#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/73/2017303.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017303_Fobs loop_ _publ_author_name 'Blanco, Maria C.' 'Palma, Alirio' 'Bahsas, Ali' 'Cobo, Justo' 'Glidewell, Christopher' _publ_section_title ; Different hydrogen-bonded structures in three 2-thienyl-substituted tetrahydro-1,4-epoxy-1-benzazepines ; _journal_coeditor_code GG3212 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o487 _journal_page_last o491 _journal_volume 65 _journal_year 2009 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.7959 _cell_length_b 14.2116 _cell_length_c 17.4303 _exptl_crystal_F_000 1424.00 _reflns_d_resolution_high 0.7694 _[local]_cod_data_source_file gg3212Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CAB52b' _shelx_refln_list_code 4 _shelx_f_calc_maximum 338.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6003.95 5496.65 112.55 o 4 0 0 15989.00 15089.18 270.81 o 6 0 0 9.99 94.60 127.19 o 8 0 0 8062.69 7865.75 311.62 o 10 0 0 2658.39 2599.07 520.97 o 12 0 0 3517.55 2710.51 418.44 o 14 0 0 320.43 1132.50 1012.64 o 2 1 0 95600.41 95049.65 884.69 o 4 1 0 8246.79 7731.77 176.91 o 6 1 0 3564.90 3795.21 126.38 o 8 1 0 4041.80 3977.59 199.04 o 10 1 0 2341.35 2407.51 206.78 o 12 1 0 242.16 -182.09 368.35 o 14 1 0 280.48 44.77 446.73 o 2 2 0 30961.51 31737.82 271.27 o 4 2 0 28155.06 27978.16 414.36 o 6 2 0 17734.40 17096.61 339.03 o 8 2 0 22933.53 23407.54 383.54 o 10 2 0 545.92 453.55 215.48 o 12 2 0 13775.68 14369.16 748.84 o 2 3 0 71028.22 71156.88 517.97 o 4 3 0 18581.88 18500.98 223.01 o 6 3 0 11975.29 11251.92 223.27 o 8 3 0 5536.44 5982.82 219.13 o 10 3 0 41678.91 43120.61 610.23 o 12 3 0 88.16 29.85 380.49 o 0 4 0 13107.71 12943.46 237.15 o 2 4 0 1583.70 1868.33 91.79 o 4 4 0 413.62 335.98 97.00 o 6 4 0 13937.88 13724.48 259.05 o 8 4 0 352.70 -124.95 149.19 o 10 4 0 261.51 137.38 157.37 o 12 4 0 205.39 103.97 333.34 o 2 5 0 63252.44 65143.71 533.15 o 4 5 0 10367.76 11155.77 208.59 o 6 5 0 17974.11 18683.31 297.72 o 8 5 0 1873.38 1960.06 165.07 o 10 5 0 8300.93 7831.90 302.17 o 12 5 0 2860.94 3042.33 458.33 o 0 6 0 46738.36 45453.89 578.31 o 2 6 0 25983.73 27825.97 315.39 o 4 6 0 7000.87 6284.85 178.68 o 6 6 0 4.98 212.79 113.97 o 8 6 0 7140.25 6854.10 251.32 o 10 6 0 3217.65 3705.15 375.18 o 12 6 0 1665.00 1186.83 304.62 o 2 7 0 3577.11 4149.52 147.89 o 4 7 0 2909.82 3107.49 193.85 o 6 7 0 3414.25 3839.19 176.99 o 8 7 0 366.16 203.03 170.71 o 10 7 0 358.46 179.80 211.52 o 12 7 0 187.58 158.27 301.43 o 0 8 0 71389.65 73474.26 880.53 o 2 8 0 2398.66 2688.56 149.24 o 4 8 0 8648.90 9017.85 212.81 o 6 8 0 3784.39 3784.13 182.86 o 8 8 0 17530.46 18681.64 409.83 o 10 8 0 917.22 481.22 217.25 o 12 8 0 1723.72 1754.89 392.41 o 2 9 0 3008.73 3081.36 191.26 o 4 9 0 156.21 408.61 141.39 o 6 9 0 13813.00 14325.60 300.14 o 8 9 0 6552.74 6025.05 230.00 o 10 9 0 2223.77 2250.59 323.56 o 12 9 0 877.67 258.13 388.28 o 0 10 0 406.45 239.25 182.22 o 2 10 0 5198.58 5227.31 246.02 o 4 10 0 13200.60 13209.49 293.09 o 6 10 0 561.48 498.03 206.54 o 8 10 0 129.16 -252.09 168.06 o 10 10 0 4.65 -310.63 372.81 o 2 11 0 19212.17 19628.23 350.34 o 4 11 0 1018.85 1059.11 183.00 o 6 11 0 5338.53 5250.63 231.98 o 8 11 0 22.12 95.32 194.16 o 10 11 0 4826.38 5119.52 500.94 o 0 12 0 1364.90 1495.13 241.33 o 2 12 0 9857.19 9906.28 271.82 o 4 12 0 7573.81 7247.15 261.46 o 6 12 0 1125.61 1302.21 227.87 o 8 12 0 30.60 -191.23 554.72 o 10 12 0 1.52 150.23 371.10 o 2 13 0 389.69 557.16 179.13 o 4 13 0 16.73 -207.53 203.11 o 6 13 0 9838.54 9555.02 381.83 o 8 13 0 1857.65 2258.08 387.79 o 0 14 0 17281.43 17234.93 556.28 o 2 14 0 1417.01 1633.08 300.58 o 4 14 0 1230.47 977.79 272.07 o 6 14 0 3.18 -92.42 296.16 o 8 14 0 7404.65 7370.93 629.76 o 2 15 0 11.59 120.06 301.38 o 4 15 0 531.67 719.54 337.01 o 6 15 0 327.77 382.21 316.59 o 8 15 0 402.94 433.40 445.25 o 0 16 0 2391.15 1457.93 455.36 o 2 16 0 74.36 -397.10 345.17 o 4 16 0 6959.40 6421.28 629.30 o 6 16 0 1628.73 1312.10 485.16 o 2 17 0 4849.58 5308.64 528.77 o 4 17 0 1129.57 365.75 530.71 o 0 18 0 201.91 325.62 676.64 o 2 18 0 0.17 -825.59 628.03 o 2 1 1 594.65 459.18 41.27 o 3 1 1 14234.67 13858.03 158.77 o 4 1 1 167.31 84.68 60.19 o 5 1 1 13044.38 12740.26 168.32 o 6 1 1 649.98 615.86 69.65 o 7 1 1 11329.48 10940.16 168.99 o 8 1 1 59.90 197.01 84.26 o 9 1 1 1801.15 1989.93 110.23 o 10 1 1 33.35 5.36 119.05 o 11 1 1 3850.10 3930.98 174.16 o 12 1 1 30.62 35.85 199.21 o 13 1 1 245.29 190.65 236.40 o 0 2 1 42.87 138.43 42.22 o 1 2 1 6181.82 5784.41 63.79 o 2 2 1 2013.26 1993.77 48.32 o 3 2 1 1343.78 1391.93 58.79 o 4 2 1 7384.89 7118.59 109.18 o 5 2 1 8325.02 7879.76 124.35 o 6 2 1 1.46 -61.86 69.65 o 7 2 1 9487.04 9495.04 168.70 o 8 2 1 704.75 834.99 98.22 o 9 2 1 8846.56 9141.24 182.05 o 10 2 1 23.82 263.83 113.89 o 11 2 1 297.61 553.11 138.80 o 12 2 1 176.48 206.38 231.47 o 13 2 1 1677.14 1529.69 343.03 o 1 3 1 2356.45 2348.11 52.95 o 2 3 1 6380.33 6496.40 87.05 o 3 3 1 4037.32 3888.62 70.16 o 4 3 1 3379.90 3277.44 80.70 o 5 3 1 253.24 182.56 59.52 o 6 3 1 191.45 210.36 86.66 o 7 3 1 47.73 92.63 86.84 o 8 3 1 802.52 604.29 115.71 o 9 3 1 27.04 115.63 96.84 o 10 3 1 445.83 385.75 115.13 o 11 3 1 46.80 244.29 169.15 o 12 3 1 0.81 -4.51 235.77 o 13 3 1 192.18 223.85 283.32 o 0 4 1 688.50 924.25 83.12 o 1 4 1 8129.37 7969.50 98.01 o 2 4 1 3525.82 3528.69 80.38 o 3 4 1 31361.40 30911.87 235.57 o 4 4 1 1068.41 1213.78 76.16 o 5 4 1 24249.33 23940.23 223.21 o 6 4 1 6160.87 6372.43 122.04 o 7 4 1 2359.44 2552.12 108.78 o 8 4 1 107.29 121.90 101.55 o 9 4 1 1432.22 1555.96 122.74 o 10 4 1 1711.58 1621.66 130.41 o 11 4 1 449.35 505.52 143.77 o 12 4 1 110.64 122.36 243.68 o 13 4 1 3485.19 3102.50 512.94 o 1 5 1 16560.23 16908.01 151.10 o 2 5 1 509.58 495.84 62.10 o 3 5 1 6970.04 6880.95 109.09 o 4 5 1 282.08 447.45 64.71 o 5 5 1 6532.08 6618.75 120.64 o 6 5 1 1726.87 1678.73 100.26 o 7 5 1 329.21 438.22 90.51 o 8 5 1 62.18 -91.65 106.95 o 9 5 1 960.60 884.01 123.03 o 10 5 1 19.48 152.07 127.25 o 11 5 1 3769.82 3835.15 174.76 o 12 5 1 45.47 192.52 270.28 o 13 5 1 301.27 1362.20 422.75 o 0 6 1 9399.17 9502.93 173.22 o 1 6 1 12509.45 12869.55 141.07 o 2 6 1 3040.77 3418.24 89.65 o 3 6 1 5016.21 5410.17 113.87 o 4 6 1 6356.46 6452.99 115.26 o 5 6 1 2638.81 2664.18 99.92 o 6 6 1 1599.72 1749.35 99.34 o 7 6 1 2068.32 2168.20 116.30 o 8 6 1 820.55 1272.88 128.48 o 9 6 1 3615.36 3624.49 162.35 o 10 6 1 132.34 200.23 143.50 o 11 6 1 274.36 182.67 166.29 o 12 6 1 324.38 480.05 200.39 o 13 6 1 15.31 -37.29 307.72 o 1 7 1 5104.48 5003.99 103.09 o 2 7 1 157.41 7.17 71.09 o 3 7 1 20397.82 20740.18 207.99 o 4 7 1 8038.43 8242.95 133.93 o 5 7 1 4102.06 4215.01 122.75 o 6 7 1 1223.46 1204.53 102.83 o 7 7 1 15787.42 16205.49 217.96 o 8 7 1 1413.68 1229.09 140.05 o 9 7 1 1047.39 876.07 147.86 o 10 7 1 1131.45 820.84 152.89 o 11 7 1 2514.23 3040.88 225.24 o 12 7 1 15.61 33.20 200.58 o 0 8 1 1960.98 2038.06 132.26 o 1 8 1 7994.74 8596.09 136.71 o 2 8 1 27.86 47.73 77.87 o 3 8 1 1535.32 1457.60 101.38 o 4 8 1 1826.35 2183.17 103.00 o 5 8 1 1652.75 1538.90 102.46 o 6 8 1 3197.43 3408.40 125.70 o 7 8 1 1830.89 1836.97 114.17 o 8 8 1 156.06 328.99 134.78 o 9 8 1 3780.25 3793.62 208.08 o 10 8 1 560.64 476.33 191.08 o 11 8 1 806.59 509.18 225.28 o 12 8 1 349.74 62.60 240.07 o 1 9 1 10402.75 10377.88 158.12 o 2 9 1 1184.97 1248.12 103.90 o 3 9 1 6605.36 6563.75 151.90 o 4 9 1 627.87 878.74 119.27 o 5 9 1 2310.55 2186.55 113.27 o 6 9 1 1296.59 1309.56 136.57 o 7 9 1 56.67 75.17 112.12 o 8 9 1 770.13 169.36 130.54 o 9 9 1 159.24 272.61 143.95 o 10 9 1 356.29 460.77 182.49 o 11 9 1 1722.24 1822.80 273.51 o 12 9 1 27.96 -94.64 274.47 o 0 10 1 2945.02 2912.35 165.62 o 1 10 1 10676.35 10785.84 172.94 o 2 10 1 897.01 991.49 105.04 o 3 10 1 17577.75 18014.66 231.63 o 4 10 1 928.63 926.21 114.23 o 5 10 1 5621.25 5531.72 150.16 o 6 10 1 3475.98 3114.16 135.48 o 7 10 1 1095.54 1008.98 120.44 o 8 10 1 4.50 67.23 120.16 o 9 10 1 1059.76 849.19 162.17 o 10 10 1 41.55 287.43 204.41 o 11 10 1 30.17 104.04 260.86 o 1 11 1 3848.66 3733.09 132.07 o 2 11 1 454.56 743.94 119.15 o 3 11 1 552.74 517.07 130.65 o 4 11 1 65.77 126.92 111.78 o 5 11 1 205.28 43.09 129.89 o 6 11 1 0.00 -178.75 119.17 o 7 11 1 1036.72 1050.46 136.87 o 8 11 1 10.69 -175.21 151.78 o 9 11 1 39.82 256.81 206.57 o 10 11 1 1008.34 510.29 314.46 o 11 11 1 3.10 125.76 428.71 o 0 12 1 2037.10 2152.06 188.15 o 1 12 1 3206.82 3282.67 133.75 o 2 12 1 2111.53 2450.38 133.12 o 3 12 1 551.12 455.29 132.39 o 4 12 1 95.00 162.71 118.65 o 5 12 1 7411.53 7603.96 185.02 o 6 12 1 71.62 36.99 145.95 o 7 12 1 1252.37 1050.60 159.37 o 8 12 1 941.70 910.71 188.35 o 9 12 1 4498.99 4753.05 290.94 o 10 12 1 37.98 -25.81 267.34 o 1 13 1 1078.54 856.92 130.54 o 2 13 1 3224.61 2984.98 152.86 o 3 13 1 5030.86 5224.21 178.19 o 4 13 1 474.99 538.31 155.79 o 5 13 1 1451.65 1396.01 178.84 o 6 13 1 1827.56 1851.09 196.43 o 7 13 1 7455.33 7499.61 275.96 o 8 13 1 31.55 -29.90 244.56 o 9 13 1 1555.37 1500.16 284.23 o 0 14 1 393.95 13.89 198.05 o 1 14 1 1084.68 920.45 148.25 o 2 14 1 3.05 151.11 161.36 o 3 14 1 797.72 822.97 192.94 o 4 14 1 1322.67 1027.44 196.07 o 5 14 1 1451.58 1500.11 195.06 o 6 14 1 24.22 -153.51 197.13 o 7 14 1 147.53 374.71 218.24 o 8 14 1 551.38 615.20 301.64 o 9 14 1 10.45 204.58 351.49 o 1 15 1 7881.62 7658.28 292.46 o 2 15 1 171.93 282.81 207.24 o 3 15 1 2695.99 2427.41 250.65 o 4 15 1 446.37 27.71 237.85 o 5 15 1 4776.62 5132.03 267.76 o 6 15 1 2.49 378.01 229.53 o 7 15 1 605.57 263.82 370.69 o 8 15 1 661.89 510.18 383.89 o 0 16 1 695.79 530.34 298.68 o 1 16 1 4953.14 4829.80 295.08 o 2 16 1 1099.05 1013.44 353.91 o 3 16 1 1993.89 2208.26 329.51 o 4 16 1 693.71 323.68 328.85 o 5 16 1 43.86 -30.87 249.45 o 6 16 1 51.55 400.88 272.75 o 1 17 1 13.71 387.88 285.49 o 2 17 1 13.63 -280.11 288.01 o 3 17 1 982.97 1134.69 391.42 o 4 17 1 92.48 -330.27 366.61 o 5 17 1 105.01 22.16 355.95 o 0 18 1 66.05 357.57 543.54 o 1 18 1 304.96 537.74 390.57 o 2 18 1 1332.82 1047.24 379.61 o 3 18 1 1394.41 827.47 458.55 o 1 0 2 1832.63 1740.79 66.71 o 2 0 2 19875.19 19999.82 444.88 o 3 0 2 9812.59 9280.48 185.31 o 4 0 2 75222.31 75584.51 829.86 o 5 0 2 6851.23 7079.32 239.29 o 6 0 2 674.52 595.46 183.43 o 7 0 2 2240.10 2386.55 221.63 o 8 0 2 4424.92 4545.71 215.58 o 9 0 2 3548.12 3565.02 261.36 o 10 0 2 341.69 365.12 191.98 o 11 0 2 201.98 39.51 215.29 o 12 0 2 1447.57 1062.36 391.21 o 13 0 2 2959.56 2513.69 445.77 o 1 1 2 6934.07 6462.17 125.38 o 2 1 2 13133.60 12763.19 122.87 o 3 1 2 1334.54 1481.97 69.37 o 4 1 2 171.68 80.46 60.00 o 5 1 2 1842.00 2023.65 82.10 o 6 1 2 3497.80 3595.32 115.50 o 7 1 2 1168.24 1199.12 106.28 o 8 1 2 34.18 16.57 86.50 o 9 1 2 33.07 -18.61 107.33 o 10 1 2 23.44 35.62 100.92 o 11 1 2 526.36 446.07 171.83 o 12 1 2 1563.29 1726.45 214.47 o 13 1 2 2636.19 2510.95 365.14 o 0 2 2 3785.47 3609.77 99.81 o 1 2 2 1156.28 1046.91 40.29 o 2 2 2 4738.01 4885.77 65.15 o 3 2 2 21556.68 21730.49 187.63 o 4 2 2 25174.49 25052.95 244.06 o 5 2 2 713.51 611.41 90.98 o 6 2 2 359.76 519.62 75.70 o 7 2 2 5021.28 4738.32 134.73 o 8 2 2 12187.00 12039.76 210.87 o 9 2 2 9266.10 9352.81 194.90 o 10 2 2 359.93 250.40 127.59 o 11 2 2 32.60 333.18 176.80 o 12 2 2 609.67 267.16 244.03 o 13 2 2 907.85 799.39 279.95 o 1 3 2 12.29 207.99 53.87 o 2 3 2 31149.65 30814.38 209.10 o 3 3 2 3078.60 3160.83 82.53 o 4 3 2 8188.75 7660.70 114.55 o 5 3 2 873.00 1026.30 78.80 o 6 3 2 35206.45 35813.59 341.86 o 7 3 2 10678.54 10387.30 177.53 o 8 3 2 56.06 196.88 117.69 o 9 3 2 729.24 643.23 119.51 o 10 3 2 4313.05 4434.87 169.73 o 11 3 2 98.51 -98.31 155.98 o 12 3 2 731.65 1021.14 263.87 o 13 3 2 536.49 285.56 284.58 o 0 4 2 74.93 188.59 72.60 o 1 4 2 0.59 157.01 55.13 o 2 4 2 11787.59 12202.60 133.06 o 3 4 2 2707.35 2489.65 68.24 o 4 4 2 1507.50 1616.99 67.75 o 5 4 2 729.74 894.12 77.61 o 6 4 2 365.56 279.12 112.97 o 7 4 2 972.20 1195.58 103.49 o 8 4 2 2033.04 1996.49 120.31 o 9 4 2 4312.48 4441.81 149.04 o 10 4 2 15.72 52.28 128.76 o 11 4 2 158.45 -115.80 174.53 o 12 4 2 533.95 563.72 269.01 o 13 4 2 224.26 1000.16 313.29 o 1 5 2 12070.87 12185.99 132.92 o 2 5 2 27148.12 26168.83 214.42 o 3 5 2 66.88 85.29 59.04 o 4 5 2 785.21 950.29 73.67 o 5 5 2 1175.84 1299.43 82.92 o 6 5 2 16089.76 16371.61 210.95 o 7 5 2 24.13 -78.73 98.39 o 8 5 2 20.08 52.43 97.09 o 9 5 2 27.45 27.75 108.44 o 10 5 2 1169.24 1399.17 136.46 o 11 5 2 201.29 -149.39 175.93 o 12 5 2 2005.33 1609.59 268.95 o 13 5 2 2121.45 2136.14 376.25 o 0 6 2 19186.48 18869.16 242.42 o 1 6 2 1524.12 1228.88 70.28 o 2 6 2 4082.04 4393.51 98.77 o 3 6 2 11987.86 12498.29 151.23 o 4 6 2 40219.40 41101.65 298.58 o 5 6 2 15.33 -26.93 74.35 o 6 6 2 1119.60 1047.35 100.06 o 7 6 2 1146.70 1237.33 109.94 o 8 6 2 7066.16 6935.64 176.50 o 9 6 2 417.48 558.53 125.95 o 10 6 2 154.96 430.20 137.86 o 11 6 2 620.17 650.56 210.66 o 12 6 2 1476.03 1737.18 298.81 o 13 6 2 286.05 475.47 348.08 o 1 7 2 3307.18 3456.83 92.36 o 2 7 2 992.09 1240.18 79.77 o 3 7 2 287.34 237.07 78.83 o 4 7 2 544.05 632.97 83.12 o 5 7 2 3620.45 3842.80 114.08 o 6 7 2 35.53 65.27 92.47 o 7 7 2 1460.91 1338.40 121.54 o 8 7 2 1342.67 1451.22 140.66 o 9 7 2 200.43 269.35 121.10 o 10 7 2 712.11 685.27 252.07 o 11 7 2 10.30 251.58 166.18 o 12 7 2 248.86 693.00 308.50 o 0 8 2 9423.48 9480.19 202.59 o 1 8 2 420.50 337.94 77.08 o 2 8 2 3567.09 3722.54 109.64 o 3 8 2 81.65 151.57 103.70 o 4 8 2 22356.83 22656.76 233.18 o 5 8 2 7198.76 7087.73 139.52 o 6 8 2 1766.82 1833.97 163.54 o 7 8 2 1134.16 1085.13 119.32 o 8 8 2 9912.47 10146.41 211.58 o 9 8 2 566.35 496.20 137.14 o 10 8 2 264.99 76.69 176.33 o 11 8 2 2852.74 2241.02 241.39 o 12 8 2 4873.41 4991.33 388.24 o 1 9 2 269.30 475.34 85.62 o 2 9 2 8019.63 8225.90 154.43 o 3 9 2 7.94 -105.05 99.87 o 4 9 2 1620.81 1719.94 114.32 o 5 9 2 70.82 83.78 94.35 o 6 9 2 7948.09 8005.76 169.07 o 7 9 2 1949.26 1840.55 120.61 o 8 9 2 24.50 95.49 123.95 o 9 9 2 513.84 424.39 143.59 o 10 9 2 2417.25 2124.82 197.82 o 11 9 2 1591.36 1618.48 246.46 o 12 9 2 1085.31 598.47 357.56 o 0 10 2 8922.55 8817.77 235.59 o 1 10 2 5056.52 5079.15 133.30 o 2 10 2 358.26 414.05 100.64 o 3 10 2 4.62 271.22 107.61 o 4 10 2 1224.04 1611.10 152.86 o 5 10 2 939.10 851.23 109.42 o 6 10 2 127.07 106.56 117.32 o 7 10 2 404.70 408.67 118.00 o 8 10 2 986.58 820.80 137.38 o 9 10 2 1323.58 1400.09 171.14 o 10 10 2 335.09 229.19 267.16 o 11 10 2 1882.50 1688.87 294.23 o 1 11 2 8287.34 8009.29 168.42 o 2 11 2 20387.42 20917.43 259.19 o 3 11 2 1419.50 1359.36 121.46 o 4 11 2 70.97 97.00 112.32 o 5 11 2 6.71 83.93 109.94 o 6 11 2 7045.66 7024.70 184.34 o 7 11 2 746.58 690.16 130.05 o 8 11 2 141.85 132.41 139.97 o 9 11 2 631.27 889.23 245.83 o 10 11 2 3052.47 2650.35 348.44 o 11 11 2 59.61 42.39 303.40 o 0 12 2 400.91 587.91 161.57 o 1 12 2 5270.88 5396.91 156.76 o 2 12 2 1068.24 1046.08 149.41 o 3 12 2 448.53 402.21 121.35 o 4 12 2 3105.96 3484.98 156.60 o 5 12 2 359.76 212.02 120.76 o 6 12 2 5.35 -1.14 137.40 o 7 12 2 780.89 838.07 159.19 o 8 12 2 1516.19 1184.38 218.44 o 9 12 2 728.95 513.02 275.46 o 10 12 2 278.53 244.73 265.67 o 1 13 2 1257.70 1361.49 133.29 o 2 13 2 5994.98 5911.47 179.62 o 3 13 2 34.36 -19.61 130.26 o 4 13 2 27.70 -14.00 151.23 o 5 13 2 204.99 132.83 157.25 o 6 13 2 1474.88 1341.60 177.42 o 7 13 2 799.74 873.80 201.29 o 8 13 2 81.34 59.92 217.83 o 9 13 2 330.18 95.67 292.29 o 0 14 2 6134.70 6105.70 276.05 o 1 14 2 58.70 67.41 149.77 o 2 14 2 48.36 -55.81 163.04 o 3 14 2 3605.59 3311.61 197.99 o 4 14 2 8175.21 7960.91 256.27 o 5 14 2 2344.80 2207.92 206.98 o 6 14 2 59.92 265.53 203.12 o 7 14 2 374.26 77.81 262.48 o 8 14 2 2833.37 2703.82 371.17 o 9 14 2 34.95 130.77 354.09 o 1 15 2 94.76 165.45 185.39 o 2 15 2 162.45 884.57 223.00 o 3 15 2 470.36 808.78 249.84 o 4 15 2 158.70 -12.74 235.00 o 5 15 2 20.43 156.32 216.16 o 6 15 2 760.87 298.44 229.49 o 7 15 2 242.91 769.21 319.04 o 8 15 2 59.57 498.22 585.25 o 0 16 2 4142.54 3760.62 398.80 o 1 16 2 526.72 674.35 257.51 o 2 16 2 14.91 215.37 258.79 o 3 16 2 58.63 227.93 260.57 o 4 16 2 1327.80 1421.23 284.30 o 5 16 2 36.36 -102.68 280.28 o 6 16 2 318.85 252.83 302.38 o 1 17 2 74.25 54.11 299.98 o 2 17 2 2443.76 2151.11 353.81 o 3 17 2 9.16 298.69 298.76 o 4 17 2 67.66 -392.67 331.92 o 5 17 2 213.76 -101.17 344.24 o 0 18 2 511.73 849.56 562.03 o 1 18 2 284.25 315.31 403.06 o 2 18 2 180.17 727.20 385.30 o 1 1 3 68613.99 67300.67 466.28 o 2 1 3 33228.48 32427.19 252.00 o 3 1 3 18008.39 17639.30 223.88 o 4 1 3 230.17 50.62 78.96 o 5 1 3 927.77 608.75 81.36 o 6 1 3 1562.24 1560.29 108.45 o 7 1 3 12313.28 12254.88 235.57 o 8 1 3 184.05 302.20 164.45 o 9 1 3 2351.33 2236.91 156.30 o 10 1 3 3351.31 3217.18 185.05 o 11 1 3 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444.45 351.81 o 4 2 21 499.57 216.86 273.18 o 5 2 21 2958.79 3453.02 392.23 o 1 3 21 81.73 221.23 242.42 o 2 3 21 42.17 -117.11 430.85 o 3 3 21 31.15 -430.28 427.61 o 4 3 21 13.20 -226.82 379.60 o 0 4 21 188.98 377.13 483.81 o 1 4 21 3419.43 3129.52 376.89 o 2 4 21 75.83 411.69 473.22 o 3 4 21 325.71 353.48 443.22 o 4 4 21 348.87 346.18 398.61 o 1 5 21 337.14 367.69 370.35 o 2 5 21 338.36 549.23 440.82 o 3 5 21 247.11 -204.14 424.80 o 0 6 21 1302.98 104.66 558.00 o 1 6 21 22.78 547.89 533.70 o 2 6 21 34.32 90.36 415.79 o 0 0 22 1677.25 1429.06 564.88 o 1 0 22 437.32 121.48 444.22 o 2 0 22 334.17 946.23 496.93 o 3 0 22 1.24 20.72 1096.55 o 1 1 22 252.54 251.81 252.93 o 2 1 22 525.67 964.46 351.82 o 3 1 22 90.67 410.49 375.66 o 0 2 22 1837.75 2271.58 669.31 o 1 2 22 418.55 404.28 323.23 o 2 2 22 4.10 208.32 294.53 o 1 3 22 390.35 23.29 471.63 o 2 3 22 1824.67 1570.40 459.00 o 0 4 22 516.92 408.05 639.88 o 1 4 22 587.32 228.99 591.97 o