#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:15:41 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180839 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/70/2017052.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017052_Fobs loop_ _publ_author_name 'Koner, Rajesh' 'Goldberg, Israel' _publ_section_title ; Two- and three-dimensional hydrated coordination polymers of diaqualanthanum(3+) ions with 2-hydroxypropanedioate, oxalate and acetate anions as bridging ligands ; _journal_coeditor_code GT3003 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m160 _journal_page_last m164 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.969 _cell_angle_gamma 90.000 _cell_length_a 9.1139 _cell_length_b 8.3883 _cell_length_c 13.6994 _exptl_crystal_F_000 716.00 _reflns_d_resolution_high 0.7531 _cod_data_source_file gt3003Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ra6' _shelx_refln_list_code 4 _shelx_f_calc_maximum 238.23 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 17852.47 16923.15 338.59 o 4 0 0 422.13 478.36 34.67 o 6 0 0 3845.33 3930.69 179.07 o 8 0 0 11364.72 11444.51 482.19 o 10 0 0 10401.88 10689.83 505.47 o 1 1 0 1694.58 1795.95 53.81 o 2 1 0 12391.12 11228.15 255.66 o 3 1 0 21.78 20.05 16.22 o 4 1 0 47311.20 47893.84 722.53 o 5 1 0 2212.07 2139.18 67.52 o 6 1 0 7910.60 8580.38 170.51 o 7 1 0 13.24 -20.05 32.15 o 8 1 0 603.29 486.73 57.44 o 9 1 0 414.17 365.20 75.18 o 10 1 0 70.77 161.23 76.59 o 11 1 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