#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/73/2017306.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017306_Fobs loop_ _publ_author_name 'Dakovi\'c, Marijana' 'Popovi\'c, Zora' _publ_section_title ; Uncommon isonicotinamide supramolecular synthons in copper(II) complexes directed by nitrate and perchlorate anions ; _journal_coeditor_code GT3009 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m361 _journal_page_last m366 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.280 _cell_angle_gamma 90.000 _cell_length_a 7.5367 _cell_length_b 9.8819 _cell_length_c 11.7402 _exptl_crystal_F_000 478.00 _reflns_d_resolution_high 0.7107 _[local]_cod_data_source_file gt3009Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Cu(NO3)2(isoniam)2 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 112.72 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 310.16 264.09 1.49 o 3 0 0 488.03 565.49 5.48 o 4 0 0 1687.15 1781.44 10.97 o 5 0 0 994.19 912.93 9.06 o 6 0 0 8.46 6.22 2.79 o 7 0 0 407.81 405.67 7.88 o 8 0 0 141.87 138.84 6.14 o 9 0 0 174.86 171.42 4.52 o 10 0 0 32.40 30.16 3.42 o 2 1 0 2102.92 2192.83 7.73 o 3 1 0 1144.62 1297.30 4.35 o 4 1 0 40.27 36.48 1.12 o 5 1 0 387.20 409.33 4.46 o 6 1 0 6.62 7.51 2.24 o 7 1 0 7.61 8.52 2.66 o 8 1 0 77.55 79.05 2.62 o 9 1 0 41.91 36.69 2.33 o 10 1 0 0.01 1.05 2.86 o 0 2 0 8937.28 8009.41 107.07 o 1 2 0 270.10 339.26 1.37 o 2 2 0 2080.27 2066.15 8.39 o 3 2 0 451.03 432.15 1.98 o 4 2 0 2457.20 2550.56 8.09 o 5 2 0 410.36 407.04 3.28 o 6 2 0 255.46 255.35 7.39 o 7 2 0 1265.41 1297.08 6.76 o 8 2 0 345.17 363.30 4.90 o 9 2 0 254.01 278.19 5.04 o 10 2 0 28.78 27.32 3.10 o 1 3 0 1534.04 1492.78 2.89 o 2 3 0 726.46 732.00 2.48 o 3 3 0 118.56 115.72 2.32 o 4 3 0 538.63 576.28 2.45 o 5 3 0 54.83 51.09 1.19 o 6 3 0 6.58 4.17 1.35 o 7 3 0 3.12 4.13 1.74 o 8 3 0 236.93 251.47 4.39 o 9 3 0 2.69 1.66 2.90 o 10 3 0 33.40 22.94 3.04 o 0 4 0 258.68 204.35 1.94 o 1 4 0 4028.18 3950.01 20.60 o 2 4 0 3640.29 3586.88 12.74 o 3 4 0 1248.44 1213.86 3.79 o 4 4 0 1024.54 973.80 4.86 o 5 4 0 1016.33 1052.32 4.17 o 6 4 0 782.20 769.24 6.68 o 7 4 0 197.39 212.16 12.01 o 8 4 0 8.73 5.75 2.57 o 9 4 0 34.78 33.47 2.84 o 10 4 0 87.21 84.65 3.32 o 1 5 0 74.71 78.66 0.95 o 2 5 0 1.37 0.72 0.57 o 3 5 0 0.91 0.87 0.64 o 4 5 0 326.72 337.90 2.75 o 5 5 0 12.77 17.25 1.44 o 6 5 0 663.09 677.12 4.51 o 7 5 0 219.15 213.89 3.37 o 8 5 0 97.40 87.32 3.02 o 9 5 0 37.82 32.66 2.88 o 0 6 0 7.85 5.48 1.12 o 1 6 0 1350.50 1328.22 3.52 o 2 6 0 772.22 753.56 3.16 o 3 6 0 1678.44 1717.45 6.05 o 4 6 0 177.50 187.89 2.10 o 5 6 0 1013.74 1042.40 5.13 o 6 6 0 387.94 387.70 3.64 o 7 6 0 31.36 33.16 2.08 o 8 6 0 123.72 115.49 3.19 o 9 6 0 137.33 138.40 5.57 o 1 7 0 636.14 642.47 2.47 o 2 7 0 15.46 16.23 0.93 o 3 7 0 145.33 148.52 1.94 o 4 7 0 131.74 133.28 2.51 o 5 7 0 8.24 10.46 1.89 o 6 7 0 0.04 0.15 0.56 o 7 7 0 48.76 50.95 2.77 o 8 7 0 25.89 21.52 3.25 o 9 7 0 4.61 4.34 3.66 o 0 8 0 189.51 189.00 2.00 o 1 8 0 705.72 711.60 2.79 o 2 8 0 667.91 667.16 3.14 o 3 8 0 1171.81 1233.14 7.55 o 4 8 0 492.92 503.52 4.03 o 5 8 0 687.87 701.52 5.56 o 6 8 0 110.79 108.12 3.09 o 7 8 0 85.46 92.90 3.32 o 8 8 0 91.83 89.57 3.62 o 1 9 0 27.93 14.16 1.01 o 2 9 0 187.32 179.06 1.84 o 3 9 0 490.78 479.31 3.45 o 4 9 0 0.13 1.23 1.56 o 5 9 0 9.90 13.38 2.32 o 6 9 0 17.60 15.97 2.43 o 7 9 0 2.48 1.53 2.26 o 8 9 0 11.81 10.76 3.33 o 0 10 0 50.51 50.84 1.82 o 1 10 0 373.77 373.42 2.49 o 2 10 0 708.35 703.60 4.14 o 3 10 0 474.93 480.11 3.74 o 4 10 0 308.39 322.67 3.78 o 5 10 0 13.34 10.77 2.46 o 6 10 0 6.79 5.47 2.62 o 7 10 0 189.28 188.45 4.42 o 1 11 0 96.49 88.96 2.13 o 2 11 0 23.86 23.56 2.12 o 3 11 0 4.62 4.40 2.16 o 4 11 0 2.04 1.38 1.85 o 5 11 0 94.30 90.71 3.30 o 6 11 0 14.71 12.47 3.63 o 0 12 0 406.86 428.49 7.67 o 1 12 0 290.10 303.55 3.46 o 2 12 0 266.07 279.77 4.27 o 3 12 0 143.55 139.63 4.28 o 4 12 0 90.07 85.29 4.10 o 5 12 0 117.62 110.05 5.92 o 1 13 0 0.02 -0.72 2.79 o 2 13 0 24.12 22.35 2.82 o 3 13 0 91.96 97.15 5.32 o -10 1 1 18.56 14.75 2.38 o -9 1 1 38.57 42.46 2.65 o -8 1 1 60.47 58.02 2.74 o -7 1 1 1312.51 1344.74 14.21 o -6 1 1 374.27 395.58 4.94 o -5 1 1 994.07 891.03 4.29 o -4 1 1 582.67 545.17 2.69 o -3 1 1 896.19 866.25 2.90 o -2 1 1 7254.60 7441.32 25.92 o 2 1 1 11205.44 10735.32 41.51 o 3 1 1 1342.79 1438.83 5.43 o 4 1 1 904.08 849.02 3.07 o 5 1 1 32.43 45.18 1.52 o 6 1 1 782.48 844.03 5.79 o 7 1 1 1009.32 1018.17 6.93 o 8 1 1 84.32 88.72 2.72 o 9 1 1 147.57 154.53 3.18 o 10 1 1 50.14 49.69 3.11 o -10 2 1 47.17 46.53 3.63 o -9 2 1 5.30 5.25 2.36 o -8 2 1 95.32 93.17 3.11 o -7 2 1 18.99 16.22 2.16 o -6 2 1 8.97 9.99 1.30 o -5 2 1 176.52 177.07 2.14 o -4 2 1 229.52 263.75 1.81 o -3 2 1 1020.02 1068.39 3.78 o -2 2 1 3590.43 3634.23 22.18 o -1 2 1 178.54 189.54 0.84 o 1 2 1 312.90 301.77 1.17 o 2 2 1 10.66 6.47 0.43 o 3 2 1 77.46 93.16 1.12 o 4 2 1 784.34 807.49 3.91 o 5 2 1 60.62 53.72 1.49 o 6 2 1 266.40 257.89 2.74 o 7 2 1 5.86 6.92 1.87 o 8 2 1 2.25 1.99 2.16 o 9 2 1 0.90 3.66 2.82 o 10 2 1 18.89 17.37 2.94 o -10 3 1 3.16 1.21 1.97 o -9 3 1 52.31 43.97 3.23 o -8 3 1 399.78 418.54 4.49 o -7 3 1 426.79 451.79 4.85 o -6 3 1 299.02 308.85 3.76 o -5 3 1 2368.37 2331.13 9.75 o -4 3 1 1119.83 1076.49 4.13 o -3 3 1 3029.18 2916.93 15.26 o -2 3 1 246.17 311.33 1.93 o -1 3 1 612.65 550.14 1.32 o 0 3 1 9330.40 8670.70 31.40 o 1 3 1 525.37 540.62 1.72 o 2 3 1 3237.24 3015.49 13.06 o 3 3 1 878.38 942.09 3.91 o 4 3 1 1234.37 1208.70 4.98 o 5 3 1 489.74 461.36 3.13 o 6 3 1 700.91 708.86 4.19 o 7 3 1 500.83 515.38 4.01 o 8 3 1 331.59 356.52 4.55 o 9 3 1 48.06 46.26 2.96 o 10 3 1 3.47 3.57 3.20 o -10 4 1 8.87 6.88 3.08 o -9 4 1 6.00 5.20 2.64 o -8 4 1 0.20 0.25 1.97 o -7 4 1 59.60 51.34 2.35 o -6 4 1 194.90 194.91 2.32 o -5 4 1 99.27 105.67 1.57 o -4 4 1 94.32 92.40 1.94 o -3 4 1 599.39 620.40 2.74 o -2 4 1 1684.61 1829.16 4.68 o -1 4 1 6607.85 6712.91 22.69 o 0 4 1 199.38 232.65 1.20 o 1 4 1 1498.01 1607.11 3.16 o 2 4 1 569.82 595.87 1.86 o 3 4 1 1102.78 1144.46 7.07 o 4 4 1 68.38 65.76 1.35 o 5 4 1 42.22 47.22 1.49 o 6 4 1 46.70 43.21 2.69 o 7 4 1 3.72 4.53 2.03 o 8 4 1 44.19 37.84 2.72 o 9 4 1 31.33 23.38 2.91 o 10 4 1 0.58 1.67 2.65 o -9 5 1 109.24 109.21 3.39 o -8 5 1 437.54 466.75 5.09 o -7 5 1 285.47 295.87 3.86 o -6 5 1 58.94 56.50 1.94 o -5 5 1 383.80 381.93 3.62 o -4 5 1 166.83 155.41 1.84 o -3 5 1 1873.97 1844.86 5.28 o -2 5 1 441.00 418.99 1.63 o -1 5 1 4347.05 4277.24 20.14 o 0 5 1 3167.51 3171.86 7.91 o 1 5 1 2107.10 2077.80 3.99 o 2 5 1 1117.88 1076.34 2.79 o 3 5 1 968.74 946.66 4.19 o 4 5 1 1851.51 1822.11 7.87 o 5 5 1 104.91 99.12 2.02 o 6 5 1 3.28 3.60 1.59 o 7 5 1 60.30 63.24 2.34 o 8 5 1 270.49 268.51 3.45 o 9 5 1 139.89 146.64 3.40 o -9 6 1 3.81 4.74 3.30 o -8 6 1 50.46 46.66 3.26 o -7 6 1 5.41 6.55 1.91 o -6 6 1 51.39 51.60 1.98 o -5 6 1 22.13 24.54 1.51 o -4 6 1 24.12 19.89 1.66 o -3 6 1 120.46 129.83 2.00 o -2 6 1 123.08 124.86 1.05 o -1 6 1 315.65 345.16 1.79 o 0 6 1 18.80 18.91 0.66 o 1 6 1 210.06 217.62 1.62 o 2 6 1 186.17 189.05 1.29 o 3 6 1 68.40 72.49 1.31 o 4 6 1 134.86 128.32 2.47 o 5 6 1 1.44 3.75 1.65 o 6 6 1 0.40 -0.04 0.77 o 7 6 1 63.96 59.59 2.32 o 8 6 1 28.47 25.16 2.13 o 9 6 1 4.70 5.53 3.07 o -9 7 1 72.68 72.30 4.48 o -8 7 1 45.63 43.89 3.27 o -7 7 1 141.04 144.16 3.50 o -6 7 1 204.76 205.43 3.47 o -5 7 1 232.22 260.10 3.55 o -4 7 1 499.40 516.20 5.01 o -3 7 1 1273.66 1284.47 4.70 o -2 7 1 1877.97 1839.09 6.61 o -1 7 1 1025.94 1032.77 3.54 o 0 7 1 12.67 10.22 0.78 o 1 7 1 1308.64 1292.62 4.38 o 2 7 1 604.49 615.59 3.17 o 3 7 1 512.22 499.45 3.53 o 4 7 1 1219.96 1279.90 6.50 o 5 7 1 847.27 889.44 8.87 o 6 7 1 302.47 291.94 4.07 o 7 7 1 109.34 118.99 3.39 o 8 7 1 27.83 24.40 2.47 o 9 7 1 89.99 100.40 3.87 o -8 8 1 17.84 15.02 3.17 o -7 8 1 4.05 5.37 2.44 o -6 8 1 5.83 7.99 2.18 o -5 8 1 181.88 183.24 3.26 o -4 8 1 34.21 32.34 1.85 o -3 8 1 2.43 7.94 1.25 o -2 8 1 14.27 14.83 1.01 o -1 8 1 10.75 9.21 0.91 o 0 8 1 52.56 54.21 1.00 o 1 8 1 48.02 45.98 1.61 o 2 8 1 12.81 11.10 1.05 o 3 8 1 90.13 83.19 1.77 o 4 8 1 57.25 58.57 2.24 o 5 8 1 201.60 207.39 5.09 o 6 8 1 16.47 11.79 2.31 o 7 8 1 8.30 6.61 2.23 o 8 8 1 0.40 1.93 2.81 o -8 9 1 3.08 3.75 3.52 o -7 9 1 1.63 1.01 3.76 o -6 9 1 404.26 421.74 6.16 o -5 9 1 503.45 518.76 4.62 o -4 9 1 607.38 588.82 4.54 o -3 9 1 726.29 711.27 4.65 o -2 9 1 989.46 1026.59 3.83 o -1 9 1 113.85 135.10 1.68 o 0 9 1 240.02 246.36 1.94 o 1 9 1 368.13 413.33 2.35 o 2 9 1 195.11 198.44 2.12 o 3 9 1 106.38 98.64 1.99 o 4 9 1 90.34 92.25 2.64 o 5 9 1 1419.80 1480.32 8.84 o 6 9 1 516.25 526.95 5.55 o 7 9 1 34.44 32.39 2.96 o -7 10 1 5.02 4.93 3.02 o -6 10 1 18.57 19.14 2.78 o -5 10 1 75.91 79.35 3.21 o -4 10 1 0.16 1.85 1.82 o -3 10 1 42.27 41.72 1.85 o -2 10 1 0.17 2.04 1.77 o -1 10 1 243.96 216.94 2.07 o 0 10 1 0.60 0.12 1.12 o 1 10 1 6.66 4.86 1.24 o 2 10 1 91.98 79.08 1.76 o 3 10 1 5.39 4.92 1.53 o 4 10 1 0.12 0.32 0.67 o 5 10 1 68.00 55.22 2.77 o 6 10 1 5.90 2.96 2.65 o 7 10 1 13.24 9.30 3.15 o -6 11 1 67.98 62.95 3.30 o -5 11 1 82.05 84.50 3.25 o -4 11 1 157.01 165.42 3.18 o -3 11 1 172.70 181.50 3.54 o -2 11 1 664.97 696.89 5.74 o -1 11 1 357.23 357.93 2.90 o 0 11 1 577.83 562.00 3.49 o 1 11 1 282.17 284.72 2.85 o 2 11 1 330.48 329.96 4.32 o 3 11 1 354.39 367.75 6.03 o 4 11 1 112.19 104.73 3.77 o 5 11 1 337.67 342.37 5.72 o 6 11 1 50.35 51.98 3.85 o -5 12 1 43.80 44.14 4.55 o -4 12 1 1.67 5.93 3.16 o -3 12 1 43.46 41.51 3.40 o -2 12 1 117.89 101.43 2.85 o -1 12 1 6.89 6.57 1.89 o 0 12 1 82.98 78.28 2.30 o 1 12 1 74.34 70.36 2.88 o 2 12 1 8.50 7.10 2.70 o 3 12 1 0.03 2.90 3.77 o 4 12 1 9.44 6.48 4.10 o 5 12 1 0.48 3.06 4.73 o -3 13 1 9.15 6.22 2.83 o -2 13 1 37.49 29.19 2.56 o -1 13 1 168.99 167.24 3.84 o 0 13 1 186.28 198.01 3.99 o 1 13 1 196.39 194.25 4.00 o 2 13 1 19.62 12.13 3.30 o 3 13 1 72.17 69.62 5.10 o -10 0 2 36.09 31.12 5.93 o -9 0 2 95.32 95.53 4.10 o -8 0 2 508.03 530.44 19.00 o -7 0 2 17.50 17.98 2.42 o -6 0 2 293.04 255.54 4.01 o -5 0 2 2048.45 1989.98 9.06 o -4 0 2 1465.53 1469.13 12.88 o -3 0 2 61.21 29.01 1.38 o -2 0 2 10351.25 10236.30 71.47 o -1 0 2 7036.46 6817.95 33.93 o 1 0 2 12706.55 12640.79 52.24 o 2 0 2 5474.09 5219.79 30.36 o 3 0 2 7103.57 7083.51 41.91 o 4 0 2 328.06 342.59 2.88 o 5 0 2 637.58 667.08 3.82 o 6 0 2 122.29 116.36 2.66 o 7 0 2 48.38 42.97 2.99 o 8 0 2 130.78 151.36 9.87 o 9 0 2 96.77 91.56 7.76 o 10 0 2 175.58 181.99 5.80 o -10 1 2 0.62 0.31 2.55 o -9 1 2 32.22 27.31 2.29 o -8 1 2 36.98 37.06 2.52 o -7 1 2 1.16 2.50 1.85 o -6 1 2 165.65 163.62 2.05 o -5 1 2 139.49 160.77 1.67 o -4 1 2 65.45 75.20 1.59 o -3 1 2 1641.54 1743.20 7.99 o -2 1 2 10630.96 10461.85 37.25 o -1 1 2 15.48 11.80 0.67 o 0 1 2 59.41 55.51 2.21 o 1 1 2 501.39 535.37 1.66 o 2 1 2 179.89 173.20 1.13 o 3 1 2 1219.54 1244.94 3.16 o 4 1 2 145.04 163.50 1.60 o 5 1 2 302.43 347.96 2.50 o 6 1 2 155.45 161.99 2.11 o 7 1 2 1.08 0.37 1.55 o 8 1 2 6.46 6.70 2.12 o 9 1 2 43.91 45.64 2.62 o 10 1 2 0.52 1.38 3.06 o -10 2 2 45.32 44.79 3.41 o -9 2 2 70.16 66.72 3.91 o -8 2 2 359.04 364.41 5.77 o -7 2 2 336.09 343.61 3.50 o -6 2 2 718.07 717.07 3.92 o -5 2 2 3488.89 3517.34 9.89 o -4 2 2 3690.82 3681.97 11.26 o -3 2 2 2400.60 2226.04 6.89 o -2 2 2 23.15 29.85 0.89 o -1 2 2 3918.93 3812.78 14.53 o 0 2 2 79.84 70.72 0.57 o 1 2 2 3676.73 3546.26 16.91 o 2 2 2 1436.87 1296.19 5.02 o 3 2 2 2133.49 2072.47 6.31 o 4 2 2 749.04 754.09 2.96 o 5 2 2 127.05 118.54 1.61 o 6 2 2 517.06 522.68 3.35 o 7 2 2 240.54 226.09 2.92 o 8 2 2 148.70 158.81 2.95 o 9 2 2 163.78 174.32 3.87 o 10 2 2 75.90 80.11 3.56 o -10 3 2 101.45 96.47 3.64 o -9 3 2 2.87 5.18 2.39 o -8 3 2 98.64 95.33 3.89 o -7 3 2 27.14 21.09 2.31 o -6 3 2 0.24 1.75 1.23 o -5 3 2 2.63 2.17 0.94 o -4 3 2 13.04 17.41 0.95 o -3 3 2 307.60 343.27 2.33 o -2 3 2 10.01 9.09 0.79 o -1 3 2 2614.81 2619.49 8.17 o 0 3 2 469.52 517.18 1.23 o 1 3 2 652.38 686.80 2.32 o 2 3 2 13.86 18.89 0.90 o 3 3 2 89.73 82.90 1.01 o 4 3 2 25.35 26.73 0.80 o 5 3 2 85.20 86.17 1.35 o 6 3 2 59.82 55.25 1.56 o 7 3 2 52.47 56.79 2.41 o 8 3 2 21.09 21.16 2.54 o 9 3 2 30.81 30.94 2.86 o 10 3 2 2.77 0.10 0.80 o -10 4 2 177.15 186.19 4.89 o -9 4 2 31.16 29.70 2.68 o -8 4 2 26.34 29.24 2.41 o -7 4 2 257.80 260.62 4.20 o -6 4 2 322.40 328.77 4.19 o -5 4 2 720.02 699.70 5.32 o -4 4 2 7.26 6.30 1.10 o -3 4 2 1111.36 1072.42 4.13 o -2 4 2 2736.68 2749.93 9.11 o -1 4 2 5506.04 5322.00 16.95 o 0 4 2 622.69 580.67 1.57 o 1 4 2 1495.72 1490.33 3.69 o 2 4 2 1496.57 1356.60 3.54 o 3 4 2 222.75 195.04 2.53 o 4 4 2 2560.99 2527.81 7.39 o 5 4 2 705.32 729.13 4.16 o 6 4 2 1470.23 1508.24 6.51 o 7 4 2 108.23 104.77 2.52 o 8 4 2 13.61 13.53 2.06 o 9 4 2 156.95 167.32 4.05 o -9 5 2 23.53 19.30 3.20 o -8 5 2 80.24 79.42 2.83 o -7 5 2 0.10 1.07 2.09 o -6 5 2 5.91 5.70 1.60 o -5 5 2 20.08 23.42 1.84 o -4 5 2 278.89 268.78 2.62 o -3 5 2 2.77 5.27 0.63 o -2 5 2 154.69 151.74 0.90 o -1 5 2 115.48 110.69 0.79 o 0 5 2 501.71 531.74 2.40 o 1 5 2 364.25 404.26 1.44 o 2 5 2 19.52 23.26 0.62 o 3 5 2 172.66 181.39 2.02 o 4 5 2 1210.76 1213.76 9.60 o 5 5 2 135.59 144.11 2.28 o 6 5 2 573.25 552.44 6.14 o 7 5 2 7.80 6.77 1.86 o 8 5 2 36.20 33.89 2.11 o 9 5 2 7.57 6.20 2.79 o -9 6 2 242.82 250.82 5.46 o -8 6 2 180.31 188.20 4.55 o -7 6 2 42.48 36.10 2.90 o -6 6 2 124.10 131.46 2.69 o -5 6 2 372.66 373.70 2.96 o -4 6 2 457.91 460.81 2.90 o -3 6 2 4012.65 3991.02 8.82 o -2 6 2 1817.33 1850.62 4.69 o -1 6 2 651.79 638.39 3.94 o 0 6 2 1685.61 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