#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:16:22 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180841 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/72/2017278.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017278_Fobs loop_ _publ_author_name 'G\'omez, Sandra L.' 'Sanabria, Carlos M.' 'Palma, Alirio' 'Bahsas, Ali' 'Cobo, Justo' 'Glidewell, Christopher' _publ_section_title ; Four differently substituted 2-aryl-2,3,4,5-tetrahydro-1H-1,4-epoxy-1-benzazepines: hydrogen-bonded structures in one, two and three dimensions ; _journal_coeditor_code FA3200 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o465 _journal_page_last o469 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.964 _cell_angle_gamma 90.000 _cell_length_a 9.2907 _cell_length_b 10.8720 _cell_length_c 13.4523 _exptl_crystal_F_000 664.00 _reflns_d_resolution_high 0.7695 _cod_data_source_file fa3200Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' jac62b2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 149.30 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 9047.15 8494.07 132.11 o 4 0 0 5005.82 4901.41 106.51 o 6 0 0 163.32 168.06 15.97 o 8 0 0 395.35 361.85 35.48 o 10 0 0 1.83 -13.63 119.11 o 12 0 0 0.47 122.06 93.60 o 1 1 0 1195.69 1119.55 41.48 o 2 1 0 19.03 9.29 7.79 o 3 1 0 3988.62 3912.56 54.66 o 4 1 0 112.65 141.17 12.85 o 5 1 0 1312.17 1300.62 30.87 o 6 1 0 2491.19 2693.93 44.49 o 7 1 0 1242.61 1184.42 28.74 o 8 1 0 817.37 796.31 27.07 o 9 1 0 657.95 685.91 37.84 o 10 1 0 294.13 350.92 37.02 o 11 1 0 2.75 11.89 63.97 o 0 2 0 4264.88 3909.22 114.09 o 1 2 0 22021.72 21270.55 388.82 o 2 2 0 5789.15 5718.46 65.55 o 3 2 0 0.88 -1.57 6.79 o 4 2 0 191.96 201.02 12.81 o 5 2 0 14.35 18.40 10.09 o 6 2 0 639.75 633.09 23.32 o 7 2 0 345.02 313.38 18.25 o 8 2 0 1093.37 1079.78 33.30 o 9 2 0 247.24 323.48 31.92 o 10 2 0 15.57 40.23 32.64 o 11 2 0 30.98 -7.60 48.00 o 1 3 0 11328.90 11638.46 188.75 o 2 3 0 691.31 704.77 14.61 o 3 3 0 36.48 55.18 8.02 o 4 3 0 1715.09 1758.38 32.19 o 5 3 0 84.44 91.58 12.38 o 6 3 0 510.88 507.38 25.95 o 7 3 0 592.38 587.87 24.25 o 8 3 0 247.24 172.02 21.60 o 9 3 0 1131.77 1167.70 65.98 o 10 3 0 56.27 80.82 33.27 o 11 3 0 316.37 377.43 64.51 o 0 4 0 1105.37 1113.63 30.36 o 1 4 0 952.15 887.90 20.02 o 2 4 0 362.41 386.05 17.17 o 3 4 0 421.63 421.61 18.89 o 4 4 0 955.51 1013.26 25.38 o 5 4 0 4737.29 4990.22 70.66 o 6 4 0 188.16 147.44 15.43 o 7 4 0 1354.09 1359.04 34.98 o 8 4 0 2384.86 2592.61 52.70 o 9 4 0 303.57 288.08 32.69 o 10 4 0 26.01 31.01 35.64 o 11 4 0 50.46 -20.50 70.17 o 1 5 0 1237.98 1165.06 25.06 o 2 5 0 3633.38 3646.45 53.65 o 3 5 0 25.66 9.02 12.24 o 4 5 0 647.72 614.74 20.71 o 5 5 0 162.80 175.50 14.83 o 6 5 0 1028.17 1057.64 28.76 o 7 5 0 713.14 754.58 28.55 o 8 5 0 1356.74 1450.30 42.04 o 9 5 0 0.48 14.62 34.33 o 10 5 0 64.95 102.72 42.93 o 11 5 0 12.72 8.54 63.76 o 0 6 0 9954.03 10827.92 712.56 o 1 6 0 18.50 13.63 9.64 o 2 6 0 186.77 178.66 12.74 o 3 6 0 27.81 14.55 12.08 o 4 6 0 117.39 109.44 12.36 o 5 6 0 824.43 809.65 24.78 o 6 6 0 33.83 13.22 15.72 o 7 6 0 1105.30 1117.22 44.45 o 8 6 0 335.88 320.89 29.93 o 9 6 0 243.73 197.59 44.10 o 10 6 0 18.53 -6.66 55.17 o 1 7 0 93.59 127.99 16.58 o 2 7 0 193.40 184.58 14.26 o 3 7 0 246.34 275.74 19.10 o 4 7 0 86.48 75.39 13.50 o 5 7 0 1.19 17.02 14.17 o 6 7 0 70.59 31.64 16.24 o 7 7 0 212.22 236.76 31.55 o 8 7 0 7.15 -0.73 28.10 o 9 7 0 66.66 25.80 51.12 o 10 7 0 78.16 42.63 63.07 o 0 8 0 18.07 15.60 28.68 o 1 8 0 391.83 375.06 30.92 o 2 8 0 0.05 -17.30 13.35 o 3 8 0 162.07 164.36 23.63 o 4 8 0 4.83 8.73 18.04 o 5 8 0 95.59 104.44 24.15 o 6 8 0 323.82 281.36 22.39 o 7 8 0 55.56 33.02 23.35 o 8 8 0 1.03 -7.86 42.78 o 9 8 0 118.49 52.84 57.70 o 1 9 0 668.56 708.90 46.18 o 2 9 0 77.15 36.11 18.65 o 3 9 0 640.68 636.24 27.23 o 4 9 0 3.26 -17.09 20.89 o 5 9 0 15.46 15.98 23.91 o 6 9 0 26.93 19.10 24.54 o 7 9 0 245.38 402.92 59.41 o 8 9 0 27.45 -15.05 53.19 o 9 9 0 45.65 130.10 80.93 o 0 10 0 905.11 933.07 69.75 o 1 10 0 511.84 544.37 42.63 o 2 10 0 216.60 197.06 37.85 o 3 10 0 76.58 71.33 24.69 o 4 10 0 133.97 91.29 29.66 o 5 10 0 417.54 398.72 39.34 o 6 10 0 33.92 47.21 52.28 o 7 10 0 0.03 -75.65 51.29 o 8 10 0 110.18 -24.66 72.40 o 1 11 0 53.93 17.86 36.79 o 2 11 0 191.30 106.30 44.33 o 3 11 0 16.71 32.56 33.81 o 4 11 0 63.11 78.81 31.28 o 5 11 0 6.27 -23.81 46.98 o 6 11 0 172.48 79.91 103.27 o 7 11 0 0.17 -4.26 59.76 o 0 12 0 0.57 -51.98 70.80 o 1 12 0 18.61 -64.79 44.67 o 2 12 0 34.02 -32.93 45.70 o 3 12 0 16.11 15.75 103.97 o 4 12 0 45.50 4.50 51.93 o 5 12 0 103.60 71.65 105.10 o 6 12 0 0.52 203.80 125.41 o 1 13 0 37.39 36.69 58.09 o 2 13 0 115.99 114.69 72.93 o 3 13 0 0.61 -83.96 82.43 o 4 13 0 24.75 15.24 119.22 o 0 14 0 18.39 61.95 143.09 o 1 14 0 7.73 -56.37 94.55 o -11 0 1 1167.73 1273.15 104.42 o -9 0 1 525.12 489.52 36.22 o -7 0 1 1236.00 1218.04 39.51 o -5 0 1 570.34 395.68 18.12 o -3 0 1 1197.93 1154.45 24.79 o 1 0 1 4419.77 4141.44 64.99 o 3 0 1 385.52 330.29 17.29 o 5 0 1 8754.35 8878.79 135.78 o 7 0 1 578.55 603.52 28.93 o 9 0 1 334.43 272.06 47.94 o 11 0 1 12.51 47.04 66.60 o -12 1 1 80.57 154.26 62.84 o -11 1 1 209.59 99.47 51.06 o -10 1 1 381.50 437.83 40.15 o -9 1 1 32.73 22.21 27.35 o -8 1 1 1970.76 2140.54 42.57 o -7 1 1 0.47 -9.11 13.15 o -6 1 1 479.32 423.22 15.51 o -5 1 1 224.02 203.48 10.97 o -4 1 1 737.34 651.59 13.98 o -3 1 1 2692.67 2633.74 31.46 o -2 1 1 14847.10 14248.07 128.18 o -1 1 1 238.97 192.25 6.67 o 1 1 1 187.87 194.39 6.54 o 2 1 1 5209.91 4874.07 57.84 o 3 1 1 27.37 23.47 7.64 o 4 1 1 38.46 14.92 8.19 o 5 1 1 19.35 29.03 12.38 o 6 1 1 3.56 27.34 12.94 o 7 1 1 627.94 595.54 22.95 o 8 1 1 826.77 812.06 28.73 o 9 1 1 82.82 102.05 28.09 o 10 1 1 0.53 13.98 40.97 o 11 1 1 103.23 8.34 48.23 o -11 2 1 1.63 -30.23 47.86 o -10 2 1 21.12 -8.15 35.53 o -9 2 1 270.03 289.86 28.60 o -8 2 1 429.20 428.18 23.11 o -7 2 1 26.91 26.82 15.05 o -6 2 1 1246.09 1300.56 28.29 o -5 2 1 1059.28 1051.67 21.97 o -4 2 1 2607.16 2750.03 37.07 o -3 2 1 0.30 -8.82 5.88 o -2 2 1 9841.51 9564.65 88.79 o -1 2 1 6518.57 6317.38 61.61 o 0 2 1 8697.38 8721.84 92.25 o 1 2 1 473.22 450.90 11.68 o 2 2 1 4152.98 3966.48 52.73 o 3 2 1 1062.86 1011.54 22.49 o 4 2 1 426.41 394.30 16.20 o 5 2 1 192.21 169.66 14.02 o 6 2 1 1112.82 1091.15 31.67 o 7 2 1 879.10 887.99 31.77 o 8 2 1 934.26 949.14 34.92 o 9 2 1 7.24 9.54 25.16 o 10 2 1 5.65 43.94 34.46 o 11 2 1 55.04 -76.06 50.70 o -11 3 1 2.73 3.01 50.85 o -10 3 1 16.83 -31.85 34.35 o -9 3 1 535.28 563.22 40.64 o -8 3 1 727.54 718.74 29.05 o -7 3 1 830.20 836.24 25.82 o -6 3 1 32.24 14.71 16.58 o -5 3 1 1.93 -2.35 10.21 o -4 3 1 130.54 168.87 9.97 o -3 3 1 1510.29 1478.26 28.93 o -2 3 1 2807.43 2759.52 32.55 o -1 3 1 2.16 5.91 5.74 o 0 3 1 18553.40 18833.82 207.84 o 1 3 1 478.64 453.11 14.90 o 2 3 1 650.49 590.08 16.43 o 3 3 1 607.02 629.53 17.85 o 4 3 1 608.18 572.44 19.55 o 5 3 1 58.34 78.38 24.36 o 6 3 1 4924.69 5437.31 79.05 o 7 3 1 16.37 17.87 17.92 o 8 3 1 0.04 3.09 21.41 o 9 3 1 165.61 172.95 33.08 o 10 3 1 711.20 730.44 44.96 o 11 3 1 128.16 110.95 53.43 o -11 4 1 29.20 57.36 53.90 o -10 4 1 434.28 494.48 55.32 o -9 4 1 125.07 93.03 33.03 o -8 4 1 468.49 407.79 24.57 o -7 4 1 399.57 426.38 26.78 o -6 4 1 227.18 225.73 15.97 o -5 4 1 599.13 651.25 17.99 o -4 4 1 1933.44 1939.55 31.12 o -3 4 1 12.39 -2.58 7.39 o -2 4 1 475.88 499.15 15.05 o -1 4 1 1932.34 1900.51 30.50 o 0 4 1 4283.74 4192.30 65.35 o 1 4 1 37.22 19.96 6.53 o 2 4 1 85.75 75.04 7.90 o 3 4 1 490.83 496.35 15.18 o 4 4 1 255.05 244.20 15.89 o 5 4 1 78.74 90.37 18.80 o 6 4 1 1.21 25.13 15.61 o 7 4 1 759.13 813.17 32.61 o 8 4 1 522.90 476.28 28.95 o 9 4 1 91.26 93.74 43.16 o 10 4 1 2.34 36.87 38.77 o 11 4 1 29.79 123.78 59.02 o -11 5 1 12.64 1.27 64.79 o -10 5 1 36.31 -8.26 50.23 o -9 5 1 11.70 74.28 31.26 o -8 5 1 7.25 -21.34 22.27 o -7 5 1 839.08 920.35 30.35 o -6 5 1 0.39 4.15 14.87 o -5 5 1 185.95 180.12 14.32 o -4 5 1 22.22 16.71 8.60 o -3 5 1 6190.57 6464.70 84.75 o -2 5 1 5586.53 6152.20 81.15 o -1 5 1 3721.99 3984.87 55.95 o 0 5 1 237.78 216.06 11.38 o 1 5 1 5.24 -10.67 10.67 o 2 5 1 848.48 809.65 22.51 o 3 5 1 9.44 13.48 8.01 o 4 5 1 1982.23 2016.30 39.04 o 5 5 1 37.14 41.05 13.98 o 6 5 1 32.29 40.17 17.97 o 7 5 1 21.12 6.09 18.61 o 8 5 1 11.99 -14.21 26.29 o 9 5 1 70.71 49.66 35.04 o 10 5 1 34.04 -6.35 48.10 o 11 5 1 55.06 60.52 65.76 o -10 6 1 115.73 144.97 56.34 o -9 6 1 607.19 725.92 46.72 o -8 6 1 487.77 410.40 42.68 o -7 6 1 919.85 944.75 30.62 o -6 6 1 47.33 31.84 17.79 o -5 6 1 216.80 203.01 14.42 o -4 6 1 159.77 163.79 14.08 o -3 6 1 651.70 622.80 21.31 o -2 6 1 512.10 536.59 19.67 o -1 6 1 456.39 379.93 14.54 o 0 6 1 3330.25 3483.27 58.10 o 1 6 1 13.73 21.30 10.16 o 2 6 1 253.59 245.12 15.11 o 3 6 1 81.44 56.70 12.34 o 4 6 1 31.31 22.65 14.33 o 5 6 1 2388.93 2529.42 46.49 o 6 6 1 53.48 16.90 22.57 o 7 6 1 62.78 50.68 22.34 o 8 6 1 366.34 378.61 34.48 o 9 6 1 6.61 57.04 41.38 o 10 6 1 22.84 -3.15 57.14 o -10 7 1 122.59 104.32 58.91 o -9 7 1 2.70 -11.52 50.02 o -8 7 1 851.43 945.24 57.85 o -7 7 1 14.04 10.33 21.39 o -6 7 1 64.61 45.57 17.39 o -5 7 1 106.48 112.26 20.14 o -4 7 1 89.89 104.11 17.10 o -3 7 1 1.00 -1.28 13.44 o -2 7 1 452.64 453.11 19.32 o -1 7 1 1457.63 1633.49 36.19 o 0 7 1 15.92 13.87 12.14 o 1 7 1 1678.10 1813.19 40.41 o 2 7 1 1621.90 1847.37 39.57 o 3 7 1 1141.38 1233.07 31.22 o 4 7 1 20.37 29.50 15.66 o 5 7 1 1849.88 2042.87 41.84 o 6 7 1 546.90 580.18 27.25 o 7 7 1 1.20 2.40 22.11 o 8 7 1 67.66 69.73 30.09 o 9 7 1 393.17 497.89 63.27 o 10 7 1 24.77 129.03 66.50 o -9 8 1 12.98 91.16 73.01 o -8 8 1 132.97 215.36 45.62 o -7 8 1 13.94 25.60 26.42 o -6 8 1 49.43 20.13 22.53 o -5 8 1 10.31 -0.77 20.41 o -4 8 1 283.11 219.13 25.87 o -3 8 1 149.95 143.33 18.35 o -2 8 1 178.23 178.23 21.43 o -1 8 1 378.73 418.19 23.62 o 0 8 1 545.75 573.70 34.13 o 1 8 1 24.18 -17.63 25.32 o 2 8 1 971.56 1052.83 30.60 o 3 8 1 3.41 -18.92 19.09 o 4 8 1 91.70 71.85 14.62 o 5 8 1 0.17 -7.26 22.75 o 6 8 1 888.06 864.12 41.08 o 7 8 1 85.00 36.88 27.46 o 8 8 1 561.02 618.03 55.31 o 9 8 1 1.19 20.65 57.13 o -9 9 1 236.74 257.94 69.04 o -8 9 1 205.69 108.00 86.15 o -7 9 1 343.94 371.36 49.56 o -6 9 1 5.16 8.67 28.96 o -5 9 1 150.95 127.45 29.95 o -4 9 1 0.82 -3.06 21.18 o -3 9 1 426.79 403.26 25.97 o -2 9 1 1.76 2.64 18.03 o -1 9 1 647.71 645.02 30.38 o 0 9 1 0.32 3.01 25.57 o 1 9 1 38.96 10.84 29.99 o 2 9 1 729.87 743.48 37.81 o 3 9 1 135.97 111.52 23.05 o 4 9 1 760.90 851.36 33.20 o 5 9 1 87.30 82.90 18.16 o 6 9 1 320.06 393.96 33.80 o 7 9 1 0.53 17.27 70.65 o 8 9 1 10.37 -47.89 53.66 o 9 9 1 1.25 -96.15 64.10 o -8 10 1 39.98 -25.73 101.33 o -7 10 1 353.29 318.20 55.89 o -6 10 1 294.47 342.30 75.02 o -5 10 1 208.70 171.91 33.86 o -4 10 1 141.95 109.80 30.10 o -3 10 1 21.00 28.22 23.98 o -2 10 1 46.10 -1.58 19.96 o -1 10 1 12.54 7.45 31.24 o 0 10 1 742.03 771.18 41.42 o 1 10 1 3.19 20.23 38.13 o 2 10 1 30.20 13.26 31.71 o 3 10 1 140.84 90.12 24.71 o 4 10 1 181.22 169.43 37.12 o 5 10 1 43.12 81.02 60.63 o 6 10 1 0.91 -5.32 44.54 o 7 10 1 57.23 -25.08 54.72 o 8 10 1 0.86 -17.82 61.28 o -7 11 1 464.17 536.61 68.75 o -6 11 1 97.99 -41.99 65.29 o -5 11 1 187.43 198.79 59.00 o -4 11 1 13.92 8.33 33.71 o -3 11 1 1334.14 1493.45 62.54 o -2 11 1 30.89 55.51 43.02 o -1 11 1 168.12 143.72 38.99 o 0 11 1 0.22 81.26 49.28 o 1 11 1 235.00 124.64 47.32 o 2 11 1 67.86 41.51 64.14 o 3 11 1 0.40 -22.46 28.97 o 4 11 1 49.36 -3.32 37.50 o 5 11 1 16.51 -50.10 44.90 o 6 11 1 56.63 9.58 53.95 o 7 11 1 0.57 -33.99 74.48 o -6 12 1 8.27 88.47 87.50 o -5 12 1 57.92 50.84 55.76 o -4 12 1 6.63 19.42 78.94 o -3 12 1 88.14 50.62 52.53 o -2 12 1 38.25 73.50 54.23 o -1 12 1 36.53 105.34 54.68 o 0 12 1 245.75 100.01 82.84 o 1 12 1 14.84 -47.27 47.97 o 2 12 1 92.84 52.19 48.22 o 3 12 1 14.44 2.89 64.64 o 4 12 1 89.93 75.25 50.49 o 5 12 1 143.03 54.14 66.57 o 6 12 1 147.26 88.12 85.66 o -4 13 1 35.62 -30.45 137.78 o -3 13 1 49.23 69.46 79.92 o -2 13 1 3.30 -34.55 106.98 o -1 13 1 6.01 -22.31 70.22 o 0 13 1 38.33 137.78 71.49 o 1 13 1 169.41 4.29 56.65 o 2 13 1 1.59 -2.09 65.87 o 3 13 1 21.85 116.35 72.76 o 4 13 1 102.92 30.45 130.70 o -1 14 1 0.49 -34.66 150.65 o 0 14 1 59.02 4.18 108.05 o 1 14 1 49.96 -38.48 94.79 o -12 0 2 212.51 187.96 91.97 o -10 0 2 1635.25 1903.95 91.06 o -8 0 2 478.96 496.92 31.00 o -6 0 2 427.01 348.61 21.91 o -4 0 2 3414.95 3360.78 61.00 o -2 0 2 2498.57 2340.69 37.12 o 0 0 2 314.89 317.29 13.72 o 2 0 2 11.84 11.10 8.34 o 4 0 2 657.56 695.92 33.94 o 6 0 2 837.26 900.42 38.96 o 8 0 2 1431.84 1366.85 55.48 o 10 0 2 411.80 447.66 69.64 o -12 1 2 1.76 -40.74 62.63 o -11 1 2 587.89 600.25 80.14 o -10 1 2 457.05 412.08 38.02 o -9 1 2 0.15 -40.21 26.81 o -8 1 2 416.41 421.42 21.07 o -7 1 2 983.43 965.74 24.32 o -6 1 2 270.70 277.52 14.18 o -5 1 2 20.40 17.92 8.00 o -4 1 2 2509.31 2415.69 30.98 o -3 1 2 2255.76 1976.37 24.07 o -2 1 2 531.23 556.02 10.20 o -1 1 2 10.33 -6.20 4.14 o 0 1 2 180.83 181.63 6.26 o 1 1 2 3283.86 3086.73 30.46 o 2 1 2 381.87 358.10 10.44 o 3 1 2 1721.15 1651.58 28.56 o 4 1 2 2670.48 2664.14 42.15 o 5 1 2 1492.07 1515.02 32.06 o 6 1 2 2498.52 2668.69 48.54 o 7 1 2 10.58 4.55 15.72 o 8 1 2 764.39 751.43 27.77 o 9 1 2 20.49 -0.62 24.52 o 10 1 2 155.14 155.46 30.63 o 11 1 2 5.57 -53.51 60.53 o -11 2 2 123.16 66.17 49.33 o -10 2 2 242.95 243.20 36.26 o -9 2 2 126.82 133.67 26.40 o -8 2 2 49.37 28.11 17.45 o -7 2 2 829.21 838.58 25.26 o -6 2 2 30.65 33.87 11.26 o -5 2 2 17.51 16.06 8.12 o -4 2 2 1338.44 1238.10 21.05 o -3 2 2 563.31 531.28 11.84 o -2 2 2 22289.18 22281.72 189.14 o -1 2 2 3374.44 3181.18 38.54 o 0 2 2 2078.69 1991.70 27.56 o 1 2 2 3.17 8.55 7.50 o 2 2 2 3363.42 3267.61 46.18 o 3 2 2 5959.67 5992.91 79.12 o 4 2 2 1512.75 1457.31 32.00 o 5 2 2 610.60 655.85 23.11 o 6 2 2 61.75 63.28 14.96 o 7 2 2 2944.69 3082.36 62.29 o 8 2 2 596.05 559.30 38.56 o 9 2 2 311.95 269.16 33.47 o 10 2 2 128.68 113.02 34.14 o 11 2 2 69.35 3.06 57.50 o -11 3 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