#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:15:41 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180839 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/70/2017067.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017067_Fobs loop_ _publ_author_name 'Jeremi\'c, Dejan' 'Kaluderovi\'c, Goran N.' 'G\'omez-Ruiz, Santiago' 'Br\D-camphor-10-sulfonato)calcium(II) ; _journal_coeditor_code SQ3182 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m143 _journal_page_last m145 _journal_volume 65 _journal_year 2009 _space_group_IT_number 20 _symmetry_space_group_name_Hall 'C 2c 2' _symmetry_space_group_name_H-M 'C 2 2 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.5020 _cell_length_b 10.8274 _cell_length_c 32.3927 _exptl_crystal_F_000 1224.00 _reflns_d_resolution_high 0.7501 _cod_data_source_file sq3182Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' c2221 in C222(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 410.69 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x, -y, -z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z+1/2' 'x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 15801.10 17027.27 105.88 o 4 0 0 5.04 15.90 11.52 o 6 0 0 2.20 22.97 48.35 o 8 0 0 7297.79 7043.62 171.10 o 10 0 0 3541.86 3871.59 208.40 o 1 1 0 254.03 244.30 8.24 o 3 1 0 50.83 49.02 7.68 o 5 1 0 394.43 391.16 12.99 o 7 1 0 201.60 182.14 37.34 o 9 1 0 53.39 339.78 109.69 o 0 2 0 168668.73 158801.00 836.85 o 2 2 0 15558.89 15483.83 105.43 o 4 2 0 1762.31 1728.02 25.26 o 6 2 0 1589.41 1553.93 49.40 o 8 2 0 1710.42 1657.27 75.88 o 1 3 0 776.08 819.38 20.67 o 3 3 0 3021.42 3086.41 36.02 o 5 3 0 2083.47 2298.36 31.63 o 7 3 0 6.06 37.99 38.32 o 9 3 0 17.15 63.12 79.92 o 0 4 0 7465.23 6833.96 62.15 o 2 4 0 1372.33 1156.39 25.25 o 4 4 0 634.96 643.69 23.27 o 6 4 0 3149.86 3166.07 50.21 o 8 4 0 84.62 76.80 57.63 o 1 5 0 3073.82 3359.84 39.36 o 3 5 0 2611.26 2591.32 38.34 o 5 5 0 6770.86 7253.22 76.53 o 7 5 0 2.53 46.37 57.02 o 9 5 0 0.01 134.97 91.04 o 0 6 0 30380.29 31364.15 154.22 o 2 6 0 645.18 705.57 27.44 o 4 6 0 835.68 842.21 30.84 o 6 6 0 3.88 -5.52 29.22 o 8 6 0 547.85 616.72 86.61 o 1 7 0 3082.15 3025.73 36.89 o 3 7 0 60.75 90.59 25.06 o 5 7 0 2808.55 3010.19 64.80 o 7 7 0 265.23 282.56 78.79 o 0 8 0 4206.61 4329.31 74.02 o 2 8 0 914.91 876.23 34.14 o 4 8 0 1074.57 960.54 39.12 o 6 8 0 689.12 747.98 47.35 o 8 8 0 499.60 601.02 113.01 o 1 9 0 488.02 421.02 33.34 o 3 9 0 733.70 751.02 38.00 o 5 9 0 199.65 190.66 44.55 o 7 9 0 269.06 450.00 101.10 o 0 10 0 265.74 329.38 50.02 o 2 10 0 1270.12 1194.95 45.49 o 4 10 0 1053.73 1032.39 53.97 o 6 10 0 33.33 45.38 63.93 o 1 11 0 59.24 42.14 35.35 o 3 11 0 1064.79 1022.25 55.13 o 5 11 0 2857.72 2946.22 119.93 o 0 12 0 200.05 254.61 67.17 o 2 12 0 324.34 368.50 46.95 o 4 12 0 328.72 247.97 51.97 o 1 13 0 1256.04 1155.21 63.32 o 3 13 0 288.74 322.42 57.41 o 0 14 0 23.33 410.05 158.07 o 2 14 0 239.75 251.98 60.53 o 2 0 1 1.88 24.69 10.05 o 4 0 1 915.98 988.54 15.38 o 6 0 1 131.30 194.58 41.03 o 8 0 1 1.88 64.85 66.27 o -9 1 1 673.09 984.00 159.00 o -7 1 1 305.21 353.93 41.36 o -5 1 1 7513.40 7472.50 41.50 o -3 1 1 1271.93 1525.24 14.42 o -1 1 1 4129.06 4129.48 21.51 o 1 1 1 4026.76 4101.44 20.51 o 3 1 1 1406.98 1658.79 15.71 o 5 1 1 7352.30 7402.45 42.30 o 7 1 1 336.90 384.21 46.29 o 9 1 1 675.32 912.46 108.51 o -8 2 1 695.91 832.19 80.90 o -6 2 1 657.15 624.17 40.49 o -4 2 1 273.84 297.78 12.60 o -2 2 1 6235.96 6274.31 44.74 o 0 2 1 500.10 477.65 11.70 o 2 2 1 6244.94 6292.73 46.03 o 4 2 1 284.85 277.52 11.63 o 6 2 1 659.06 601.85 38.77 o 8 2 1 684.55 819.31 88.01 o -9 3 1 89.02 96.05 79.04 o -7 3 1 261.61 255.95 38.10 o -5 3 1 15055.08 15093.38 73.97 o -3 3 1 29421.47 30753.68 146.86 o -1 3 1 1674.68 1533.89 23.57 o 1 3 1 1650.05 1547.98 25.36 o 3 3 1 29593.15 31303.78 162.23 o 5 3 1 14877.83 14950.99 79.20 o 7 3 1 255.66 280.28 50.68 o 9 3 1 88.38 81.93 78.96 o -8 4 1 832.17 766.84 72.96 o -6 4 1 1012.31 936.72 44.80 o -4 4 1 195.03 187.76 19.05 o -2 4 1 993.03 981.14 24.85 o 0 4 1 2088.52 1910.01 24.85 o 2 4 1 1024.51 1022.81 24.40 o 4 4 1 204.78 206.89 19.27 o 6 4 1 981.12 942.90 31.90 o 8 4 1 801.67 756.23 75.13 o -9 5 1 207.81 292.14 72.19 o -7 5 1 1905.68 1932.40 90.07 o -5 5 1 10774.21 10977.17 77.85 o -3 5 1 6150.03 6526.21 56.26 o -1 5 1 6757.05 7125.32 71.61 o 1 5 1 6693.87 7034.21 49.47 o 3 5 1 6150.49 6599.59 57.10 o 5 5 1 10821.96 11064.86 72.07 o 7 5 1 1897.33 1751.84 86.71 o 9 5 1 203.14 255.17 87.80 o -8 6 1 492.68 571.49 84.07 o -6 6 1 57.49 75.78 29.22 o -4 6 1 967.41 969.19 32.75 o -2 6 1 26.57 44.15 20.25 o 0 6 1 8167.78 8386.30 59.00 o 2 6 1 17.65 9.00 20.63 o 4 6 1 982.86 967.31 31.73 o 6 6 1 52.01 85.66 30.80 o 8 6 1 494.39 607.67 78.66 o -7 7 1 1039.08 1031.57 102.50 o -5 7 1 3263.44 3168.02 72.90 o -3 7 1 1133.49 1131.44 35.16 o -1 7 1 462.03 451.36 19.97 o 1 7 1 449.93 487.12 21.66 o 3 7 1 1268.99 1191.65 36.23 o 5 7 1 3259.70 3354.54 75.66 o 7 7 1 1018.93 1104.89 103.57 o -8 8 1 1013.88 1222.75 119.95 o -6 8 1 37.67 94.95 39.71 o -4 8 1 229.13 234.35 32.49 o -2 8 1 3726.49 3631.86 55.83 o 0 8 1 9623.00 9848.54 88.52 o 2 8 1 3698.72 3606.18 55.32 o 4 8 1 243.01 246.70 30.40 o 6 8 1 42.42 38.64 41.70 o 8 8 1 1009.30 870.60 90.11 o -7 9 1 461.88 523.56 96.54 o -5 9 1 173.81 198.42 43.56 o -3 9 1 2163.81 2056.70 48.44 o -1 9 1 1449.13 1412.00 41.82 o 1 9 1 1508.60 1538.91 44.25 o 3 9 1 2287.71 2272.14 50.13 o 5 9 1 177.67 179.71 54.26 o 7 9 1 415.73 366.66 87.86 o -6 10 1 173.67 223.31 58.64 o -4 10 1 536.32 523.07 45.28 o -2 10 1 3366.49 3340.13 63.54 o 0 10 1 3709.58 3776.19 67.21 o 2 10 1 3295.37 3287.11 63.29 o 4 10 1 519.91 455.30 45.66 o 6 10 1 177.43 198.19 58.44 o -5 11 1 248.78 409.58 116.01 o -3 11 1 90.23 123.63 39.09 o -1 11 1 178.91 170.75 37.45 o 1 11 1 189.83 205.33 38.50 o 3 11 1 93.16 127.59 41.68 o 5 11 1 275.86 366.75 80.64 o -4 12 1 105.52 117.44 49.37 o -2 12 1 367.24 373.34 47.36 o 0 12 1 3020.19 2956.06 74.57 o 2 12 1 321.70 285.46 46.27 o 4 12 1 101.60 174.20 57.77 o -3 13 1 297.21 269.19 56.06 o -1 13 1 249.99 344.89 50.41 o 1 13 1 237.78 286.84 46.87 o 3 13 1 312.81 449.72 59.75 o -2 14 1 342.92 330.98 61.50 o 0 14 1 1333.06 1221.50 67.55 o 2 14 1 314.15 291.74 61.11 o 2 0 2 4597.48 5073.51 31.06 o 4 0 2 1341.79 1427.76 24.85 o 6 0 2 9290.19 9381.17 102.99 o 8 0 2 2249.41 2305.66 88.69 o -9 1 2 578.70 727.81 87.57 o -7 1 2 7602.15 7599.87 102.62 o -5 1 2 51.74 76.89 11.45 o -3 1 2 1387.78 1305.32 18.53 o -1 1 2 44826.15 45169.58 163.72 o 1 1 2 44762.19 44858.43 140.41 o 3 1 2 1384.09 1298.07 18.02 o 5 1 2 55.89 83.23 13.30 o 7 1 2 7643.90 7537.87 112.08 o 9 1 2 586.35 771.89 98.80 o -8 2 2 1627.50 1582.20 90.72 o -6 2 2 264.50 218.60 29.58 o -4 2 2 2154.89 2375.07 23.03 o -2 2 2 4221.30 4147.05 33.83 o 0 2 2 2844.05 2905.44 22.49 o 2 2 2 4070.79 4001.75 32.90 o 4 2 2 2095.62 2323.30 23.90 o 6 2 2 244.34 220.58 30.83 o 8 2 2 1644.24 1759.22 105.22 o -9 3 2 539.61 1281.46 691.74 o -7 3 2 2059.63 1983.71 68.19 o -5 3 2 3161.53 3296.70 34.58 o -3 3 2 3086.41 3327.19 36.10 o -1 3 2 7055.36 7416.52 61.58 o 1 3 2 6944.94 7232.97 66.98 o 3 3 2 3169.57 3390.26 35.00 o 5 3 2 3245.44 3356.27 34.44 o 7 3 2 2110.77 2096.26 103.19 o 9 3 2 552.25 1065.91 382.59 o -8 4 2 604.80 650.88 71.20 o -6 4 2 1222.58 1188.32 48.94 o -4 4 2 1742.85 1742.29 29.27 o -2 4 2 1133.59 1223.19 25.27 o 0 4 2 37.90 8.20 14.79 o 2 4 2 988.09 1063.76 24.85 o 4 4 2 1652.98 1643.88 28.81 o 6 4 2 1274.17 1244.42 36.39 o 8 4 2 563.63 663.24 78.38 o -9 5 2 446.89 534.42 78.56 o -7 5 2 2813.57 2648.09 98.76 o -5 5 2 2928.14 3034.83 46.92 o -3 5 2 1146.84 1168.52 29.45 o -1 5 2 4503.35 4767.65 47.71 o 1 5 2 4444.36 4682.78 44.59 o 3 5 2 1182.49 1171.19 23.48 o 5 5 2 2958.27 3034.65 44.35 o 7 5 2 2855.63 2793.12 114.50 o 9 5 2 462.21 504.67 95.23 o -8 6 2 464.92 536.84 74.91 o -6 6 2 386.76 406.21 34.24 o -4 6 2 1660.63 1661.12 40.87 o -2 6 2 2691.24 2772.35 42.06 o 0 6 2 10772.56 10408.56 77.27 o 2 6 2 2476.66 2529.03 38.69 o 4 6 2 1576.29 1641.57 42.33 o 6 6 2 422.12 426.13 36.75 o 8 6 2 424.18 564.59 75.78 o -7 7 2 1092.87 1036.74 88.99 o -5 7 2 3579.81 3532.62 88.15 o -3 7 2 239.56 244.61 27.41 o -1 7 2 1164.80 1140.52 32.55 o 1 7 2 1106.18 1121.68 27.36 o 3 7 2 293.18 305.47 29.53 o 5 7 2 3526.98 3536.32 77.11 o 7 7 2 1102.57 1088.39 155.85 o -8 8 2 789.51 801.02 111.23 o -6 8 2 96.44 109.65 41.41 o -4 8 2 1114.40 1055.81 43.15 o -2 8 2 1321.43 1238.78 37.67 o 0 8 2 9752.60 9924.70 75.92 o 2 8 2 1351.46 1251.51 38.39 o 4 8 2 1091.42 1083.48 41.46 o 6 8 2 77.04 143.32 44.59 o 8 8 2 735.52 759.79 89.79 o -7 9 2 143.16 248.55 96.00 o -5 9 2 2766.62 2692.33 66.86 o -3 9 2 1284.37 1247.73 41.41 o -1 9 2 4114.25 4090.31 59.42 o 1 9 2 4064.75 4065.76 67.66 o 3 9 2 1287.31 1323.33 41.92 o 5 9 2 2756.93 2625.43 73.77 o 7 9 2 112.32 233.65 101.27 o -6 10 2 84.41 108.95 58.73 o -4 10 2 1258.07 1215.85 52.48 o -2 10 2 794.28 754.71 38.42 o 0 10 2 1511.96 1445.55 51.05 o 2 10 2 852.33 801.48 39.26 o 4 10 2 1231.46 1220.56 51.05 o 6 10 2 81.61 91.27 56.21 o -5 11 2 1731.28 1840.82 102.69 o -3 11 2 656.11 667.74 47.30 o -1 11 2 201.21 215.95 37.05 o 1 11 2 184.68 205.66 38.89 o 3 11 2 654.12 753.90 52.21 o 5 11 2 1670.64 1854.55 113.33 o -4 12 2 520.91 567.48 61.91 o -2 12 2 562.54 540.55 49.98 o 0 12 2 192.21 265.04 42.43 o 2 12 2 548.68 521.19 50.79 o 4 12 2 492.44 506.18 63.19 o -3 13 2 476.78 614.75 63.72 o -1 13 2 549.86 582.15 54.32 o 1 13 2 535.03 510.38 49.99 o 3 13 2 517.89 612.25 61.68 o -2 14 2 57.28 48.58 56.10 o 0 14 2 10.67 44.08 51.12 o 2 14 2 56.73 126.61 57.84 o 2 0 3 49916.55 50013.62 247.78 o 4 0 3 6456.40 7077.03 52.50 o 6 0 3 2702.76 2747.92 63.01 o 8 0 3 6.79 78.24 52.65 o -9 1 3 112.66 211.72 77.60 o -7 1 3 473.48 633.79 45.94 o -5 1 3 6329.49 6279.21 49.62 o -3 1 3 710.63 819.03 17.39 o -1 1 3 72.34 80.87 8.81 o 1 1 3 102.62 113.52 10.68 o 3 1 3 795.30 894.81 17.09 o 5 1 3 6326.81 6425.40 42.43 o 7 1 3 434.88 457.69 46.87 o 9 1 3 98.01 295.95 145.74 o -8 2 3 727.24 736.31 74.27 o -6 2 3 1117.67 1156.94 40.05 o -4 2 3 8966.16 9226.98 50.20 o -2 2 3 5848.11 5770.34 49.09 o 0 2 3 8199.22 8769.91 38.31 o 2 2 3 5933.11 5880.76 41.88 o 4 2 3 8942.83 9256.81 51.79 o 6 2 3 1062.67 1063.50 33.83 o 8 2 3 712.04 1103.18 250.90 o -9 3 3 2023.26 1998.95 163.45 o -7 3 3 1273.75 1234.29 61.70 o -5 3 3 5254.77 5290.82 41.63 o -3 3 3 9011.36 8919.82 56.17 o -1 3 3 16090.41 17098.41 97.59 o 1 3 3 16328.92 17411.68 94.50 o 3 3 3 9017.13 8881.68 59.59 o 5 3 3 5193.03 5297.01 43.91 o 7 3 3 1141.20 1218.22 57.67 o 9 3 3 2022.18 1905.33 175.70 o -8 4 3 1219.95 1205.51 130.78 o -6 4 3 651.46 661.73 42.85 o -4 4 3 2779.38 2753.94 39.40 o -2 4 3 715.59 558.88 20.58 o 0 4 3 369.26 395.42 18.12 o 2 4 3 719.25 579.39 21.72 o 4 4 3 2817.47 2790.39 37.56 o 6 4 3 614.71 638.33 32.67 o 8 4 3 1176.25 1260.16 118.78 o -9 5 3 321.16 399.07 77.05 o -7 5 3 3176.89 3121.79 118.32 o -5 5 3 7163.56 7135.14 66.06 o -3 5 3 3722.66 3753.02 49.78 o -1 5 3 8586.73 9352.54 64.50 o 1 5 3 8735.01 9421.54 61.01 o 3 5 3 3723.14 3676.94 37.73 o 5 5 3 7138.51 7082.11 66.74 o 7 5 3 3029.55 3093.36 110.29 o 9 5 3 307.42 316.08 103.08 o -8 6 3 117.76 112.97 69.75 o -6 6 3 1233.49 1256.64 49.61 o -4 6 3 321.56 314.24 27.89 o -2 6 3 2422.85 2334.27 39.89 o 0 6 3 9208.61 9461.01 71.92 o 2 6 3 2542.25 2507.18 39.04 o 4 6 3 358.78 340.77 30.09 o 6 6 3 1187.28 1142.88 50.79 o 8 6 3 123.87 105.81 69.97 o -7 7 3 1529.81 1578.44 108.89 o -5 7 3 2157.70 2112.27 53.19 o -3 7 3 1422.24 1553.71 41.53 o -1 7 3 1194.43 1203.99 33.59 o 1 7 3 1160.87 1121.07 32.15 o 3 7 3 1502.18 1699.41 40.10 o 5 7 3 2130.86 2026.38 55.93 o 7 7 3 1439.00 1501.16 174.74 o -8 8 3 242.50 221.13 103.10 o -6 8 3 431.76 458.93 47.32 o -4 8 3 2367.41 2206.98 56.97 o -2 8 3 502.32 477.16 30.47 o 0 8 3 2299.36 2380.97 42.20 o 2 8 3 555.11 541.32 32.27 o 4 8 3 2363.54 2208.17 51.18 o 6 8 3 420.95 434.83 52.74 o 8 8 3 246.66 354.08 98.71 o -7 9 3 404.49 355.06 89.90 o -5 9 3 1550.83 1559.05 66.01 o -3 9 3 1609.59 1538.71 47.03 o -1 9 3 426.72 455.52 33.66 o 1 9 3 479.49 511.50 35.18 o 3 9 3 1664.72 1599.02 44.71 o 5 9 3 1495.02 1569.65 62.35 o 7 9 3 352.74 439.19 161.18 o -6 10 3 273.28 397.82 63.10 o -4 10 3 1523.26 1396.09 53.12 o -2 10 3 1308.84 1257.97 44.00 o 0 10 3 617.25 535.66 41.06 o 2 10 3 1278.72 1215.86 43.45 o 4 10 3 1542.07 1459.93 55.36 o 6 10 3 272.83 374.08 66.38 o -5 11 3 989.64 1135.09 82.83 o -3 11 3 797.19 781.72 48.31 o -1 11 3 615.99 655.61 45.78 o 1 11 3 662.37 716.80 45.98 o 3 11 3 806.09 736.83 50.62 o 5 11 3 978.87 1150.79 88.92 o -4 12 3 24.07 37.92 54.74 o -2 12 3 336.92 316.01 46.69 o 0 12 3 3732.01 3694.92 80.42 o 2 12 3 349.19 336.39 46.22 o 4 12 3 36.85 60.40 55.34 o -3 13 3 442.53 533.77 61.73 o -1 13 3 77.33 104.35 46.94 o 1 13 3 72.93 108.43 48.70 o 3 13 3 432.76 544.72 60.02 o -2 14 3 5.60 145.36 62.94 o 0 14 3 1319.71 1229.60 68.04 o 2 14 3 12.36 73.20 59.07 o 2 0 4 522.77 608.96 18.82 o 4 0 4 2951.75 3133.42 35.60 o 6 0 4 5483.57 5469.56 63.42 o 8 0 4 521.31 539.01 61.61 o -9 1 4 143.07 1239.37 152.38 o -7 1 4 4.03 53.97 33.78 o -5 1 4 2340.63 2389.11 36.52 o -3 1 4 2386.77 2165.03 28.24 o -1 1 4 1717.39 1659.02 16.89 o 1 1 4 1774.76 1742.01 17.67 o 3 1 4 2289.22 2084.48 30.06 o 5 1 4 2323.28 2485.11 27.13 o 7 1 4 10.94 42.65 39.09 o 9 1 4 139.34 2021.97 218.70 o -8 2 4 627.30 746.31 74.79 o -6 2 4 1354.15 1341.52 43.41 o -4 2 4 6131.83 6556.96 48.65 o -2 2 4 1612.00 1548.83 23.38 o 0 2 4 71.02 71.95 13.37 o 2 2 4 1502.11 1436.42 21.21 o 4 2 4 6218.48 6686.50 42.72 o 6 2 4 1451.57 1437.76 34.52 o 8 2 4 642.13 845.36 121.74 o -9 3 4 231.51 1054.50 611.55 o -7 3 4 835.97 747.52 52.59 o -5 3 4 251.17 278.21 16.87 o -3 3 4 5525.50 5388.15 44.39 o -1 3 4 31752.21 32221.76 108.60 o 1 3 4 31476.02 32075.07 185.75 o 3 3 4 5428.16 5285.18 48.20 o 5 3 4 269.89 287.52 19.22 o 7 3 4 846.67 843.99 52.36 o 9 3 4 222.14 1179.87 598.84 o -8 4 4 1831.30 1867.48 97.97 o -6 4 4 1396.02 1437.72 54.28 o -4 4 4 3197.77 3252.50 37.66 o -2 4 4 1147.86 1131.96 24.83 o 0 4 4 1273.98 1483.97 27.23 o 2 4 4 1110.82 1084.20 24.96 o 4 4 4 3189.19 3204.85 38.14 o 6 4 4 1505.91 1581.61 41.55 o 8 4 4 1934.04 1891.30 118.17 o -9 5 4 542.09 547.44 82.91 o -7 5 4 1694.84 1824.36 76.95 o -5 5 4 270.26 293.39 26.23 o -3 5 4 1057.82 1060.40 30.52 o -1 5 4 2953.86 2890.54 38.96 o 1 5 4 2889.52 2808.61 40.65 o 3 5 4 1085.88 1038.03 28.70 o 5 5 4 240.68 253.43 25.91 o 7 5 4 1678.90 1658.75 89.47 o 9 5 4 558.70 566.23 99.46 o -8 6 4 879.46 878.09 101.17 o -6 6 4 4771.53 4994.80 97.36 o -4 6 4 41.80 54.22 27.12 o -2 6 4 5399.48 5573.84 56.90 o 0 6 4 777.23 599.63 24.76 o 2 6 4 5297.42 5459.30 53.71 o 4 6 4 68.49 96.57 27.44 o 6 6 4 4852.96 4842.93 84.54 o 8 6 4 929.62 1006.97 85.58 o -7 7 4 1563.09 1670.68 216.99 o -5 7 4 1135.15 1107.66 44.02 o -3 7 4 1018.59 976.66 36.35 o -1 7 4 2552.42 2619.58 43.36 o 1 7 4 2545.62 2674.65 43.20 o 3 7 4 959.84 904.14 33.06 o 5 7 4 1061.79 958.30 42.12 o 7 7 4 1575.81 1649.11 231.24 o -8 8 4 1607.68 1633.90 122.54 o -6 8 4 2997.58 3123.07 74.34 o -4 8 4 942.52 826.50 42.77 o -2 8 4 7691.44 7821.54 81.85 o 0 8 4 2114.53 2065.73 42.32 o 2 8 4 7560.29 7747.64 76.65 o 4 8 4 882.52 780.46 39.78 o 6 8 4 3104.36 3124.42 88.07 o 8 8 4 1657.60 1689.92 107.45 o -7 9 4 385.09 335.38 78.34 o -5 9 4 200.43 234.16 43.48 o -3 9 4 1529.93 1376.11 48.89 o -1 9 4 2129.80 2040.10 47.00 o 1 9 4 1986.70 1921.11 46.51 o 3 9 4 1500.63 1424.88 42.64 o 5 9 4 204.03 206.11 41.08 o 7 9 4 404.68 442.42 117.64 o -6 10 4 614.79 692.36 70.69 o -4 10 4 2038.40 1917.52 62.73 o -2 10 4 1562.16 1625.96 45.48 o 0 10 4 976.74 884.00 39.64 o 2 10 4 1509.56 1478.19 46.14 o 4 10 4 1993.37 1840.96 58.96 o 6 10 4 661.95 828.44 73.21 o -5 11 4 259.11 336.34 61.92 o -3 11 4 978.55 939.04 48.16 o -1 11 4 301.17 287.23 39.04 o 1 11 4 254.96 238.98 36.96 o 3 11 4 978.02 998.73 48.08 o 5 11 4 296.88 363.54 62.30 o -4 12 4 9.15 -9.96 53.59 o -2 12 4 1033.76 921.14 55.37 o 0 12 4 520.37 552.72 46.42 o 2 12 4 1017.76 982.74 57.31 o 4 12 4 7.45 83.68 62.24 o -3 13 4 321.43 357.64 62.98 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