#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/71/2017159.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017159_Fobs loop_ _publ_author_name 'Matczak-Jon, Ewa' '\'Slepokura, Katarzyna' 'Kafarski, Pawe\/l' 'Skrzy\'nska, Izabela' 'Jon, Marek' _publ_section_title ; Conformational isomers of the [(5-methyl-2-pyridinio)aminomethylene]diphosphonate dianion and [(5-methyl-2-pyridyl)aminomethylene]diphosphonate trianion in salts with 4-aminopyridine and ammonia ; _journal_coeditor_code TR3053 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o261 _journal_page_last o266 _journal_volume 65 _journal_year 2009 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.890 _cell_angle_gamma 90.000 _cell_length_a 20.3850 _cell_length_b 17.8380 _cell_length_c 13.0380 _exptl_crystal_F_000 2160.00 _reflns_d_resolution_high 0.7108 _[local]_cod_data_source_file tr3053Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mj01dc in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 424.82 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 21918.26 24388.36 154.81 o 6 0 0 97086.08 107755.45 573.99 o 8 0 0 709.91 1050.95 14.41 o 10 0 0 10596.50 10655.31 82.49 o 12 0 0 31106.13 33875.97 180.50 o 14 0 0 5212.82 5280.12 83.87 o 16 0 0 29605.59 28508.59 216.30 o 18 0 0 1496.59 1576.84 23.53 o 20 0 0 7836.50 7570.97 106.59 o 22 0 0 1634.92 1753.82 33.92 o 24 0 0 1687.10 1682.52 40.78 o 26 0 0 1296.15 1191.79 86.73 o 28 0 0 275.48 128.54 45.49 o 3 1 0 19043.45 19497.63 122.72 o 5 1 0 118133.97 129276.50 607.03 o 7 1 0 92693.17 101057.75 256.69 o 9 1 0 54.16 157.94 7.17 o 11 1 0 10956.28 11444.58 57.27 o 13 1 0 11511.85 11928.02 98.93 o 15 1 0 121.98 125.54 9.52 o 17 1 0 132.96 144.59 9.84 o 19 1 0 27.01 0.00 10.71 o 21 1 0 668.74 654.67 18.61 o 23 1 0 11.45 4.19 8.82 o 25 1 0 15.86 0.00 11.53 o 27 1 0 1250.32 1380.04 39.96 o 2 2 0 2317.70 2482.66 47.02 o 4 2 0 45305.64 50418.22 199.07 o 6 2 0 1999.18 1879.39 15.28 o 8 2 0 2492.96 2777.29 28.91 o 10 2 0 1382.76 1755.49 18.06 o 12 2 0 636.68 761.69 13.59 o 14 2 0 200.87 292.22 9.89 o 16 2 0 16484.61 15851.45 195.47 o 18 2 0 505.17 457.14 12.27 o 20 2 0 5118.80 4796.07 69.20 o 22 2 0 567.61 484.31 17.03 o 24 2 0 1175.11 1169.93 32.13 o 26 2 0 144.08 86.27 25.94 o 1 3 0 16614.11 17276.63 202.73 o 3 3 0 32481.89 37976.97 312.34 o 5 3 0 8399.61 7755.67 46.38 o 7 3 0 12052.68 10882.99 85.19 o 9 3 0 16229.65 16486.33 149.91 o 11 3 0 22525.33 24881.75 238.86 o 13 3 0 17596.59 17459.12 209.08 o 15 3 0 368.55 345.66 9.89 o 17 3 0 3018.49 3306.50 32.97 o 19 3 0 68.51 42.01 12.31 o 21 3 0 1.24 11.88 16.26 o 23 3 0 609.66 591.08 19.41 o 25 3 0 118.18 85.93 23.80 o 27 3 0 3308.26 3608.12 53.27 o 0 4 0 351.77 253.10 10.01 o 2 4 0 73530.09 79839.09 329.20 o 4 4 0 3486.95 2808.53 21.20 o 6 4 0 6065.09 5947.04 70.08 o 8 4 0 5259.98 5879.48 49.29 o 10 4 0 16984.03 17426.04 176.80 o 12 4 0 6011.06 5936.32 55.94 o 14 4 0 12633.96 12723.54 123.67 o 16 4 0 12.47 9.37 12.43 o 18 4 0 3088.97 3122.52 27.93 o 20 4 0 1282.79 1274.57 21.98 o 22 4 0 0.29 0.00 12.76 o 24 4 0 579.64 613.86 25.66 o 26 4 0 32.30 54.51 28.20 o 1 5 0 33457.23 38992.85 237.66 o 3 5 0 43349.75 48758.68 360.22 o 5 5 0 50258.15 55174.11 613.91 o 7 5 0 644.78 785.13 14.94 o 9 5 0 1744.20 1859.84 24.31 o 11 5 0 2143.14 2039.22 19.71 o 13 5 0 3444.64 3411.24 23.99 o 15 5 0 823.41 869.23 13.47 o 17 5 0 2915.56 2684.40 36.12 o 19 5 0 2716.73 2583.34 33.41 o 21 5 0 19.19 28.81 10.62 o 23 5 0 154.84 199.97 22.30 o 25 5 0 1971.73 2077.65 27.67 o 27 5 0 707.64 830.91 30.62 o 0 6 0 15653.99 14865.41 49.33 o 2 6 0 2890.88 2595.93 18.56 o 4 6 0 2482.90 3308.57 40.37 o 6 6 0 975.45 1295.02 20.90 o 8 6 0 71.02 96.43 7.78 o 10 6 0 2050.92 2224.19 22.81 o 12 6 0 1160.38 1254.96 16.29 o 14 6 0 16618.74 16200.37 103.21 o 16 6 0 1.15 2.17 7.75 o 18 6 0 303.23 291.26 12.19 o 20 6 0 284.35 293.99 14.36 o 22 6 0 48.90 10.55 14.93 o 24 6 0 25.07 27.88 20.18 o 26 6 0 654.30 770.67 38.87 o 1 7 0 11609.25 10307.93 57.65 o 3 7 0 25.98 29.12 9.55 o 5 7 0 8.96 27.32 8.29 o 7 7 0 329.98 410.17 9.97 o 9 7 0 449.61 559.56 9.64 o 11 7 0 0.81 27.66 8.76 o 13 7 0 110.80 115.17 8.53 o 15 7 0 4458.74 4188.19 29.19 o 17 7 0 10595.93 10571.95 103.74 o 19 7 0 2139.44 2111.94 30.59 o 21 7 0 4226.63 4286.55 41.45 o 23 7 0 325.78 290.35 32.39 o 25 7 0 920.45 976.39 28.90 o 0 8 0 5976.14 6409.47 95.54 o 2 8 0 2961.60 3190.81 23.26 o 4 8 0 2787.17 2877.39 36.17 o 6 8 0 11460.31 12878.73 124.41 o 8 8 0 1638.67 1596.60 21.37 o 10 8 0 5319.45 4982.72 51.78 o 12 8 0 542.85 636.48 11.06 o 14 8 0 2375.80 2275.93 22.70 o 16 8 0 4024.37 3848.84 35.42 o 18 8 0 1099.83 1144.07 15.78 o 20 8 0 0.33 0.00 13.15 o 22 8 0 589.55 595.20 25.11 o 24 8 0 747.56 685.52 29.54 o 26 8 0 61.58 28.42 25.76 o 1 9 0 13598.47 14720.33 80.63 o 3 9 0 3101.58 3493.51 29.46 o 5 9 0 32.13 87.27 9.39 o 7 9 0 5161.44 5624.77 66.23 o 9 9 0 43.29 68.09 8.98 o 11 9 0 4237.86 3908.28 26.81 o 13 9 0 2878.04 2891.32 28.96 o 15 9 0 9364.84 9050.95 84.59 o 17 9 0 5963.45 6037.92 70.84 o 19 9 0 569.39 511.19 14.91 o 21 9 0 705.00 632.16 22.75 o 23 9 0 23.67 6.36 9.44 o 25 9 0 202.89 214.85 33.54 o 0 10 0 98.72 24.38 11.36 o 2 10 0 534.08 861.66 13.27 o 4 10 0 11801.45 12272.96 128.89 o 6 10 0 7290.97 7361.18 73.83 o 8 10 0 25726.65 26365.17 243.28 o 10 10 0 0.23 0.72 3.34 o 12 10 0 8177.46 7588.11 62.56 o 14 10 0 263.60 213.75 10.33 o 16 10 0 802.65 757.19 13.72 o 18 10 0 3.13 0.00 6.96 o 20 10 0 83.07 70.13 15.06 o 22 10 0 353.30 373.90 21.02 o 24 10 0 739.31 786.50 25.13 o 1 11 0 3186.64 3522.71 26.37 o 3 11 0 7069.10 8340.64 54.94 o 5 11 0 1590.84 1447.93 16.19 o 7 11 0 106.09 183.87 8.85 o 9 11 0 1462.10 1444.62 20.47 o 11 11 0 408.57 332.21 10.84 o 13 11 0 2212.89 2120.58 18.50 o 15 11 0 1106.96 1170.48 25.44 o 17 11 0 953.32 879.98 24.87 o 19 11 0 80.41 42.30 17.11 o 21 11 0 0.60 0.00 19.54 o 23 11 0 176.52 132.57 27.55 o 25 11 0 27.89 60.10 47.70 o 0 12 0 12486.01 12304.02 48.69 o 2 12 0 1881.60 1757.32 18.06 o 4 12 0 1512.39 1557.05 17.76 o 6 12 0 1652.77 1650.33 15.70 o 8 12 0 5412.74 5099.67 42.34 o 10 12 0 270.17 266.48 10.16 o 12 12 0 1538.44 1398.16 22.57 o 14 12 0 228.50 224.42 12.78 o 16 12 0 1245.88 1228.83 30.06 o 18 12 0 98.77 128.23 16.94 o 20 12 0 3082.15 3103.21 88.26 o 22 12 0 21.02 13.73 27.03 o 24 12 0 942.36 1016.26 50.73 o 1 13 0 4443.96 4161.60 34.93 o 3 13 0 1717.47 1837.52 24.17 o 5 13 0 3185.50 3398.96 32.71 o 7 13 0 1572.82 1470.66 17.29 o 9 13 0 2450.87 2364.26 17.16 o 11 13 0 355.15 373.53 10.72 o 13 13 0 1466.23 1477.14 27.78 o 15 13 0 1098.24 1086.48 19.29 o 17 13 0 2244.84 2287.07 27.00 o 19 13 0 165.51 222.76 19.41 o 21 13 0 1111.48 1138.07 31.76 o 23 13 0 39.08 0.00 26.27 o 0 14 0 1232.89 1476.34 28.03 o 2 14 0 699.13 727.51 14.01 o 4 14 0 1098.18 1166.98 18.44 o 6 14 0 4513.36 4679.06 47.82 o 8 14 0 533.17 437.08 13.04 o 10 14 0 2223.34 2312.31 27.87 o 12 14 0 804.95 787.48 17.29 o 14 14 0 7065.45 7020.07 60.04 o 16 14 0 3765.62 3820.40 84.80 o 18 14 0 1.04 0.00 18.18 o 20 14 0 1747.16 1675.81 64.37 o 22 14 0 351.55 369.00 42.56 o 1 15 0 166.45 61.10 11.83 o 3 15 0 949.11 923.42 14.71 o 5 15 0 5222.89 5000.43 56.57 o 7 15 0 5510.77 5792.91 48.31 o 9 15 0 3339.25 3249.59 41.68 o 11 15 0 1710.53 1827.88 26.75 o 13 15 0 1533.04 1600.95 30.77 o 15 15 0 1544.21 1686.28 27.15 o 17 15 0 81.92 79.44 17.37 o 19 15 0 371.05 316.93 19.39 o 21 15 0 362.87 336.98 29.40 o 0 16 0 702.83 805.05 45.17 o 2 16 0 1640.66 1502.20 26.78 o 4 16 0 72.29 53.80 12.13 o 6 16 0 440.07 390.88 15.77 o 8 16 0 1.51 3.85 7.78 o 10 16 0 247.78 207.58 14.76 o 12 16 0 45.80 49.79 14.96 o 14 16 0 328.95 324.18 17.34 o 16 16 0 2168.39 2105.19 34.64 o 18 16 0 1800.18 1784.27 45.88 o 20 16 0 3159.60 3150.77 34.81 o 1 17 0 33.38 60.90 12.89 o 3 17 0 1047.59 1085.03 29.82 o 5 17 0 4108.14 3660.78 38.28 o 7 17 0 6.75 14.86 16.58 o 9 17 0 1548.71 1518.70 20.69 o 11 17 0 1764.61 1889.64 41.02 o 13 17 0 1350.46 1373.81 61.63 o 15 17 0 3952.16 3949.24 60.90 o 17 17 0 165.86 135.34 19.50 o 19 17 0 33.31 47.13 22.81 o 0 18 0 1378.72 1320.73 26.21 o 2 18 0 390.75 325.82 14.17 o 4 18 0 10.50 15.52 11.72 o 6 18 0 8.01 0.00 14.76 o 8 18 0 0.21 0.00 10.54 o 10 18 0 303.48 315.83 17.08 o 12 18 0 24.15 45.48 18.84 o 14 18 0 413.45 390.69 20.74 o 16 18 0 286.75 229.57 21.32 o 18 18 0 0.07 0.00 20.47 o 1 19 0 17.99 13.93 16.14 o 3 19 0 818.87 856.15 20.40 o 5 19 0 524.99 511.98 24.71 o 7 19 0 836.36 832.33 18.66 o 9 19 0 812.03 795.84 19.37 o 11 19 0 292.22 367.77 19.15 o 13 19 0 1616.01 1581.22 30.68 o 15 19 0 0.22 0.00 16.23 o 17 19 0 216.00 215.55 23.09 o 0 20 0 1445.55 1581.59 51.75 o 2 20 0 480.92 453.35 16.18 o 4 20 0 357.04 340.43 25.49 o 6 20 0 51.43 31.34 18.58 o 8 20 0 66.71 67.07 18.41 o 10 20 0 638.41 559.23 22.67 o 12 20 0 339.41 309.72 21.02 o 14 20 0 182.43 180.90 23.12 o 16 20 0 537.87 544.80 24.86 o 1 21 0 5529.31 5982.25 73.87 o 3 21 0 4.86 13.87 20.52 o 5 21 0 2304.54 2534.41 39.39 o 7 21 0 40.00 16.77 12.27 o 9 21 0 458.05 417.23 20.11 o 11 21 0 531.36 541.29 23.90 o 13 21 0 50.48 69.99 22.55 o 15 21 0 1765.06 1920.10 32.17 o 0 22 0 28.81 28.96 26.10 o 2 22 0 505.41 455.27 21.12 o 4 22 0 374.15 352.94 21.49 o 6 22 0 242.23 270.71 20.09 o 8 22 0 1699.29 1734.51 33.34 o 10 22 0 2149.57 2203.72 42.98 o 12 22 0 228.11 201.06 23.22 o 1 23 0 5022.05 5505.55 59.66 o 3 23 0 1372.75 1455.93 42.93 o 5 23 0 1538.93 1657.40 29.86 o 7 23 0 71.19 88.96 23.50 o 9 23 0 566.06 621.27 27.73 o 11 23 0 15.46 0.00 13.85 o 0 24 0 10.78 26.10 30.84 o 2 24 0 2380.13 2484.54 36.86 o 4 24 0 479.61 527.38 27.56 o 6 24 0 2459.99 2726.67 34.80 o 8 24 0 3496.84 3760.27 44.57 o 1 25 0 613.24 686.27 41.37 o -27 1 1 9.48 0.00 27.39 o -25 1 1 359.22 366.02 26.30 o -23 1 1 372.35 372.55 18.99 o -21 1 1 1825.80 1697.85 21.08 o -19 1 1 2161.49 1973.02 25.97 o -17 1 1 9792.93 9165.73 123.27 o -15 1 1 10899.64 10956.91 109.53 o -13 1 1 190.10 266.75 9.06 o -11 1 1 61.56 78.17 6.38 o -9 1 1 3600.69 3985.40 43.85 o -7 1 1 635.22 824.91 9.97 o -5 1 1 1082.23 1424.22 16.41 o -3 1 1 3203.64 3498.11 49.28 o 3 1 1 58424.75 66752.02 635.72 o 5 1 1 28940.95 31207.66 157.53 o 7 1 1 20675.59 21133.29 234.15 o 9 1 1 617.72 934.96 10.50 o 11 1 1 689.04 1066.60 14.40 o 13 1 1 3286.42 2776.61 37.56 o 15 1 1 326.81 319.38 10.24 o 17 1 1 927.03 892.28 12.48 o 19 1 1 1687.24 1749.17 21.99 o 21 1 1 88.99 111.85 17.36 o 23 1 1 771.99 699.64 21.26 o 25 1 1 1338.07 1421.70 53.62 o 27 1 1 2.45 0.00 18.43 o -28 2 1 618.06 622.53 35.55 o -26 2 1 191.47 155.44 23.26 o -24 2 1 1206.42 1246.77 21.60 o -22 2 1 16.87 9.38 13.20 o -20 2 1 19.37 6.39 13.29 o -18 2 1 294.39 333.13 12.91 o -16 2 1 804.64 784.60 14.34 o -14 2 1 8313.89 8335.68 91.85 o -12 2 1 4239.48 4487.14 45.71 o -10 2 1 475.33 765.21 18.73 o -8 2 1 16596.91 16250.22 65.56 o -6 2 1 14979.78 15234.11 124.12 o -4 2 1 273.55 483.70 7.89 o -2 2 1 5545.39 6008.32 45.20 o 0 2 1 3159.74 2684.63 13.46 o 2 2 1 10194.97 11990.73 69.17 o 4 2 1 13272.96 15751.99 132.11 o 6 2 1 1655.02 2440.32 23.18 o 8 2 1 2110.31 2629.75 26.90 o 10 2 1 1846.05 1752.33 20.09 o 12 2 1 2579.48 2368.13 39.94 o 14 2 1 535.14 444.41 9.03 o 16 2 1 988.85 1040.10 20.18 o 18 2 1 283.04 367.18 11.28 o 20 2 1 903.81 907.22 23.01 o 22 2 1 790.76 703.07 27.82 o 24 2 1 748.26 762.19 26.60 o 26 2 1 807.09 818.01 50.05 o -27 3 1 6.32 0.00 21.36 o -25 3 1 4.22 0.00 13.06 o -23 3 1 0.35 0.00 9.16 o -21 3 1 0.01 0.00 8.22 o -19 3 1 3714.39 3665.57 48.85 o -17 3 1 670.39 618.42 12.49 o -15 3 1 3984.45 3784.05 43.07 o -13 3 1 7602.13 7485.66 93.83 o -11 3 1 2026.97 1860.72 16.09 o -9 3 1 3525.50 3618.54 34.04 o -7 3 1 27299.05 29103.40 102.08 o -5 3 1 137.28 124.76 7.23 o -3 3 1 350.21 282.12 6.99 o -1 3 1 71.83 92.79 7.18 o 1 3 1 248.51 198.15 8.67 o 3 3 1 37017.59 38209.17 176.87 o 5 3 1 3266.54 2804.58 30.77 o 7 3 1 881.39 809.74 9.39 o 9 3 1 13403.50 14724.43 112.00 o 11 3 1 0.27 6.52 5.30 o 13 3 1 199.01 214.80 7.74 o 15 3 1 3241.96 3108.94 36.38 o 17 3 1 3.02 33.65 10.11 o 19 3 1 343.71 293.14 13.31 o 21 3 1 557.88 508.15 20.37 o 23 3 1 13.52 0.00 14.30 o 25 3 1 712.84 679.93 26.05 o 27 3 1 1003.42 977.12 37.82 o -26 4 1 362.18 342.54 26.37 o -24 4 1 182.93 165.49 17.78 o -22 4 1 20.65 8.80 13.25 o -20 4 1 805.70 813.97 17.88 o -18 4 1 158.81 129.85 10.98 o -16 4 1 177.06 152.47 11.24 o -14 4 1 6457.64 6267.47 66.14 o -12 4 1 46.83 113.41 7.82 o -10 4 1 5216.83 4635.59 45.65 o -8 4 1 437.59 432.92 7.54 o -6 4 1 26465.00 27576.21 286.67 o -4 4 1 668.42 659.62 11.02 o -2 4 1 28249.56 28684.18 236.71 o 0 4 1 11817.88 12221.71 46.08 o 2 4 1 9897.40 10507.96 75.00 o 4 4 1 71.63 15.89 7.63 o 6 4 1 1841.95 1771.29 17.17 o 8 4 1 116.53 101.45 7.79 o 10 4 1 5613.39 4794.12 31.77 o 12 4 1 208.30 220.62 7.72 o 14 4 1 381.14 510.54 9.57 o 16 4 1 2476.79 2536.40 29.85 o 18 4 1 2418.02 2203.79 35.42 o 20 4 1 466.11 473.11 16.70 o 22 4 1 27.48 35.38 15.50 o 24 4 1 186.03 194.75 20.06 o 26 4 1 245.16 303.99 31.66 o -27 5 1 831.22 1049.26 32.07 o -25 5 1 86.07 93.24 21.73 o -23 5 1 641.43 636.84 19.04 o -21 5 1 150.92 244.51 15.24 o -19 5 1 95.03 92.56 11.75 o -17 5 1 423.17 396.37 11.23 o -15 5 1 41795.36 42217.98 335.91 o -13 5 1 1739.51 1781.61 18.55 o -11 5 1 765.29 672.60 10.53 o -9 5 1 2648.48 2467.18 24.29 o -7 5 1 18954.82 19124.88 135.97 o -5 5 1 833.21 940.42 17.52 o -3 5 1 54866.89 56003.11 309.72 o -1 5 1 14877.82 16196.42 96.07 o 1 5 1 63063.46 71837.74 527.53 o 3 5 1 5341.44 5013.96 43.30 o 5 5 1 5998.22 5311.46 63.11 o 7 5 1 28.93 22.17 7.71 o 9 5 1 487.98 451.53 11.94 o 11 5 1 24282.03 25092.90 216.69 o 13 5 1 3874.18 4017.63 29.12 o 15 5 1 2452.97 2235.59 16.87 o 17 5 1 1265.37 1232.11 19.81 o 19 5 1 1881.89 1904.76 34.30 o 21 5 1 1684.84 1815.97 26.89 o 23 5 1 77.76 109.21 18.76 o 25 5 1 878.79 895.41 27.60 o 27 5 1 2743.41 3227.29 100.27 o -26 6 1 194.25 187.64 24.80 o -24 6 1 95.13 85.66 20.49 o -22 6 1 1374.91 1488.47 31.97 o -20 6 1 101.11 54.99 13.46 o -18 6 1 5099.77 4814.03 49.90 o -16 6 1 321.43 371.69 9.72 o -14 6 1 130.15 78.07 8.41 o -12 6 1 8205.61 8381.01 64.38 o -10 6 1 923.22 924.97 14.25 o -8 6 1 1545.99 1364.97 25.39 o -6 6 1 28.60 181.53 10.97 o -4 6 1 14581.05 14699.38 76.45 o -2 6 1 72931.73 81627.25 452.14 o 0 6 1 56237.71 64411.08 450.33 o 2 6 1 17399.76 17390.11 63.85 o 4 6 1 11692.24 11883.01 87.80 o 6 6 1 30709.55 31331.40 360.47 o 8 6 1 3030.61 3094.42 39.85 o 10 6 1 471.38 533.45 9.78 o 12 6 1 8753.48 8299.63 53.54 o 14 6 1 3782.41 3836.85 33.75 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