#------------------------------------------------------------------------------
#$Date: 2009-11-11 20:41:08 +0200 (Wed, 11 Nov 2009) $
#$Revision: 840 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2017362.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2017362_Fobs
loop_
_publ_author_name
'Grzechnik, Andrzej'
_publ_section_title
;
 Bi~4~Ge~3~O~12~ at the onset of pressure-induced amorphization
;
_journal_coeditor_code           SQ3206
_journal_issue                   10
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              i63
_journal_page_last               i65
_journal_volume                  65
_journal_year                    2009
_space_group_IT_number           220
_symmetry_space_group_name_Hall  'I -4bd 2c 3'
_symmetry_space_group_name_H-M   'I -4 3 d'
_[local]_cod_data_source_file    sq3206Isup2.hkl
_[local]_cod_data_source_block   I
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_meas
_refln_F_calc
_refln_F_sigma
_refln_observed_status
-1 1 2 164.07 155.44 1.90 o
1 1 2 146.32 139.51 1.75 o
0 2 2 75.51 73.41 2.43 o
0 1 3 273.97 298.44 2.82 o
-1 2 3 212.87 217.98 2.23 o
1 2 3 221.41 226.66 2.29 o
-2 3 3 118.86 103.36 1.87 o
2 3 3 119.71 105.82 1.61 o
0 0 4 191.15 190.49 2.77 o
-2 2 4 273.11 299.61 2.87 o
0 2 4 58.23 61.47 2.35 o
2 2 4 256.98 287.03 2.68 o
-1 3 4 176.50 159.87 2.01 o
1 3 4 191.19 173.44 2.10 o
-4 4 4 273.54 285.55 3.15 o
0 4 4 34.20 26.07 7.32 <
4 4 4 285.13 299.59 2.97 o
0 1 5 195.23 179.86 2.14 o
-1 2 5 29.73 24.19 5.60 <
1 2 5 31.04 28.45 4.57 o
-2 3 5 187.82 184.02 2.06 o
0 3 5 183.18 181.55 2.03 o
2 3 5 174.63 174.34 1.86 o
-3 4 5 143.25 138.73 1.77 o
-1 4 5 206.93 211.13 2.24 o
1 4 5 212.11 219.96 2.24 o
3 4 5 142.85 142.33 1.59 o
-2 5 5 210.54 208.37 2.51 o
2 5 5 183.91 190.91 2.16 o
-1 1 6 216.28 218.03 2.37 o
1 1 6 222.78 219.69 2.40 o
0 2 6 231.56 232.59 2.41 o
-3 3 6 90.42 89.38 2.99 o
-1 3 6 154.13 149.42 1.92 o
1 3 6 155.98 156.21 1.81 o
3 3 6 84.11 85.62 2.10 o
-2 4 6 115.29 109.74 2.04 o
0 4 6 93.10 85.52 2.72 o
2 4 6 110.11 105.28 1.72 o
-5 5 6 171.17 169.62 2.38 o
-3 5 6 101.54 99.56 2.24 o
-1 5 6 48.62 50.68 4.09 o
1 5 6 52.72 55.90 4.08 o
3 5 6 101.58 97.75 1.67 o
5 5 6 163.55 164.22 1.94 o
-4 6 6 106.73 103.67 2.81 o
0 6 6 271.57 284.59 3.30 o
4 6 6 101.12 98.14 2.10 o
0 1 7 141.05 139.54 1.86 o
-1 2 7 76.40 73.88 2.47 o
1 2 7 72.13 70.43 2.21 o
-2 3 7 126.75 130.29 2.16 o
0 3 7 92.02 86.17 2.16 o
2 3 7 135.15 138.32 1.77 o
-3 4 7 166.15 165.33 2.23 o
-1 4 7 149.54 133.87 2.09 o
1 4 7 143.55 132.41 1.99 o
3 4 7 163.83 168.20 1.88 o
-4 5 7 33.56 23.89 6.01 <
-2 5 7 161.40 155.37 2.20 o
0 5 7 73.23 76.71 3.42 o
2 5 7 156.89 154.59 1.94 o
4 5 7 46.00 30.39 2.89 o
-5 6 7 115.02 115.58 2.73 o
-3 6 7 140.13 133.76 2.28 o
-1 6 7 36.92 35.39 7.47 <
1 6 7 47.68 38.37 5.20 o
3 6 7 144.17 140.16 1.89 o
5 6 7 117.87 119.24 2.44 o
-6 7 7 53.21 51.77 7.54 o
-2 7 7 134.31 127.41 2.98 o
2 7 7 134.62 131.07 2.60 o
6 7 7 52.50 42.57 7.08 o
0 0 8 108.30 116.08 2.95 o
-2 2 8 189.11 191.19 2.43 o
0 2 8 39.25 20.76 4.49 o
2 2 8 178.53 178.93 2.29 o
-1 3 8 115.95 113.15 2.17 o
1 3 8 113.47 110.82 2.02 o
-4 4 8 188.51 187.64 3.05 o
-2 4 8 63.25 64.55 5.06 o
0 4 8 119.65 118.34 2.29 o
2 4 8 60.59 62.36 3.03 o
4 4 8 177.96 182.41 2.18 o
-3 5 8 116.83 109.16 2.36 o
-1 5 8 163.69 160.11 2.48 o
1 5 8 157.27 156.67 2.19 o
3 5 8 115.52 114.62 1.76 o
-6 6 8 152.73 159.09 3.24 o
-4 6 8 55.50 47.86 6.02 o
-2 6 8 76.02 74.18 3.94 o
0 6 8 24.40 7.30 8.74 <
2 6 8 76.91 72.31 2.74 o
4 6 8 56.48 49.63 5.18 o
6 6 8 164.26 163.42 2.89 o
-5 7 8 44.29 33.11 7.66 <
-3 7 8 137.75 133.35 3.02 o
-1 7 8 81.44 85.75 6.70 o
1 7 8 92.59 85.43 5.00 o
3 7 8 129.18 128.94 3.55 o
5 7 8 24.94 27.52 12.09 <
-4 8 8 88.27 125.35 7.01 o
0 8 8 164.37 148.99 4.99 o
4 8 8 110.15 123.21 4.09 o
0 1 9 118.09 123.12 1.88 o
-1 2 9 178.39 183.86 2.10 o
1 2 9 180.22 186.64 2.09 o
-2 3 9 35.43 15.14 6.71 <
0 3 9 34.27 16.59 5.97 <
2 3 9 29.89 13.01 6.17 <
-3 4 9 61.14 60.56 5.35 o
-1 4 9 93.73 108.23 3.62 o
1 4 9 111.06 106.61 2.46 o
3 4 9 58.25 56.22 2.97 o
-4 5 9 99.66 100.98 4.18 o
-2 5 9 73.01 74.08 6.94 o
0 5 9 147.76 149.95 2.60 o
2 5 9 74.29 73.22 4.90 o
4 5 9 99.46 93.76 3.21 o
-5 6 9 85.22 81.07 5.65 o
-3 6 9 21.70 29.82 19.33 <
-1 6 9 86.75 92.68 6.57 o
1 6 9 93.92 87.84 4.81 o
3 6 9 36.75 29.10 11.42 <
5 6 9 80.29 85.81 3.49 o
-4 7 9 96.13 109.57 4.77 o
-2 7 9 62.16 61.36 12.68 <
0 7 9 131.66 120.26 5.32 o
2 7 9 67.49 62.75 5.49 o
4 7 9 101.72 105.32 3.80 o
6 7 9 108.87 112.80 4.21 o
-5 8 9 80.09 72.36 13.27 o
-3 8 9 46.11 42.73 12.61 <
-1 8 9 89.77 90.22 7.02 o
1 8 9 99.45 92.88 4.78 o
3 8 9 61.55 45.55 8.15 o
5 8 9 92.88 81.60 4.93 o
-2 9 9 12.36 20.44 60.98 <
2 9 9 18.60 14.92 29.84 <
-1 1 10 143.18 145.41 2.08 o
1 1 10 147.28 153.04 2.16 o
0 2 10 36.53 23.77 4.56 o
-3 3 10 13.85 33.16 68.73 <
-1 3 10 93.84 94.68 3.17 o
1 3 10 104.29 97.56 3.70 o
3 3 10 53.71 35.62 9.68 <
-2 4 10 177.41 183.40 3.35 o
0 4 10 53.60 46.02 7.90 o
2 4 10 170.94 187.65 2.75 o
-5 5 10 89.86 68.12 10.70 o
-3 5 10 125.05 118.22 3.38 o
1 5 10 55.59 31.80 11.37 <
3 5 10 119.99 124.50 3.58 o
5 5 10 79.34 73.05 5.65 o
-4 6 10 52.85 53.95 11.35 <
-2 6 10 28.48 15.18 27.94 <
0 6 10 74.49 97.60 8.67 o
2 6 10 36.60 15.18 15.41 <
4 6 10 56.75 57.47 6.34 o
-3 7 10 126.82 122.09 6.11 o
-1 7 10 41.30 27.34 16.36 <
1 7 10 38.75 30.75 26.52 <
3 7 10 135.83 125.76 4.34 o
5 7 10 78.97 66.93 8.17 o
-2 8 10 149.89 131.37 4.41 o
0 8 10 40.21 4.86 14.62 <
2 8 10 134.66 134.59 3.61 o
4 8 10 14.59 29.52 52.10 <
-1 9 10 115.67 88.26 5.71 o
1 9 10 77.81 79.76 7.28 o
0 1 11 23.22 8.54 10.11 <
-1 2 11 101.21 94.82 2.88 o
1 2 11 92.57 89.26 3.41 o
-2 3 11 97.68 92.84 3.33 o
0 3 11 85.59 81.11 3.99 o
2 3 11 88.23 86.85 4.01 o
-3 4 11 91.49 92.92 6.73 o
-1 4 11 45.53 36.83 8.22 <
1 4 11 37.38 34.59 11.94 <
3 4 11 96.42 91.93 3.49 o
-4 5 11 90.14 91.66 6.74 o
-2 5 11 51.98 37.90 7.65 o
0 5 11 98.66 100.41 4.84 o
2 5 11 50.61 41.52 8.46 <
4 5 11 83.00 91.69 4.63 o
-3 6 11 76.89 101.26 7.34 o
-1 6 11 47.15 105.86 16.58 <
3 6 11 98.71 96.83 9.87 o
0 7 11 24.32 109.92 34.24 <
-1 8 11 48.71 46.42 13.90 <
1 8 11 83.00 48.26 8.40 o
0 0 12 211.45 225.03 3.55 o
-2 2 12 90.15 86.28 4.93 o
0 2 12 42.90 30.43 6.19 o
2 2 12 82.54 90.81 5.73 o
-1 3 12 125.13 124.79 2.78 o
1 3 12 108.25 122.13 3.42 o
-4 4 12 37.46 49.22 18.24 <
-2 4 12 48.20 2.27 10.16 <
0 4 12 105.18 101.52 3.98 o
2 4 12 31.36 2.27 10.17 <
4 4 12 12.46 36.16 44.35 <
-3 5 12 90.26 77.12 6.83 o
1 5 12 59.23 60.33 9.48 o
3 5 12 63.27 76.50 8.96 o
0 1 13 52.40 52.90 5.55 o
-1 2 13 53.70 49.66 6.62 o
1 2 13 58.87 54.82 5.32 o
-2 3 13 103.24 90.51 7.16 o
0 3 13 92.26 84.74 3.94 o
2 3 13 100.03 95.08 5.23 o
1 4 13 13.44 24.79 47.44 <