#------------------------------------------------------------------------------ #$Date: 2009-10-12 18:56:40 +0300 (Mon, 12 Oct 2009) $ #$Revision: 830 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2017304.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017304_Fobs loop_ _publ_author_name 'Blanco, Maria C.' 'Palma, Alirio' 'Bahsas, Ali' 'Cobo, Justo' 'Glidewell, Christopher' _publ_section_title ; Different hydrogen-bonded structures in three 2-thienyl-substituted tetrahydro-1,4-epoxy-1-benzazepines ; _journal_coeditor_code GG3212 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o487 _journal_page_last o491 _journal_volume 65 _journal_year 2009 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.3789 _cell_length_b 9.6964 _cell_length_c 30.9520 _exptl_crystal_F_000 1088.00 _reflns_d_resolution_high 0.7699 _[local]_cod_data_source_file gg3212IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' CAB99' _shelx_refln_list_code 4 _shelx_f_calc_maximum 242.06 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 22682.61 21000.44 527.31 o 4 0 0 300.09 161.10 20.36 o 6 0 0 1816.03 1783.91 55.92 o 8 0 0 2398.51 2419.64 108.82 o 10 0 0 154.81 119.62 79.40 o 2 1 0 21833.10 20545.45 232.77 o 4 1 0 32.57 32.89 9.09 o 6 1 0 2844.75 2659.95 53.67 o 8 1 0 14.94 -9.21 32.83 o 10 1 0 973.53 1327.87 101.51 o 0 2 0 3880.94 3926.32 50.07 o 2 2 0 316.10 264.42 8.65 o 4 2 0 7796.54 7903.71 88.85 o 6 2 0 4864.19 5445.90 80.87 o 8 2 0 1073.50 1086.80 83.06 o 10 2 0 123.60 110.80 47.80 o 2 3 0 2872.54 2773.61 34.64 o 4 3 0 680.04 710.19 20.34 o 6 3 0 3887.59 4263.90 78.61 o 8 3 0 355.89 364.60 38.28 o 10 3 0 558.07 637.29 117.85 o 0 4 0 7942.31 8223.12 112.78 o 2 4 0 177.39 214.87 10.14 o 4 4 0 9164.07 10165.32 134.00 o 6 4 0 2059.82 2256.09 74.93 o 8 4 0 205.12 145.09 48.48 o 10 4 0 8.34 -65.07 101.04 o 2 5 0 1950.83 1923.15 32.40 o 4 5 0 2609.71 2892.23 52.80 o 6 5 0 24.90 -6.16 41.71 o 8 5 0 291.36 232.06 62.60 o 0 6 0 16.69 -21.25 14.16 o 2 6 0 13.11 22.64 11.17 o 4 6 0 185.64 137.80 21.16 o 6 6 0 445.10 440.66 51.92 o 8 6 0 106.52 -36.54 68.64 o 2 7 0 2113.25 2209.83 42.35 o 4 7 0 213.77 162.60 46.96 o 6 7 0 7.55 15.53 39.58 o 8 7 0 0.03 -166.93 111.29 o 0 8 0 1431.95 1506.73 61.04 o 2 8 0 581.97 507.32 36.08 o 4 8 0 470.97 534.52 101.21 o 6 8 0 440.61 372.12 78.38 o 8 8 0 0.30 -110.51 120.90 o 2 9 0 45.66 72.28 33.95 o 4 9 0 388.88 392.83 47.42 o 0 10 0 50.72 62.01 79.79 o 2 10 0 1664.05 1912.72 103.99 o 4 10 0 0.90 8.01 48.16 o 2 11 0 714.99 750.19 131.68 o 4 11 0 161.16 157.85 123.18 o 0 12 0 416.27 432.21 142.13 o 2 12 0 111.36 70.14 107.59 o 1 1 1 5688.46 5396.04 56.08 o 2 1 1 78.02 82.92 4.88 o 3 1 1 49.62 37.53 5.03 o 4 1 1 24.40 15.53 6.15 o 5 1 1 230.93 250.19 12.65 o 6 1 1 6.93 15.11 11.36 o 7 1 1 23.27 1.46 13.82 o 8 1 1 211.36 185.09 20.47 o 9 1 1 0.41 -1.56 26.12 o 10 1 1 187.19 118.21 34.44 o 0 2 1 984.34 909.50 12.23 o 1 2 1 2238.12 2142.44 17.28 o 2 2 1 677.95 682.79 9.37 o 3 2 1 50.28 52.58 5.95 o 4 2 1 33.09 22.49 7.88 o 5 2 1 289.40 269.76 11.70 o 6 2 1 372.16 399.49 19.75 o 7 2 1 10.12 4.63 13.93 o 8 2 1 109.53 87.47 21.19 o 9 2 1 5.67 29.04 35.60 o 10 2 1 10.68 125.64 47.09 o 1 3 1 23.09 12.60 4.34 o 2 3 1 113.38 103.35 5.26 o 3 3 1 0.04 -1.27 5.10 o 4 3 1 44.94 42.05 7.22 o 5 3 1 0.02 0.57 8.91 o 6 3 1 3.73 8.93 12.57 o 7 3 1 500.01 546.29 25.18 o 8 3 1 438.66 375.39 31.26 o 9 3 1 0.02 24.59 36.25 o 10 3 1 0.01 35.65 46.20 o 0 4 1 224.72 211.06 8.36 o 1 4 1 4.88 -0.86 4.18 o 2 4 1 2384.58 2665.44 27.32 o 3 4 1 409.72 385.94 10.69 o 4 4 1 739.85 694.79 17.00 o 5 4 1 619.62 666.84 19.22 o 6 4 1 1114.55 1083.89 35.91 o 7 4 1 276.69 273.58 35.18 o 8 4 1 468.06 402.88 34.62 o 9 4 1 27.71 14.14 37.58 o 10 4 1 0.52 110.70 52.79 o 1 5 1 80.09 63.53 7.68 o 2 5 1 594.79 639.13 14.05 o 3 5 1 118.62 98.69 11.77 o 4 5 1 170.68 137.48 13.77 o 5 5 1 36.69 40.82 16.06 o 6 5 1 2054.76 2160.36 103.55 o 7 5 1 6.82 -21.14 28.21 o 8 5 1 162.76 140.24 33.60 o 9 5 1 31.87 26.58 40.29 o 0 6 1 1597.02 1636.83 29.14 o 1 6 1 2.04 1.34 7.18 o 2 6 1 458.88 489.54 13.13 o 3 6 1 482.91 511.15 15.82 o 4 6 1 35.90 38.06 12.44 o 5 6 1 24.65 8.47 21.78 o 6 6 1 10.31 9.57 28.40 o 7 6 1 162.48 90.64 36.57 o 8 6 1 0.83 54.70 50.50 o 9 6 1 108.52 78.98 62.36 o 1 7 1 443.15 407.26 14.18 o 2 7 1 375.93 386.02 13.88 o 3 7 1 105.75 98.82 14.80 o 4 7 1 21.26 29.27 22.76 o 5 7 1 417.94 353.62 34.34 o 6 7 1 428.49 343.44 46.59 o 7 7 1 135.06 66.90 34.97 o 8 7 1 4.72 -80.95 62.58 o 9 7 1 12.89 -121.18 123.01 o 0 8 1 45.07 13.35 19.29 o 1 8 1 221.28 245.30 18.83 o 2 8 1 27.26 40.57 13.54 o 3 8 1 439.22 391.17 27.48 o 4 8 1 66.53 26.02 24.76 o 5 8 1 570.35 600.41 54.57 o 6 8 1 237.00 146.75 47.85 o 7 8 1 42.59 12.34 52.64 o 8 8 1 2.05 37.65 84.30 o 1 9 1 201.71 219.35 20.20 o 2 9 1 40.79 26.37 20.68 o 3 9 1 723.48 693.95 47.80 o 4 9 1 11.71 3.67 31.24 o 5 9 1 267.87 123.37 54.20 o 6 9 1 0.80 12.21 66.54 o 0 10 1 541.79 614.63 77.81 o 1 10 1 429.07 444.58 46.12 o 2 10 1 937.81 959.78 54.73 o 3 10 1 89.52 65.18 36.13 o 4 10 1 147.79 86.49 50.62 o 5 10 1 160.15 94.28 46.73 o 6 10 1 6.63 34.73 140.85 o 1 11 1 590.34 573.56 123.07 o 2 11 1 457.88 463.50 82.88 o 3 11 1 154.20 224.74 104.62 o 4 11 1 431.29 414.76 124.79 o 5 11 1 161.98 111.55 83.40 o 0 12 1 536.68 813.47 142.51 o 1 12 1 398.99 704.46 146.40 o 2 12 1 5.31 -13.05 72.40 o 3 12 1 175.05 313.36 139.35 o 1 0 2 32974.39 28207.08 632.84 o 2 0 2 1884.46 1928.26 24.81 o 3 0 2 6606.02 6559.20 77.68 o 4 0 2 440.38 438.42 14.33 o 5 0 2 246.12 194.13 14.90 o 6 0 2 633.16 579.61 25.94 o 7 0 2 1021.87 1108.76 37.80 o 8 0 2 163.20 182.39 26.79 o 9 0 2 0.09 -38.25 47.54 o 10 0 2 2.73 69.01 43.95 o 1 1 2 135.98 130.72 3.89 o 2 1 2 1679.14 1790.11 17.32 o 3 1 2 1788.87 1654.26 17.73 o 4 1 2 930.93 1044.17 15.19 o 5 1 2 1738.43 1701.81 22.22 o 6 1 2 1829.48 1745.65 28.04 o 7 1 2 1576.83 1682.97 33.30 o 8 1 2 1272.75 1309.45 41.81 o 9 1 2 36.42 21.83 23.37 o 10 1 2 195.32 226.66 42.40 o 0 2 2 17573.13 16925.25 147.06 o 1 2 2 508.06 555.67 7.65 o 2 2 2 1971.24 1860.75 18.59 o 3 2 2 11357.55 11551.54 82.77 o 4 2 2 2222.54 2193.70 25.16 o 5 2 2 904.71 846.83 17.37 o 6 2 2 375.81 421.61 16.28 o 7 2 2 617.12 634.81 25.96 o 8 2 2 626.28 573.29 26.02 o 9 2 2 725.46 845.91 38.32 o 10 2 2 90.18 38.51 41.36 o 1 3 2 746.15 728.81 9.20 o 2 3 2 0.39 5.54 4.32 o 3 3 2 1726.35 1571.06 18.88 o 4 3 2 41.94 42.56 7.06 o 5 3 2 396.06 306.63 12.46 o 6 3 2 1056.03 1064.37 21.84 o 7 3 2 5238.92 5866.18 87.56 o 8 3 2 64.67 19.71 26.71 o 9 3 2 2.51 20.66 32.60 o 10 3 2 261.17 345.53 56.04 o 0 4 2 1016.33 920.47 15.89 o 1 4 2 58.06 26.94 4.79 o 2 4 2 149.79 142.39 8.47 o 3 4 2 390.47 318.13 10.78 o 4 4 2 1077.18 1088.34 19.36 o 5 4 2 3000.76 3197.73 42.68 o 6 4 2 208.15 220.39 19.85 o 7 4 2 772.37 772.36 36.12 o 8 4 2 358.05 356.16 33.43 o 9 4 2 63.84 47.90 40.86 o 10 4 2 1.01 -10.87 44.27 o 1 5 2 151.88 169.11 7.03 o 2 5 2 4863.27 5111.43 49.03 o 3 5 2 169.70 150.64 10.11 o 4 5 2 41.38 26.99 10.52 o 5 5 2 218.84 171.74 14.61 o 6 5 2 717.37 728.60 34.23 o 7 5 2 35.34 -0.04 27.63 o 8 5 2 0.55 -31.19 32.29 o 9 5 2 594.41 501.75 70.01 o 0 6 2 897.05 823.75 20.33 o 1 6 2 674.86 671.06 16.19 o 2 6 2 212.48 192.99 10.35 o 3 6 2 378.48 391.74 15.25 o 4 6 2 4880.61 5180.82 60.66 o 5 6 2 141.91 171.85 28.96 o 6 6 2 29.80 28.67 24.65 o 7 6 2 0.17 1.74 29.32 o 8 6 2 171.22 152.54 45.48 o 9 6 2 225.88 176.67 61.17 o 1 7 2 2583.64 2665.32 31.33 o 2 7 2 1858.31 1867.29 26.91 o 3 7 2 685.42 685.57 20.83 o 4 7 2 279.13 266.63 26.51 o 5 7 2 15.32 26.59 24.86 o 6 7 2 687.17 698.98 57.70 o 7 7 2 1.73 22.40 37.75 o 8 7 2 120.16 58.79 64.20 o 0 8 2 234.85 222.16 22.30 o 1 8 2 142.24 110.42 14.79 o 2 8 2 183.19 172.64 23.22 o 3 8 2 443.22 406.52 28.67 o 4 8 2 904.29 968.58 46.11 o 5 8 2 526.64 509.37 59.87 o 6 8 2 109.15 88.63 45.54 o 7 8 2 6.02 10.01 70.50 o 1 9 2 151.61 139.76 23.43 o 2 9 2 2348.71 2551.35 55.63 o 3 9 2 260.02 134.08 34.95 o 4 9 2 5.56 -12.48 28.14 o 5 9 2 454.24 341.98 76.76 o 7 9 2 7.09 93.40 119.35 o 0 10 2 894.84 950.93 72.16 o 1 10 2 3.61 -11.01 32.63 o 2 10 2 227.96 178.81 33.16 o 3 10 2 9.76 -9.23 31.50 o 4 10 2 1.95 50.87 36.44 o 5 10 2 112.72 116.13 52.35 o 1 11 2 40.30 33.13 51.85 o 2 11 2 121.01 175.86 66.02 o 3 11 2 450.50 589.37 86.70 o 4 11 2 267.04 297.90 85.76 o 5 11 2 27.50 106.49 78.76 o 0 12 2 12.93 139.96 84.57 o 1 12 2 101.98 160.03 70.19 o 2 12 2 157.10 485.71 144.40 o 1 1 3 19688.28 18415.67 131.55 o 2 1 3 2335.02 2250.47 19.70 o 3 1 3 106.69 136.01 5.68 o 4 1 3 275.66 287.99 8.71 o 5 1 3 268.11 278.05 10.62 o 6 1 3 540.69 521.99 17.52 o 7 1 3 1.21 5.45 15.41 o 8 1 3 277.93 274.12 20.77 o 9 1 3 143.69 80.55 28.63 o 10 1 3 63.49 83.92 45.56 o 0 2 3 1194.80 1200.98 16.72 o 1 2 3 51810.67 49004.27 326.05 o 2 2 3 1353.67 1272.30 14.15 o 3 2 3 123.55 157.71 6.15 o 4 2 3 386.40 394.60 10.07 o 5 2 3 1769.22 1896.80 26.87 o 6 2 3 9.87 -5.70 10.30 o 7 2 3 670.40 666.48 29.35 o 8 2 3 213.35 226.93 26.14 o 9 2 3 18.73 -16.15 29.79 o 10 2 3 65.27 28.88 42.46 o 1 3 3 67.07 50.36 4.42 o 2 3 3 619.62 643.46 10.77 o 3 3 3 942.95 938.68 16.07 o 4 3 3 5.35 14.82 6.95 o 5 3 3 1726.19 1698.75 26.94 o 6 3 3 145.10 143.36 18.51 o 7 3 3 3.15 -11.41 18.16 o 8 3 3 134.62 126.42 27.57 o 9 3 3 2.22 -9.19 27.21 o 10 3 3 151.67 148.01 45.65 o 0 4 3 1208.17 1210.88 18.57 o 1 4 3 144.40 112.23 5.15 o 2 4 3 15.55 10.11 5.74 o 3 4 3 2620.90 2750.36 32.39 o 4 4 3 285.24 263.85 15.43 o 5 4 3 1.97 0.51 10.45 o 6 4 3 440.76 399.84 21.03 o 7 4 3 899.91 904.64 34.20 o 8 4 3 148.23 68.80 30.70 o 9 4 3 18.85 -4.30 29.15 o 10 4 3 37.30 8.86 64.96 o 1 5 3 344.70 344.81 9.23 o 2 5 3 2382.08 2433.15 27.50 o 3 5 3 565.55 525.52 12.91 o 4 5 3 13.68 5.02 10.13 o 5 5 3 447.25 445.46 22.12 o 6 5 3 498.49 462.84 27.20 o 7 5 3 371.25 294.54 32.21 o 8 5 3 29.90 39.31 30.80 o 9 5 3 58.08 5.08 74.47 o 0 6 3 2.40 7.65 9.69 o 1 6 3 3052.67 3147.37 33.69 o 2 6 3 237.11 242.73 11.03 o 3 6 3 16.63 3.98 9.75 o 4 6 3 1002.05 971.78 24.09 o 5 6 3 638.73 605.13 41.33 o 6 6 3 57.35 65.50 22.64 o 7 6 3 5.57 -17.12 34.31 o 8 6 3 46.90 -36.24 52.32 o 9 6 3 47.87 46.88 82.89 o 1 7 3 88.41 66.45 10.97 o 2 7 3 487.65 472.56 14.74 o 3 7 3 870.06 847.99 22.47 o 4 7 3 64.01 79.73 26.47 o 5 7 3 371.07 374.32 46.37 o 6 7 3 479.08 542.69 41.81 o 7 7 3 17.79 -32.96 42.06 o 8 7 3 1.62 -60.60 56.15 o 9 7 3 657.44 741.18 188.69 o 0 8 3 380.98 347.01 24.42 o 1 8 3 3.65 -4.69 13.14 o 2 8 3 20.28 23.23 16.57 o 3 8 3 265.11 226.40 24.28 o 4 8 3 624.98 578.00 38.14 o 5 8 3 5.90 0.43 27.89 o 6 8 3 0.20 -9.39 22.24 o 7 8 3 38.52 12.94 53.03 o 1 9 3 165.38 158.14 20.95 o 2 9 3 600.75 598.78 27.77 o 3 9 3 0.14 -12.86 22.73 o 4 9 3 1.70 -44.63 29.75 o 5 9 3 41.88 -19.63 37.57 o 6 9 3 282.66 101.72 74.79 o 7 9 3 54.90 157.85 117.29 o 0 10 3 638.49 661.60 100.07 o 1 10 3 99.31 31.63 32.35 o 2 10 3 0.43 16.37 35.72 o 3 10 3 128.90 132.01 35.52 o 4 10 3 27.51 25.40 41.43 o 5 10 3 24.91 0.50 59.00 o 6 10 3 3.13 -111.51 118.01 o 1 11 3 140.04 54.19 47.44 o 2 11 3 483.51 523.83 116.51 o 3 11 3 103.78 73.96 44.75 o 4 11 3 26.76 -16.88 54.20 o 5 11 3 4.25 57.52 70.40 o 0 12 3 543.67 495.10 130.07 o 1 12 3 144.98 102.46 61.36 o 2 12 3 0.66 94.14 62.39 o 1 0 4 14862.28 14084.24 128.50 o 2 0 4 19.04 10.53 4.70 o 3 0 4 1361.43 1315.43 20.34 o 4 0 4 101.74 88.75 10.24 o 5 0 4 501.54 504.68 17.66 o 6 0 4 132.11 136.10 16.08 o 7 0 4 1385.72 1460.37 43.67 o 8 0 4 292.70 337.90 31.51 o 9 0 4 6.09 61.13 38.64 o 1 1 4 193.49 143.80 4.60 o 2 1 4 297.35 272.10 5.41 o 3 1 4 2145.50 1986.25 20.09 o 4 1 4 62.16 57.62 7.56 o 5 1 4 9.50 21.45 8.47 o 6 1 4 107.77 71.54 10.93 o 7 1 4 1835.05 1829.09 36.78 o 8 1 4 9.62 21.73 19.67 o 9 1 4 83.95 130.72 30.47 o 10 1 4 7.46 -15.23 46.06 o 0 2 4 832.95 768.67 13.60 o 1 2 4 42292.43 40287.67 292.56 o 2 2 4 1365.88 1352.09 15.51 o 3 2 4 798.26 703.47 11.56 o 4 2 4 154.62 133.08 7.74 o 5 2 4 211.28 174.09 9.78 o 6 2 4 439.35 427.09 15.25 o 7 2 4 1078.41 1089.51 30.17 o 8 2 4 648.44 691.43 37.65 o 9 2 4 28.89 24.66 30.15 o 10 2 4 25.07 4.80 37.16 o 1 3 4 31.03 9.99 4.36 o 2 3 4 2359.15 2399.39 24.10 o 3 3 4 3727.29 3852.89 36.06 o 4 3 4 12.46 13.74 9.66 o 5 3 4 475.41 423.04 16.42 o 6 3 4 101.91 78.23 14.21 o 7 3 4 9.97 -11.87 15.48 o 8 3 4 22.95 10.14 19.37 o 9 3 4 309.02 328.64 33.60 o 10 3 4 3.24 10.79 46.99 o 0 4 4 148.29 151.93 8.18 o 1 4 4 4407.11 4409.39 37.57 o 2 4 4 78.64 79.31 6.11 o 3 4 4 4189.91 4531.49 46.38 o 4 4 4 32.88 33.85 10.48 o 5 4 4 45.99 13.72 18.12 o 6 4 4 341.16 344.56 27.12 o 7 4 4 184.63 170.59 26.79 o 8 4 4 0.96 -6.34 24.93 o 9 4 4 242.30 205.22 33.99 o 10 4 4 54.07 41.20 84.89 o 1 5 4 7282.17 7697.97 64.02 o 2 5 4 162.45 157.67 8.83 o 3 5 4 3601.81 3691.10 39.46 o 4 5 4 144.60 103.30 13.09 o 5 5 4 1.18 -11.72 11.70 o 6 5 4 53.85 -1.49 21.74 o 7 5 4 1033.68 992.38 48.43 o 8 5 4 45.16 17.30 36.69 o 9 5 4 366.36 343.84 67.15 o 0 6 4 45.24 38.71 11.23 o 1 6 4 49.52 5.39 7.02 o 2 6 4 69.83 47.39 10.01 o 3 6 4 2329.00 2502.35 32.91 o 4 6 4 809.47 838.10 24.85 o 5 6 4 6271.78 7109.99 100.98 o 6 6 4 27.56 11.22 24.79 o 7 6 4 47.63 32.22 35.93 o 8 6 4 313.89 477.44 117.46 o 9 6 4 39.95 -36.20 66.22 o 1 7 4 839.14 815.39 20.44 o 2 7 4 0.26 7.93 12.45 o 3 7 4 1096.89 1064.98 26.71 o 4 7 4 287.90 289.59 27.74 o 5 7 4 544.81 584.10 36.13 o 6 7 4 207.79 88.32 37.23 o 7 7 4 237.60 328.24 71.08 o 8 7 4 57.00 -34.88 64.32 o 0 8 4 11.91 11.70 18.10 o 1 8 4 396.05 425.87 18.28 o 2 8 4 805.94 772.24 29.40 o 3 8 4 175.55 166.60 25.23 o 4 8 4 142.52 97.17 37.93 o 5 8 4 947.15 894.23 45.29 o 6 8 4 145.31 72.09 44.42 o 7 8 4 0.47 20.35 54.55 o 8 8 4 12.25 46.94 63.09 o 1 9 4 1124.35 1150.03 35.57 o 2 9 4 37.78 54.71 23.00 o 3 9 4 2037.74 2175.52 58.11 o 4 9 4 36.06 19.13 44.91 o 5 9 4 398.29 490.94 96.12 o 6 9 4 33.73 131.12 52.12 o 7 9 4 59.55 98.45 120.23 o 0 10 4 1.44 40.59 41.29 o 1 10 4 430.79 419.78 37.23 o 2 10 4 159.30 105.78 42.63 o 3 10 4 134.22 173.16 42.02 o 4 10 4 93.92 65.16 64.83 o 5 10 4 201.23 92.95 95.90 o 6 10 4 53.68 -19.79 82.76 o 1 11 4 592.64 589.82 86.57 o 2 11 4 12.92 -31.78 42.43 o 3 11 4 30.85 -15.71 42.78 o 4 11 4 180.73 211.64 54.73 o 5 11 4 193.77 77.29 124.35 o 0 12 4 20.72 26.22 119.93 o 1 12 4 97.80 22.58 100.43 o 2 12 4 4.04 -61.97 58.35 o 3 12 4 3.80 32.68 61.44 o 1 1 5 5446.34 5331.57 39.34 o 2 1 5 2417.09 2486.53 22.22 o 3 1 5 1293.51 1412.16 15.08 o 4 1 5 1261.28 1378.18 17.51 o 5 1 5 111.54 98.53 8.31 o 6 1 5 0.02 9.09 9.57 o 7 1 5 157.23 132.00 15.18 o 8 1 5 637.93 698.19 28.22 o 9 1 5 326.89 319.63 40.77 o 10 1 5 1.49 31.35 40.99 o 0 2 5 8765.54 8611.85 91.01 o 1 2 5 1408.38 1359.39 16.48 o 2 2 5 1598.89 1586.62 17.77 o 3 2 5 2235.94 2414.64 23.18 o 4 2 5 705.61 758.21 14.34 o 5 2 5 466.84 488.15 14.03 o 6 2 5 113.42 78.29 10.11 o 7 2 5 85.23 63.29 15.21 o 8 2 5 195.66 205.96 23.95 o 9 2 5 6.77 -1.23 26.29 o 10 2 5 32.93 99.48 40.69 o 1 3 5 5579.60 5801.96 47.38 o 2 3 5 9876.79 10486.83 79.93 o 3 3 5 3388.50 3605.72 37.76 o 4 3 5 208.26 205.07 10.65 o 5 3 5 138.97 123.90 12.99 o 6 3 5 422.35 395.33 16.86 o 7 3 5 720.92 695.12 26.72 o 8 3 5 774.21 765.24 29.70 o 9 3 5 375.66 309.81 35.61 o 10 3 5 4.98 -0.57 49.39 o 0 4 5 723.38 661.68 15.10 o 1 4 5 1545.01 1470.34 18.73 o 2 4 5 1185.64 1397.92 19.95 o 3 4 5 2043.88 2195.72 28.10 o 4 4 5 2222.12 2256.28 28.60 o 5 4 5 864.10 842.94 21.36 o 6 4 5 3.62 19.44 15.57 o 7 4 5 8.84 10.73 22.17 o 8 4 5 247.18 190.38 31.46 o 9 4 5 1.78 65.65 41.62 o 10 4 5 1.31 -69.74 61.96 o 1 5 5 3938.35 4168.25 43.41 o 2 5 5 3.27 14.09 6.96 o 3 5 5 1431.33 1475.79 23.01 o 4 5 5 44.52 53.67 12.47 o 5 5 5 1034.32 973.33 25.12 o 6 5 5 2247.37 2405.94 56.25 o 7 5 5 146.14 77.66 24.35 o 8 5 5 63.24 39.95 46.26 o 9 5 5 48.97 95.72 61.33 o 0 6 5 766.11 769.15 22.03 o 1 6 5 33.27 21.03 9.72 o 2 6 5 133.39 147.43 11.59 o 3 6 5 307.41 251.62 14.63 o 4 6 5 1158.00 1148.93 27.59 o 5 6 5 88.76 105.52 20.21 o 6 6 5 26.64 9.95 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