaction
;
_journal_coeditor_code           GA3120
_journal_issue                   4
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              o171
_journal_page_last               o175
_journal_volume                  65
_journal_year                    2009
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                104.176
_cell_angle_beta                 113.759
_cell_angle_gamma                101.367
_cell_length_a                   8.8340
_cell_length_b                   9.0750
_cell_length_c                   10.7283
_exptl_crystal_F_000             344.00
_reflns_d_resolution_high        0.7284
_[local]_cod_data_source_file    ga3120IIIsup4.hkl
_[local]_cod_data_source_block   III
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     '  AMB333   IPDS2  -100DEG    P-1'
_shelx_refln_list_code           4
_shelx_F_calc_maximum            74.77
_shelx_F_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 1543.74 1516.16 33.53 o
4 0 0 706.07 624.66 16.31 o
5 0 0 608.40 580.01 12.44 o
6 0 0 876.76 897.09 16.94 o
7 0 0 701.75 708.42 15.10 o
8 0 0 77.93 73.82 2.59 o
9 0 0 41.26 39.59 2.85 o
10 0 0 1.30 3.41 2.71 o
-10 1 0 229.17 242.47 4.85 o
-9 1 0 610.68 650.79 10.34 o
-8 1 0 578.43 578.89 7.86 o
-7 1 0 743.31 767.29 16.21 o
-6 1 0 714.63 699.98 16.70 o
-5 1 0 699.50 699.33 16.65 o
-4 1 0 3319.09 3370.18 19.20 o
-3 1 0 2984.22 2965.50 56.85 o
-2 1 0 261.22 259.50 3.86 o
-1 1 0 113.38 116.39 3.38 o
0 1 0 170.58 200.92 5.71 o
1 1 0 990.67 1040.10 7.21 o
2 1 0 18.19 15.47 1.88 o
3 1 0 8.44 9.21 2.35 o
4 1 0 697.30 736.84 19.37 o
5 1 0 464.80 473.46 4.30 o
6 1 0 77.83 80.35 2.48 o
7 1 0 231.59 247.87 3.00 o
8 1 0 249.87 261.84 5.94 o
9 1 0 229.10 236.68 9.13 o
10 1 0 138.11 125.27 6.34 o
-10 2 0 5.47 7.82 2.23 o
-9 2 0 13.34 13.65 2.26 o
-8 2 0 162.82 166.26 3.43 o
-7 2 0 1.01 7.00 1.99 o
-6 2 0 8.17 3.06 2.10 o
-5 2 0 188.72 177.56 6.67 o
-4 2 0 963.84 955.68 8.30 o
-3 2 0 2771.03 2799.21 35.18 o
-2 2 0 2746.19 2736.50 14.16 o
-1 2 0 1579.96 1694.35 9.70 o
1 2 0 547.81 519.03 4.23 o
2 2 0 3623.39 3562.93 32.19 o
3 2 0 2945.37 2812.60 36.81 o
4 2 0 197.61 181.28 2.94 o
5 2 0 1799.71 1820.67 70.79 o
6 2 0 1344.58 1381.50 19.84 o
7 2 0 296.73 303.13 4.42 o
8 2 0 138.01 143.20 5.75 o
9 2 0 143.15 144.48 4.63 o
-11 3 0 25.10 18.56 2.49 o
-10 3 0 10.64 9.81 2.27 o
-9 3 0 577.66 548.28 14.78 o
-8 3 0 309.55 299.66 4.48 o
-7 3 0 413.37 411.54 5.83 o
-6 3 0 2428.81 2521.69 14.56 o
-5 3 0 1287.45 1370.11 25.38 o
-4 3 0 2011.06 1984.69 20.25 o
-2 3 0 4422.89 4453.54 28.58 o
-1 3 0 2054.34 2074.82 9.96 o
0 3 0 776.94 744.83 54.39 o
1 3 0 854.49 831.32 4.88 o
2 3 0 1285.67 1311.83 8.52 o
3 3 0 1107.35 1117.18 6.84 o
4 3 0 661.77 693.49 19.85 o
5 3 0 2.11 8.10 2.62 o
6 3 0 132.36 142.03 8.01 o
7 3 0 132.70 138.49 3.16 o
8 3 0 12.85 14.84 2.24 o
9 3 0 6.48 6.38 1.99 o
-11 4 0 163.78 156.60 2.89 o
-10 4 0 401.93 395.91 9.05 o
-9 4 0 176.31 188.09 5.88 o
-8 4 0 86.25 96.25 2.36 o
-7 4 0 281.10 287.69 3.05 o
-6 4 0 1133.33 1198.07 6.03 o
-5 4 0 206.48 210.92 2.78 o
-4 4 0 18.10 25.22 1.98 o
-3 4 0 465.38 529.19 9.94 o
-2 4 0 641.07 715.62 4.15 o
-1 4 0 608.46 613.20 53.79 o
0 4 0 566.82 574.33 42.42 o
1 4 0 83.31 100.27 3.07 o
2 4 0 1241.04 1233.64 15.73 o
3 4 0 2189.02 2210.81 18.26 o
4 4 0 59.29 66.69 2.34 o
5 4 0 424.11 433.77 6.63 o
6 4 0 293.58 310.60 8.47 o
7 4 0 43.60 49.67 2.33 o
8 4 0 139.26 136.40 2.69 o
-11 5 0 43.31 32.11 2.16 o
-10 5 0 0.18 3.88 2.18 o
-9 5 0 239.15 224.98 2.77 o
-8 5 0 84.21 87.62 2.74 o
-7 5 0 38.78 44.66 2.25 o
-6 5 0 1080.75 1165.24 40.67 o
-5 5 0 449.23 462.11 13.31 o
-4 5 0 618.60 569.14 9.54 o
-3 5 0 1968.17 2027.25 24.62 o
-2 5 0 1589.38 1647.61 9.60 o
-1 5 0 2480.02 2476.33 172.93 o
0 5 0 2713.50 2698.10 180.27 o
1 5 0 872.49 871.99 72.85 o
2 5 0 482.33 453.15 4.23 o
3 5 0 159.10 143.62 2.70 o
4 5 0 489.76 482.16 7.08 o
5 5 0 604.16 588.21 5.81 o
6 5 0 184.37 186.64 3.08 o
7 5 0 31.16 32.67 2.85 o
-10 6 0 188.36 180.33 3.92 o
-9 6 0 473.09 473.89 5.72 o
-8 6 0 428.67 441.41 3.76 o
-7 6 0 380.65 406.66 14.14 o
-6 6 0 1026.92 1096.76 20.16 o
-5 6 0 755.58 789.67 4.40 o
-4 6 0 113.76 92.87 2.17 o
-3 6 0 714.07 730.23 19.99 o
-2 6 0 6.92 3.15 3.64 o
-1 6 0 137.09 134.27 4.19 o
0 6 0 41.62 41.23 1.83 o
1 6 0 11.08 16.25 1.79 o
2 6 0 7.41 10.91 2.07 o
3 6 0 62.89 60.91 2.60 o
4 6 0 103.30 101.12 3.09 o
5 6 0 330.60 314.99 3.96 o
6 6 0 45.60 43.90 2.01 o
7 6 0 0.78 1.31 3.51 o
-10 7 0 89.47 83.59 2.13 o
-9 7 0 39.77 39.22 4.22 o
-8 7 0 58.08 62.35 1.94 o
-7 7 0 8.72 7.31 2.61 o
-6 7 0 429.19 437.53 3.35 o
-5 7 0 35.46 40.06 2.06 o
-4 7 0 170.08 178.04 3.94 o
-3 7 0 316.99 302.95 18.73 o
-2 7 0 63.26 76.15 5.70 o
-1 7 0 42.53 34.44 2.26 o
0 7 0 666.37 646.11 47.33 o
1 7 0 307.37 303.85 17.71 o
2 7 0 668.30 670.88 41.39 o
3 7 0 168.34 166.34 3.27 o
4 7 0 5.28 6.02 1.65 o
5 7 0 12.22 13.56 2.00 o
6 7 0 29.92 26.86 5.78 o
-10 8 0 58.74 52.90 2.27 o
-9 8 0 46.41 46.57 2.17 o
-8 8 0 234.22 243.19 8.37 o
-7 8 0 356.16 366.57 3.11 o
-6 8 0 72.14 74.26 2.47 o
-5 8 0 124.11 140.85 3.76 o
-4 8 0 360.56 371.56 24.37 o
-3 8 0 881.95 874.87 69.66 o
-2 8 0 92.97 90.53 10.22 o
-1 8 0 647.52 655.93 54.77 o
0 8 0 508.80 508.39 32.54 o
1 8 0 35.32 42.46 7.43 o
2 8 0 150.59 152.67 8.35 o
3 8 0 115.63 124.01 5.34 o
4 8 0 41.76 46.95 2.26 o
5 8 0 4.95 5.85 2.00 o
-9 9 0 86.62 85.48 2.70 o
-8 9 0 105.24 109.67 3.93 o
-7 9 0 155.32 162.53 3.99 o
-6 9 0 137.83 146.32 9.49 o
-5 9 0 335.46 357.18 13.37 o
-4 9 0 63.37 72.16 8.18 o
-3 9 0 8.87 7.55 2.43 o
-2 9 0 36.56 38.41 2.38 o
-1 9 0 30.35 29.68 3.33 o
0 9 0 165.47 165.71 11.22 o
1 9 0 7.91 9.87 5.10 o
2 9 0 69.90 67.27 6.97 o
3 9 0 75.66 67.89 2.83 o
4 9 0 6.56 10.23 2.33 o
-8 10 0 0.32 -0.99 1.86 o
-7 10 0 78.59 78.31 2.19 o
-6 10 0 55.92 53.62 4.81 o
-5 10 0 96.30 88.35 3.06 o
-4 10 0 107.84 99.13 14.13 o
-3 10 0 381.27 356.15 25.62 o
-2 10 0 139.60 136.56 12.95 o
-1 10 0 172.81 169.02 10.68 o
0 10 0 31.60 31.47 4.76 o
1 10 0 21.23 20.84 1.80 o
2 10 0 36.65 33.04 2.59 o
-7 11 0 16.96 17.60 1.83 o
-6 11 0 68.09 64.51 2.17 o
-5 11 0 55.90 60.85 8.41 o
-4 11 0 49.72 51.35 1.84 o
-3 11 0 21.19 20.46 2.08 o
-2 11 0 33.62 36.04 2.09 o
-1 11 0 31.50 34.72 3.17 o
0 11 0 4.96 5.11 1.92 o
-4 12 0 5.28 10.60 1.71 o
-3 12 0 6.95 0.09 1.58 o
2 -12 1 245.96 189.39 105.50 o
3 -12 1 56.69 53.55 7.57 o
4 -12 1 2.24 5.91 3.41 o
5 -12 1 52.41 46.30 2.20 o
-1 -11 1 185.51 157.08 13.93 o
0 -11 1 2.90 0.40 3.96 o
1 -11 1 0.32 -2.58 5.11 o
2 -11 1 12.45 8.73 2.44 o
3 -11 1 5.14 7.29 2.89 o
4 -11 1 8.24 11.27 2.02 o
5 -11 1 1.56 -0.75 2.50 o
6 -11 1 28.47 26.22 2.13 o
7 -11 1 135.86 128.07 2.44 o
-3 -10 1 51.83 50.68 2.82 o
-2 -10 1 204.38 191.32 9.58 o
-1 -10 1 194.53 197.34 10.07 o
0 -10 1 310.31 305.59 17.14 o
1 -10 1 83.13 79.38 8.62 o
2 -10 1 196.16 191.85 11.33 o
3 -10 1 698.62 699.65 25.22 o
4 -10 1 459.44 479.23 22.03 o
5 -10 1 309.98 311.84 8.50 o
6 -10 1 113.10 114.87 4.46 o
7 -10 1 318.84 316.51 20.53 o
8 -10 1 104.78 103.12 6.77 o
-4 -9 1 291.98 277.24 8.89 o
-3 -9 1 38.52 34.68 2.64 o
-2 -9 1 112.05 110.81 4.41 o
-1 -9 1 32.64 41.13 5.11 o
0 -9 1 22.57 21.82 1.95 o
1 -9 1 188.62 178.56 7.45 o
2 -9 1 63.45 61.98 6.02 o
3 -9 1 18.25 15.63 2.07 o
4 -9 1 231.63 230.59 7.58 o
5 -9 1 65.68 60.55 1.86 o
6 -9 1 17.07 17.66 2.00 o
7 -9 1 19.33 22.37 2.51 o
8 -9 1 79.23 74.15 6.46 o
9 -9 1 30.47 30.93 2.19 o
-5 -8 1 23.23 23.32 2.13 o
-4 -8 1 30.77 29.89 2.57 o
-3 -8 1 2.51 1.33 2.09 o
-2 -8 1 102.19 101.52 6.69 o
-1 -8 1 32.16 31.59 3.60 o
0 -8 1 3.53 5.96 1.80 o
1 -8 1 88.07 89.61 6.40 o
2 -8 1 10.16 12.63 1.96 o
3 -8 1 80.82 79.45 2.49 o
4 -8 1 571.60 572.26 15.69 o
5 -8 1 1453.86 1490.63 77.32 o
6 -8 1 266.67 289.48 4.48 o
7 -8 1 158.98 178.97 4.22 o
8 -8 1 169.19 180.73 2.96 o
9 -8 1 145.87 141.65 2.76 o
-6 -7 1 153.25 147.87 4.22 o
-5 -7 1 43.89 42.83 2.76 o
-4 -7 1 135.15 135.51 2.58 o
-3 -7 1 212.39 213.56 3.24 o
-2 -7 1 908.96 895.65 50.32 o
-1 -7 1 491.96 495.47 21.44 o
0 -7 1 718.63 724.89 34.96 o
1 -7 1 3002.55 3058.94 113.12 o
2 -7 1 1058.96 1064.99 64.00 o
3 -7 1 134.40 121.16 2.62 o
4 -7 1 563.08 563.80 24.12 o
5 -7 1 107.39 113.55 3.75 o
6 -7 1 57.30 64.45 2.21 o
7 -7 1 731.37 746.54 10.86 o
8 -7 1 74.89 76.09 6.59 o
9 -7 1 5.35 9.72 2.15 o
10 -7 1 7.07 8.06 2.01 o
-7 -6 1 301.92 297.05 5.69 o
-6 -6 1 33.85 34.81 2.73 o
-5 -6 1 104.40 106.85 2.12 o
-4 -6 1 202.48 204.45 2.59 o
-3 -6 1 487.81 439.20 9.73 o
-2 -6 1 124.29 114.43 1.99 o
-1 -6 1 286.37 283.44 13.16 o
0 -6 1 18.66 19.07 3.45 o
1 -6 1 50.53 57.61 5.28 o
2 -6 1 59.32 75.01 2.46 o
3 -6 1 103.80 122.38 2.55 o
4 -6 1 69.79 81.96 1.89 o
5 -6 1 29.81 33.45 5.60 o
6 -6 1 104.46 114.67 2.79 o
7 -6 1 181.14 194.00 4.80 o
8 -6 1 90.15 99.82 2.08 o
9 -6 1 153.73 159.90 3.22 o
10 -6 1 179.64 178.30 4.34 o
-8 -5 1 1.35 6.49 2.31 o
-7 -5 1 1.75 1.23 2.20 o
-6 -5 1 89.28 94.01 2.42 o
-5 -5 1 18.05 21.68 2.11 o
-4 -5 1 296.13 292.38 2.64 o
-3 -5 1 110.63 109.60 2.46 o
-2 -5 1 269.85 264.12 5.58 o
-1 -5 1 566.03 558.57 14.59 o
0 -5 1 335.02 335.21 20.27 o
1 -5 1 1328.53 1361.86 82.99 o
2 -5 1 1633.22 1615.48 72.85 o
3 -5 1 2015.78 2038.09 11.10 o
4 -5 1 2203.50 2416.95 48.78 o
5 -5 1 453.67 484.63 6.60 o
6 -5 1 220.74 222.23 3.11 o
7 -5 1 1370.03 1397.80 6.47 o
8 -5 1 381.43 375.76 3.24 o
9 -5 1 270.00 259.05 3.29 o
10 -5 1 123.26 114.85 2.35 o
-9 -4 1 21.55 12.68 4.67 o
-8 -4 1 154.82 158.83 2.78 o
-7 -4 1 266.28 294.69 15.23 o
-6 -4 1 113.03 116.42 2.47 o
-5 -4 1 1395.94 1390.78 58.95 o
-4 -4 1 176.52 175.61 5.05 o
-3 -4 1 91.70 86.55 2.69 o
-2 -4 1 1882.19 1890.66 39.29 o
-1 -4 1 2051.33 1969.09 33.62 o
0 -4 1 142.42 99.76 4.04 o
1 -4 1 913.71 871.51 43.55 o
2 -4 1 1761.02 1821.49 12.03 o
3 -4 1 90.12 117.23 2.67 o
4 -4 1 85.13 74.43 2.32 o
5 -4 1 126.21 115.36 2.43 o
6 -4 1 11.43 9.45 1.84 o
7 -4 1 150.81 154.42 2.29 o
8 -4 1 69.56 67.17 2.30 o
9 -4 1 17.88 18.81 1.97 o
10 -4 1 2.03 0.06 2.21 o
-9 -3 1 77.85 69.43 5.10 o
-8 -3 1 75.56 78.41 4.94 o
-7 -3 1 40.29 46.41 2.85 o
-6 -3 1 5.50 6.97 1.90 o
-5 -3 1 856.71 867.00 15.04 o
-4 -3 1 28.55 34.00 4.03 o
-3 -3 1 12.01 13.57 2.09 o
-2 -3 1 410.36 447.34 11.90 o
-1 -3 1 329.06 363.04 13.17 o
0 -3 1 452.88 492.15 11.67 o
1 -3 1 182.96 199.30 9.53 o
2 -3 1 37.21 46.82 2.03 o
3 -3 1 316.18 303.00 3.60 o
4 -3 1 411.34 388.61 3.62 o
5 -3 1 537.65 524.05 8.51 o
6 -3 1 214.17 215.84 4.70 o
7 -3 1 283.01 290.57 3.20 o
8 -3 1 12.38 17.28 2.17 o
9 -3 1 298.27 298.00 6.53 o
10 -3 1 355.27 345.89 11.29 o
-10 -2 1 6.11 4.03 2.19 o
-9 -2 1 10.55 7.30 1.98 o
-8 -2 1 59.84 58.95 2.34 o
-7 -2 1 1.53 0.36 1.92 o
-6 -2 1 434.92 457.66 7.27 o
-5 -2 1 950.02 947.23 24.21 o
-4 -2 1 906.72 885.52 29.42 o
-3 -2 1 408.14 352.54 3.20 o
-2 -2 1 4450.81 4458.91 16.46 o
-1 -2 1 4334.22 4335.97 62.59 o
0 -2 1 952.63 964.18 18.43 o
1 -2 1 1909.27 1925.32 15.85 o
2 -2 1 2636.12 2684.93 20.37 o
3 -2 1 262.31 202.26 4.31 o
4 -2 1 3035.64 3027.66 15.32 o
5 -2 1 1656.57 1688.11 29.74 o
6 -2 1 1310.17 1294.73 37.33 o
7 -2 1 676.77 679.55 18.19 o
8 -2 1 219.46 206.54 4.33 o
9 -2 1 1.62 1.80 2.56 o
10 -2 1 0.93 3.45 2.72 o
-10 -1 1 63.82 67.36 3.60 o
-9 -1 1 57.18 55.51 3.85 o
-8 -1 1 352.43 356.10 3.27 o
-7 -1 1 1273.86 1307.99 27.75 o
-6 -1 1 542.06 554.24 6.15 o
-5 -1 1 2116.97 2131.38 19.89 o
-4 -1 1 1050.55 954.68 4.88 o
-3 -1 1 1054.77 1020.68 5.53 o
-2 -1 1 2293.27 2280.05 10.00 o
-1 -1 1 156.44 175.17 3.07 o
0 -1 1 26.40 41.08 1.96 o
1 -1 1 1693.28 1646.58 36.88 o
2 -1 1 80.26 78.67 2.89 o
3 -1 1 1.35 6.25 2.25 o
4 -1 1 377.45 411.45 12.03 o
5 -1 1 349.95 357.99 7.55 o
6 -1 1 379.13 398.23 4.04 o
7 -1 1 447.71 453.20 7.85 o
8 -1 1 19.95 28.24 2.27 o
9 -1 1 21.50 23.41 2.38 o
10 -1 1 129.18 139.59 3.28 o
-10 0 1 90.84 90.87 2.42 o
-9 0 1 53.71 65.92 2.38 o
-8 0 1 93.59 103.84 2.79 o
-7 0 1 114.48 107.13 2.38 o
-6 0 1 27.32 22.73 2.14 o
-5 0 1 163.62 181.21 3.91 o
-4 0 1 23.87 31.51 2.47 o
-3 0 1 175.60 147.79 5.77 o
-2 0 1 1020.52 1018.62 6.88 o
-1 0 1 1371.90 1515.07 10.00 o
0 0 1 11.09 11.88 1.93 o
2 0 1 2449.22 2280.47 36.24 o
3 0 1 417.29 398.54 5.68 o
4 0 1 2251.68 2342.57 60.17 o
5 0 1 83.26 81.59 2.15 o
6 0 1 155.07 148.05 4.00 o
7 0 1 362.22 384.06 9.49 o
8 0 1 298.94 293.68 10.71 o
9 0 1 239.17 249.19 7.80 o
10 0 1 95.34 88.94 3.02 o
-11 1 1 9.81 7.99 3.08 o
-10 1 1 67.09 62.39 2.71 o
-9 1 1 20.28 22.88 2.44 o
-8 1 1 9.97 12.74 2.04 o
-7 1 1 474.62 481.21 15.27 o
-6 1 1 246.71 233.84 2.96 o
-5 1 1 1126.87 1044.25 29.52 o
-4 1 1 189.13 144.28 2.75 o
-3 1 1 169.42 135.12 2.63 o
-2 1 1 4452.89 4364.16 98.20 o
-1 1 1 3832.07 3935.05 53.03 o
2 1 1 1909.52 1789.41 24.39 o
3 1 1 479.37 429.00 4.77 o
4 1 1 904.48 908.76 11.34 o
5 1 1 4.60 5.69 2.10 o
6 1 1 525.42 541.43 14.80 o
7 1 1 117.42 125.03 2.67 o
8 1 1 0.40 2.31 3.56 o
9 1 1 59.37 68.20 3.25 o
-11 2 1 209.21 202.15 8.12 o
-10 2 1 179.54 179.57 5.70 o
-9 2 1 171.72 176.21 5.96 o
-8 2 1 1910.60 1904.35 32.87 o
-7 2 1 788.80 803.97 12.50 o
-6 2 1 458.79 480.05 8.54 o
-5 2 1 804.45 824.89 4.57 o
-4 2 1 1950.52 2010.84 8.89 o
-3 2 1 1218.80 1234.76 6.47 o
-2 2 1 139.71 161.06 4.30 o
-1 2 1 1001.59 1037.15 38.17 o
0 2 1 57.04 74.04 3.92 o
1 2 1 56.28 39.42 2.79 o
2 2 1 83.07 102.22 1.99 o
3 2 1 91.40 79.58 1.99 o
4 2 1 1171.65 1154.34 31.51 o
5 2 1 11.12 12.82 2.67 o
6 2 1 74.13 76.49 3.43 o
7 2 1 296.09 310.82 3.22 o
8 2 1 53.44 54.37 2.86 o
9 2 1 131.99 126.34 3.18 o
-11 3 1 6.34 7.02 2.31 o
-10 3 1 13.42 17.35 2.28 o
-9 3 1 5.97 6.42 2.00 o
-8 3 1 31.18 29.06 1.96 o
-7 3 1 82.99 88.07 9.28 o
-6 3 1 12.65 16.78 2.53 o
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