#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:15:59 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180840 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/71/2017142.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017142_Fobs loop_ _publ_author_name 'G\"orbitz, Carl Henrik' 'Rissanen, Kari' 'Valkonen, Arto' 'Husab\/o, \%Asmund' _publ_section_title ; Molecular aggregation in selected crystalline 1:1 complexes of hydrophobic D- and L-amino acids. IV. The L-phenylalanine series ; _journal_coeditor_code SK3316 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o267 _journal_page_last o272 _journal_volume 65 _journal_year 2009 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 4.7869 _cell_length_b 9.9558 _cell_length_c 28.4234 _exptl_crystal_F_000 576.00 _reflns_d_resolution_high 0.8403 _cod_data_source_file sk3316Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' LFDaaB in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 138.86 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1249.89 1334.79 40.36 o 4 0 0 72.53 66.04 4.91 o 1 1 0 1.00 1.58 1.06 o 2 1 0 4.26 4.81 1.13 o 3 1 0 36.88 56.62 2.75 o 4 1 0 14.79 19.23 2.56 o 5 1 0 10.69 11.07 3.53 o 0 2 0 552.17 689.46 10.51 o 1 2 0 2133.83 2125.14 20.97 o 2 2 0 205.26 210.65 16.57 o 3 2 0 222.92 362.50 8.67 o 4 2 0 21.89 22.22 2.98 o 5 2 0 37.39 46.62 5.38 o 1 3 0 1380.32 1576.72 16.33 o 2 3 0 81.76 90.00 3.20 o 3 3 0 18.22 17.85 2.29 o 4 3 0 3.16 2.91 3.49 o 5 3 0 15.80 9.97 4.02 o 0 4 0 109.24 167.61 4.95 o 1 4 0 944.93 1002.60 10.81 o 2 4 0 193.85 186.81 4.10 o 3 4 0 27.71 39.70 6.94 o 4 4 0 95.19 107.81 5.06 o 5 4 0 323.41 325.01 14.36 o 1 5 0 22.47 21.34 1.95 o 2 5 0 8.42 13.59 1.95 o 3 5 0 110.44 122.69 4.36 o 4 5 0 47.99 49.94 3.91 o 5 5 0 21.45 22.36 5.13 o 0 6 0 123.67 131.35 5.47 o 1 6 0 25.74 25.21 2.29 o 2 6 0 21.31 21.85 2.41 o 3 6 0 4.62 15.70 2.80 o 4 6 0 3.96 3.89 2.64 o 1 7 0 369.77 371.34 6.81 o 2 7 0 241.27 243.72 6.51 o 3 7 0 396.66 379.24 10.46 o 4 7 0 719.62 608.58 15.28 o 0 8 0 48.44 67.22 7.21 o 1 8 0 28.61 34.52 4.30 o 2 8 0 18.40 29.71 6.62 o 3 8 0 37.30 41.21 4.17 o 4 8 0 4.94 3.76 4.62 o 1 9 0 640.70 683.02 14.02 o 2 9 0 92.73 99.73 7.15 o 3 9 0 20.98 31.56 10.21 o 0 10 0 2.05 -2.13 5.10 o 1 10 0 36.28 42.92 5.08 o 2 10 0 1.39 2.79 3.74 o 3 10 0 104.48 98.11 9.80 o 1 11 0 9.64 8.01 5.79 o 2 11 0 1.12 5.45 4.74 o 1 0 1 1297.40 1195.74 19.23 o 2 0 1 3458.90 3217.84 31.52 o 3 0 1 13.74 16.01 1.61 o 4 0 1 12.63 12.31 2.28 o 5 0 1 9.96 13.78 3.65 o 0 1 1 61.85 61.57 1.72 o 1 1 1 1774.26 1574.44 11.05 o 2 1 1 583.81 620.77 8.66 o 3 1 1 114.85 161.15 9.41 o 4 1 1 145.97 159.60 3.89 o 5 1 1 90.72 93.06 4.71 o 0 2 1 2106.61 2370.18 25.11 o 1 2 1 3356.16 3258.08 21.48 o 2 2 1 937.79 917.22 7.13 o 3 2 1 925.97 897.10 8.16 o 4 2 1 31.96 36.35 2.54 o 5 2 1 24.57 38.59 3.73 o 0 3 1 496.42 608.95 7.21 o 1 3 1 1757.42 1839.83 12.80 o 2 3 1 255.60 233.90 3.01 o 3 3 1 45.12 50.28 1.97 o 4 3 1 4.51 7.96 1.99 o 5 3 1 10.83 12.81 2.98 o 0 4 1 792.53 1098.77 16.24 o 1 4 1 350.07 363.99 3.76 o 2 4 1 84.08 96.33 3.01 o 3 4 1 314.94 279.23 4.24 o 4 4 1 115.08 121.65 3.74 o 5 4 1 20.30 31.30 3.91 o 0 5 1 3.26 5.94 1.54 o 1 5 1 756.52 797.06 6.79 o 2 5 1 96.99 99.71 2.38 o 3 5 1 177.11 184.18 3.59 o 4 5 1 7.27 10.67 2.05 o 5 5 1 15.16 14.80 3.66 o 0 6 1 344.67 480.68 7.26 o 1 6 1 274.79 281.68 3.85 o 2 6 1 154.05 151.77 3.08 o 3 6 1 101.10 114.92 3.19 o 4 6 1 34.66 41.95 3.01 o 0 7 1 75.46 92.17 3.81 o 1 7 1 80.57 85.76 2.76 o 2 7 1 385.71 364.18 5.22 o 3 7 1 48.50 76.15 3.34 o 4 7 1 107.94 145.13 6.44 o 0 8 1 448.24 565.25 12.08 o 1 8 1 113.97 114.21 4.23 o 2 8 1 435.86 429.81 6.75 o 3 8 1 46.12 54.38 3.42 o 4 8 1 7.98 -0.86 3.57 o 0 9 1 71.96 86.16 5.70 o 1 9 1 461.49 479.71 8.14 o 2 9 1 189.07 185.06 6.77 o 3 9 1 55.40 55.19 5.27 o 0 10 1 25.38 24.11 5.36 o 1 10 1 7.70 10.60 3.03 o 2 10 1 52.41 44.09 3.84 o 3 10 1 74.33 85.38 5.61 o 0 11 1 5.03 5.51 4.55 o 1 11 1 29.84 35.41 3.76 o 2 11 1 98.53 110.45 6.66 o 1 0 2 32.37 37.85 1.88 o 2 0 2 35.26 47.26 7.42 o 3 0 2 0.02 1.65 1.36 o 4 0 2 11.91 13.45 2.79 o 5 0 2 13.90 8.81 3.64 o 0 1 2 931.72 965.28 21.64 o 1 1 2 5823.91 5294.48 37.84 o 2 1 2 1725.11 1624.91 11.37 o 3 1 2 641.81 668.96 8.21 o 4 1 2 114.48 139.91 4.02 o 5 1 2 13.62 14.66 3.00 o 0 2 2 3096.71 3526.43 56.36 o 1 2 2 2382.40 2364.93 16.44 o 2 2 2 383.19 384.10 3.93 o 3 2 2 156.32 221.02 10.02 o 4 2 2 104.43 105.67 3.73 o 5 2 2 55.93 65.34 4.61 o 0 3 2 0.32 2.72 1.88 o 1 3 2 1446.91 1511.67 11.11 o 2 3 2 157.92 162.81 2.68 o 3 3 2 32.23 39.96 1.70 o 4 3 2 26.44 27.22 2.71 o 5 3 2 138.57 141.70 9.22 o 0 4 2 1.45 1.51 1.18 o 1 4 2 133.09 142.87 2.39 o 2 4 2 582.87 563.38 5.48 o 3 4 2 48.50 63.20 2.28 o 4 4 2 1.01 11.64 2.02 o 5 4 2 83.74 84.41 5.16 o 0 5 2 11.30 11.80 2.00 o 1 5 2 111.76 125.84 2.42 o 2 5 2 236.48 245.04 3.55 o 3 5 2 297.31 326.44 8.45 o 4 5 2 1.61 3.40 1.83 o 5 5 2 28.61 25.14 3.46 o 0 6 2 48.60 45.57 2.54 o 1 6 2 415.91 448.08 4.86 o 2 6 2 87.80 89.83 2.54 o 3 6 2 204.34 187.09 3.83 o 4 6 2 145.34 145.59 4.92 o 0 7 2 70.80 86.34 4.13 o 1 7 2 94.56 94.78 2.92 o 2 7 2 57.94 62.08 2.58 o 3 7 2 6.81 11.80 1.94 o 4 7 2 346.28 305.34 9.41 o 0 8 2 22.22 23.44 4.02 o 1 8 2 60.25 53.61 3.12 o 2 8 2 309.07 301.50 6.08 o 3 8 2 235.26 208.58 6.08 o 4 8 2 12.99 6.46 3.48 o 0 9 2 41.04 53.83 6.01 o 1 9 2 409.13 423.32 7.61 o 2 9 2 36.91 48.80 3.85 o 3 9 2 12.56 19.49 3.48 o 0 10 2 15.64 12.12 4.27 o 1 10 2 16.37 15.65 3.07 o 2 10 2 22.32 21.17 3.28 o 3 10 2 19.89 25.50 4.28 o 0 11 2 6.68 6.39 4.48 o 1 11 2 37.98 32.60 3.82 o 2 11 2 73.78 93.85 5.93 o 1 0 3 3080.57 3040.40 45.06 o 2 0 3 265.31 272.84 3.91 o 3 0 3 1.62 9.16 2.87 o 4 0 3 28.02 29.78 4.43 o 5 0 3 108.40 117.90 7.30 o 0 1 3 262.85 245.60 6.14 o 1 1 3 9899.66 9204.93 62.31 o 2 1 3 1055.84 1022.92 10.85 o 3 1 3 175.04 222.87 8.17 o 4 1 3 433.77 404.19 6.68 o 5 1 3 148.50 138.51 5.69 o 0 2 3 175.39 232.47 4.75 o 1 2 3 117.57 118.75 1.80 o 2 2 3 242.72 244.63 2.77 o 3 2 3 105.46 156.77 8.81 o 4 2 3 84.99 84.82 3.33 o 5 2 3 168.18 174.00 7.98 o 0 3 3 964.46 1020.98 14.00 o 1 3 3 493.92 447.58 4.20 o 2 3 3 403.88 359.44 3.88 o 3 3 3 11.14 18.90 1.81 o 4 3 3 48.45 55.11 2.98 o 5 3 3 2.17 7.96 2.62 o 0 4 3 498.81 486.42 6.07 o 1 4 3 424.64 435.56 4.41 o 2 4 3 216.80 248.02 5.53 o 3 4 3 47.46 57.16 2.14 o 4 4 3 96.91 95.65 3.38 o 5 4 3 62.56 71.01 5.57 o 0 5 3 556.39 704.13 8.92 o 1 5 3 401.07 422.21 4.69 o 2 5 3 4.98 7.15 1.31 o 3 5 3 673.70 647.90 7.71 o 4 5 3 5.87 6.57 1.81 o 5 5 3 18.67 22.27 3.12 o 0 6 3 589.42 700.95 9.30 o 1 6 3 523.98 574.47 5.69 o 2 6 3 171.36 177.66 3.26 o 3 6 3 10.71 25.58 2.41 o 4 6 3 76.08 86.02 3.69 o 0 7 3 74.03 88.29 4.20 o 1 7 3 91.32 96.87 3.20 o 2 7 3 17.76 27.05 2.14 o 3 7 3 73.42 82.97 3.34 o 4 7 3 39.83 45.98 3.61 o 0 8 3 1566.56 1835.03 23.49 o 1 8 3 497.02 508.17 7.45 o 2 8 3 23.55 40.14 3.98 o 3 8 3 4.63 24.12 5.17 o 4 8 3 6.00 6.79 5.34 o 0 9 3 57.32 67.02 5.36 o 1 9 3 205.95 218.03 5.71 o 2 9 3 180.50 182.94 5.56 o 3 9 3 0.48 4.99 2.99 o 0 10 3 74.18 76.98 6.02 o 1 10 3 77.90 78.41 4.24 o 2 10 3 34.63 36.39 3.69 o 3 10 3 27.99 34.58 4.41 o 0 11 3 8.19 6.08 4.36 o 1 11 3 8.94 9.07 3.19 o 2 11 3 88.41 98.39 5.72 o 0 0 4 310.45 259.50 8.38 o 1 0 4 3209.16 3158.98 51.00 o 2 0 4 12.01 20.25 2.64 o 3 0 4 173.82 174.77 4.34 o 4 0 4 66.58 69.49 5.23 o 5 0 4 7.11 12.62 3.70 o 0 1 4 2939.14 2880.97 53.13 o 1 1 4 3135.41 2898.49 24.87 o 2 1 4 850.64 776.65 6.68 o 3 1 4 255.74 259.38 3.64 o 4 1 4 84.90 129.05 7.62 o 5 1 4 49.21 48.38 3.73 o 0 2 4 722.95 670.81 9.13 o 1 2 4 98.15 88.54 1.65 o 2 2 4 397.54 383.19 3.67 o 3 2 4 772.43 715.09 6.37 o 4 2 4 70.53 81.37 3.37 o 5 2 4 5.51 18.30 3.13 o 0 3 4 55.56 62.14 2.42 o 1 3 4 2027.75 2011.16 14.40 o 2 3 4 44.97 48.53 1.52 o 3 3 4 193.19 176.66 3.71 o 4 3 4 29.08 36.24 2.79 o 5 3 4 39.96 42.78 3.68 o 0 4 4 1322.26 1536.81 16.17 o 1 4 4 1177.58 1224.86 9.54 o 2 4 4 1372.06 1349.66 10.70 o 3 4 4 13.41 13.95 1.54 o 4 4 4 87.89 89.85 3.44 o 5 4 4 1.09 3.31 2.43 o 0 5 4 221.02 260.19 4.45 o 1 5 4 685.43 773.29 8.20 o 2 5 4 7.95 5.48 1.29 o 3 5 4 136.31 173.12 8.86 o 4 5 4 10.28 9.52 2.56 o 5 5 4 15.73 19.73 3.45 o 0 6 4 89.72 96.31 3.43 o 1 6 4 241.61 236.39 3.68 o 2 6 4 198.09 193.62 3.68 o 3 6 4 328.80 261.62 5.27 o 4 6 4 29.30 34.50 2.75 o 0 7 4 55.77 65.56 3.85 o 1 7 4 78.13 81.65 2.89 o 2 7 4 352.21 327.98 5.17 o 3 7 4 1.24 5.94 2.02 o 4 7 4 8.85 17.40 2.61 o 0 8 4 36.44 53.55 4.15 o 1 8 4 322.44 320.14 5.52 o 2 8 4 643.17 588.39 7.76 o 3 8 4 40.12 35.00 3.38 o 4 8 4 2.21 1.04 3.19 o 0 9 4 102.38 108.06 6.15 o 1 9 4 151.20 143.37 4.84 o 2 9 4 14.54 18.00 3.01 o 3 9 4 6.53 12.23 3.52 o 0 10 4 105.31 124.53 7.00 o 1 10 4 41.05 47.73 3.70 o 2 10 4 6.31 8.01 3.04 o 0 11 4 0.00 0.82 3.97 o 1 11 4 16.31 14.31 3.36 o 2 11 4 104.29 111.19 5.36 o 1 0 5 2009.58 1908.70 28.61 o 2 0 5 2036.74 1973.19 23.35 o 3 0 5 5.43 12.78 1.91 o 4 0 5 0.01 1.92 2.83 o 5 0 5 261.68 259.20 10.81 o 0 1 5 691.63 671.16 12.86 o 1 1 5 2305.47 2233.74 18.49 o 2 1 5 84.07 90.67 2.02 o 3 1 5 100.44 123.28 2.94 o 4 1 5 443.16 404.75 7.65 o 5 1 5 42.73 50.52 3.70 o 0 2 5 4008.64 4418.30 78.67 o 1 2 5 492.66 486.15 4.05 o 2 2 5 444.02 446.92 4.19 o 3 2 5 142.12 182.42 7.68 o 4 2 5 88.19 91.92 3.51 o 5 2 5 349.80 358.66 8.22 o 0 3 5 170.31 160.27 3.71 o 1 3 5 1366.89 1343.38 9.70 o 2 3 5 131.63 123.09 2.15 o 3 3 5 246.61 237.89 3.64 o 4 3 5 100.00 119.16 3.96 o 5 3 5 19.75 15.30 3.17 o 0 4 5 1631.36 1689.77 26.41 o 1 4 5 98.00 95.99 2.31 o 2 4 5 426.10 417.31 6.41 o 3 4 5 13.83 12.69 1.60 o 4 4 5 45.72 45.08 2.84 o 5 4 5 67.22 64.80 4.64 o 0 5 5 434.86 489.10 6.48 o 1 5 5 129.88 143.44 2.54 o 2 5 5 88.37 94.96 2.43 o 3 5 5 164.77 158.76 4.49 o 4 5 5 142.50 134.56 4.13 o 5 5 5 26.99 30.51 4.31 o 0 6 5 3767.38 4161.16 42.23 o 1 6 5 359.68 391.00 4.92 o 2 6 5 183.06 166.13 3.46 o 3 6 5 186.17 177.55 5.69 o 4 6 5 4.52 5.07 2.16 o 0 7 5 197.56 209.39 6.05 o 1 7 5 9.12 9.73 1.91 o 2 7 5 321.31 303.88 4.99 o 3 7 5 59.32 64.52 3.55 o 4 7 5 103.98 101.86 5.00 o 0 8 5 1106.02 1242.01 17.54 o 1 8 5 46.49 52.84 3.73 o 2 8 5 96.31 108.63 3.61 o 3 8 5 35.72 35.55 4.07 o 4 8 5 2.81 -1.59 3.07 o 0 9 5 6.34 1.45 3.40 o 1 9 5 423.56 427.84 7.67 o 2 9 5 35.94 38.57 3.45 o 3 9 5 40.60 45.73 4.05 o 0 10 5 76.70 98.39 6.52 o 1 10 5 12.37 10.14 2.98 o 2 10 5 8.20 8.55 2.87 o 0 11 5 30.82 25.71 4.94 o 1 11 5 16.25 19.95 3.53 o 0 0 6 5081.98 4871.07 96.98 o 1 0 6 42.81 45.56 1.94 o 2 0 6 280.45 320.86 9.65 o 3 0 6 139.03 125.96 3.89 o 4 0 6 9.76 8.33 3.30 o 5 0 6 25.12 40.03 7.30 o 0 1 6 2212.57 2115.78 28.97 o 1 1 6 5339.74 5289.27 37.35 o 2 1 6 411.10 375.38 4.34 o 3 1 6 344.21 328.56 4.79 o 4 1 6 66.89 84.43 7.56 o 5 1 6 24.52 30.83 3.23 o 0 2 6 76.74 84.91 2.78 o 1 2 6 1.17 0.10 0.69 o 2 2 6 312.79 286.24 3.16 o 3 2 6 181.07 193.19 7.36 o 4 2 6 36.08 42.81 2.72 o 5 2 6 48.82 62.97 5.15 o 0 3 6 301.36 314.67 5.29 o 1 3 6 1586.98 1590.69 10.80 o 2 3 6 89.04 96.45 2.00 o 3 3 6 34.54 47.03 2.65 o 4 3 6 379.12 384.01 7.09 o 5 3 6 31.63 31.27 3.66 o 0 4 6 279.42 321.20 5.81 o 1 4 6 195.31 195.35 2.62 o 2 4 6 11.42 9.25 1.27 o 3 4 6 13.48 13.30 1.57 o 4 4 6 26.22 23.58 2.48 o 5 4 6 30.84 29.66 3.63 o 0 5 6 4.76 4.47 1.92 o 1 5 6 81.07 75.99 1.96 o 2 5 6 256.49 245.12 3.59 o 3 5 6 17.95 24.18 1.96 o 4 5 6 80.63 87.79 3.69 o 5 5 6 21.90 25.33 3.99 o 0 6 6 196.75 243.77 5.58 o 1 6 6 300.72 309.03 4.71 o 2 6 6 260.72 244.67 4.09 o 3 6 6 85.79 82.19 3.12 o 4 6 6 135.29 127.71 4.62 o 0 7 6 15.37 12.69 2.95 o 1 7 6 152.12 148.01 3.65 o 2 7 6 88.06 95.76 3.76 o 3 7 6 74.97 64.82 3.82 o 4 7 6 183.55 166.87 5.64 o 0 8 6 92.63 99.16 7.66 o 1 8 6 189.57 178.78 4.23 o 2 8 6 135.72 132.40 3.85 o 3 8 6 35.59 33.67 3.26 o 4 8 6 8.88 5.06 3.97 o 0 9 6 73.91 73.60 7.04 o 1 9 6 223.04 220.99 5.34 o 2 9 6 10.11 10.07 2.50 o 3 9 6 86.96 78.36 4.56 o 0 10 6 256.44 268.44 9.22 o 1 10 6 5.17 8.58 2.88 o 2 10 6 8.63 12.28 3.33 o 0 11 6 143.83 148.72 7.87 o 1 11 6 6.55 4.82 3.09 o 1 0 7 123.94 110.16 2.80 o 2 0 7 562.32 527.46 10.79 o 3 0 7 1.44 5.30 2.59 o 4 0 7 15.78 21.44 3.72 o 5 0 7 135.28 150.25 7.72 o 0 1 7 14.96 11.54 1.27 o 1 1 7 223.58 253.56 2.83 o 2 1 7 34.25 35.86 1.60 o 3 1 7 83.71 91.10 3.47 o 4 1 7 286.41 271.02 6.29 o 5 1 7 94.73 99.86 4.42 o 0 2 7 62.73 74.90 3.55 o 1 2 7 1588.39 1553.61 11.27 o 2 2 7 388.27 347.19 3.87 o 3 2 7 615.39 586.78 6.99 o 4 2 7 107.16 96.91 3.84 o 5 2 7 7.06 12.28 2.39 o 0 3 7 58.53 56.70 2.41 o 1 3 7 2806.37 2804.67 19.68 o 2 3 7 1490.88 1426.51 11.01 o 3 3 7 320.07 286.63 4.45 o 4 3 7 405.94 397.35 6.78 o 5 3 7 3.53 2.77 2.43 o 0 4 7 3410.84 3657.58 39.51 o 1 4 7 631.97 664.63 5.70 o 2 4 7 20.88 24.99 1.35 o 3 4 7 114.85 108.78 2.74 o 4 4 7 42.26 45.53 3.12 o 5 4 7 30.06 33.06 3.73 o 0 5 7 43.71 44.66 2.83 o 1 5 7 651.10 633.80 6.34 o 2 5 7 28.91 30.88 1.66 o 3 5 7 10.67 6.97 1.66 o 4 5 7 6.61 8.98 2.71 o 5 5 7 45.77 43.94 4.92 o 0 6 7 1236.12 1363.21 16.33 o 1 6 7 3.57 3.71 1.63 o 2 6 7 189.56 181.21 3.76 o 3 6 7 79.27 81.09 3.18 o 4 6 7 1.89 5.37 2.33 o 0 7 7 1.40 0.40 2.59 o 1 7 7 287.33 286.02 4.90 o 2 7 7 374.62 326.22 5.56 o 3 7 7 24.01 30.09 2.75 o 4 7 7 19.40 28.93 3.20 o 0 8 7 8.54 6.16 3.06 o 1 8 7 79.53 77.99 3.17 o 2 8 7 86.79 90.21 3.37 o 3 8 7 5.47 5.18 2.44 o 4 8 7 0.23 1.03 3.97 o 0 9 7 18.08 20.37 3.49 o 1 9 7 205.11 199.03 5.11 o 2 9 7 30.95 31.63 3.21 o 3 9 7 7.18 9.54 3.32 o 0 10 7 38.98 39.54 5.06 o 1 10 7 71.89 71.56 4.14 o 2 10 7 68.50 53.48 4.42 o 0 11 7 0.71 3.89 4.13 o 1 11 7 16.84 23.43 3.54 o 0 0 8 19281.18 18782.89 249.02 o 1 0 8 3967.59 3827.81 41.05 o 2 0 8 86.02 85.61 3.21 o 3 0 8 49.02 58.38 3.89 o 4 0 8 0.71 1.46 2.80 o 5 0 8 16.39 21.22 4.18 o 0 1 8 2855.16 2855.83 42.86 o 1 1 8 30.78 34.55 1.20 o 2 1 8 72.47 76.35 1.97 o 3 1 8 140.13 129.79 3.48 o 4 1 8 203.19 194.27 5.01 o 5 1 8 16.63 13.02 2.68 o 0 2 8 714.58 674.51 13.07 o 1 2 8 2115.47 2039.79 13.89 o 2 2 8 671.77 649.18 6.01 o 3 2 8 289.43 281.89 7.30 o 4 2 8 69.15 70.13 3.48 o 5 2 8 57.36 60.81 3.68 o 0 3 8 3.52 2.11 1.33 o 1 3 8 929.02 961.48 7.67 o 2 3 8 108.34 122.23 2.79 o 3 3 8 2.20 6.61 1.55 o 4 3 8 22.19 32.97 4.32 o 5 3 8 17.12 20.36 2.86 o 0 4 8 225.92 230.48 4.96 o 1 4 8 754.29 758.34 6.54 o 2 4 8 117.16 115.31 2.29 o 3 4 8 84.72 88.20 2.57 o 4 4 8 78.03 77.92 3.99 o 5 4 8 52.12 50.77 3.95 o 0 5 8 128.60 140.27 4.38 o 1 5 8 820.97 829.75 7.45 o 2 5 8 763.76 685.85 7.34 o 3 5 8 59.67 59.42 2.74 o 4 5 8 29.36 35.93 3.35 o 0 6 8 29.19 29.09 2.94 o 1 6 8 259.34 230.83 4.18 o 2 6 8 70.67 61.86 2.73 o 3 6 8 24.40 26.19 2.97 o 4 6 8 46.81 34.28 3.14 o 0 7 8 206.06 191.23 5.57 o 1 7 8 59.60 63.66 2.87 o 2 7 8 304.57 297.58 5.42 o 3 7 8 61.67 56.92 3.19 o 4 7 8 234.17 197.68 6.68 o 0 8 8 12.70 9.79 3.18 o 1 8 8 94.42 97.81 3.42 o 2 8 8 36.25 34.18 2.90 o 3 8 8 25.16 28.29 3.77 o 0 9 8 93.69 90.92 5.03 o 1 9 8 357.38 323.25 5.66 o 2 9 8 4.01 4.72 2.70 o 3 9 8 50.71 45.70 3.94 o 0 10 8 54.04 51.52 5.35 o 1 10 8 15.01 18.61 3.14 o 2 10 8 5.14 11.37 3.68 o 0 11 8 4.61 -0.81 3.96 o 1 11 8 42.03 43.87 3.98 o 1 0 9 3204.28 3178.77 30.89 o 2 0 9 1505.09 1502.39 17.97 o 3 0 9 4.16 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33.36 2.96 o 0 2 19 58.01 56.54 2.77 o 1 2 19 93.40 94.84 2.60 o 2 2 19 94.34 92.03 3.38 o 3 2 19 243.20 231.82 5.17 o 4 2 19 53.01 56.89 3.75 o 0 3 19 31.66 34.66 2.89 o 1 3 19 87.94 81.91 2.89 o 2 3 19 191.33 187.68 4.57 o 3 3 19 91.20 83.03 3.97 o 4 3 19 66.49 66.17 3.91 o 0 4 19 76.90 69.07 3.73 o 1 4 19 61.80 62.90 2.83 o 2 4 19 195.84 176.21 5.13 o 3 4 19 55.42 47.07 3.71 o 4 4 19 3.44 6.09 2.91 o 0 5 19 38.75 36.09 2.88 o 1 5 19 351.55 327.24 5.63 o 2 5 19 10.30 8.76 2.49 o 3 5 19 38.77 32.30 3.50 o 4 5 19 32.02 29.27 3.71 o 0 6 19 95.05 96.69 4.51 o 1 6 19 39.43 41.27 2.49 o 2 6 19 13.97 13.27 2.71 o 3 6 19 13.34 20.72 3.34 o 0 7 19 165.30 161.71 5.68 o 1 7 19 249.57 229.89 5.52 o 2 7 19 61.09 59.84 3.50 o 3 7 19 26.67 24.82 3.53 o 0 8 19 148.28 134.94 6.57 o 1 8 19 42.72 43.02 3.04 o 2 8 19 7.91 9.85 2.48 o 0 9 19 68.73 75.33 8.34 o 1 9 19 3.22 4.21 2.35 o 0 0 20 51.83 70.67 4.31 o 1 0 20 190.09 186.03 5.28 o 2 0 20 109.54 116.35 5.40 o 3 0 20 6.74 7.42 2.94 o 4 0 20 11.05 9.46 3.44 o 0 1 20 1.13 -0.31 1.74 o 1 1 20 179.54 167.89 4.35 o 2 1 20 564.48 537.48 7.70 o 3 1 20 278.30 269.61 5.65 o 4 1 20 40.97 42.25 3.24 o 0 2 20 6.17 4.66 1.92 o 1 2 20 227.59 228.86 4.12 o 2 2 20 22.26 21.61 2.33 o 3 2 20 35.49 37.64 2.99 o 4 2 20 37.86 34.59 3.36 o 0 3 20 149.67 141.48 4.78 o 1 3 20 188.30 173.64 3.91 o 2 3 20 249.12 236.23 5.09 o 3 3 20 119.84 113.54 4.46 o 4 3 20 49.45 57.94 3.85 o 0 4 20 527.34 521.63 9.23 o 1 4 20 59.19 63.05 2.87 o 2 4 20 83.28 87.35 3.87 o 3 4 20 67.04 69.96 4.28 o 4 4 20 16.14 17.21 3.34 o 0 5 20 31.79 27.92 3.16 o 1 5 20 389.31 353.20 5.86 o 2 5 20 46.63 42.53 3.45 o 3 5 20 42.98 44.76 3.82 o 0 6 20 35.23 31.35 3.15 o 1 6 20 50.52 54.13 2.89 o 2 6 20 301.29 265.85 6.33 o 3 6 20 13.36 15.61 3.24 o 0 7 20 5.75 6.40 3.33 o 1 7 20 11.83 17.53 2.29 o 2 7 20 47.07 51.78 3.39 o 3 7 20 2.61 2.41 4.21 o 0 8 20 27.15 16.77 3.96 o 1 8 20 36.85 41.84 3.12 o 2 8 20 10.54 11.82 2.66 o 0 9 20 3.70 7.13 4.34 o 1 9 20 12.34 12.80 4.02 o 1 0 21 341.91 342.36 7.20 o 2 0 21 142.75 135.63 5.83 o 3 0 21 30.27 28.76 3.77 o 4 0 21 3.85 1.86 3.29 o 0 1 21 7.09 7.94 2.07 o 1 1 21 9.02 10.01 1.76 o 2 1 21 4.69 2.30 2.09 o 3 1 21 126.71 125.02 4.19 o 4 1 21 13.86 13.16 2.65 o 0 2 21 0.15 -1.74 1.74 o 1 2 21 222.13 215.15 4.33 o 2 2 21 18.94 22.29 2.58 o 3 2 21 8.52 13.91 2.55 o 4 2 21 52.73 48.73 3.72 o 0 3 21 4.96 3.60 2.38 o 1 3 21 622.99 599.77 8.30 o 2 3 21 102.97 108.24 4.61 o 3 3 21 0.62 1.41 2.55 o 4 3 21 0.65 -0.21 2.36 o 0 4 21 38.25 36.43 3.22 o 1 4 21 50.31 47.00 2.66 o 2 4 21 57.72 59.65 3.47 o 3 4 21 6.15 8.26 2.90 o 4 4 21 31.61 31.68 3.73 o 0 5 21 3.42 1.23 2.82 o 1 5 21 115.12 117.62 3.69 o 2 5 21 40.55 40.48 3.26 o 3 5 21 7.53 7.77 2.98 o 0 6 21 0.45 -0.15 2.88 o 1 6 21 10.71 10.25 2.30 o 2 6 21 93.38 89.43 4.75 o 3 6 21 20.18 24.40 5.14 o 0 7 21 11.01 10.69 3.57 o 1 7 21 8.00 9.13 2.64 o 2 7 21 8.90 9.61 3.65 o 0 8 21 9.47 14.60 4.48 o 1 8 21 110.63 100.40 4.35 o 2 8 21 6.21 8.38 4.10 o 0 9 21 1.68 -0.97 7.20 o 1 9 21 5.02 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o 1 0 23 7.17 8.13 2.67 o 2 0 23 110.95 113.63 5.59 o 3 0 23 3.12 3.78 2.97 o 4 0 23 0.40 -3.26 3.26 o 0 1 23 32.83 37.47 2.78 o 1 1 23 61.80 72.20 2.82 o 2 1 23 164.18 164.13 4.51 o 3 1 23 48.30 46.46 3.19 o 4 1 23 19.99 19.30 3.10 o 0 2 23 138.31 142.95 5.61 o 1 2 23 2.97 2.30 1.89 o 2 2 23 50.27 50.21 3.24 o 3 2 23 23.84 25.44 3.30 o 4 2 23 6.87 5.51 2.75 o 0 3 23 0.28 1.63 2.71 o 1 3 23 27.65 31.24 2.63 o 2 3 23 13.42 14.45 2.92 o 3 3 23 74.28 78.53 4.59 o 0 4 23 33.73 36.86 3.80 o 1 4 23 51.97 54.48 3.38 o 2 4 23 45.42 46.32 3.75 o 3 4 23 14.52 11.24 3.14 o 0 5 23 36.27 35.30 3.95 o 1 5 23 58.58 63.82 3.64 o 2 5 23 42.77 40.29 3.75 o 3 5 23 7.49 6.67 3.79 o 0 6 23 5.57 5.39 3.15 o 1 6 23 14.86 19.79 2.90 o 2 6 23 67.69 70.53 4.08 o 3 6 23 1.52 -3.32 3.58 o 0 7 23 45.57 42.68 7.20 o 1 7 23 20.59 21.00 3.04 o 2 7 23 5.37 6.69 2.66 o 0 8 23 111.50 112.03 8.71 o 1 8 23 31.04 33.63 4.83 o 0 0 24 91.71 78.73 9.70 o 1 0 24 158.12 164.92 6.58 o 2 0 24 75.81 84.78 5.21 o 3 0 24 10.53 14.95 3.61 o 4 0 24 32.52 19.36 7.10 o 0 1 24 53.45 64.99 3.75 o 1 1 24 272.96 267.51 4.74 o 2 1 24 16.29 16.85 2.48 o 3 1 24 17.83 18.81 2.89 o 0 2 24 366.20 349.05 8.49 o 1 2 24 12.52 11.63 2.23 o 2 2 24 184.38 174.92 5.00 o 3 2 24 82.85 88.47 4.29 o 0 3 24 17.14 20.21 3.35 o 1 3 24 80.05 81.29 3.51 o 2 3 24 95.02 80.04 4.36 o 3 3 24 5.15 7.75 3.01 o 0 4 24 158.52 150.98 6.11 o 1 4 24 23.68 25.42 2.87 o 2 4 24 2.95 1.29 2.66 o 3 4 24 8.02 7.92 3.10 o 0 5 24 0.64 4.53 3.12 o 1 5 24 127.55 130.79 4.75 o 2 5 24 13.06 9.78 3.02 o 3 5 24 3.58 -0.30 2.90 o 0 6 24 24.60 28.45 5.65 o 1 6 24 14.62 17.17 2.95 o 2 6 24 0.52 1.20 2.79 o 0 7 24 32.48 39.42 4.57 o 1 7 24 14.69 14.24 3.34 o 2 7 24 34.83 36.40 3.54 o 0 8 24 2.32 -0.58 3.43 o 1 8 24 1.79 1.07 3.59 o 1 0 25 177.62 180.93 5.75 o 2 0 25 64.88 72.92 4.98 o 3 0 25 74.52 73.37 5.34 o 0 1 25 24.05 27.45 3.64 o 1 1 25 209.48 205.77 4.27 o 2 1 25 220.83 238.64 5.81 o 3 1 25 5.36 1.94 2.37 o 0 2 25 181.66 160.34 6.00 o 1 2 25 8.07 5.56 2.10 o 2 2 25 70.17 73.64 4.24 o 3 2 25 14.51 11.85 3.23 o 0 3 25 129.85 139.71 5.86 o 1 3 25 43.43 44.70 3.17 o 2 3 25 56.84 66.44 4.19 o 3 3 25 50.30 65.40 4.53 o 0 4 25 67.44 73.16 4.82 o 1 4 25 35.73 41.94 3.30 o 2 4 25 51.80 53.32 4.75 o 3 4 25 23.97 20.60 3.53 o 0 5 25 56.90 61.59 4.72 o 1 5 25 53.67 52.83 3.61 o 2 5 25 3.22 2.01 2.91 o 0 6 25 29.00 28.46 4.66 o 1 6 25 9.37 7.86 3.45 o 2 6 25 34.25 33.92 5.40 o 0 7 25 0.00 -1.22 3.17 o 1 7 25 91.89 100.14 5.16 o 0 0 26 1.48 0.10 4.02 o 1 0 26 22.92 27.45 3.28 o 2 0 26 24.83 20.06 3.79 o 3 0 26 34.27 29.50 4.28 o 0 1 26 17.33 23.18 3.54 o 1 1 26 120.16 121.04 3.72 o 2 1 26 4.58 3.86 2.45 o 3 1 26 99.98 106.40 4.71 o 0 2 26 4.87 14.68 3.95 o 1 2 26 1.56 1.23 2.18 o 2 2 26 53.81 44.43 3.77 o 3 2 26 11.24 9.92 3.30 o 0 3 26 5.64 4.61 2.96 o 1 3 26 58.15 56.58 3.49 o 2 3 26 37.64 43.85 3.84 o 3 3 26 25.06 24.29 3.68 o 0 4 26 98.02 102.21 5.55 o 1 4 26 17.85 22.21 2.94 o 2 4 26 19.39 17.31 3.33 o 3 4 26 7.90 6.94 3.32 o 0 5 26 53.20 65.31 7.34 o 1 5 26 1.32 1.95 2.71 o 2 5 26 33.46 39.55 3.98 o 0 6 26 27.02 27.85 5.65 o 1 6 26 132.06 146.68 5.66 o 2 6 26 1.48 4.63 3.07 o 0 7 26 3.28 7.40 3.69 o 1 7 26 13.30 16.30 3.62 o 1 0 27 23.08 32.14 3.39 o 2 0 27 132.66 134.33 6.43 o 3 0 27 81.83 92.77 6.84 o 0 1 27 57.89 51.68 5.25 o 1 1 27 154.94 163.87 4.88 o 2 1 27 92.94 104.06 4.46 o 3 1 27 11.62 12.43 2.91 o 0 2 27 156.29 157.51 7.71 o 1 2 27 82.92 100.19 4.17 o 2 2 27 28.03 31.43 3.59 o 3 2 27 34.04 32.05 3.88 o 0 3 27 9.42 6.38 4.02 o 1 3 27 11.26 9.81 2.57 o 2 3 27 56.93 64.47 4.35 o 3 3 27 33.24 37.57 4.16 o 0 4 27 5.75 2.30 3.94 o 1 4 27 1.12 3.25 2.79 o 2 4 27 52.07 58.79 4.35 o 0 5 27 0.04 -1.88 3.05 o 1 5 27 53.76 58.66 4.25 o 2 5 27 15.20 9.94 3.34 o 0 6 27 0.52 1.35 3.29 o 1 6 27 8.80 14.17 3.79 o 0 7 27 0.58 0.02 4.78 o 0 0 28 324.68 301.13 12.05 o 1 0 28 221.01 236.42 6.76 o 2 0 28 115.46 125.30 7.57 o 3 0 28 25.99 35.95 5.13 o 0 1 28 55.57 54.94 5.40 o 1 1 28 5.46 6.60 2.40 o 2 1 28 19.50 20.49 3.27 o 3 1 28 56.99 58.76 6.23 o 0 2 28 3.76 6.99 3.88 o 1 2 28 17.16 22.95 2.91 o 2 2 28 3.46 2.51 2.88 o 3 2 28 35.50 39.14 4.20 o 0 3 28 0.24 0.76 4.77 o 1 3 28 15.05 17.93 3.15 o 2 3 28 34.35 37.16 4.58 o 0 4 28 79.27 85.19 6.89 o 1 4 28 3.17 5.12 2.82 o 2 4 28 2.34 0.78 3.85 o 0 5 28 47.65 64.54 6.43 o 1 5 28 133.44 137.23 5.74 o 2 5 28 24.91 25.20 3.76 o 0 6 28 22.25 33.22 5.51 o 1 6 28 50.70 59.66 4.36 o 1 0 29 55.39 65.35 5.47 o 2 0 29 7.34 9.65 7.17 o 0 1 29 0.01 0.46 3.56 o 1 1 29 36.77 43.11 3.68 o 2 1 29 7.07 1.94 4.25 o 0 2 29 52.23 62.23 6.04 o 1 2 29 83.87 101.09 4.81 o 2 2 29 22.26 23.65 3.60 o 0 3 29 0.00 0.02 4.26 o 1 3 29 0.67 0.71 2.68 o 2 3 29 31.40 37.27 3.98 o 0 4 29 34.08 39.21 5.55 o 1 4 29 7.73 6.59 2.95 o 2 4 29 13.91 21.14 3.69 o 0 5 29 10.11 13.91 6.21 o 1 5 29 17.80 22.41 5.30 o 0 6 29 1.03 3.05 5.58 o 0 0 30 199.70 236.84 16.96 o 1 0 30 1.89 4.04 6.07 o 2 0 30 49.92 57.71 5.91 o 0 1 30 33.33 31.13 4.93 o 1 1 30 60.95 70.74 4.72 o 2 1 30 10.42 14.80 3.42 o 0 2 30 0.35 3.43 4.05 o 1 2 30 38.50 37.84 3.71 o 2 2 30 12.38 10.77 3.37 o 0 3 30 12.51 11.82 4.56 o 1 3 30 6.86 8.60 2.97 o 2 3 30 48.49 53.47 4.46 o 0 4 30 0.78 -1.14 4.54 o 1 4 30 36.93 36.61 3.92 o 0 5 30 38.37 42.37 6.00 o 1 5 30 13.07 16.27 3.97 o 1 0 31 0.15 5.40 7.32 o 2 0 31 7.37 13.82 4.56 o 0 1 31 56.39 66.69 6.10 o 1 1 31 64.17 70.72 5.59 o 2 1 31 40.34 52.19 5.26 o 0 2 31 4.37 8.09 4.41 o 1 2 31 4.31 7.08 3.89 o 2 2 31 6.20 8.84 3.41 o 0 3 31 8.12 10.22 4.58 o 1 3 31 18.17 22.68 3.53 o 0 4 31 68.72 83.35 7.00 o 1 4 31 0.90 1.68 2.91 o 0 0 32 8.06 16.57 8.29 o 1 0 32 0.01 3.66 7.32 o 0 1 32 56.69 64.96 6.29 o 1 1 32 2.17 7.34 3.79 o 0 2 32 18.47 15.05 4.77 o 1 2 32 20.82 26.02 4.59 o 0 3 32 49.29 57.77 6.28 o 1 3 32 8.90 8.80 4.05 o 1 0 33 102.43 140.10 15.61 o 0 1 33 0.20 3.02 4.17 o 1 1 33 26.75 34.68 5.52 o 0 2 33 9.56 9.15 4.46 o