#------------------------------------------------------------------------------ #$Date: 2009-05-13 10:52:48 +0300 (Wed, 13 May 2009) $ #$Revision: 717 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2017072.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017072_Fobs loop_ _publ_author_name 'Yong, Ken W. L.' 'Garson, Mary J.' 'Bernhardt, Paul V.' _publ_section_title ; Absolute structures and conformations of the spongian diterpenes spongia-13(16),14-dien-3-one, epispongiadiol and spongiadiol ; _journal_coeditor_code SQ3189 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o167 _journal_page_last o170 _journal_volume 65 _journal_year 2009 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.734 _cell_angle_gamma 90.000 _cell_length_a 9.5317 _cell_length_b 7.8958 _cell_length_c 11.6742 _exptl_crystal_F_000 360.00 _reflns_d_resolution_high 0.8699 _[local]_cod_data_source_file sq3189IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' 153ky2 in P 1 21 1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 67.26 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 -8 0 48.50 55.18 1.93 o 2 -7 0 15.40 18.02 1.48 o 3 -7 0 25.36 28.24 1.33 o 6 -7 0 51.84 63.87 2.27 o 2 -6 0 228.66 281.20 5.19 o 3 -6 0 23.39 25.13 1.68 o 4 -6 0 53.51 55.29 1.18 o 5 -6 0 29.82 40.39 0.93 o 6 -6 0 54.93 61.96 1.97 o 7 -6 0 5.95 5.84 0.52 o 8 -6 0 95.35 126.40 2.82 o 1 -5 0 117.21 123.53 2.90 o 2 -5 0 14.00 13.66 1.06 o 3 -5 0 39.44 53.02 1.46 o 4 -5 0 30.96 39.29 1.30 o 5 -5 0 19.30 25.00 0.67 o 6 -5 0 21.17 25.53 0.80 o 7 -5 0 31.45 31.00 0.90 o 8 -5 0 68.05 86.50 1.55 o 0 -4 0 889.58 999.29 4.22 o 1 -4 0 82.61 102.63 0.85 o 2 -4 0 385.53 467.57 3.42 o 3 -4 0 47.05 59.96 0.90 o 4 -4 0 301.51 352.43 3.53 o 5 -4 0 10.71 11.74 0.42 o 6 -4 0 237.70 249.13 1.91 o 7 -4 0 133.96 151.97 1.44 o 8 -4 0 4.26 3.46 0.45 o 9 -4 0 134.54 147.58 2.01 o 1 -3 0 619.82 675.51 4.11 o 2 -3 0 380.85 455.11 1.79 o 3 -3 0 1539.56 1695.26 7.48 o 4 -3 0 7.77 6.95 0.34 o 5 -3 0 308.28 330.17 1.86 o 6 -3 0 140.72 158.81 1.34 o 7 -3 0 602.10 627.56 4.03 o 8 -3 0 394.43 422.60 2.59 o 9 -3 0 27.54 28.61 0.88 o 10 -3 0 36.65 39.96 1.26 o 0 -2 0 950.54 945.41 2.53 o 1 -2 0 468.56 479.46 4.49 o 2 -2 0 2090.94 2121.34 10.72 o 3 -2 0 23.92 25.22 0.81 o 4 -2 0 17.95 17.47 0.38 o 5 -2 0 7.15 8.02 0.27 o 6 -2 0 250.75 282.10 3.43 o 7 -2 0 441.51 453.63 2.41 o 8 -2 0 24.75 25.56 0.65 o 9 -2 0 96.01 100.25 1.62 o 10 -2 0 44.32 50.84 1.26 o 1 -1 0 864.28 837.61 11.99 o 2 -1 0 339.90 329.95 3.47 o 3 -1 0 362.88 383.44 2.62 o 4 -1 0 141.79 141.05 1.59 o 5 -1 0 140.72 148.27 1.47 o 6 -1 0 490.71 495.92 4.50 o 7 -1 0 82.67 77.94 1.03 o 8 -1 0 40.52 40.32 0.72 o 9 -1 0 269.18 264.85 2.14 o 10 -1 0 9.67 11.24 0.68 o 1 0 0 85.18 83.27 0.57 o 2 0 0 540.80 525.14 1.48 o 3 0 0 1367.72 1297.38 4.01 o 4 0 0 93.96 89.00 0.74 o 5 0 0 342.58 353.70 2.70 o 6 0 0 78.30 79.38 0.77 o 7 0 0 63.38 60.51 0.71 o 8 0 0 38.02 38.74 0.80 o 9 0 0 18.75 18.24 0.71 o 10 0 0 0.14 0.29 0.51 o 1 1 0 863.06 765.96 2.55 o 2 1 0 339.13 314.17 2.52 o 3 1 0 361.88 355.70 4.19 o 4 1 0 143.04 136.89 1.03 o 5 1 0 139.54 141.72 1.24 o 6 1 0 490.94 463.36 6.05 o 7 1 0 81.45 72.64 1.00 o 8 1 0 40.29 38.78 0.87 o 9 1 0 269.79 251.08 2.10 o 10 1 0 9.61 9.89 0.58 o 0 2 0 954.79 846.30 2.94 o 1 2 0 467.90 439.53 5.18 o 2 2 0 2091.94 1885.20 4.43 o 3 2 0 23.30 20.57 0.51 o 4 2 0 18.02 15.65 0.67 o 5 2 0 7.30 6.97 0.43 o 6 2 0 250.19 252.08 1.53 o 7 2 0 438.95 405.86 2.29 o 8 2 0 24.28 21.43 0.67 o 9 2 0 97.37 89.81 1.81 o 10 2 0 44.54 43.02 1.28 o 1 3 0 618.40 583.78 5.63 o 2 3 0 380.22 376.11 1.90 o 3 3 0 1546.85 1431.18 10.64 o 4 3 0 7.44 5.57 0.29 o 5 3 0 308.51 289.84 2.34 o 6 3 0 141.12 135.33 1.32 o 7 3 0 603.57 543.81 4.28 o 8 3 0 393.09 360.21 3.06 o 9 3 0 27.05 23.06 0.95 o 10 3 0 37.46 34.75 2.12 o 0 4 0 884.34 834.03 4.27 o 1 4 0 82.61 84.90 1.56 o 2 4 0 384.74 389.19 11.83 o 3 4 0 47.09 47.88 0.97 o 4 4 0 299.84 283.90 2.84 o 5 4 0 10.38 9.10 0.32 o 6 4 0 238.10 199.10 1.80 o 7 4 0 134.64 122.81 1.95 o 8 4 0 4.12 2.91 0.34 o 9 4 0 134.62 119.94 2.18 o 1 5 0 117.92 93.48 2.51 o 2 5 0 13.85 9.30 0.45 o 3 5 0 40.19 39.01 0.73 o 4 5 0 31.35 29.34 0.59 o 5 5 0 19.40 19.01 0.43 o 6 5 0 21.36 19.21 0.41 o 7 5 0 31.32 24.24 0.55 o 8 5 0 68.10 68.61 1.30 o 0 6 0 592.54 551.85 4.29 o 1 6 0 140.57 119.53 1.43 o 2 6 0 229.16 205.66 1.96 o 3 6 0 23.59 18.34 0.58 o 4 6 0 53.77 40.13 0.80 o 5 6 0 29.64 27.92 0.81 o 6 6 0 54.85 46.50 1.20 o 7 6 0 5.84 3.79 0.38 o 1 7 0 923.53 809.67 3.77 o 2 7 0 15.80 13.48 0.51 o 3 7 0 25.63 21.31 0.91 o 4 7 0 212.93 176.50 2.12 o 5 7 0 79.96 83.23 1.23 o 6 7 0 51.79 45.83 0.86 o 0 8 0 46.80 43.79 1.17 o 1 8 0 4.78 4.80 0.40 o 2 8 0 4.88 4.57 0.43 o 3 8 0 4.10 4.66 0.35 o 4 8 0 48.62 45.19 0.73 o 5 8 0 46.26 41.03 1.03 o -4 -8 1 40.48 42.21 1.66 o -6 -7 1 43.47 56.10 2.14 o -5 -7 1 3.98 5.19 0.94 o -4 -7 1 88.75 99.40 3.42 o -3 -7 1 46.44 57.86 2.54 o -2 -7 1 68.87 85.52 3.06 o 2 -7 1 40.71 49.74 2.40 o 3 -7 1 52.91 60.28 1.85 o 4 -7 1 1.24 1.48 0.84 o 5 -7 1 38.64 37.88 1.73 o 6 -7 1 7.10 7.86 0.54 o -8 -6 1 68.23 86.76 1.43 o -7 -6 1 47.37 53.55 1.50 o -6 -6 1 9.30 15.05 0.92 o -5 -6 1 48.70 50.74 1.80 o -4 -6 1 3.35 7.36 1.20 o -3 -6 1 5.71 6.68 0.73 o -2 -6 1 156.71 183.63 4.02 o 2 -6 1 98.70 112.80 3.18 o 3 -6 1 108.88 118.27 2.48 o 4 -6 1 15.98 14.81 0.70 o 5 -6 1 8.78 15.03 0.60 o 6 -6 1 2.99 3.59 0.85 o 7 -6 1 4.37 6.55 0.50 o -9 -5 1 4.38 4.59 0.62 o -8 -5 1 4.94 5.51 0.47 o -7 -5 1 43.17 44.49 0.79 o -6 -5 1 28.43 30.13 0.65 o -5 -5 1 44.03 47.62 0.96 o -4 -5 1 10.67 12.10 0.60 o -3 -5 1 183.66 224.13 4.01 o -2 -5 1 143.80 180.19 3.66 o -1 -5 1 367.58 414.85 2.99 o 0 -5 1 48.56 49.84 3.10 o 2 -5 1 307.59 373.00 5.27 o 3 -5 1 121.38 125.77 3.22 o 4 -5 1 154.02 179.80 2.04 o 5 -5 1 92.38 99.54 1.41 o 6 -5 1 105.61 125.51 1.57 o 7 -5 1 0.54 0.91 0.51 o 8 -5 1 13.25 16.16 0.72 o -9 -4 1 84.68 98.00 1.42 o -8 -4 1 49.11 50.57 1.30 o -7 -4 1 285.37 309.86 2.03 o -6 -4 1 172.88 199.31 1.80 o -5 -4 1 16.08 16.72 0.67 o -4 -4 1 63.38 82.09 1.26 o -3 -4 1 33.55 38.74 0.72 o -2 -4 1 327.41 394.58 1.83 o -1 -4 1 16.33 14.98 0.33 o 0 -4 1 267.72 313.96 3.28 o 1 -4 1 293.19 347.55 2.20 o 2 -4 1 245.56 283.56 3.21 o 3 -4 1 20.11 31.93 0.85 o 4 -4 1 1.76 2.29 0.33 o 5 -4 1 95.13 114.93 1.25 o 6 -4 1 685.40 745.44 3.97 o 7 -4 1 42.04 43.28 0.74 o 8 -4 1 71.06 78.02 1.54 o 9 -4 1 60.15 69.66 1.99 o -10 -3 1 32.66 35.02 1.34 o -9 -3 1 15.41 17.88 0.65 o -8 -3 1 164.61 185.25 1.51 o -7 -3 1 25.60 27.72 0.71 o -6 -3 1 61.14 62.96 0.71 o -5 -3 1 178.89 212.97 2.23 o -4 -3 1 68.65 79.49 1.23 o -3 -3 1 1885.13 2077.98 11.48 o -2 -3 1 1124.90 1261.34 5.16 o -1 -3 1 287.31 311.19 1.44 o 0 -3 1 419.78 450.57 1.56 o 1 -3 1 14.58 19.74 0.31 o 2 -3 1 1134.33 1288.80 4.10 o 3 -3 1 299.54 366.80 2.32 o 4 -3 1 274.23 306.78 3.27 o 5 -3 1 113.42 115.65 0.93 o 6 -3 1 205.16 242.11 1.53 o 7 -3 1 396.75 422.51 2.83 o 8 -3 1 77.98 82.83 1.29 o 9 -3 1 40.08 43.99 1.03 o -10 -2 1 10.77 11.43 0.82 o -9 -2 1 2.93 2.72 0.41 o -8 -2 1 11.76 13.10 0.50 o -7 -2 1 108.96 107.06 1.37 o -6 -2 1 162.91 166.78 1.64 o -5 -2 1 76.06 79.74 0.89 o -4 -2 1 118.89 117.29 1.03 o -3 -2 1 63.83 60.23 0.57 o -2 -2 1 2344.71 2241.15 13.95 o -1 -2 1 41.01 46.93 0.73 o 0 -2 1 1021.42 1002.31 5.82 o 1 -2 1 588.18 580.73 2.72 o 2 -2 1 273.76 273.58 2.70 o 3 -2 1 567.48 615.70 3.83 o 4 -2 1 26.55 31.48 0.42 o 5 -2 1 31.95 36.19 0.56 o 6 -2 1 337.81 374.06 3.46 o 7 -2 1 98.01 104.88 1.20 o 8 -2 1 34.75 39.33 0.73 o 9 -2 1 81.66 89.90 1.33 o 10 -2 1 22.15 23.60 0.85 o -10 -1 1 19.16 18.88 0.72 o -9 -1 1 32.15 31.93 0.98 o -8 -1 1 30.28 33.40 0.73 o -7 -1 1 59.71 57.26 0.79 o -6 -1 1 91.30 92.40 0.90 o -5 -1 1 22.80 23.92 0.50 o -4 -1 1 87.64 83.39 0.62 o -3 -1 1 2264.17 2199.17 8.38 o 1 -1 1 515.73 497.56 19.33 o 2 -1 1 460.28 445.91 1.42 o 3 -1 1 387.43 407.37 2.19 o 4 -1 1 169.65 174.10 0.96 o 5 -1 1 164.01 178.94 1.42 o 6 -1 1 144.41 160.80 1.87 o 7 -1 1 50.32 49.50 0.81 o 8 -1 1 55.36 52.12 0.90 o 9 -1 1 65.18 62.55 1.07 o 10 -1 1 25.81 26.72 0.94 o -10 0 1 106.14 104.91 1.88 o -9 0 1 952.24 924.15 4.88 o -8 0 1 271.99 273.01 1.83 o -7 0 1 3.68 5.29 0.27 o -6 0 1 111.44 109.02 0.93 o -5 0 1 37.50 32.91 0.46 o -4 0 1 311.29 284.50 2.99 o -3 0 1 75.63 69.04 1.26 o -2 0 1 1931.58 1763.47 83.30 o -1 0 1 777.28 746.18 6.79 o 0 0 1 1.18 1.17 0.14 o 1 0 1 537.71 499.07 3.92 o 2 0 1 171.72 163.57 0.92 o 3 0 1 425.26 443.18 1.95 o 4 0 1 640.75 731.51 2.15 o 5 0 1 44.28 41.91 0.72 o 6 0 1 174.20 178.06 1.83 o 7 0 1 1.05 0.61 0.27 o 8 0 1 330.68 309.81 2.38 o 9 0 1 40.66 39.24 0.96 o 10 0 1 34.67 35.12 0.90 o -10 1 1 19.20 17.99 0.80 o -9 1 1 31.62 31.18 0.83 o -8 1 1 29.97 32.28 0.74 o -7 1 1 59.50 53.45 0.79 o -6 1 1 92.19 89.27 0.92 o -5 1 1 23.31 22.94 0.64 o -4 1 1 87.91 78.16 0.92 o -3 1 1 2265.91 2015.79 14.95 o 1 1 1 520.15 463.53 2.77 o 2 1 1 461.82 436.85 3.70 o 3 1 1 393.81 394.85 3.54 o 4 1 1 167.42 161.13 1.26 o 5 1 1 164.10 171.57 1.75 o 6 1 1 145.00 153.80 1.19 o 7 1 1 50.66 47.43 0.83 o 8 1 1 55.17 50.72 0.91 o 9 1 1 64.94 60.35 1.17 o 10 1 1 26.34 24.95 0.75 o -10 2 1 10.67 10.83 0.50 o -9 2 1 2.94 4.00 0.94 o -8 2 1 11.84 10.87 0.55 o -7 2 1 109.51 95.05 1.18 o -6 2 1 162.67 151.19 1.17 o -5 2 1 74.90 71.04 1.11 o -4 2 1 120.92 107.36 1.59 o -3 2 1 62.48 49.90 0.66 o -2 2 1 2339.43 2051.87 7.65 o -1 2 1 40.57 40.54 0.68 o 0 2 1 1022.04 902.72 2.90 o 1 2 1 589.76 526.60 2.57 o 2 2 1 269.17 238.19 3.39 o 3 2 1 566.18 554.50 3.18 o 4 2 1 26.52 29.30 0.60 o 5 2 1 32.04 33.58 0.63 o 6 2 1 336.88 331.30 1.78 o 7 2 1 96.61 91.58 1.39 o 8 2 1 34.28 32.72 0.88 o 9 2 1 80.41 80.49 1.67 o 10 2 1 22.13 18.91 0.76 o -10 3 1 33.11 28.73 1.18 o -9 3 1 15.26 14.18 0.82 o -8 3 1 165.90 156.85 2.27 o -7 3 1 25.45 23.57 0.57 o -6 3 1 62.58 53.64 0.90 o -5 3 1 178.18 180.28 3.85 o -4 3 1 68.55 68.21 2.02 o -3 3 1 1884.91 1782.99 11.30 o -2 3 1 1131.11 1099.18 3.99 o -1 3 1 288.68 267.82 1.34 o 0 3 1 418.22 392.77 3.14 o 1 3 1 14.69 16.73 0.30 o 2 3 1 1135.74 1107.08 5.99 o 3 3 1 297.92 300.50 2.17 o 4 3 1 273.50 251.19 2.69 o 5 3 1 115.15 99.80 0.99 o 6 3 1 203.39 203.56 1.46 o 7 3 1 398.63 355.08 2.22 o 8 3 1 79.47 73.58 1.53 o 9 3 1 40.88 38.02 1.11 o -9 4 1 83.84 70.73 1.81 o -8 4 1 49.65 41.52 1.16 o -7 4 1 284.34 249.31 2.43 o -6 4 1 171.73 161.32 2.13 o -5 4 1 15.42 12.63 0.37 o -4 4 1 63.85 65.46 1.28 o -3 4 1 32.97 30.92 0.69 o -2 4 1 328.31 336.19 2.11 o -1 4 1 17.43 13.05 0.40 o 0 4 1 269.95 254.32 3.31 o 1 4 1 295.17 308.32 2.59 o 2 4 1 245.05 231.84 10.83 o 3 4 1 19.87 24.09 0.56 o 4 4 1 1.84 2.01 0.21 o 5 4 1 93.40 88.83 1.02 o 6 4 1 683.51 578.06 11.26 o 7 4 1 41.96 34.86 0.71 o 8 4 1 70.97 66.03 1.82 o 9 4 1 60.03 55.20 2.85 o -9 5 1 4.49 3.11 0.82 o -8 5 1 4.80 4.07 0.33 o -7 5 1 42.89 33.37 0.68 o -6 5 1 28.40 23.55 0.43 o -5 5 1 44.22 35.45 0.55 o -4 5 1 10.78 8.68 0.36 o -3 5 1 184.35 174.39 1.94 o -2 5 1 144.25 136.37 1.30 o -1 5 1 368.53 338.87 3.53 o 0 5 1 48.55 42.27 0.65 o 1 5 1 119.66 111.73 1.21 o 2 5 1 305.42 276.32 5.38 o 3 5 1 123.37 98.69 1.73 o 4 5 1 154.95 134.93 1.33 o 5 5 1 92.54 79.27 1.12 o 6 5 1 105.95 95.61 1.95 o 7 5 1 0.52 0.45 0.28 o 8 5 1 13.49 13.13 0.48 o -8 6 1 67.25 68.55 1.98 o -7 6 1 46.99 41.16 1.02 o -6 6 1 9.54 11.64 0.45 o -5 6 1 48.19 34.11 0.79 o -4 6 1 3.37 4.76 0.35 o -3 6 1 5.46 4.13 0.33 o -2 6 1 155.24 124.12 2.34 o -1 6 1 304.82 250.67 3.88 o 0 6 1 570.26 473.88 6.49 o 1 6 1 117.07 105.11 1.43 o 2 6 1 96.68 80.20 1.11 o 3 6 1 108.23 87.53 1.21 o 4 6 1 15.69 11.56 0.49 o 5 6 1 8.58 10.44 0.43 o 6 6 1 3.10 2.90 0.36 o 7 6 1 4.35 4.55 0.43 o -6 7 1 43.46 43.48 0.75 o -5 7 1 3.96 3.29 0.30 o -4 7 1 87.58 71.54 1.00 o -3 7 1 46.10 40.06 0.84 o -2 7 1 67.72 59.53 1.29 o -1 7 1 73.11 66.17 2.18 o 0 7 1 97.18 84.43 1.52 o 1 7 1 118.79 106.00 1.32 o 2 7 1 40.66 37.04 0.77 o 3 7 1 52.64 43.74 1.00 o 4 7 1 1.18 1.09 0.28 o 5 7 1 39.11 28.38 0.87 o 6 7 1 7.12 6.19 0.39 o -5 8 1 23.41 24.83 0.66 o -4 8 1 40.60 33.04 0.57 o -3 8 1 13.99 13.16 0.43 o -2 8 1 17.78 15.33 0.76 o -1 8 1 4.65 3.80 0.46 o 0 8 1 1.14 1.41 0.34 o 1 8 1 10.56 9.73 0.47 o 2 8 1 3.52 2.72 0.35 o 3 8 1 20.45 17.49 0.66 o 4 8 1 43.93 43.39 0.99 o -6 -7 2 7.03 5.30 0.92 o -5 -7 2 30.11 28.42 1.68 o -4 -7 2 0.12 0.79 0.82 o -3 -7 2 12.63 14.14 1.39 o -2 -7 2 403.99 472.76 14.02 o -1 -7 2 4.40 6.37 1.16 o 1 -7 2 23.26 24.06 1.59 o 2 -7 2 40.24 47.53 2.88 o 3 -7 2 128.73 152.20 2.76 o 4 -7 2 54.30 68.71 2.39 o 5 -7 2 85.96 102.31 2.72 o 6 -7 2 2.84 3.69 0.46 o -8 -6 2 18.34 19.06 0.74 o -7 -6 2 17.60 22.78 1.52 o -6 -6 2 15.84 19.40 1.56 o -5 -6 2 77.42 83.23 1.31 o -4 -6 2 204.46 251.43 3.63 o -3 -6 2 49.21 56.43 2.28 o -2 -6 2 18.95 19.86 1.57 o 2 -6 2 145.73 167.46 2.91 o 3 -6 2 121.21 134.83 2.13 o 4 -6 2 78.46 81.19 1.44 o 5 -6 2 91.49 103.01 1.46 o 6 -6 2 58.22 73.60 2.54 o 7 -6 2 10.70 11.71 0.66 o -9 -5 2 3.27 3.42 0.46 o -8 -5 2 2.71 2.76 0.51 o -7 -5 2 2.26 2.70 0.43 o -6 -5 2 2.90 3.09 0.37 o -5 -5 2 18.40 20.41 1.23 o -4 -5 2 70.97 88.93 1.62 o -3 -5 2 153.39 169.06 3.82 o -2 -5 2 38.05 45.79 2.05 o -1 -5 2 5.82 3.85 0.70 o 2 -5 2 38.95 45.71 1.35 o 3 -5 2 25.60 29.21 0.82 o 4 -5 2 46.69 57.10 1.17 o 5 -5 2 175.66 195.61 2.31 o 6 -5 2 10.13 12.37 0.48 o 7 -5 2 159.76 178.83 2.66 o 8 -5 2 10.02 10.96 0.77 o -9 -4 2 0.45 0.40 0.41 o -8 -4 2 41.64 47.79 0.82 o -7 -4 2 94.38 101.55 1.78 o -6 -4 2 49.88 56.17 0.85 o -5 -4 2 54.11 54.69 1.02 o -4 -4 2 156.05 174.67 2.05 o -3 -4 2 1281.22 1497.71 9.91 o -2 -4 2 487.75 542.44 4.71 o -1 -4 2 18.17 18.84 0.40 o 0 -4 2 224.02 233.72 2.08 o 1 -4 2 421.76 462.77 3.09 o 2 -4 2 204.75 253.99 2.02 o 3 -4 2 100.39 117.25 1.41 o 4 -4 2 31.07 33.25 0.67 o 5 -4 2 225.98 263.45 1.79 o 6 -4 2 421.35 477.12 2.78 o 7 -4 2 39.77 40.29 0.71 o 8 -4 2 1.10 1.25 0.54 o 9 -4 2 36.53 45.28 1.32 o -10 -3 2 1.31 2.27 0.45 o -9 -3 2 48.93 54.55 1.04 o -8 -3 2 134.50 143.32 1.33 o -7 -3 2 175.27 185.91 1.44 o -6 -3 2 30.98 36.15 0.58 o -5 -3 2 102.79 106.50 1.04 o -4 -3 2 62.30 76.82 0.89 o -3 -3 2 77.97 90.94 0.84 o -2 -3 2 2061.55 2167.27 5.49 o -1 -3 2 643.31 652.24 2.33 o 0 -3 2 989.91 1044.19 4.76 o 1 -3 2 262.96 304.95 2.43 o 2 -3 2 1393.98 1561.73 6.96 o 3 -3 2 16.37 17.74 0.36 o 4 -3 2 5.61 7.19 0.37 o 5 -3 2 239.73 278.46 1.82 o 6 -3 2 761.79 810.44 4.01 o 7 -3 2 229.84 235.44 1.66 o 8 -3 2 179.87 198.37 3.14 o 9 -3 2 1.60 1.68 0.48 o -10 -2 2 14.50 15.22 0.82 o -9 -2 2 3.39 3.14 0.36 o -8 -2 2 158.09 172.97 1.54 o -7 -2 2 8.71 9.25 0.34 o -6 -2 2 69.40 75.56 0.91 o -5 -2 2 43.69 46.12 0.67 o -4 -2 2 431.59 430.66 2.46 o -3 -2 2 1448.46 1628.35 7.97 o -2 -2 2 155.00 160.65 1.05 o -1 -2 2 525.85 525.72 2.08 o 0 -2 2 336.38 316.37 2.80 o 1 -2 2 240.71 259.71 2.11 o 2 -2 2 470.93 496.00 1.66 o 3 -2 2 202.98 196.77 1.06 o 4 -2 2 132.52 136.19 1.20 o 5 -2 2 93.67 92.97 0.73 o 6 -2 2 559.61 578.20 2.61 o 7 -2 2 10.01 11.50 0.39 o 8 -2 2 174.42 172.43 1.57 o 9 -2 2 9.31 11.15 0.53 o -10 -1 2 309.04 323.27 3.23 o -9 -1 2 34.38 33.86 0.88 o -8 -1 2 18.41 21.55 0.55 o -7 -1 2 93.21 96.70 0.89 o -6 -1 2 133.39 140.17 1.75 o -5 -1 2 371.69 350.55 1.86 o -4 -1 2 214.46 213.04 1.61 o -3 -1 2 423.72 454.15 2.08 o -2 -1 2 804.06 841.37 2.78 o -1 -1 2 352.14 333.79 2.69 o 0 -1 2 221.12 193.68 1.03 o 1 -1 2 890.94 825.23 3.04 o 2 -1 2 643.48 639.94 2.80 o 3 -1 2 114.07 122.83 0.70 o 4 -1 2 866.68 904.47 6.07 o 5 -1 2 179.23 201.53 1.35 o 6 -1 2 43.77 40.74 0.55 o 7 -1 2 121.08 124.81 2.73 o 8 -1 2 52.94 53.52 1.00 o 9 -1 2 195.22 200.49 2.04 o 10 -1 2 2.18 1.72 0.51 o -10 0 2 163.31 175.23 3.36 o -9 0 2 79.39 82.40 1.56 o -8 0 2 19.64 17.46 0.51 o -7 0 2 0.18 0.57 0.25 o -6 0 2 21.92 22.87 0.43 o -5 0 2 48.48 49.32 0.83 o -4 0 2 258.14 248.72 1.76 o -3 0 2 1879.15 1803.60 5.17 o 0 0 2 345.56 303.48 1.25 o 1 0 2 92.25 94.21 0.57 o 2 0 2 0.01 0.23 0.09 o 3 0 2 580.06 564.85 3.48 o 4 0 2 1410.14 1449.85 4.87 o 5 0 2 7.68 12.74 0.41 o 6 0 2 4.65 5.85 0.27 o 7 0 2 0.41 2.40 0.57 o 8 0 2 112.28 113.04 1.39 o 9 0 2 0.75 0.63 0.50 o 10 0 2 255.04 269.09 2.66 o -10 1 2 307.21 296.60 2.63 o -9 1 2 35.00 31.78 0.86 o -8 1 2 18.68 20.05 0.66 o -7 1 2 93.96 93.69 1.02 o -6 1 2 132.54 134.09 1.64 o -5 1 2 369.42 328.04 2.56 o -4 1 2 213.73 205.94 1.88 o -3 1 2 425.31 417.41 4.26 o -2 1 2 804.69 811.19 7.85 o -1 1 2 352.76 307.63 3.63 o 0 1 2 223.52 185.91 0.88 o 1 1 2 892.07 794.07 8.50 o 2 1 2 639.76 587.47 4.16 o 3 1 2 113.98 117.35 0.91 o 4 1 2 867.23 863.50 4.49 o 5 1 2 180.91 197.94 1.76 o 6 1 2 44.49 40.07 0.66 o 7 1 2 119.65 114.22 1.40 o 8 1 2 53.65 51.06 1.08 o 9 1 2 195.00 190.16 2.23 o 10 1 2 1.95 2.13 0.54 o -10 2 2 14.45 13.12 0.56 o -9 2 2 3.50 2.71 0.40 o -8 2 2 156.96 147.38 2.18 o -7 2 2 9.00 8.08 0.45 o -6 2 2 69.57 68.03 1.02 o -5 2 2 43.83 43.36 0.84 o -4 2 2 431.80 380.79 1.99 o -3 2 2 1447.26 1418.04 8.37 o -2 2 2 153.93 145.08 1.91 o -1 2 2 528.03 479.26 1.90 o 0 2 2 335.87 294.07 2.12 o 1 2 2 240.57 248.39 0.74 o 2 2 2 470.34 460.14 5.01 o 3 2 2 202.57 177.63 1.57 o 4 2 2 131.41 123.31 1.42 o 5 2 2 95.38 85.68 1.00 o 6 2 2 557.68 507.49 2.60 o 7 2 2 10.07 8.77 0.51 o 8 2 2 174.20 154.91 1.83 o 9 2 2 9.06 9.96 0.57 o 10 2 2 7.91 8.31 0.96 o -10 3 2 1.30 2.07 0.46 o -9 3 2 48.74 45.31 0.98 o -8 3 2 134.30 120.56 1.47 o -7 3 2 175.76 157.86 1.76 o -6 3 2 31.64 30.29 0.50 o -5 3 2 102.99 91.59 1.19 o -4 3 2 63.44 64.96 1.17 o -3 3 2 78.21 77.59 1.02 o -2 3 2 2059.66 1885.90 13.17 o -1 3 2 643.77 567.48 1.96 o 0 3 2 987.19 903.94 10.81 o 1 3 2 266.19 270.43 1.67 o 2 3 2 1390.70 1323.19 13.52 o 3 3 2 16.15 14.07 0.45 o 4 3 2 5.68 6.33 0.24 o 5 3 2 240.22 237.59 2.04 o 6 3 2 764.19 700.41 4.27 o 7 3 2 229.29 202.68 2.43 o 8 3 2 179.93 165.35 2.44 o 9 3 2 1.62 1.79 0.49 o -9 4 2 0.51 0.04 0.44 o -8 4 2 42.01 39.20 0.75 o -7 4 2 93.89 80.20 0.99 o -6 4 2 48.89 44.64 0.61 o -5 4 2 55.39 45.87 0.72 o -4 4 2 155.00 141.51 2.21 o -3 4 2 1283.28 1225.27 8.65 o -2 4 2 488.51 450.88 3.08 o -1 4 2 17.60 16.27 0.66 o 0 4 2 223.79 187.06 2.81 o 1 4 2 422.80 374.06 16.74 o 2 4 2 204.97 204.29 9.22 o 3 4 2 101.15 97.96 1.47 o 4 4 2 31.32 27.66 0.49 o 5 4 2 223.52 212.22 1.71 o 6 4 2 423.60 385.72 4.90 o 7 4 2 40.42 33.36 0.79 o 8 4 2 1.03 0.47 0.47 o 9 4 2 36.49 35.37 0.94 o -9 5 2 3.13 3.42 0.80 o -8 5 2 2.68 2.63 0.31 o -7 5 2 2.42 2.20 0.28 o -6 5 2 2.79 2.09 0.25 o -5 5 2 18.02 14.48 0.43 o -4 5 2 70.98 64.58 1.08 o -3 5 2 153.92 128.14 2.48 o -2 5 2 38.02 33.62 0.68 o -1 5 2 5.85 3.64 0.30 o 0 5 2 568.25 519.72 2.31 o 1 5 2 76.41 69.99 0.76 o 2 5 2 38.45 35.08 0.56 o 3 5 2 26.22 22.38 0.48 o 4 5 2 46.72 44.44 0.65 o 5 5 2 175.93 153.45 1.65 o 6 5 2 9.90 9.12 0.43 o 7 5 2 160.90 139.72 1.67 o 8 5 2 10.10 8.75 0.52 o -8 6 2 17.84 14.15 0.99 o -7 6 2 18.21 17.26 0.61 o -6 6 2 15.69 15.89 0.51 o -5 6 2 77.46 60.92 1.24 o -4 6 2 203.81 183.01 4.19 o -3 6 2 50.06 41.34 0.99 o -2 6 2 19.30 15.12 0.41 o -1 6 2 220.94 195.15 4.28 o 0 6 2 442.19 387.84 4.27 o 1 6 2 72.24 69.14 1.70 o 2 6 2 147.79 127.52 2.26 o 3 6 2 120.30 100.82 1.21 o 4 6 2 77.69 58.34 0.92 o 5 6 2 91.73 77.23 1.12 o 6 6 2 58.11 57.29 1.33 o 7 6 2 10.38 8.34 0.52 o -6 7 2 6.82 4.32 0.27 o -5 7 2 30.50 22.51 0.51 o -4 7 2 0.10 0.68 0.24 o -3 7 2 12.97 10.65 0.44 o -2 7 2 403.23 343.52 4.80 o -1 7 2 4.67 3.45 0.29 o 0 7 2 174.75 160.39 3.73 o 1 7 2 23.01 18.88 0.73 o 2 7 2 39.75 36.01 0.71 o 3 7 2 128.09 109.08 1.32 o 4 7 2 53.88 50.41 0.99 o 5 7 2 85.58 78.04 1.12 o 6 7 2 2.81 3.12 0.29 o -5 8 2 26.00 26.79 0.69 o -4 8 2 0.51 0.38 0.23 o -3 8 2 10.03 8.67 0.38 o -2 8 2 53.71 53.71 0.92 o -1 8 2 25.24 24.42 0.63 o 0 8 2 22.96 22.23 0.74 o 1 8 2 6.59 6.37 0.35 o 2 8 2 37.56 32.61 0.78 o 3 8 2 5.42 5.13 0.33 o 4 8 2 3.18 2.93 0.29 o 3 -8 3 2.08 3.69 0.84 o -6 -7 3 1.48 2.76 0.55 o -5 -7 3 45.76 56.61 2.15 o -3 -7 3 51.83 57.49 2.03 o -2 -7 3 90.43 110.70 3.46 o -1 -7 3 207.56 234.44 4.96 o 0 -7 3 84.58 97.72 3.04 o 1 -7 3 111.58 121.05 5.20 o 2 -7 3 319.52 373.62 5.95 o 4 -7 3 166.88 179.39 3.75 o 5 -7 3 34.54 45.92 1.84 o -8 -6 3 95.26 116.39 3.69 o -7 -6 3 26.65 33.72 0.88 o -6 -6 3 1.22 1.08 0.59 o -5 -6 3 66.31 95.78 1.56 o -4 -6 3 87.87 101.56 1.88 o -3 -6 3 26.24 31.89 1.94 o -2 -6 3 121.09 150.15 4.00 o -1 -6 3 66.30 78.86 2.74 o 1 -6 3 81.97 88.13 2.32 o 2 -6 3 11.38 15.72 0.80 o 3 -6 3 32.82 40.53 1.21 o 4 -6 3 40.87 41.93 1.10 o 5 -6 3 27.86 35.42 1.32 o 6 -6 3 47.10 55.02 2.18 o 7 -6 3 100.24 126.68 2.95 o -9 -5 3 9.62 9.29 0.58 o -8 -5 3 23.83 27.36 0.98 o -7 -5 3 43.25 49.78 0.85 o -6 -5 3 179.88 198.50 2.29 o -5 -5 3 49.75 59.93 1.08 o -4 -5 3 109.75 137.81 1.76 o -3 -5 3 91.56 106.00 2.53 o -2 -5 3 11.87 17.21 3.46 o -1 -5 3 104.64 125.92 3.16 o 0 -5 3 125.09 142.32 2.21 o 1 -5 3 13.41 13.02 0.63 o 2 -5 3 110.89 124.53 1.85 o 3 -5 3 24.06 26.77 0.97 o 4 -5 3 106.68 121.71 1.26 o 5 -5 3 59.80 74.06 0.85 o 6 -5 3 3.29 3.39 0.38 o 7 -5 3 14.61 18.78 0.77 o 8 -5 3 32.05 42.53 1.25 o -9 -4 3 1.95 2.54 0.42 o -8 -4 3 52.68 57.20 1.23 o -7 -4 3 88.68 90.52 0.98 o -6 -4 3 240.71 250.53 2.42 o -5 -4 3 124.29 138.83 1.70 o -4 -4 3 115.31 125.54 1.31 o -3 -4 3 109.02 113.09 1.35 o -2 -4 3 62.07 86.08 1.89 o -1 -4 3 63.50 81.00 1.13 o 0 -4 3 87.87 91.75 1.18 o 1 -4 3 35.61 40.92 0.67 o 2 -4 3 3.72 3.40 0.32 o 3 -4 3 94.91 107.66 1.36 o 4 -4 3 115.26 128.88 1.15 o 5 -4 3 601.08 658.46 2.65 o 6 -4 3 5.36 4.31 0.35 o 7 -4 3 84.13 97.23 1.79 o 8 -4 3 4.43 5.77 0.55 o -10 -3 3 45.23 49.76 1.20 o -9 -3 3 16.48 18.67 0.65 o -8 -3 3 222.82 251.72 1.70 o -7 -3 3 161.58 167.17 1.46 o -6 -3 3 56.83 54.41 0.87 o -5 -3 3 337.28 369.57 2.46 o -4 -3 3 816.55 956.26 9.87 o -3 -3 3 489.21 572.89 2.68 o -2 -3 3 652.80 659.80 4.53 o -1 -3 3 404.18 420.81 3.24 o 0 -3 3 445.75 477.20 1.92 o 1 -3 3 91.58 104.60 0.81 o 2 -3 3 66.28 81.54 0.77 o 3 -3 3 82.28 85.41 1.15 o 4 -3 3 122.82 128.51 0.99 o 5 -3 3 94.24 107.18 0.89 o 6 -3 3 271.28 288.71 1.80 o 7 -3 3 5.46 4.92 0.38 o 8 -3 3 106.90 113.10 1.67 o 9 -3 3 16.08 16.87 0.73 o -10 -2 3 92.68 89.63 2.02 o -9 -2 3 29.35 31.46 0.75 o -8 -2 3 135.54 138.70 1.28 o -7 -2 3 91.77 94.03 0.95 o -6 -2 3 24.36 25.67 0.51 o -5 -2 3 114.84 120.34 1.43 o -4 -2 3 184.18 194.10 1.80 o -3 -2 3 1333.08 1384.59 4.09 o -2 -2 3 354.53 340.75 1.88 o -1 -2 3 398.03 402.41 2.52 o 0 -2 3 437.47 414.82 1.49 o 1 -2 3 4.82 3.87 0.19 o 2 -2 3 110.62 114.51 0.75 o 3 -2 3 223.74 237.40 1.68 o 4 -2 3 275.67 291.40 1.79 o 5 -2 3 306.59 328.81 1.50 o 6 -2 3 157.85 171.15 1.14 o 7 -2 3 0.58 0.40 0.30 o 8 -2 3 71.69 74.99 1.23 o 9 -2 3 15.86 18.92 0.62 o -10 -1 3 10.40 10.28 0.65 o -9 -1 3 7.08 8.61 0.49 o -8 -1 3 69.95 71.67 1.01 o -7 -1 3 103.46 103.43 0.97 o -6 -1 3 1.03 1.60 0.22 o -5 -1 3 69.97 75.29 0.74 o -4 -1 3 856.19 881.86 2.87 o -3 -1 3 2009.15 2074.60 9.94 o -2 -1 3 1520.81 1477.51 10.37 o -1 -1 3 418.84 391.09 2.48 o 0 -1 3 2010.79 1918.65 6.33 o 1 -1 3 174.83 176.88 1.27 o 2 -1 3 204.06 219.07 1.08 o 3 -1 3 1394.94 1487.66 3.72 o 4 -1 3 70.28 83.08 0.65 o 5 -1 3 215.55 248.77 1.13 o 6 -1 3 73.74 79.38 0.88 o 7 -1 3 73.82 66.85 1.19 o 8 -1 3 203.80 183.00 1.95 o 9 -1 3 8.18 9.22 0.50 o -10 0 3 419.13 447.41 4.73 o -9 0 3 99.27 98.03 1.88 o -8 0 3 26.47 27.99 0.65 o -7 0 3 58.04 58.56 0.84 o -6 0 3 65.03 66.83 0.70 o -5 0 3 0.94 1.75 0.27 o -4 0 3 48.95 52.54 0.57 o -3 0 3 1930.57 1958.88 17.63 o -1 0 3 357.06 343.34 1.87 o 0 0 3 1614.98 1500.06 20.74 o 1 0 3 456.78 452.14 1.40 o 2 0 3 236.18 237.71 1.59 o 3 0 3 4524.34 4780.95 34.63 o 4 0 3 247.84 266.46 1.90 o 5 0 3 477.85 517.29 3.47 o 6 0 3 1199.80 1196.75 6.30 o 7 0 3 26.63 26.28 0.66 o 8 0 3 258.57 242.21 2.60 o 9 0 3 2.16 3.25 0.45 o -10 1 3 10.53 9.49 0.56 o -9 1 3 7.25 7.91 0.46 o -8 1 3 69.65 67.16 1.33 o -7 1 3 103.24 97.40 1.08 o -6 1 3 1.06 1.33 0.24 o -5 1 3 70.74 73.91 0.90 o -4 1 3 855.89 816.91 3.26 o -3 1 3 2013.26 1947.83 16.17 o -2 1 3 1520.80 1378.34 4.06 o -1 1 3 415.44 372.79 3.02 o 0 1 3 2005.27 1845.19 26.09 o 1 1 3 173.03 167.84 1.28 o 2 1 3 205.85 205.93 1.46 o 3 1 3 1390.05 1437.85 4.13 o 4 1 3 71.23 83.16 2.47 o 5 1 3 215.69 238.12 1.94 o 6 1 3 73.97 75.61 0.97 o 7 1 3 73.03 62.85 1.07 o 8 1 3 203.09 178.50 2.33 o 9 1 3 8.09 10.18 0.50 o -10 2 3 91.81 80.33 1.65 o -9 2 3 29.78 27.53 0.74 o -8 2 3 135.31 119.63 1.46 o -7 2 3 92.09 84.76 1.29 o -6 2 3 24.50 23.52 0.51 o -5 2 3 114.57 108.84 1.81 o -4 2 3 186.01 173.67 2.21 o -3 2 3 1330.58 1286.43 4.95 o -2 2 3 351.95 313.18 1.88 o -1 2 3 395.04 360.90 1.85 o 0 2 3 437.90 372.71 2.57 o 1 2 3 4.78 3.73 0.14 o 2 2 3 109.90 104.58 1.13 o 3 2 3 222.45 219.43 1.84 o 4 2 3 275.07 268.84 9.15 o 5 2 3 305.37 296.98 1.54 o 6 2 3 158.08 151.61 1.35 o 7 2 3 0.64 0.09 0.42 o 8 2 3 70.63 64.91 1.61 o 9 2 3 15.67 17.19 0.79 o -10 3 3 45.26 40.46 0.82 o -9 3 3 16.27 14.75 0.61 o -8 3 3 222.97 208.07 2.02 o -7 3 3 160.28 141.90 1.58 o -6 3 3 57.75 45.99 0.64 o -5 3 3 338.86 312.75 2.49 o -4 3 3 815.18 802.16 4.13 o -3 3 3 492.74 496.85 2.99 o -2 3 3 651.34 576.80 3.02 o -1 3 3 404.22 368.50 1.78 o 0 3 3 444.72 417.13 4.38 o 1 3 3 91.38 89.48 1.10 o 2 3 3 64.77 67.36 1.16 o 3 3 3 82.39 73.40 1.18 o 4 3 3 122.37 113.39 0.79 o 5 3 3 94.27 92.58 0.92 o 6 3 3 271.73 247.47 1.99 o 7 3 3 5.30 4.26 0.37 o 8 3 3 108.89 98.48 1.84 o 9 3 3 17.03 13.69 0.89 o -9 4 3 1.89 1.86 0.45 o -8 4 3 52.69 46.46 1.23 o -7 4 3 88.18 70.83 1.18 o -6 4 3 241.51 205.50 2.49 o -5 4 3 124.13 111.86 1.36 o -4 4 3 113.91 100.39 1.23 o -3 4 3 108.77 94.13 1.47 o -2 4 3 62.57 70.96 1.22 o -1 4 3 62.88 65.23 1.10 o 0 4 3 88.13 73.78 1.16 o 1 4 3 36.14 32.33 1.02 o 2 4 3 3.72 3.14 0.19 o 3 4 3 95.09 89.21 0.69 o 4 4 3 114.87 106.04 0.93 o 5 4 3 600.42 543.92 4.78 o 6 4 3 5.26 3.34 0.36 o 7 4 3 83.48 77.55 1.37 o 8 4 3 4.42 4.34 0.53 o -9 5 3 9.52 6.13 0.40 o -8 5 3 23.55 20.79 0.65 o -7 5 3 43.35 39.44 0.73 o -6 5 3 181.20 154.29 1.44 o -5 5 3 50.82 46.84 0.71 o -4 5 3 108.70 104.14 1.35 o -3 5 3 90.70 81.43 1.86 o -2 5 3 12.25 12.72 0.35 o -1 5 3 104.15 99.16 1.43 o 0 5 3 125.49 106.40 1.22 o 1 5 3 13.50 9.66 0.28 o 2 5 3 111.39 99.72 1.37 o 3 5 3 24.60 20.57 0.43 o 4 5 3 106.47 94.68 1.26 o 5 5 3 60.47 57.88 0.86 o 6 5 3 3.06 2.75 0.36 o 7 5 3 14.83 15.44 0.58 o 8 5 3 32.15 35.36 1.61 o -8 6 3 94.19 86.95 3.35 o -7 6 3 26.97 26.36 0.74 o -6 6 3 1.24 0.96 0.26 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