#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/70/2017062.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017062_Fobs loop_ _publ_author_name 'Palma, Alirio' 'Bahsas, Ali' 'Y\'epes, Andr\'es F.' 'Cobo, Justo' 'Hursthouse, Michael B.' 'Glidewell, Christopher' _publ_section_title ; (2R,4S)-7-Bromo-2-phenyl-2,3,4,5-tetrahydro-1,4-epoxynaphtho[1,2-b]azepine, (2RS,4SR)-7-bromo-2-(4-chlorophenyl-2,3,4,5-tetrahydro-1,4-epoxynaphtho[1,2-b]azepine and (2RS,4SR)-2-(4-fluorophenyl)-2,3,4,5-tetrahydro-1,4-epoxynaphtho[1,2-b]azepine: hydrogen-bonded structures in two and three dimensions ; _journal_coeditor_code SK3295 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o140 _journal_page_last o145 _journal_volume 65 _journal_year 2009 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.7758 _cell_length_b 9.8211 _cell_length_c 33.1740 _exptl_crystal_F_000 1616.00 _reflns_d_resolution_high 0.7692 _[local]_cod_data_source_file sk3295IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' AF135' _shelx_refln_list_code 4 _shelx_F_calc_maximum 434.92 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 27412.01 23679.55 787.25 o 4 0 0 4366.65 4343.30 243.08 o 6 0 0 7979.29 7171.34 309.06 o 8 0 0 15592.32 15384.70 732.21 o 10 0 0 3634.42 3829.70 229.74 o 12 0 0 2014.76 1715.94 256.83 o 2 1 0 72088.80 72481.77 914.64 o 4 1 0 47803.89 45707.98 894.12 o 6 1 0 19112.03 18268.81 359.21 o 8 1 0 228.45 235.89 84.15 o 10 1 0 1115.93 1163.68 107.48 o 12 1 0 56.21 -37.23 149.50 o 0 2 0 2784.19 2372.17 79.34 o 2 2 0 21904.23 23263.75 324.75 o 4 2 0 188.80 126.95 42.21 o 6 2 0 16.69 -35.96 67.87 o 8 2 0 4478.60 4771.93 164.02 o 10 2 0 45.66 466.68 105.45 o 12 2 0 1285.55 1063.77 172.50 o 2 3 0 32279.67 32457.09 427.54 o 4 3 0 7753.24 6910.00 184.37 o 6 3 0 13951.69 13826.15 319.08 o 8 3 0 432.87 414.03 96.05 o 10 3 0 1946.84 1822.26 176.43 o 12 3 0 2359.69 1970.62 188.97 o 0 4 0 24847.89 25105.64 536.80 o 2 4 0 18276.16 18044.73 267.66 o 4 4 0 3461.39 4303.83 144.08 o 6 4 0 2132.19 1935.59 104.08 o 8 4 0 18339.12 17824.68 382.83 o 10 4 0 4907.31 4864.44 252.53 o 12 4 0 41.79 80.03 141.77 o 2 5 0 5567.36 5266.85 120.27 o 4 5 0 4513.13 4388.02 154.68 o 6 5 0 497.27 725.50 92.49 o 8 5 0 381.18 462.15 92.59 o 10 5 0 1247.67 1172.87 159.36 o 0 6 0 13657.59 15330.75 425.91 o 2 6 0 2470.41 2665.39 94.71 o 4 6 0 2133.70 2214.59 159.89 o 6 6 0 5.13 95.36 99.99 o 8 6 0 266.60 115.21 95.88 o 10 6 0 1307.70 1639.20 186.97 o 2 7 0 3948.71 3934.89 143.15 o 4 7 0 16930.09 18009.19 541.21 o 6 7 0 4242.49 4297.17 219.17 o 8 7 0 2314.70 2310.61 171.49 o 10 7 0 3.30 185.92 138.55 o 0 8 0 7597.67 7291.51 263.95 o 2 8 0 3621.66 3599.66 130.10 o 4 8 0 110.80 61.44 108.92 o 6 8 0 47.55 245.08 131.00 o 8 8 0 1879.88 1999.16 171.22 o 2 9 0 2828.40 2791.35 122.75 o 4 9 0 56.63 -91.10 125.02 o 6 9 0 194.60 42.23 147.18 o 8 9 0 6.23 -103.46 153.55 o 0 10 0 104.68 121.19 162.56 o 2 10 0 2847.57 2626.48 174.68 o 4 10 0 1948.27 1602.09 235.87 o 6 10 0 272.49 479.17 228.78 o 2 11 0 35.58 100.40 134.07 o 4 11 0 1393.05 1373.03 249.26 o 6 11 0 5175.01 5627.72 416.52 o 0 12 0 4349.26 3911.74 328.74 o 2 12 0 93.87 -109.23 155.40 o 4 12 0 282.01 -95.65 338.31 o 2 1 1 38966.13 38654.53 369.78 o 3 1 1 3546.83 3331.92 45.97 o 4 1 1 51552.31 50152.90 791.48 o 5 1 1 26.53 113.77 30.87 o 6 1 1 4773.25 4361.46 94.23 o 7 1 1 1460.66 1448.81 76.20 o 8 1 1 9033.45 8983.87 160.11 o 9 1 1 484.76 394.81 68.93 o 10 1 1 1179.60 1118.25 78.43 o 11 1 1 14.09 -71.97 76.95 o 12 1 1 1402.28 1160.82 117.88 o 0 2 1 22837.12 22841.89 496.43 o 1 2 1 7289.51 7843.75 78.09 o 2 2 1 42918.37 43657.05 429.70 o 3 2 1 1380.25 1256.02 39.85 o 4 2 1 6820.84 7357.36 112.38 o 5 2 1 5491.28 5816.82 120.82 o 6 2 1 5760.59 5635.36 101.01 o 7 2 1 2787.39 2788.02 82.92 o 8 2 1 18853.38 18991.32 279.39 o 9 2 1 17.13 16.73 55.54 o 10 2 1 6249.13 6113.81 147.18 o 11 2 1 26.01 -93.37 80.25 o 12 2 1 556.11 465.68 111.38 o 1 3 1 7477.63 7688.75 79.58 o 2 3 1 18915.56 19235.25 181.02 o 3 3 1 331.37 296.51 22.53 o 4 3 1 1306.60 992.53 45.62 o 5 3 1 5004.09 5240.08 107.04 o 6 3 1 8342.92 8649.03 159.26 o 7 3 1 380.34 376.56 58.36 o 8 3 1 32.07 20.03 54.02 o 9 3 1 56.17 96.96 60.59 o 10 3 1 201.70 290.70 73.81 o 11 3 1 265.59 361.95 103.26 o 12 3 1 408.63 537.38 150.59 o 0 4 1 463.04 349.46 29.93 o 1 4 1 2874.11 2965.03 48.35 o 2 4 1 5056.20 5084.77 68.84 o 3 4 1 2831.66 2951.52 67.08 o 4 4 1 1331.23 1665.79 62.99 o 5 4 1 43.35 47.99 41.15 o 6 4 1 238.82 349.36 53.32 o 7 4 1 159.97 202.35 73.91 o 8 4 1 140.94 486.67 70.23 o 9 4 1 3211.87 2964.18 101.31 o 10 4 1 538.36 732.74 104.70 o 11 4 1 6.29 293.38 93.70 o 12 4 1 325.25 401.52 152.31 o 1 5 1 242.54 297.40 33.48 o 2 5 1 9570.19 9501.26 129.96 o 3 5 1 366.96 493.96 66.99 o 4 5 1 8007.69 7545.58 165.04 o 5 5 1 4.32 23.82 46.61 o 6 5 1 14761.49 14889.47 244.77 o 7 5 1 34.19 46.61 57.23 o 8 5 1 3588.51 3286.10 108.14 o 9 5 1 40.42 168.20 70.35 o 10 5 1 160.99 235.94 83.71 o 11 5 1 63.42 82.06 100.08 o 0 6 1 38686.36 40399.30 703.98 o 1 6 1 0.53 -11.23 30.77 o 2 6 1 7140.67 6717.28 121.49 o 3 6 1 1995.22 2126.03 86.04 o 4 6 1 146.69 197.65 65.43 o 5 6 1 94.74 122.57 67.71 o 6 6 1 1248.84 1232.13 70.94 o 7 6 1 136.85 146.47 60.32 o 8 6 1 3196.07 3369.66 132.30 o 9 6 1 447.94 358.30 82.82 o 10 6 1 2662.49 2559.04 130.07 o 11 6 1 2.04 -81.31 98.19 o 1 7 1 2567.31 2695.65 68.12 o 2 7 1 738.87 794.16 55.10 o 3 7 1 237.31 200.92 63.18 o 4 7 1 25.61 -73.16 87.97 o 5 7 1 2976.37 2760.94 120.73 o 6 7 1 615.71 636.28 107.27 o 7 7 1 1599.26 1614.45 100.29 o 8 7 1 201.11 210.28 78.33 o 9 7 1 120.86 45.97 86.11 o 10 7 1 81.25 158.79 104.93 o 0 8 1 255.20 234.85 71.70 o 1 8 1 1257.42 1357.05 61.36 o 2 8 1 1682.94 1696.90 68.62 o 3 8 1 2739.58 2647.74 110.74 o 4 8 1 5397.22 5542.85 170.98 o 5 8 1 73.00 147.61 84.31 o 6 8 1 491.68 472.75 98.84 o 7 8 1 2117.17 1875.53 135.82 o 8 8 1 1151.38 1450.89 121.13 o 9 8 1 189.67 347.16 122.65 o 1 9 1 227.36 226.46 52.43 o 2 9 1 3541.15 3538.77 98.57 o 3 9 1 630.73 676.09 81.82 o 4 9 1 880.01 975.82 102.95 o 5 9 1 1459.36 1585.64 131.31 o 6 9 1 5320.14 5354.46 191.67 o 7 9 1 330.25 205.56 104.49 o 8 9 1 927.13 782.12 124.61 o 9 9 1 530.43 472.06 177.28 o 0 10 1 2159.92 2209.61 166.85 o 1 10 1 136.59 234.36 88.86 o 2 10 1 1310.15 1483.85 106.98 o 3 10 1 46.09 31.86 106.21 o 4 10 1 695.52 641.49 169.42 o 5 10 1 287.07 285.38 216.68 o 6 10 1 150.09 264.54 153.93 o 7 10 1 104.61 17.05 204.63 o 1 11 1 48.17 -62.27 90.18 o 2 11 1 142.71 26.63 93.75 o 3 11 1 176.84 -19.93 136.16 o 4 11 1 375.08 238.15 176.86 o 5 11 1 54.79 68.91 168.01 o 6 11 1 43.49 309.32 182.14 o 0 12 1 273.35 132.54 152.22 o 1 12 1 4.02 -113.96 108.64 o 2 12 1 1813.73 1586.86 156.99 o 3 12 1 156.35 -57.91 170.05 o 4 12 1 1447.56 1405.81 443.48 o 2 0 2 10230.91 9033.13 160.10 o 3 0 2 2082.50 1869.87 59.08 o 4 0 2 6502.58 6058.49 127.87 o 5 0 2 126.36 146.89 48.10 o 6 0 2 1741.46 1696.93 93.26 o 7 0 2 1980.38 1970.23 113.87 o 8 0 2 4242.61 4089.17 177.90 o 9 0 2 505.74 565.21 101.73 o 10 0 2 11314.15 11503.46 288.85 o 11 0 2 611.95 452.33 170.76 o 12 0 2 4611.42 3980.88 226.84 o 1 1 2 3654.50 1896.09 95.03 o 2 1 2 7471.86 7593.06 81.69 o 3 1 2 749.75 768.52 21.88 o 4 1 2 5220.62 4986.24 71.64 o 5 1 2 7874.73 8436.19 133.62 o 6 1 2 8016.96 7757.07 133.31 o 7 1 2 489.07 578.64 51.26 o 8 1 2 3057.24 2978.80 88.19 o 9 1 2 751.60 708.69 64.46 o 10 1 2 1.76 128.57 64.60 o 11 1 2 253.74 224.31 82.43 o 12 1 2 1532.90 1487.33 159.00 o 0 2 2 19.54 31.92 14.75 o 1 2 2 34415.18 36197.35 306.38 o 2 2 2 14507.90 14874.04 155.93 o 3 2 2 1853.41 1798.60 34.65 o 4 2 2 1721.44 1737.18 51.61 o 5 2 2 1114.86 1248.58 71.28 o 6 2 2 1079.89 1057.70 44.80 o 7 2 2 904.48 1009.65 63.23 o 8 2 2 2405.15 2473.33 86.60 o 9 2 2 382.12 428.14 72.19 o 10 2 2 42.10 606.31 135.93 o 11 2 2 1.14 85.02 76.76 o 12 2 2 20.59 74.45 98.40 o 1 3 2 358.81 343.26 17.17 o 2 3 2 7476.35 7107.54 81.33 o 3 3 2 531.92 499.01 24.62 o 4 3 2 33447.63 34224.97 419.94 o 5 3 2 49.91 93.29 37.57 o 6 3 2 15718.78 15858.37 250.21 o 7 3 2 2.82 57.13 33.20 o 8 3 2 493.26 521.82 75.03 o 9 3 2 36.91 85.03 63.45 o 10 3 2 25.50 -1.20 68.85 o 11 3 2 292.86 252.70 87.04 o 12 3 2 1424.37 1241.96 117.99 o 0 4 2 19744.71 19883.05 291.31 o 1 4 2 360.72 416.79 22.19 o 2 4 2 20926.34 21422.43 233.77 o 3 4 2 2574.67 2544.96 61.53 o 4 4 2 692.46 572.30 47.13 o 5 4 2 1366.54 1567.85 61.38 o 6 4 2 1034.95 1006.81 61.22 o 7 4 2 333.47 486.11 67.50 o 8 4 2 7448.36 7433.15 148.19 o 9 4 2 981.76 1078.12 85.28 o 10 4 2 5331.45 5370.76 154.94 o 11 4 2 9.77 -143.66 95.78 o 12 4 2 1834.79 1651.14 145.38 o 1 5 2 602.62 647.93 33.49 o 2 5 2 908.04 980.46 44.44 o 3 5 2 398.55 368.33 50.73 o 4 5 2 662.18 666.40 67.34 o 5 5 2 4662.21 5055.47 112.85 o 6 5 2 1797.96 1860.52 77.94 o 7 5 2 1559.28 1621.00 77.47 o 8 5 2 753.50 924.40 77.41 o 9 5 2 179.48 363.62 83.84 o 10 5 2 1.09 -15.11 78.07 o 11 5 2 3.99 209.64 97.28 o 0 6 2 16569.41 16781.67 324.47 o 1 6 2 402.65 500.75 37.45 o 2 6 2 5129.82 5243.59 104.95 o 3 6 2 1733.64 1842.68 73.67 o 4 6 2 542.35 668.31 79.88 o 5 6 2 115.38 170.26 74.19 o 6 6 2 1016.81 1124.33 67.49 o 7 6 2 195.64 223.38 60.95 o 8 6 2 1522.28 1585.43 102.01 o 9 6 2 111.58 56.19 79.88 o 10 6 2 1834.61 1715.18 117.52 o 11 6 2 25.03 -159.96 106.64 o 1 7 2 1.64 -54.14 36.23 o 2 7 2 7746.53 8100.73 145.49 o 3 7 2 676.84 837.87 79.32 o 4 7 2 18701.80 19258.91 388.34 o 5 7 2 116.17 286.04 73.49 o 6 7 2 11018.36 10757.45 228.20 o 7 7 2 1.11 140.24 77.21 o 8 7 2 1433.97 1506.63 104.59 o 9 7 2 24.93 -9.25 86.11 o 10 7 2 287.70 191.60 118.01 o 0 8 2 7753.99 7706.40 194.05 o 1 8 2 73.23 114.94 47.08 o 2 8 2 5417.76 5443.34 113.53 o 3 8 2 264.40 224.42 71.59 o 4 8 2 2291.52 2306.68 113.15 o 5 8 2 2939.62 2952.80 134.24 o 6 8 2 492.65 564.72 129.69 o 7 8 2 1.00 181.20 89.15 o 8 8 2 2123.07 2023.64 124.10 o 9 8 2 17.77 67.25 126.02 o 1 9 2 147.66 116.97 59.18 o 2 9 2 5.02 19.14 58.58 o 3 9 2 430.09 346.78 74.21 o 4 9 2 25.19 16.39 96.49 o 5 9 2 140.80 106.23 94.56 o 6 9 2 12.35 94.31 113.45 o 7 9 2 47.85 10.44 94.53 o 8 9 2 284.06 128.64 108.15 o 0 10 2 8816.97 8928.44 308.20 o 1 10 2 264.64 236.03 112.68 o 2 10 2 2593.47 2626.85 124.62 o 3 10 2 188.29 22.19 94.54 o 4 10 2 1659.88 1736.84 143.64 o 5 10 2 0.17 -121.46 116.89 o 6 10 2 1724.33 1964.59 166.55 o 7 10 2 436.26 281.13 135.33 o 1 11 2 167.98 16.04 98.05 o 2 11 2 3788.63 3476.15 146.25 o 3 11 2 91.08 69.38 120.09 o 4 11 2 6787.83 7048.58 300.16 o 5 11 2 357.06 546.33 203.48 o 6 11 2 1255.65 1316.63 244.47 o 0 12 2 2029.54 1914.51 196.59 o 1 12 2 628.15 487.21 117.14 o 2 12 2 948.10 880.06 132.62 o 3 12 2 9.24 15.59 313.06 o 4 12 2 695.76 656.32 414.91 o 1 1 3 5712.10 5472.70 71.03 o 2 1 3 139.08 198.72 14.21 o 3 1 3 6236.29 6362.32 72.62 o 4 1 3 2992.79 2627.54 46.84 o 5 1 3 4768.84 4871.80 87.47 o 6 1 3 19028.67 18883.62 260.12 o 7 1 3 0.64 133.45 46.92 o 8 1 3 1258.42 1487.68 70.17 o 9 1 3 86.58 86.74 56.75 o 10 1 3 72.36 136.62 65.30 o 11 1 3 18.56 195.08 76.07 o 12 1 3 1651.71 1314.82 149.77 o 0 2 3 14224.41 14005.76 237.45 o 1 2 3 1087.52 1058.70 19.68 o 2 2 3 8617.42 8064.35 91.54 o 3 2 3 1169.39 1078.39 28.81 o 4 2 3 11098.57 11038.97 149.35 o 5 2 3 32.82 25.76 36.50 o 6 2 3 176.42 238.00 37.64 o 7 2 3 32.02 80.81 36.03 o 8 2 3 7753.30 8148.22 160.77 o 9 2 3 1652.37 1550.62 77.09 o 10 2 3 9814.01 9936.39 185.80 o 11 2 3 31.87 12.84 78.05 o 12 2 3 2333.59 1994.40 124.32 o 1 3 3 2249.60 2318.14 34.81 o 2 3 3 243.44 261.03 18.82 o 3 3 3 3444.48 3585.71 56.24 o 4 3 3 6093.17 6509.39 102.10 o 5 3 3 11.79 47.98 37.43 o 6 3 3 759.28 684.19 57.69 o 7 3 3 593.42 650.63 52.69 o 8 3 3 2661.15 2718.50 93.99 o 9 3 3 952.48 1097.85 72.64 o 10 3 3 115.59 176.18 69.21 o 11 3 3 251.35 202.51 89.56 o 12 3 3 573.54 167.43 141.27 o 0 4 3 25744.38 27273.80 387.68 o 1 4 3 1429.34 1667.90 33.53 o 2 4 3 3864.40 3885.43 64.67 o 3 4 3 928.34 1007.31 42.51 o 4 4 3 2.33 54.53 38.56 o 5 4 3 700.72 765.43 52.94 o 6 4 3 1398.08 1451.03 67.19 o 7 4 3 49.02 106.13 60.16 o 8 4 3 1101.28 1349.78 75.72 o 9 4 3 1178.40 1146.81 88.84 o 10 4 3 248.41 278.94 95.69 o 11 4 3 6.85 52.32 89.88 o 12 4 3 104.86 148.05 126.22 o 1 5 3 24.82 14.16 23.96 o 2 5 3 10375.28 10641.19 154.31 o 3 5 3 57.95 48.92 40.39 o 4 5 3 22942.35 23322.35 399.39 o 5 5 3 39.18 176.29 47.32 o 6 5 3 9779.79 9552.94 176.62 o 7 5 3 15.95 3.35 58.92 o 8 5 3 2530.63 2754.52 105.31 o 9 5 3 0.98 110.02 77.30 o 10 5 3 15.22 -8.22 78.61 o 11 5 3 46.23 -55.88 108.99 o 0 6 3 16947.14 18165.01 346.02 o 1 6 3 275.53 318.09 35.09 o 2 6 3 14872.10 15451.88 215.60 o 3 6 3 0.63 81.88 47.46 o 4 6 3 431.31 490.21 77.07 o 5 6 3 455.99 578.04 84.19 o 6 6 3 1141.55 1204.29 75.48 o 7 6 3 3.81 72.53 57.09 o 8 6 3 5289.66 5130.42 218.92 o 9 6 3 453.51 551.42 92.36 o 10 6 3 3654.84 3739.02 145.54 o 11 6 3 0.83 -99.18 110.79 o 1 7 3 22.52 14.29 36.05 o 2 7 3 528.95 500.97 52.95 o 3 7 3 594.93 562.20 67.08 o 4 7 3 246.95 434.48 105.31 o 5 7 3 74.38 76.20 76.21 o 6 7 3 446.50 348.46 102.07 o 7 7 3 149.15 170.93 71.58 o 8 7 3 960.54 859.77 102.52 o 9 7 3 9.47 101.83 102.22 o 10 7 3 70.36 81.71 123.68 o 0 8 3 11325.84 12186.27 267.57 o 1 8 3 36.45 37.02 48.03 o 2 8 3 5913.33 6051.76 119.69 o 3 8 3 316.80 254.08 81.54 o 4 8 3 27.30 -121.68 81.12 o 5 8 3 192.97 49.83 95.94 o 6 8 3 1826.41 1957.65 123.90 o 7 8 3 285.11 294.93 92.34 o 8 8 3 4827.00 4683.67 178.26 o 9 8 3 447.78 441.89 117.49 o 1 9 3 169.51 85.64 63.63 o 2 9 3 7268.02 7389.61 151.21 o 3 9 3 150.92 80.96 69.57 o 4 9 3 18497.13 18417.06 392.06 o 5 9 3 129.75 109.48 146.05 o 6 9 3 4343.45 4243.98 175.77 o 7 9 3 120.21 77.26 96.13 o 8 9 3 395.56 272.70 116.01 o 0 10 3 8298.96 8203.73 252.32 o 1 10 3 3.19 -38.08 76.48 o 2 10 3 2925.82 2923.69 119.32 o 3 10 3 194.08 181.28 97.62 o 4 10 3 6.11 -140.86 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95.12 o 4 8 8 212.13 212.93 78.44 o 5 8 8 21.32 132.02 84.47 o 6 8 8 176.93 184.44 115.02 o 7 8 8 1.05 -81.16 97.21 o 8 8 8 1711.81 1617.20 126.27 o 9 8 8 13.78 7.00 118.59 o 1 9 8 260.75 331.32 65.38 o 2 9 8 320.00 224.63 70.38 o 3 9 8 0.45 99.87 114.26 o 4 9 8 234.87 219.08 115.81 o 5 9 8 291.15 36.08 182.98 o 6 9 8 6.16 38.44 109.48 o 7 9 8 406.89 490.40 114.28 o 8 9 8 218.85 194.84 115.58 o 0 10 8 1472.10 1363.21 146.68 o 1 10 8 374.17 366.86 79.64 o 2 10 8 2774.81 2745.93 117.73 o 3 10 8 27.40 -19.65 95.91 o 4 10 8 833.77 884.80 146.49 o 5 10 8 547.25 678.70 137.33 o 6 10 8 1687.25 1866.21 224.32 o 7 10 8 5.13 47.54 126.98 o 1 11 8 269.30 184.72 117.73 o 2 11 8 4455.69 4510.97 190.67 o 3 11 8 12.23 43.30 121.37 o 4 11 8 6444.14 6019.18 246.62 o 5 11 8 105.31 260.45 166.27 o 6 11 8 1063.72 854.19 471.64 o 0 12 8 6512.36 6321.45 292.51 o 1 12 8 7.90 -58.52 113.89 o 2 12 8 396.28 220.54 132.03 o 3 12 8 34.65 -57.27 162.24 o 1 1 9 4.13 11.77 10.85 o 2 1 9 9270.01 8998.25 81.00 o 3 1 9 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105.34 o 10 6 9 4063.06 4151.67 217.24 o 1 7 9 4201.19 4170.41 107.34 o 2 7 9 40.06 12.32 60.15 o 3 7 9 174.35 224.89 73.67 o 4 7 9 12.28 -10.15 72.76 o 5 7 9 771.05 599.60 84.56 o 6 7 9 1301.86 1273.77 89.30 o 7 7 9 128.97 237.95 93.67 o 8 7 9 3.49 50.81 90.18 o 9 7 9 0.39 -29.55 105.24 o 10 7 9 208.50 350.78 121.60 o 0 8 9 685.49 947.80 102.86 o 1 8 9 2521.42 2712.20 95.68 o 2 8 9 5722.49 6027.53 149.59 o 3 8 9 6780.61 6910.03 195.99 o 4 8 9 6.73 141.29 80.75 o 5 8 9 1224.07 1361.39 107.70 o 6 8 9 1023.25 1181.13 94.55 o 7 8 9 13.76 -7.54 86.51 o 8 8 9 581.71 575.25 119.66 o 9 8 9 560.96 315.07 160.46 o 1 9 9 2285.53 2357.47 97.66 o 2 9 9 1950.10 1900.32 121.32 o 3 9 9 0.78 50.28 88.93 o 4 9 9 2841.75 2851.14 158.59 o 5 9 9 343.67 177.11 113.49 o 6 9 9 4606.46 4709.32 189.95 o 7 9 9 1080.70 1058.72 130.08 o 8 9 9 281.38 369.04 160.99 o 0 10 9 4478.57 4624.56 191.40 o 1 10 9 3.42 -36.02 79.38 o 2 10 9 658.62 787.41 88.28 o 3 10 9 39.25 128.23 90.06 o 4 10 9 5.48 177.60 118.85 o 5 10 9 40.74 281.90 128.61 o 6 10 9 305.70 328.56 135.34 o 7 10 9 0.12 69.14 159.59 o 1 11 9 1169.00 1106.48 106.83 o 2 11 9 214.08 147.25 109.27 o 3 11 9 302.13 200.36 117.12 o 4 11 9 14.48 246.54 137.13 o 5 11 9 144.54 46.64 148.78 o 0 12 9 4703.05 4230.21 250.33 o 1 12 9 459.29 332.56 137.29 o 2 12 9 2071.02 1885.13 166.53 o 3 12 9 1106.86 888.65 229.15 o 0 0 10 95569.30 90514.42 3199.40 o 1 0 10 117.02 96.97 22.45 o 2 0 10 56168.15 55734.90 646.77 o 3 0 10 1869.97 1632.37 38.30 o 4 0 10 192.41 236.74 24.27 o 5 0 10 776.18 768.16 37.68 o 6 0 10 6798.81 6265.49 129.09 o 7 0 10 561.78 608.79 68.44 o 8 0 10 21865.16 22103.22 439.43 o 9 0 10 287.16 382.87 82.33 o 10 0 10 5055.48 4996.09 195.84 o 11 0 10 38.73 214.41 148.66 o 12 0 10 1378.01 1219.60 261.94 o 1 1 10 1385.64 1411.21 22.25 o 2 1 10 20481.46 20467.77 169.10 o 3 1 10 59.51 61.69 15.29 o 4 1 10 25033.77 25453.05 234.07 o 5 1 10 565.75 616.86 27.87 o 6 1 10 5800.21 5381.57 94.14 o 7 1 10 116.24 105.91 37.92 o 8 1 10 220.76 256.39 58.80 o 9 1 10 158.54 98.88 56.84 o 10 1 10 883.48 945.01 80.07 o 11 1 10 149.33 187.12 121.10 o 12 1 10 310.47 398.53 123.03 o 0 2 10 4259.82 4312.92 86.67 o 1 2 10 9733.89 10420.99 101.88 o 2 2 10 3114.73 3201.13 42.59 o 3 2 10 2.94 40.63 17.06 o 4 2 10 881.70 974.89 32.24 o 5 2 10 228.32 320.23 28.69 o 6 2 10 207.66 235.13 34.24 o 7 2 10 257.70 261.10 50.53 o 8 2 10 12.52 92.55 53.66 o 9 2 10 1140.94 1102.87 69.87 o 10 2 10 48.89 137.07 68.95 o 11 2 10 148.88 203.24 111.53 o 12 2 10 180.92 91.63 133.47 o 1 3 10 3754.96 4009.71 56.94 o 2 3 10 23317.34 24058.88 241.03 o 3 3 10 694.23 678.49 26.52 o 4 3 10 27765.99 27698.50 308.00 o 5 3 10 1862.98 1753.12 54.56 o 6 3 10 3335.49 3246.10 75.22 o 7 3 10 401.49 336.55 51.83 o 8 3 10 839.37 932.74 66.77 o 9 3 10 162.29 87.21 66.50 o 10 3 10 108.08 145.68 75.94 o 11 3 10 393.23 503.96 129.49 o 0 4 10 108564.15 115204.44 1895.71 o 1 4 10 571.64 650.96 34.35 o 2 4 10 19553.46 20124.41 236.83 o 3 4 10 333.05 344.52 27.66 o 4 4 10 19.51 1.02 45.70 o 5 4 10 30.79 88.43 42.96 o 6 4 10 6551.47 6332.11 122.15 o 7 4 10 868.61 836.49 52.49 o 8 4 10 6031.54 6306.27 136.37 o 9 4 10 1096.47 1198.98 84.39 o 10 4 10 2081.74 2234.29 128.76 o 11 4 10 407.90 372.47 123.17 o 1 5 10 1103.40 1074.15 58.26 o 2 5 10 13586.54 14114.83 225.15 o 3 5 10 1053.87 955.88 42.13 o 4 5 10 7842.18 8210.42 160.86 o 5 5 10 236.79 145.30 57.49 o 6 5 10 6936.82 7200.63 136.55 o 7 5 10 1935.86 1877.16 72.93 o 8 5 10 78.20 48.30 66.90 o 9 5 10 1143.65 1083.61 95.10 o 10 5 10 274.69 358.89 147.95 o 11 5 10 70.61 97.68 121.75 o 0 6 10 1532.06 1474.75 91.92 o 1 6 10 1364.04 1386.54 63.33 o 2 6 10 368.29 415.45 52.48 o 3 6 10 2910.69 3141.58 102.27 o 4 6 10 110.69 149.26 53.41 o 5 6 10 11.47 19.86 73.75 o 6 6 10 7.94 66.72 56.55 o 7 6 10 60.82 104.90 55.39 o 8 6 10 382.79 208.34 87.10 o 9 6 10 506.71 460.88 107.23 o 10 6 10 595.64 763.31 181.42 o 1 7 10 1925.39 1826.53 76.84 o 2 7 10 4264.43 4283.55 124.50 o 3 7 10 1116.40 1252.32 79.45 o 4 7 10 5095.26 5288.26 159.38 o 5 7 10 1722.32 1723.66 112.30 o 6 7 10 8347.90 8532.76 198.11 o 7 7 10 205.96 39.14 86.97 o 8 7 10 414.73 346.48 94.66 o 9 7 10 486.14 372.23 143.49 o 10 7 10 26.66 78.99 161.63 o 0 8 10 2985.46 3019.91 164.64 o 1 8 10 156.21 132.51 60.62 o 2 8 10 1730.03 1782.70 87.76 o 3 8 10 2570.69 2615.36 125.32 o 4 8 10 29.11 79.67 89.82 o 5 8 10 272.88 301.51 115.69 o 6 8 10 1040.35 1316.35 98.25 o 7 8 10 8.61 -90.04 96.81 o 8 8 10 3520.08 3433.30 215.15 o 9 8 10 6.65 114.19 139.55 o 1 9 10 133.85 80.60 70.54 o 2 9 10 0.70 -5.95 68.87 o 3 9 10 48.42 -127.83 85.22 o 4 9 10 25.39 114.85 105.31 o 5 9 10 259.53 278.20 129.43 o 6 9 10 127.84 251.05 110.41 o 7 9 10 17.16 56.32 118.13 o 8 9 10 18.17 123.98 144.80 o 0 10 10 2250.50 2099.87 142.38 o 1 10 10 551.43 578.70 88.82 o 2 10 10 1231.06 1419.02 115.17 o 3 10 10 548.09 595.05 106.67 o 4 10 10 1358.47 1522.72 142.45 o 5 10 10 58.74 -149.43 133.20 o 6 10 10 16.74 72.29 148.39 o 7 10 10 241.98 55.53 167.00 o 1 11 10 7.79 -57.77 86.32 o 2 11 10 620.87 707.47 139.24 o 3 11 10 148.77 238.39 120.01 o 4 11 10 4361.60 4041.77 211.21 o 5 11 10 134.38 -11.72 195.68 o 0 12 10 705.56 423.20 161.40 o 1 12 10 86.05 303.85 130.38 o 2 12 10 632.30 293.86 152.44 o 3 12 10 553.67 41.12 217.40 o 1 1 11 374.40 404.06 14.07 o 2 1 11 16211.91 16063.36 143.16 o 3 1 11 288.87 398.78 18.15 o 4 1 11 17692.05 16975.53 158.86 o 5 1 11 2013.72 1994.41 42.71 o 6 1 11 9830.20 9599.23 132.11 o 7 1 11 657.23 650.61 46.18 o 8 1 11 2133.96 1997.91 74.11 o 9 1 11 530.69 363.13 64.80 o 10 1 11 12.88 119.28 84.48 o 11 1 11 1.06 62.98 111.95 o 12 1 11 1181.98 1029.30 340.14 o 0 2 11 69847.60 69599.09 929.02 o 1 2 11 13519.85 14402.67 140.05 o 2 2 11 25981.89 25226.19 236.35 o 3 2 11 3886.27 3920.38 56.72 o 4 2 11 397.21 321.42 24.06 o 5 2 11 2372.89 2318.02 48.92 o 6 2 11 5506.59 5290.92 83.65 o 7 2 11 477.91 502.50 46.45 o 8 2 11 10111.16 10180.47 175.48 o 9 2 11 69.84 219.38 58.36 o 10 2 11 3263.16 3504.63 150.05 o 11 2 11 377.23 327.94 115.10 o 12 2 11 501.89 206.29 122.38 o 1 3 11 685.86 521.90 23.01 o 2 3 11 17688.39 18150.65 197.79 o 3 3 11 26.83 36.38 21.01 o 4 3 11 11063.15 10740.46 136.73 o 5 3 11 1518.41 1613.65 53.15 o 6 3 11 4852.88 4812.98 95.04 o 7 3 11 1495.04 1361.85 57.16 o 8 3 11 353.09 432.16 59.38 o 9 3 11 98.18 -32.97 61.41 o 10 3 11 1314.40 1229.04 147.80 o 11 3 11 17.41 -24.29 110.88 o 0 4 11 4836.94 5570.89 137.93 o 1 4 11 12356.07 13838.56 188.23 o 2 4 11 1405.71 1522.56 45.09 o 3 4 11 72.63 48.09 22.08 o 4 4 11 956.92 1007.16 41.77 o 5 4 11 710.25 655.72 45.81 o 6 4 11 668.32 725.13 53.60 o 7 4 11 2686.39 2601.54 76.33 o 8 4 11 24.59 93.58 56.80 o 9 4 11 722.49 746.35 96.13 o 10 4 11 1185.07 1412.80 133.70 o 11 4 11 364.19 191.89 108.93 o 1 5 11 443.36 400.65 47.66 o 2 5 11 4113.57 3904.05 88.55 o 3 5 11 1116.08 1191.56 55.46 o 4 5 11 9113.63 9005.73 172.70 o 5 5 11 632.71 639.71 53.36 o 6 5 11 8518.30 8699.19 154.45 o 7 5 11 73.22 116.63 49.08 o 8 5 11 1785.36 1980.31 107.10 o 9 5 11 1247.24 1251.19 102.64 o 10 5 11 338.59 181.12 114.97 o 11 5 11 178.08 173.59 162.41 o 0 6 11 24865.83 24828.43 511.44 o 1 6 11 461.40 388.50 53.60 o 2 6 11 7136.23 7251.53 151.21 o 3 6 11 96.40 120.34 52.38 o 4 6 11 240.19 282.18 54.53 o 5 6 11 5966.83 5785.40 140.50 o 6 6 11 517.05 531.23 62.50 o 7 6 11 90.14 85.14 69.26 o 8 6 11 8500.95 8420.42 222.07 o 9 6 11 220.31 341.67 118.41 o 10 6 11 6489.32 6184.70 299.52 o 1 7 11 981.76 972.33 69.83 o 2 7 11 1661.63 1609.31 91.37 o 3 7 11 415.26 506.56 66.07 o 4 7 11 1460.02 1556.08 97.45 o 5 7 11 633.29 626.97 90.67 o 6 7 11 162.23 180.08 79.33 o 7 7 11 345.73 259.75 83.42 o 8 7 11 669.96 509.09 98.68 o 9 7 11 321.77 274.98 131.35 o 10 7 11 1041.74 703.86 520.71 o 0 8 11 2726.76 2850.63 139.39 o 1 8 11 170.67 156.82 63.23 o 2 8 11 2488.32 2460.89 105.07 o 3 8 11 728.66 790.18 91.67 o 4 8 11 1309.51 1348.58 104.90 o 5 8 11 147.56 212.40 115.86 o 6 8 11 119.69 202.71 111.22 o 7 8 11 50.92 -33.08 83.26 o 8 8 11 1154.54 1392.16 163.16 o 9 8 11 17.85 288.12 160.96 o 1 9 11 644.31 487.80 102.23 o 2 9 11 2381.23 2357.85 110.19 o 3 9 11 315.09 350.03 102.73 o 4 9 11 2595.51 2926.36 160.50 o 5 9 11 2.15 -76.25 110.37 o 6 9 11 3842.97 3853.73 179.12 o 7 9 11 4.34 151.15 129.54 o 8 9 11 2613.26 2239.18 221.04 o 0 10 11 2449.24 2461.35 154.93 o 1 10 11 351.29 549.44 82.08 o 2 10 11 1867.47 1810.67 127.49 o 3 10 11 254.25 252.16 99.88 o 4 10 11 714.12 779.73 134.85 o 5 10 11 56.95 -16.31 135.14 o 6 10 11 24.15 142.67 205.06 o 7 10 11 92.31 18.01 165.17 o 1 11 11 401.55 285.45 103.80 o 2 11 11 58.00 -91.51 103.05 o 3 11 11 155.71 84.41 118.96 o 4 11 11 22.36 50.43 144.36 o 5 11 11 387.94 250.18 194.13 o 0 12 11 680.79 620.91 163.18 o 1 12 11 7.46 -195.07 130.05 o 2 12 11 716.48 434.59 191.63 o 0 0 12 20710.95 19872.61 488.69 o 1 0 12 1429.46 1473.62 37.75 o 2 0 12 14961.93 13947.92 188.25 o 3 0 12 5323.46 4966.13 91.86 o 4 0 12 258.22 147.63 33.88 o 5 0 12 1819.51 1791.88 51.82 o 6 0 12 2988.75 2769.39 80.84 o 7 0 12 151.59 181.65 56.74 o 8 0 12 2389.22 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2 6 35 1972.65 2153.72 202.62 o 3 6 35 27.42 154.21 165.29 o 4 6 35 16.73 -32.63 164.14 o 1 7 35 298.12 389.24 188.09 o 2 7 35 19.02 11.52 163.44 o 0 0 36 838.97 925.15 175.67 o 1 0 36 1712.13 1719.33 145.36 o 2 0 36 1609.13 2099.79 215.67 o 3 0 36 55.84 36.95 131.44 o 4 0 36 13.60 225.52 392.55 o 5 0 36 14.67 15.89 153.08 o 6 0 36 320.00 298.97 139.96 o 7 0 36 130.05 481.93 392.03 o 1 1 36 128.86 5.12 90.14 o 2 1 36 761.80 854.33 95.24 o 3 1 36 57.11 48.41 92.56 o 4 1 36 1888.00 1989.37 150.07 o 5 1 36 20.79 129.98 121.90 o 6 1 36 837.91 1029.02 154.08 o 0 2 36 166.52 385.77 227.13 o 1 2 36 17.95 -42.10 107.50 o 2 2 36 165.08 44.67 125.96 o 3 2 36 262.75 301.96 140.33 o 4 2 36 23.73 -200.01 151.19 o 5 2 36 496.09 346.30 248.17 o 6 2 36 3.11 -19.29 123.42 o 1 3 36 791.43 1028.12 159.57 o 2 3 36 1142.91 1400.86 169.39 o 3 3 36 432.08 426.03 178.77 o 4 3 36 3959.23 3779.15 230.57 o 5 3 36 282.65 188.63 152.60 o 6 3 36 959.87 1288.67 266.94 o 0 4 36 9532.93 9834.44 489.98 o 1 4 36 78.86 359.94 148.40 o 2 4 36 3359.82 3425.14 208.49 o 3 4 36 18.74 -91.15 146.33 o 4 4 36 655.64 732.83 178.84 o 5 4 36 65.47 116.56 170.19 o 1 5 36 677.73 306.30 216.74 o 2 5 36 3161.38 3252.41 258.94 o 3 5 36 1.88 95.83 167.53 o 4 5 36 591.77 543.82 187.96 o 0 6 36 730.98 828.42 258.49 o 1 6 36 1129.25 1584.46 296.62 o 2 6 36 34.15 293.40 227.74 o 3 6 36 1030.56 860.18 216.96 o 1 1 37 1717.38 1689.95 105.76 o 2 1 37 2463.91 2465.74 125.41 o 3 1 37 91.18 186.25 99.44 o 4 1 37 1551.86 1691.71 188.65 o 5 1 37 94.17 29.65 190.09 o 6 1 37 732.74 569.31 132.01 o 0 2 37 15502.81 16904.09 663.09 o 1 2 37 336.41 440.67 130.40 o 2 2 37 2595.00 2557.04 171.33 o 3 2 37 847.93 749.77 146.87 o 4 2 37 124.03 -47.59 146.88 o 5 2 37 1592.13 1876.89 190.25 o 6 2 37 959.25 960.53 179.69 o 1 3 37 11.29 -25.88 166.85 o 2 3 37 2157.21 2116.22 177.90 o 3 3 37 72.39 15.29 127.61 o 4 3 37 2407.39 2604.28 206.81 o 5 3 37 246.40 337.23 226.64 o 0 4 37 36.82 -32.33 618.85 o 1 4 37 4.97 258.53 231.81 o 2 4 37 15.78 284.24 139.44 o 3 4 37 1541.49 1255.61 228.46 o 4 4 37 1626.56 1613.13 194.61 o 5 4 37 118.86 -14.59 165.66 o 1 5 37 1348.91 1748.81 192.42 o 2 5 37 367.35 595.94 215.30 o 3 5 37 320.05 567.57 172.79 o 4 5 37 1565.29 1048.33 198.98 o 0 6 37 2528.92 2884.61 331.77 o 1 6 37 238.06 -42.71 176.62 o 2 6 37 1476.44 1808.81 215.88 o 0 0 38 358.54 679.72 272.88 o 1 0 38 1095.59 1328.85 143.57 o 2 0 38 2184.46 1687.42 152.96 o 3 0 38 3495.31 3533.54 198.96 o 4 0 38 424.54 214.94 197.83 o 5 0 38 3118.14 2640.04 215.95 o 1 1 38 390.04 281.86 108.76 o 2 1 38 697.16 969.47 100.78 o 3 1 38 1070.88 960.50 109.13 o 4 1 38 840.30 1072.06 141.92 o 5 1 38 68.12 358.58 127.91 o 0 2 38 959.72 1251.93 212.81 o 1 2 38 3.20 -0.84 127.94 o 2 2 38 8.45 -190.34 126.89 o 3 2 38 1.44 45.94 125.76 o 4 2 38 33.25 -5.55 160.15 o 5 2 38 335.64 448.69 167.08 o 1 3 38 935.88 1168.86 147.09 o 2 3 38 466.80 331.90 216.66 o 3 3 38 112.38 302.04 178.96 o 4 3 38 1086.58 1138.53 181.70 o 5 3 38 371.75 286.73 160.08 o 0 4 38 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