#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/72/2017296.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017296_Fobs loop_ _publ_author_name 'Lipstman, Sophia' 'Goldberg, Israel' _publ_section_title ; Unsolvated 5,10,15,20-tetra-4-pyridylporphyrin, its sesquihydrate and its 2-chlorophenol disolvate: conformational versatility of the ligand ; _journal_coeditor_code GD3300 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o447 _journal_page_last o452 _journal_volume 65 _journal_year 2009 _space_group_IT_number 122 _symmetry_space_group_name_Hall 'I -4 2bw' _symmetry_space_group_name_H-M 'I -4 2 d' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 15.2155 _cell_length_b 15.2155 _cell_length_c 13.5388 _exptl_crystal_F_000 1352.00 _reflns_d_resolution_high 0.7608 _[local]_cod_data_source_file gd3300IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' Compound so126 (symmetry I-42d)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 344.73 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'x, -y+1/2, -z+1/4' '-x, y+1/2, -z+1/4' 'y, x+1/2, z+1/4' '-y, -x+1/2, z+1/4' '-y, x, -z' 'y, -x, -z' 'x+1/2, y+1/2, z+1/2' '-x+1/2, -y+1/2, z+1/2' 'x+1/2, -y+1, -z+3/4' '-x+1/2, y+1, -z+3/4' 'y+1/2, x+1, z+3/4' '-y+1/2, -x+1, z+3/4' '-y+1/2, x+1/2, -z+1/2' 'y+1/2, -x+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 2 0 809.85 671.89 25.86 o 2 2 0 9343.88 9240.60 165.45 o 1 3 0 1750.55 1703.80 28.51 o 0 4 0 38071.12 34126.88 572.32 o 2 4 0 1687.73 1649.14 43.28 o 4 4 0 2397.84 2242.00 52.17 o 1 5 0 0.93 -6.63 6.96 o 3 5 0 4736.35 4498.22 66.10 o 0 6 0 11420.36 11077.63 202.90 o 2 6 0 1456.99 1485.28 50.79 o 4 6 0 41.66 36.62 8.33 o 6 6 0 181.88 146.82 14.60 o 1 7 0 14639.19 14766.19 186.35 o 3 7 0 8080.15 8490.46 116.64 o 5 7 0 244.60 290.65 12.36 o 0 8 0 419.83 381.63 20.86 o 2 8 0 1191.78 1190.22 23.83 o 4 8 0 73.35 65.47 9.12 o 6 8 0 56.07 53.83 10.56 o 8 8 0 62.10 77.65 16.97 o 1 9 0 72.81 79.18 10.30 o 3 9 0 77.45 96.77 9.82 o 5 9 0 515.36 503.99 16.52 o 7 9 0 1052.73 1145.73 29.35 o 0 10 0 718.92 709.90 26.60 o 2 10 0 161.95 167.92 13.70 o 4 10 0 1699.62 1784.00 35.67 o 6 10 0 114.47 117.59 11.44 o 8 10 0 1309.63 1355.00 34.48 o 10 10 0 1404.54 1384.72 53.80 o 1 11 0 134.03 136.77 12.33 o 3 11 0 948.19 937.79 23.54 o 5 11 0 257.78 228.58 14.38 o 7 11 0 63.54 58.59 12.10 o 9 11 0 524.67 550.42 22.70 o 0 12 0 1155.01 1155.54 42.13 o 2 12 0 327.76 366.71 16.31 o 4 12 0 1636.43 1620.93 35.91 o 6 12 0 9.57 10.91 9.54 o 8 12 0 1773.66 1820.60 49.12 o 10 12 0 359.67 306.97 20.17 o 12 12 0 722.30 836.13 46.78 o 1 13 0 1243.77 1368.18 33.28 o 3 13 0 316.64 300.62 15.54 o 5 13 0 22.15 33.94 12.19 o 7 13 0 34.76 42.30 9.45 o 9 13 0 32.77 24.74 11.85 o 11 13 0 85.84 82.97 19.67 o 0 14 0 390.16 402.78 29.00 o 2 14 0 76.95 80.93 12.50 o 4 14 0 125.89 96.61 18.93 o 6 14 0 412.13 379.15 43.74 o 8 14 0 0.08 24.65 23.55 o 10 14 0 7.74 12.68 41.90 o 12 14 0 117.77 359.28 149.04 o 14 14 0 12.38 92.90 102.86 o 1 15 0 51.07 33.77 14.22 o 3 15 0 441.90 441.16 26.83 o 5 15 0 0.19 9.73 21.56 o 7 15 0 26.94 32.71 24.30 o 9 15 0 427.97 497.87 164.24 o 11 15 0 12.98 58.82 62.74 o 13 15 0 61.25 87.19 70.39 o 0 16 0 458.98 467.33 31.25 o 2 16 0 67.91 33.57 24.20 o 4 16 0 3.33 37.34 27.11 o 6 16 0 178.51 192.55 64.12 o 8 16 0 37.89 60.64 31.88 o 10 16 0 6.94 8.88 44.45 o 12 16 0 41.18 -11.42 82.59 o 1 17 0 16.51 11.07 16.13 o 3 17 0 0.23 21.95 25.23 o 5 17 0 60.69 53.32 29.45 o 7 17 0 5.33 26.30 32.82 o 9 17 0 46.34 87.93 85.02 o 0 18 0 8.42 26.31 32.50 o 2 18 0 35.33 12.69 50.63 o 4 18 0 38.14 20.12 79.85 o 6 18 0 52.68 72.44 107.77 o 8 18 0 0.03 67.11 55.31 o 1 19 0 21.86 80.23 69.81 o 3 19 0 44.60 96.09 47.40 o 5 19 0 2.29 -24.41 84.92 o 1 2 1 4596.68 4213.85 42.45 o 0 3 1 4950.32 4635.08 62.98 o 2 3 1 29037.71 26791.42 233.86 o 1 4 1 9815.13 8827.51 84.55 o 3 4 1 168.76 137.31 5.83 o 0 5 1 3210.76 2920.44 44.66 o 2 5 1 1701.09 1572.12 21.77 o 4 5 1 5636.61 5902.44 58.60 o 1 6 1 3440.32 3301.67 35.02 o 3 6 1 3114.49 3366.47 37.86 o 5 6 1 1060.09 1021.17 16.72 o 0 7 1 6806.32 6955.57 93.39 o 2 7 1 1380.31 1630.46 20.40 o 4 7 1 259.31 291.70 8.11 o 6 7 1 1366.96 1515.36 21.06 o 1 8 1 1202.53 1186.27 16.58 o 3 8 1 287.28 270.36 8.63 o 5 8 1 980.15 1015.21 16.98 o 7 8 1 1547.19 1667.99 26.06 o 0 9 1 29.67 48.98 13.83 o 2 9 1 1239.86 1276.79 18.32 o 4 9 1 688.69 597.76 26.19 o 6 9 1 332.60 317.40 10.93 o 8 9 1 922.15 939.13 22.70 o 1 10 1 16.66 13.20 6.92 o 3 10 1 1059.40 1113.62 21.09 o 5 10 1 436.78 460.63 14.25 o 7 10 1 35.43 25.01 7.51 o 9 10 1 352.31 318.49 12.40 o 0 11 1 175.91 185.41 13.35 o 2 11 1 3.75 21.71 7.42 o 4 11 1 458.04 447.39 16.74 o 6 11 1 115.18 86.58 10.93 o 8 11 1 78.77 61.58 7.86 o 10 11 1 7.02 19.22 9.19 o 1 12 1 405.20 411.65 12.05 o 3 12 1 4089.83 4248.25 52.05 o 5 12 1 82.25 76.05 12.72 o 7 12 1 333.17 292.06 35.86 o 9 12 1 355.14 340.51 18.30 o 11 12 1 2.88 0.00 10.03 o 0 13 1 2.17 17.39 11.59 o 2 13 1 17.03 14.20 7.40 o 4 13 1 1299.78 1298.59 27.15 o 6 13 1 404.49 385.12 17.76 o 8 13 1 58.30 48.51 11.51 o 10 13 1 25.53 39.53 13.12 o 12 13 1 48.58 41.44 23.70 o 1 14 1 17.82 20.72 8.90 o 3 14 1 187.36 149.01 13.00 o 5 14 1 167.50 111.45 16.12 o 7 14 1 343.41 276.72 15.86 o 9 14 1 75.15 70.52 13.24 o 11 14 1 87.81 68.55 28.67 o 13 14 1 1.65 43.16 49.42 o 0 15 1 94.03 77.15 13.73 o 2 15 1 157.96 128.55 9.47 o 4 15 1 171.84 158.86 13.22 o 6 15 1 25.07 21.28 13.52 o 8 15 1 62.47 60.55 14.72 o 10 15 1 71.58 144.43 23.72 o 12 15 1 39.57 64.24 48.12 o 1 16 1 161.41 162.64 12.43 o 3 16 1 56.27 40.78 12.46 o 5 16 1 19.08 5.49 22.52 o 7 16 1 39.65 60.00 23.13 o 9 16 1 46.33 0.50 25.69 o 11 16 1 38.96 106.29 47.39 o 0 17 1 6.45 31.71 16.58 o 2 17 1 8.90 21.85 13.00 o 4 17 1 8.99 59.31 20.56 o 6 17 1 56.98 81.26 26.50 o 8 17 1 91.67 144.96 31.45 o 10 17 1 14.01 79.04 55.31 o 1 18 1 18.87 58.48 21.33 o 3 18 1 56.96 75.64 26.68 o 5 18 1 11.19 32.14 27.32 o 7 18 1 35.89 81.82 34.87 o 0 19 1 155.94 253.38 76.45 o 2 19 1 18.70 41.64 36.73 o 4 19 1 53.65 95.47 37.42 o 6 19 1 79.65 133.99 48.68 o 1 1 2 3954.95 3604.01 51.86 o 1 3 2 14102.01 12613.42 117.15 o 3 3 2 6578.87 6126.47 82.87 o 0 4 2 11513.65 10360.12 157.49 o 2 4 2 5262.96 4920.92 55.26 o 1 5 2 1052.10 1014.28 17.46 o 3 5 2 3683.75 3557.54 42.57 o 5 5 2 11853.60 12455.45 164.32 o 0 6 2 4094.79 4458.09 65.69 o 2 6 2 4047.51 4072.52 46.47 o 4 6 2 841.42 918.77 16.52 o 1 7 2 1059.44 1334.78 21.64 o 3 7 2 566.47 610.74 13.73 o 5 7 2 431.69 427.38 9.33 o 7 7 2 3706.38 4051.16 63.94 o 0 8 2 4063.36 4159.31 61.23 o 2 8 2 2633.19 2752.19 35.90 o 4 8 2 2269.73 2370.93 32.89 o 6 8 2 368.35 377.37 9.69 o 1 9 2 299.67 325.66 9.56 o 3 9 2 102.28 113.85 9.37 o 5 9 2 68.83 67.77 9.61 o 7 9 2 32.05 20.75 6.08 o 9 9 2 3249.55 3366.81 65.27 o 0 10 2 110.21 96.90 11.12 o 2 10 2 5416.81 5959.72 70.23 o 4 10 2 137.48 128.62 11.00 o 6 10 2 734.25 803.85 19.44 o 8 10 2 159.62 175.65 8.65 o 1 11 2 90.05 97.98 8.26 o 3 11 2 909.98 886.74 19.58 o 5 11 2 536.79 558.50 17.50 o 7 11 2 132.30 124.98 12.13 o 9 11 2 389.47 359.45 22.29 o 11 11 2 11.95 10.27 14.38 o 0 12 2 560.02 541.04 39.25 o 2 12 2 1662.52 1818.43 33.47 o 4 12 2 1443.16 1431.60 29.36 o 6 12 2 502.99 534.06 18.42 o 8 12 2 94.65 63.56 13.60 o 10 12 2 70.97 105.23 19.86 o 1 13 2 25.97 17.84 7.46 o 3 13 2 77.02 63.68 11.49 o 5 13 2 1241.56 1153.40 49.64 o 7 13 2 119.92 112.51 13.04 o 9 13 2 119.36 109.82 25.54 o 11 13 2 5.42 10.40 19.45 o 13 13 2 11.34 -5.07 72.69 o 0 14 2 21.94 33.75 12.18 o 2 14 2 1846.75 1802.43 45.86 o 4 14 2 248.88 246.63 14.48 o 6 14 2 101.56 86.51 17.41 o 8 14 2 31.00 28.77 13.52 o 10 14 2 45.79 59.41 24.86 o 12 14 2 20.38 5.72 32.49 o 1 15 2 215.61 209.27 11.86 o 3 15 2 14.68 24.04 11.49 o 5 15 2 57.97 67.88 21.65 o 7 15 2 121.12 117.83 16.68 o 9 15 2 70.04 64.32 30.62 o 11 15 2 75.09 101.43 38.06 o 13 15 2 23.63 251.42 179.35 o 0 16 2 62.65 46.45 12.85 o 2 16 2 114.62 109.62 13.58 o 4 16 2 24.63 35.53 12.59 o 6 16 2 10.62 31.12 17.05 o 8 16 2 27.07 40.49 35.04 o 10 16 2 8.52 30.79 37.51 o 1 17 2 5.12 23.43 12.77 o 3 17 2 27.87 59.34 17.50 o 5 17 2 5.76 9.02 22.05 o 7 17 2 41.39 49.23 33.30 o 9 17 2 4.78 40.10 41.23 o 0 18 2 0.01 58.95 36.84 o 2 18 2 1.82 16.38 20.07 o 4 18 2 53.54 112.05 35.72 o 6 18 2 4.39 44.98 61.61 o 8 18 2 83.88 122.72 46.19 o 1 19 2 137.18 187.63 42.74 o 3 19 2 51.10 60.42 40.43 o 5 19 2 33.26 54.09 40.17 o 0 1 3 91482.16 88901.13 1019.65 o 1 2 3 10272.40 9428.87 88.06 o 0 3 3 5089.86 5087.85 73.78 o 2 3 3 199.79 212.94 7.41 o 1 4 3 948.26 891.44 14.27 o 3 4 3 530.42 538.55 10.18 o 0 5 3 861.58 773.24 18.65 o 2 5 3 2873.87 2558.49 30.05 o 4 5 3 2465.71 2420.27 27.47 o 1 6 3 743.48 726.34 12.94 o 3 6 3 2776.76 2963.73 36.34 o 5 6 3 73.74 80.69 6.43 o 0 7 3 3448.63 3411.13 56.88 o 2 7 3 6568.17 6903.97 72.39 o 4 7 3 66.34 78.32 9.09 o 6 7 3 101.61 106.10 7.80 o 1 8 3 2148.35 2148.05 25.88 o 3 8 3 468.65 416.59 13.20 o 5 8 3 736.18 746.76 19.71 o 7 8 3 1523.53 1577.09 24.84 o 0 9 3 0.14 4.55 10.88 o 2 9 3 67.59 59.26 9.29 o 4 9 3 1316.94 1402.31 24.90 o 6 9 3 100.82 99.00 10.55 o 8 9 3 143.49 151.68 9.48 o 1 10 3 259.86 266.98 9.04 o 3 10 3 1113.69 1162.01 22.92 o 5 10 3 577.26 600.20 17.14 o 7 10 3 430.09 380.53 17.49 o 9 10 3 1362.96 1312.32 28.53 o 0 11 3 466.24 423.18 20.57 o 2 11 3 555.71 553.68 17.17 o 4 11 3 352.38 295.79 14.10 o 6 11 3 549.26 541.36 29.16 o 8 11 3 325.03 341.60 50.82 o 10 11 3 152.80 175.80 14.10 o 1 12 3 1942.70 2088.73 29.93 o 3 12 3 1244.22 1178.06 31.58 o 5 12 3 99.53 90.14 12.99 o 7 12 3 113.03 86.44 14.80 o 9 12 3 459.55 376.57 19.03 o 11 12 3 30.67 11.31 11.68 o 0 13 3 7.02 -6.90 12.99 o 2 13 3 55.06 39.22 11.81 o 4 13 3 1072.18 961.40 38.01 o 6 13 3 144.22 155.86 13.67 o 8 13 3 69.49 62.21 15.49 o 10 13 3 160.72 123.96 22.41 o 12 13 3 48.13 86.02 26.07 o 1 14 3 733.23 776.01 29.66 o 3 14 3 291.64 330.20 16.11 o 5 14 3 30.47 11.21 15.93 o 7 14 3 92.27 85.52 16.70 o 9 14 3 177.08 116.12 26.16 o 11 14 3 23.64 31.03 23.69 o 13 14 3 32.26 48.34 162.70 o 0 15 3 5.71 17.32 16.15 o 2 15 3 60.81 45.14 12.06 o 4 15 3 164.41 162.07 15.33 o 6 15 3 99.78 99.92 17.93 o 8 15 3 105.59 109.45 27.41 o 10 15 3 29.17 11.87 30.06 o 12 15 3 22.82 68.28 50.32 o 1 16 3 259.86 238.85 21.07 o 3 16 3 154.88 152.97 15.72 o 5 16 3 45.91 30.42 15.78 o 7 16 3 45.42 44.39 19.66 o 9 16 3 86.64 23.25 29.82 o 11 16 3 17.14 -54.32 57.25 o 0 17 3 32.70 126.60 34.17 o 2 17 3 21.55 16.53 16.60 o 4 17 3 104.56 109.59 30.53 o 6 17 3 100.25 126.10 26.09 o 8 17 3 99.60 105.39 31.17 o 1 18 3 12.64 8.84 33.96 o 3 18 3 43.54 61.56 29.39 o 5 18 3 13.33 43.38 29.07 o 7 18 3 46.61 113.77 33.61 o 0 19 3 0.64 -15.90 72.61 o 2 19 3 12.71 31.87 43.86 o 4 19 3 8.81 9.22 40.66 o 0 0 4 118836.76 122374.51 5158.48 o 0 2 4 166.34 189.17 22.11 o 2 2 4 6882.97 6480.45 91.84 o 1 3 4 5749.61 5619.44 59.45 o 0 4 4 85.95 81.67 9.89 o 2 4 4 354.68 310.59 9.06 o 4 4 4 2325.14 2539.27 40.38 o 1 5 4 2155.21 2051.48 26.60 o 3 5 4 638.74 683.27 12.46 o 0 6 4 3714.95 3790.72 59.13 o 2 6 4 2240.37 2225.38 27.66 o 4 6 4 442.19 468.01 12.22 o 6 6 4 959.90 1010.34 24.73 o 1 7 4 516.48 585.43 12.63 o 3 7 4 2140.39 2248.56 33.56 o 5 7 4 393.81 448.78 14.05 o 0 8 4 3009.73 3261.37 52.85 o 2 8 4 493.84 536.29 16.26 o 4 8 4 193.63 208.31 11.27 o 6 8 4 270.36 266.17 13.99 o 8 8 4 569.53 537.57 19.08 o 1 9 4 8.43 19.26 10.86 o 3 9 4 513.95 502.73 15.29 o 5 9 4 822.06 821.41 20.04 o 7 9 4 929.33 970.93 21.98 o 0 10 4 5.04 12.74 14.07 o 2 10 4 680.70 685.71 20.72 o 4 10 4 1082.06 1170.15 24.74 o 6 10 4 523.20 554.37 18.66 o 8 10 4 508.03 515.87 21.05 o 10 10 4 1244.77 1340.37 31.29 o 1 11 4 160.96 176.91 9.13 o 3 11 4 829.80 805.55 20.32 o 5 11 4 286.24 280.86 25.48 o 7 11 4 232.68 219.18 14.81 o 9 11 4 152.16 121.13 13.39 o 0 12 4 1089.65 1042.93 29.15 o 2 12 4 369.23 376.48 17.97 o 4 12 4 434.47 396.42 21.58 o 6 12 4 7.95 10.20 12.61 o 8 12 4 777.67 778.66 28.59 o 10 12 4 45.82 36.64 14.08 o 12 12 4 10.36 49.97 29.74 o 1 13 4 180.59 165.45 13.44 o 3 13 4 2463.81 2652.20 53.50 o 5 13 4 25.12 26.18 15.32 o 7 13 4 501.96 459.34 28.02 o 9 13 4 71.43 61.34 14.93 o 11 13 4 133.89 99.27 23.87 o 0 14 4 16.52 8.86 14.35 o 2 14 4 10.08 10.96 17.45 o 4 14 4 467.41 356.51 20.27 o 6 14 4 261.50 290.60 25.64 o 8 14 4 52.96 71.97 15.66 o 10 14 4 25.74 40.43 23.80 o 12 14 4 17.89 51.55 42.11 o 1 15 4 85.17 83.39 11.88 o 3 15 4 263.94 279.77 26.55 o 5 15 4 107.03 91.57 15.61 o 7 15 4 16.49 1.37 18.70 o 9 15 4 5.38 27.72 21.56 o 11 15 4 10.34 42.57 54.56 o 0 16 4 9.28 4.94 26.76 o 2 16 4 96.09 89.99 15.54 o 4 16 4 79.77 115.29 18.51 o 6 16 4 64.87 83.74 19.86 o 8 16 4 15.28 -19.48 25.40 o 10 16 4 3.23 22.53 38.74 o 1 17 4 91.98 72.31 18.19 o 3 17 4 57.07 65.56 19.20 o 5 17 4 48.84 95.68 22.84 o 7 17 4 7.28 35.16 26.83 o 9 17 4 104.97 216.21 47.51 o 0 18 4 35.51 37.46 39.31 o 2 18 4 1.72 16.12 25.78 o 4 18 4 4.33 26.85 34.11 o 6 18 4 27.84 23.66 36.97 o 1 19 4 13.10 87.07 60.80 o 3 19 4 8.95 27.06 39.13 o 0 1 5 20305.57 19617.05 342.46 o 1 2 5 157.69 171.52 8.61 o 0 3 5 8843.10 8854.05 147.43 o 2 3 5 603.62 647.23 13.00 o 1 4 5 3499.89 3466.09 45.48 o 3 4 5 484.36 572.97 13.64 o 0 5 5 0.95 -17.55 11.70 o 2 5 5 1229.84 1194.10 18.06 o 4 5 5 1390.81 1474.30 21.18 o 1 6 5 1661.84 1654.35 23.85 o 3 6 5 381.69 384.20 13.97 o 5 6 5 1524.38 1633.74 25.02 o 0 7 5 136.80 129.24 13.08 o 2 7 5 1065.97 1093.77 17.77 o 4 7 5 1309.12 1440.97 26.50 o 6 7 5 649.82 687.12 15.39 o 1 8 5 1456.88 1647.96 27.45 o 3 8 5 271.45 248.97 13.69 o 5 8 5 373.13 370.35 15.71 o 7 8 5 17.99 13.86 7.94 o 0 9 5 416.13 392.97 48.27 o 2 9 5 114.05 148.63 17.71 o 4 9 5 424.53 389.15 15.29 o 6 9 5 161.12 163.50 17.79 o 8 9 5 1543.56 1620.56 32.33 o 1 10 5 1468.43 1496.63 36.80 o 3 10 5 158.47 146.07 12.94 o 5 10 5 142.05 133.68 13.58 o 7 10 5 276.88 313.02 15.46 o 9 10 5 953.10 1071.48 37.81 o 0 11 5 88.98 65.29 12.04 o 2 11 5 2032.24 2251.93 39.74 o 4 11 5 9.88 8.61 11.74 o 6 11 5 444.80 386.12 18.07 o 8 11 5 502.64 480.17 18.49 o 10 11 5 82.48 78.79 10.81 o 1 12 5 618.62 633.48 19.42 o 3 12 5 753.43 740.36 24.32 o 5 12 5 684.57 713.35 23.73 o 7 12 5 174.30 160.40 19.48 o 9 12 5 274.61 277.95 17.41 o 11 12 5 98.61 94.37 22.63 o 0 13 5 0.47 -7.62 9.98 o 2 13 5 289.95 265.15 29.92 o 4 13 5 653.11 669.44 30.36 o 6 13 5 227.19 230.23 17.69 o 8 13 5 317.41 289.38 19.87 o 10 13 5 47.83 56.29 19.03 o 12 13 5 28.34 33.62 32.62 o 1 14 5 579.30 526.96 19.40 o 3 14 5 689.64 654.35 24.82 o 5 14 5 56.19 31.43 15.62 o 7 14 5 186.23 190.79 19.20 o 9 14 5 6.03 -0.01 19.33 o 11 14 5 25.96 103.25 34.74 o 13 14 5 4.01 30.96 62.60 o 0 15 5 10.63 -2.84 28.47 o 2 15 5 79.96 74.72 13.43 o 4 15 5 34.74 55.63 15.98 o 6 15 5 36.56 37.84 17.44 o 8 15 5 28.50 40.39 73.73 o 10 15 5 2.48 25.18 37.46 o 1 16 5 85.17 91.77 12.87 o 3 16 5 6.08 49.57 21.30 o 5 16 5 16.82 0.08 18.09 o 7 16 5 2.60 13.59 23.20 o 9 16 5 5.83 47.02 37.78 o 0 17 5 1.27 -10.15 32.78 o 2 17 5 63.27 68.78 20.58 o 4 17 5 87.32 80.54 49.41 o 6 17 5 59.56 72.85 27.21 o 8 17 5 18.26 139.63 246.23 o 1 18 5 56.38 59.46 33.04 o 3 18 5 16.34 66.75 31.01 o 5 18 5 24.28 119.92 48.81 o 0 19 5 127.87 137.89 76.84 o 2 19 5 33.65 -34.43 55.88 o 1 1 6 930.40 994.14 23.76 o 0 2 6 13569.05 13739.35 183.87 o 1 3 6 740.32 741.44 14.51 o 3 3 6 1193.27 1273.31 91.75 o 0 4 6 2934.14 2964.48 54.36 o 2 4 6 181.93 181.81 9.96 o 1 5 6 1680.82 1840.85 27.79 o 3 5 6 775.38 795.25 16.01 o 5 5 6 759.60 692.69 32.84 o 0 6 6 0.94 8.09 17.83 o 2 6 6 911.19 986.60 17.30 o 4 6 6 2046.06 2163.76 29.34 o 1 7 6 0.92 17.63 25.08 o 3 7 6 10.60 20.76 7.93 o 5 7 6 248.32 293.00 10.74 o 7 7 6 1850.84 1821.98 39.74 o 0 8 6 189.52 182.62 14.14 o 2 8 6 354.36 395.03 11.56 o 4 8 6 968.23 953.51 31.48 o 6 8 6 561.24 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