#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/72/2017218.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017218_Fobs loop_ _publ_author_name 'Ho\/ly\'nska, Ma\/lgorzata' 'Kubiak, Maria' _publ_section_title ; Supramolecular motifs in the first structures of organic carboxylate salts of 1-(diaminomethylene)thiourea (HATU) ; _journal_coeditor_code FA3194 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o410 _journal_page_last o413 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 111.890 _cell_angle_beta 90.820 _cell_angle_gamma 91.020 _cell_length_a 7.0060 _cell_length_b 7.2210 _cell_length_c 7.8370 _exptl_crystal_F_000 190.00 _reflns_d_resolution_high 0.5923 _[local]_cod_data_source_file fa3194IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' hasz1dc in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 111.64 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2713.05 2795.92 21.35 o 3 0 0 2.81 3.00 0.49 o 4 0 0 1328.08 1432.61 2.78 o 5 0 0 34.55 33.62 0.71 o 6 0 0 138.75 136.63 2.80 o 7 0 0 0.29 1.48 0.79 o 8 0 0 56.72 59.75 1.86 o 9 0 0 18.19 15.16 1.81 o -9 1 0 87.31 86.82 3.33 o -8 1 0 50.84 52.10 1.83 o -7 1 0 13.22 12.43 0.61 o -6 1 0 58.68 56.96 0.88 o -5 1 0 180.92 173.15 2.16 o -4 1 0 5.37 4.43 0.61 o -3 1 0 17.72 12.71 0.59 o -2 1 0 978.30 1038.68 1.57 o -1 1 0 185.91 192.17 0.92 o 0 1 0 242.33 222.00 1.14 o 1 1 0 107.41 123.76 0.55 o 2 1 0 12463.58 12091.46 31.38 o 3 1 0 7.45 7.15 0.36 o 4 1 0 1019.26 1036.17 4.53 o 5 1 0 10.35 10.18 0.60 o 6 1 0 535.79 538.01 2.82 o 7 1 0 0.70 1.13 0.95 o 8 1 0 116.55 116.54 1.78 o 9 1 0 0.56 1.00 1.43 o -9 2 0 42.79 40.94 2.03 o -8 2 0 22.89 21.96 1.70 o -7 2 0 180.07 187.41 2.27 o -6 2 0 115.02 107.90 2.70 o -5 2 0 59.74 58.32 1.23 o -4 2 0 320.24 318.44 1.73 o -3 2 0 728.46 755.37 2.28 o -2 2 0 91.31 90.86 0.81 o -1 2 0 634.64 633.10 1.97 o 0 2 0 1233.96 1328.63 14.63 o 1 2 0 1315.36 1499.30 6.91 o 2 2 0 5.39 5.58 0.34 o 3 2 0 195.45 189.98 1.86 o 4 2 0 2065.63 2262.88 5.51 o 5 2 0 159.03 159.67 1.98 o 6 2 0 250.49 242.20 2.06 o 7 2 0 47.44 47.34 1.31 o 8 2 0 92.87 87.47 2.18 o 9 2 0 8.50 8.14 1.78 o 10 2 0 13.10 12.80 1.77 o -8 3 0 109.65 113.00 2.01 o -7 3 0 98.70 100.66 1.75 o -6 3 0 397.97 402.09 6.80 o -5 3 0 208.48 202.90 2.36 o -4 3 0 2.89 3.41 0.48 o -3 3 0 1.06 0.74 0.37 o -2 3 0 118.93 132.14 0.89 o -1 3 0 203.94 193.18 1.41 o 0 3 0 33.78 37.46 1.23 o 1 3 0 64.41 53.15 1.52 o 2 3 0 551.31 615.53 6.40 o 3 3 0 289.62 294.10 1.29 o 4 3 0 0.38 1.22 0.56 o 5 3 0 125.64 121.42 1.18 o 6 3 0 590.73 609.85 5.68 o 7 3 0 81.85 79.79 1.78 o 8 3 0 172.79 170.63 2.24 o 9 3 0 76.92 81.89 2.42 o 10 3 0 42.35 38.02 2.65 o 11 3 0 20.08 20.63 2.16 o -8 4 0 90.83 97.81 3.12 o -7 4 0 165.73 167.14 3.30 o -6 4 0 177.49 180.04 3.11 o -5 4 0 355.26 353.43 3.39 o -4 4 0 1217.77 1250.42 13.25 o -3 4 0 644.79 623.38 9.90 o -2 4 0 393.79 383.38 4.36 o -1 4 0 106.07 97.56 1.25 o 0 4 0 115.13 103.24 1.77 o 1 4 0 196.62 195.21 2.21 o 2 4 0 148.02 152.60 0.89 o 3 4 0 23.13 19.96 0.46 o 4 4 0 1.23 2.67 0.49 o 5 4 0 34.92 35.31 0.81 o 6 4 0 55.41 50.57 1.16 o 7 4 0 23.29 21.94 1.20 o 8 4 0 67.18 61.85 1.73 o 9 4 0 0.86 1.34 1.80 o 10 4 0 61.23 55.87 2.53 o -7 5 0 1.63 3.50 2.10 o -6 5 0 155.62 152.29 3.27 o -5 5 0 28.21 28.15 1.88 o -4 5 0 90.57 88.52 1.57 o -3 5 0 202.17 201.12 2.06 o -2 5 0 1143.70 1182.85 4.67 o -1 5 0 471.84 443.52 2.63 o 0 5 0 311.71 323.39 2.24 o 1 5 0 139.32 135.91 1.16 o 2 5 0 85.14 83.44 0.98 o 3 5 0 176.06 181.70 1.51 o 4 5 0 98.16 97.94 1.26 o 5 5 0 56.37 57.09 1.19 o 6 5 0 7.26 7.67 1.21 o 7 5 0 19.40 19.35 1.54 o 8 5 0 61.14 59.85 2.12 o 9 5 0 23.01 22.43 2.59 o 10 5 0 0.01 0.96 2.17 o -6 6 0 109.19 113.77 2.03 o -5 6 0 0.36 1.00 1.04 o -4 6 0 469.00 474.88 4.44 o -3 6 0 12.21 11.98 1.07 o -2 6 0 181.05 180.36 2.72 o -1 6 0 6.80 7.50 1.58 o 0 6 0 1156.08 1205.97 4.61 o 1 6 0 37.55 37.50 1.23 o 2 6 0 375.43 387.35 2.34 o 3 6 0 0.00 0.40 0.63 o 4 6 0 76.27 77.52 2.05 o 5 6 0 3.37 4.48 0.95 o 6 6 0 33.55 30.20 1.45 o 7 6 0 1.90 1.52 1.33 o 8 6 0 0.04 0.75 1.58 o 9 6 0 0.28 -0.53 2.27 o -5 7 0 1.54 1.36 1.28 o -4 7 0 43.78 47.10 1.84 o -3 7 0 5.12 4.64 1.06 o -2 7 0 409.50 422.36 3.68 o -1 7 0 7.98 8.26 1.19 o 0 7 0 130.21 131.78 3.33 o 1 7 0 3.70 3.33 0.97 o 2 7 0 780.70 803.26 7.12 o 3 7 0 13.59 15.83 1.14 o 4 7 0 401.61 412.85 3.70 o 5 7 0 3.92 4.18 1.21 o 6 7 0 116.18 119.80 2.71 o 7 7 0 5.35 5.21 1.52 o 8 7 0 37.20 36.78 2.53 o -3 8 0 57.42 54.12 2.69 o -2 8 0 0.09 1.07 1.32 o -1 8 0 3.85 3.78 2.26 o 0 8 0 116.37 120.63 2.71 o 1 8 0 35.66 35.35 1.68 o 2 8 0 3.98 4.60 2.51 o 3 8 0 1.63 2.56 1.10 o 4 8 0 184.19 189.67 3.07 o 5 8 0 8.77 6.36 1.40 o 6 8 0 137.52 140.20 3.12 o 7 8 0 0.02 0.39 2.21 o 0 9 0 0.35 0.91 1.84 o 5 9 0 28.50 26.69 2.46 o 6 9 0 32.00 31.00 2.06 o -7 -9 1 0.17 0.98 2.18 o -6 -9 1 55.45 55.00 2.63 o -5 -9 1 1.81 1.78 1.79 o -2 -9 1 6.33 8.75 2.87 o -1 -9 1 0.82 0.89 2.12 o 0 -9 1 50.88 45.63 2.68 o 1 -9 1 95.89 100.19 2.04 o 2 -9 1 9.48 7.95 1.58 o -8 -8 1 53.32 50.43 2.21 o -7 -8 1 11.05 10.82 1.92 o -6 -8 1 192.49 198.10 3.40 o -5 -8 1 0.11 1.85 1.65 o -4 -8 1 81.96 83.90 2.30 o -3 -8 1 0.72 1.88 1.51 o -2 -8 1 149.62 151.38 2.34 o -1 -8 1 13.40 14.29 1.57 o 0 -8 1 13.84 16.06 1.13 o 1 -8 1 5.04 3.79 1.24 o 2 -8 1 110.86 122.11 3.83 o 3 -8 1 178.52 199.93 2.57 o 4 -8 1 50.86 48.42 2.33 o -9 -7 1 12.74 13.91 2.68 o -8 -7 1 7.36 6.18 2.34 o -7 -7 1 5.64 4.15 1.68 o -6 -7 1 20.59 21.20 2.26 o -5 -7 1 73.36 76.87 1.46 o -4 -7 1 203.95 206.35 2.63 o -3 -7 1 55.42 56.92 1.20 o -2 -7 1 8.60 10.23 1.31 o -1 -7 1 0.04 0.25 0.86 o 0 -7 1 67.34 67.64 2.16 o 1 -7 1 26.17 28.76 1.35 o 2 -7 1 25.75 23.32 1.43 o 3 -7 1 38.25 30.69 1.44 o 4 -7 1 12.73 14.31 3.09 o 5 -7 1 91.13 104.25 1.98 o 6 -7 1 18.92 17.12 2.46 o -9 -6 1 12.66 12.46 2.02 o -8 -6 1 0.85 0.98 1.55 o -7 -6 1 20.84 20.97 2.12 o -6 -6 1 10.61 9.18 1.23 o -5 -6 1 10.75 10.64 1.13 o -4 -6 1 7.95 8.20 0.84 o -3 -6 1 130.42 128.70 1.35 o -2 -6 1 443.73 450.82 2.50 o -1 -6 1 288.42 291.35 1.49 o 0 -6 1 1.73 1.61 0.78 o 1 -6 1 42.01 41.40 1.25 o 2 -6 1 58.50 61.16 1.30 o 3 -6 1 165.34 163.99 2.42 o 4 -6 1 116.84 113.46 1.88 o 5 -6 1 4.65 3.56 1.03 o 6 -6 1 28.79 28.49 2.58 o 7 -6 1 90.17 102.73 2.95 o -10 -5 1 39.04 40.01 2.74 o -9 -5 1 0.46 -0.47 1.64 o -8 -5 1 12.69 10.61 1.84 o -7 -5 1 8.75 6.58 0.98 o -6 -5 1 34.39 34.17 2.14 o -5 -5 1 3.66 4.49 0.75 o -4 -5 1 14.29 13.89 0.74 o -3 -5 1 23.86 26.70 1.12 o -2 -5 1 92.36 86.33 1.31 o -1 -5 1 0.13 2.17 0.67 o 0 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14.34 0.31 o 0 -3 1 9.73 14.33 0.61 o 1 -3 1 140.35 147.38 1.22 o 2 -3 1 1173.31 1144.37 5.04 o 3 -3 1 49.38 53.82 0.87 o 4 -3 1 50.77 53.56 1.08 o 5 -3 1 25.77 23.36 0.87 o 6 -3 1 71.06 66.11 1.31 o 7 -3 1 8.29 7.21 1.67 o 8 -3 1 8.86 9.69 1.48 o -11 -2 1 3.44 5.10 2.21 o -10 -2 1 38.16 34.77 1.97 o -9 -2 1 17.71 15.56 1.72 o -8 -2 1 183.34 182.92 2.42 o -7 -2 1 21.04 18.51 0.97 o -6 -2 1 913.87 928.80 11.10 o -5 -2 1 1.02 1.47 0.53 o -4 -2 1 704.05 729.80 2.22 o -3 -2 1 95.60 93.64 1.35 o -2 -2 1 230.24 244.42 8.78 o -1 -2 1 672.93 742.59 1.24 o 0 -2 1 0.38 2.43 0.70 o 1 -2 1 372.55 390.43 2.21 o 2 -2 1 122.69 131.01 0.85 o 3 -2 1 871.22 937.21 8.48 o 4 -2 1 460.33 411.47 2.48 o 5 -2 1 389.18 392.78 4.51 o 6 -2 1 43.36 45.83 1.26 o 7 -2 1 31.99 28.67 1.44 o 8 -2 1 0.09 1.00 1.20 o 9 -2 1 20.52 20.21 2.96 o -10 -1 1 1.58 1.96 1.40 o -9 -1 1 20.92 22.41 2.22 o -8 -1 1 1.72 1.80 1.09 o -7 -1 1 12.73 13.21 0.97 o -6 -1 1 6.60 6.95 0.83 o -5 -1 1 0.93 2.25 0.46 o -4 -1 1 1367.22 1486.55 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1 1848.98 1877.90 24.68 o 1 1 1 195.51 243.57 1.65 o 2 1 1 77.00 75.45 0.93 o 3 1 1 22.39 20.77 0.78 o 4 1 1 0.25 0.90 0.35 o 5 1 1 251.32 247.73 1.81 o 6 1 1 79.98 73.16 1.26 o 7 1 1 36.74 35.65 1.14 o 8 1 1 242.89 245.19 2.40 o 9 1 1 57.12 61.62 2.22 o -8 2 1 185.95 189.04 4.95 o -7 2 1 0.55 0.80 1.08 o -6 2 1 99.64 93.63 1.57 o -5 2 1 20.97 19.58 0.57 o -4 2 1 284.26 273.68 2.39 o -3 2 1 164.54 192.93 1.03 o -2 2 1 11.53 13.98 0.39 o -1 2 1 327.63 342.96 2.29 o 0 2 1 3170.97 3228.96 16.65 o 1 2 1 717.48 811.64 1.79 o 2 2 1 146.07 185.67 1.26 o 3 2 1 21.94 21.54 0.64 o 4 2 1 3.27 4.52 0.40 o 5 2 1 31.71 33.16 0.77 o 6 2 1 3.38 2.71 1.20 o 7 2 1 25.09 22.92 0.99 o 8 2 1 4.43 3.96 0.91 o 9 2 1 3.18 2.64 1.54 o 10 2 1 81.26 84.27 2.86 o -8 3 1 184.56 191.44 2.51 o -7 3 1 89.73 93.99 2.82 o -6 3 1 258.30 269.21 3.07 o -5 3 1 5.49 4.88 0.72 o -4 3 1 74.48 66.80 1.18 o -3 3 1 0.14 0.50 0.35 o -2 3 1 561.05 533.18 1.98 o -1 3 1 87.57 106.70 1.14 o 0 3 1 4.32 6.32 0.45 o 1 3 1 40.59 39.82 1.02 o 2 3 1 2306.73 2462.12 5.78 o 3 3 1 290.10 309.49 2.78 o 4 3 1 88.18 71.93 1.14 o 5 3 1 37.20 37.13 0.99 o 6 3 1 61.14 58.28 1.35 o 7 3 1 62.31 62.61 1.51 o 8 3 1 12.93 13.87 1.30 o 9 3 1 4.63 2.79 1.73 o 10 3 1 4.23 4.43 1.88 o 11 3 1 10.46 10.00 1.91 o -8 4 1 35.30 30.49 2.86 o -7 4 1 25.92 22.79 1.88 o -6 4 1 217.20 221.62 2.88 o -5 4 1 1.02 1.90 0.91 o -4 4 1 297.10 295.87 1.87 o -3 4 1 78.59 76.51 1.28 o -2 4 1 0.68 1.02 0.98 o -1 4 1 81.05 74.77 1.13 o 0 4 1 144.14 129.85 1.46 o 1 4 1 275.63 288.87 1.94 o 2 4 1 157.83 168.50 2.70 o 3 4 1 36.80 34.71 1.00 o 4 4 1 432.90 428.58 1.81 o 5 4 1 109.45 111.12 1.31 o 6 4 1 22.71 21.29 1.15 o 7 4 1 19.82 21.00 2.14 o 8 4 1 14.08 15.45 1.64 o 9 4 1 17.81 16.78 1.79 o 10 4 1 7.74 10.65 2.55 o -7 5 1 0.02 0.77 1.28 o -6 5 1 21.52 20.82 1.52 o -5 5 1 32.25 29.80 1.39 o -4 5 1 276.63 282.10 2.53 o -3 5 1 0.74 1.38 0.73 o -2 5 1 533.86 522.38 2.99 o -1 5 1 169.78 169.32 2.49 o 0 5 1 42.58 36.73 1.08 o 1 5 1 195.67 191.48 1.80 o 2 5 1 158.27 158.86 2.37 o 3 5 1 471.53 482.35 2.50 o 4 5 1 83.53 85.97 1.25 o 5 5 1 171.24 172.02 2.04 o 6 5 1 70.09 67.53 1.62 o 7 5 1 143.69 146.73 2.92 o 8 5 1 0.42 1.48 1.79 o 9 5 1 51.63 53.33 2.61 o 10 5 1 1.56 0.74 1.92 o -6 6 1 6.21 3.46 1.55 o -5 6 1 0.93 0.91 1.28 o -4 6 1 47.21 50.44 1.77 o -3 6 1 13.73 11.95 1.13 o -2 6 1 22.72 20.16 1.34 o -1 6 1 9.94 9.60 1.04 o 0 6 1 181.83 185.82 1.98 o 1 6 1 25.39 24.30 1.38 o 2 6 1 8.38 8.95 1.51 o 3 6 1 27.08 25.17 1.60 o 4 6 1 85.68 82.65 1.45 o 5 6 1 149.71 151.65 2.79 o 6 6 1 32.18 32.36 1.92 o 7 6 1 85.42 92.02 2.66 o 8 6 1 16.65 16.07 2.10 o 9 6 1 60.80 65.17 3.10 o -4 7 1 9.31 8.97 2.40 o -3 7 1 26.43 22.52 1.87 o -2 7 1 161.51 155.96 3.22 o -1 7 1 53.05 48.65 1.92 o 0 7 1 26.14 25.39 2.11 o 1 7 1 0.61 1.38 0.94 o 2 7 1 5.67 4.25 0.96 o 3 7 1 18.06 16.39 1.26 o 4 7 1 20.90 19.20 1.92 o 5 7 1 4.69 4.11 1.29 o 6 7 1 2.27 1.81 1.46 o 7 7 1 26.81 22.94 2.23 o 8 7 1 47.77 45.00 2.66 o -2 8 1 0.76 0.24 2.21 o -1 8 1 0.03 -0.46 1.75 o 0 8 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134.10 129.30 2.14 o 2 1 8 0.01 0.55 1.27 o 3 1 8 17.53 19.04 1.74 o -2 2 8 0.82 0.72 1.18 o -1 2 8 145.62 156.62 1.97 o 0 2 8 26.72 24.71 1.27 o 1 2 8 72.19 75.49 1.83 o 2 2 8 97.08 92.46 2.06 o 3 2 8 134.31 144.41 3.57 o 5 2 8 11.16 14.83 2.40 o 6 2 8 0.43 0.47 1.93 o 5 3 8 105.72 101.61 2.81 o 6 3 8 16.15 15.93 2.52 o 7 3 8 20.13 17.18 1.77 o 5 4 8 0.75 1.06 2.37 o 4 5 8 17.85 18.36 2.63 o -2 -7 9 12.68 12.02 1.69 o -1 -7 9 13.98 11.48 2.11 o -8 -6 9 4.47 4.56 2.08 o -7 -6 9 13.74 13.54 2.18 o -6 -6 9 29.61 32.44 2.27 o -3 -6 9 52.46 45.29 2.30 o -2 -6 9 95.23 93.83 2.78 o -1 -6 9 26.25 28.94 2.31 o 3 -6 9 2.73 2.94 1.84 o -8 -5 9 43.15 44.51 2.66 o -7 -5 9 2.79 2.46 1.76 o -6 -5 9 28.89 27.02 1.91 o -5 -5 9 3.83 4.05 1.61 o -3 -5 9 23.59 21.16 2.30 o -2 -5 9 0.03 0.34 2.00 o -1 -5 9 28.82 23.22 1.92 o 0 -5 9 79.20 84.45 2.78 o 1 -5 9 1.93 1.92 1.88 o 2 -5 9 24.33 23.41 2.14 o 3 -5 9 35.82 34.89 2.50 o -8 -4 9 2.21 4.90 2.79 o -7 -4 9 0.90 0.70 1.95 o -6 -4 9 118.03 127.04 2.91 o -5 -4 9 9.80 9.17 1.33 o -4 -4 9 138.68 145.43 2.02 o -3 -4 9 53.59 46.80 2.45 o -2 -4 9 305.74 307.94 4.24 o -1 -4 9 10.33 9.02 1.75 o 0 -4 9 19.08 19.49 2.42 o 1 -4 9 1.29 2.84 1.55 o 2 -4 9 135.02 142.45 4.20 o 3 -4 9 55.74 61.27 1.99 o 4 -4 9 13.06 12.29 1.83 o -8 -3 9 8.18 9.85 2.65 o -7 -3 9 38.07 35.33 2.10 o -6 -3 9 3.14 2.82 1.79 o -4 -3 9 49.38 50.53 3.01 o -3 -3 9 8.60 7.33 2.31 o -2 -3 9 92.74 92.49 2.51 o -1 -3 9 60.75 56.73 2.51 o 0 -3 9 343.57 348.80 4.72 o 1 -3 9 23.71 22.90 1.74 o 2 -3 9 25.98 24.94 1.71 o 3 -3 9 0.67 0.66 1.31 o 4 -3 9 158.01 168.40 2.56 o -4 -2 9 10.98 10.58 2.64 o -3 -2 9 81.43 78.16 2.47 o -2 -2 9 0.82 0.98 1.56 o -1 -2 9 68.54 60.63 2.25 o 0 -2 9 4.77 3.81 1.71 o 1 -2 9 158.58 151.01 2.29 o 2 -2 9 130.63 134.89 2.25 o 3 -2 9 82.99 79.80 2.35 o -3 -1 9 96.63 99.97 3.00 o -2 -1 9 3.63 2.38 1.68 o -1 -1 9 98.24 92.31 2.76 o 0 -1 9 0.59 1.16 0.94 o 1 -1 9 62.45 57.17 1.93 o 2 -1 9 0.02 0.13 1.39 o 3 -1 9 178.44 175.99 2.64 o -2 0 9 10.29 9.95 2.58 o -1 0 9 17.99 15.97 1.95 o 0 0 9 43.27 41.40 1.49 o 1 0 9 23.88 19.74 1.74 o 2 0 9 45.29 44.85 2.93 o -1 1 9 37.56 32.89 1.53 o 0 1 9 38.26 39.51 1.67 o 1 1 9 8.72 6.20 2.33 o 5 2 9 3.03 5.38 2.15 o 5 3 9 43.93 43.75 2.72 o -7 -6 10 17.13 15.18 2.23 o -7 -5 10 53.57 57.44 3.00 o -6 -5 10 25.40 22.20 2.43 o -2 -5 10 0.57 1.35 2.20 o 0 -5 10 32.03 34.08 2.48 o 1 -5 10 164.25 178.53 3.70 o 2 -5 10 27.44 28.24 2.75 o -7 -4 10 6.87 7.63 1.85 o -2 -4 10 1.40 2.61 2.32 o 0 -4 10 13.57 11.90 2.81 o 1 -4 10 87.82 96.03 3.19 o 2 -4 10 1.11 1.74 1.31 o -2 -3 10 2.72 2.71 2.17 o -1 -3 10 107.75 100.85 3.05 o 0 -3 10 24.62 22.42 1.91 o 1 -3 10 87.74 93.94 3.05 o 2 -3 10 40.62 37.37 2.64 o -2 -2 10 119.82 130.74 3.13 o -1 -2 10 7.25 5.77 2.02 o 1 -2 10 37.84 34.05 3.12 o 2 -2 10 9.94 7.65 2.50 o -1 -1 10 86.54 92.82 3.34 o