#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:16:39 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180842 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/73/2017370.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017370_Fobs loop_ _publ_author_name 'Kuratieva, Natalia V.' 'Mikhailova, Daria' 'Ehrenberg, Helmut' _publ_section_title ; A new polymorph of Cu~3~B~2~O~6~ ; _journal_coeditor_code BD3006 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i85 _journal_page_last i86 _journal_volume 65 _journal_year 2009 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.913 _cell_angle_gamma 90.000 _cell_length_a 17.8198 _cell_length_b 8.5232 _cell_length_c 9.1706 _exptl_crystal_F_000 1740.00 _reflns_d_resolution_high 0.7502 _cod_data_source_file bd3006Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Cu3B2O6 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 967.93 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4852.68 5109.20 71.28 o 2 0 0 23230.57 24280.70 322.61 o 3 0 0 1.03 0.00 41.94 o 4 0 0 8634.09 9310.77 185.56 o 5 0 0 7123.92 6937.26 176.80 o 6 0 0 92290.98 86879.25 1074.44 o 7 0 0 19036.36 16677.39 236.01 o 8 0 0 9226.22 9067.56 180.65 o 9 0 0 18276.03 18898.30 272.74 o 10 0 0 155854.14 153627.80 1942.90 o 11 0 0 23054.37 22907.83 417.67 o 12 0 0 2920.21 3033.49 355.31 o 13 0 0 13140.27 13103.31 340.07 o 14 0 0 15820.14 15732.43 376.56 o 15 0 0 10442.81 10522.93 406.91 o 16 0 0 18884.28 18766.83 437.86 o 17 0 0 36536.22 36824.01 628.08 o 18 0 0 142.67 529.31 221.26 o 19 0 0 36536.71 37156.50 657.64 o 20 0 0 8318.23 8932.02 372.06 o 21 0 0 5.33 46.94 240.15 o 22 0 0 31.29 38.13 253.92 o 23 0 0 2893.92 3133.88 298.17 o 1 1 0 1747.22 1985.82 63.52 o 2 1 0 801.42 886.98 44.95 o 3 1 0 245.30 270.52 41.79 o 4 1 0 15.66 74.85 45.24 o 5 1 0 13428.84 12550.40 132.94 o 6 1 0 4623.17 4921.25 101.76 o 7 1 0 37755.47 36533.34 291.99 o 8 1 0 19429.12 18286.62 223.64 o 9 1 0 8.40 0.00 51.02 o 10 1 0 6923.22 7255.00 148.37 o 11 1 0 26413.85 25574.39 267.56 o 12 1 0 22824.10 21773.51 279.99 o 13 1 0 9703.40 9566.00 214.82 o 14 1 0 14268.53 14330.46 255.55 o 15 1 0 2993.10 3258.19 191.67 o 16 1 0 2212.02 2247.90 217.44 o 17 1 0 462.80 373.07 154.63 o 18 1 0 650.16 776.43 156.97 o 19 1 0 999.13 860.83 168.35 o 20 1 0 523.89 526.99 186.75 o 21 1 0 6062.86 5732.59 221.15 o 22 1 0 978.66 1038.30 429.28 o 23 1 0 865.50 979.96 314.52 o 0 2 0 3825.24 3729.25 152.61 o 1 2 0 14716.85 15605.96 186.03 o 2 2 0 673.16 853.88 76.54 o 3 2 0 14157.53 14311.33 195.82 o 4 2 0 7179.27 7345.99 152.16 o 5 2 0 9168.15 9250.99 115.99 o 6 2 0 3484.84 3591.32 93.93 o 7 2 0 65247.39 64019.65 503.92 o 8 2 0 19621.07 19236.66 214.66 o 9 2 0 3529.63 3478.62 88.51 o 10 2 0 5025.78 4785.76 138.67 o 11 2 0 8861.77 8937.99 165.08 o 12 2 0 2404.31 2432.89 146.55 o 13 2 0 3618.42 3839.43 168.54 o 14 2 0 840.37 745.35 156.02 o 15 2 0 18.39 170.66 155.71 o 16 2 0 2839.04 2837.50 165.60 o 17 2 0 3978.44 4027.16 191.93 o 18 2 0 2346.10 2477.62 175.17 o 19 2 0 12698.47 12736.48 328.77 o 20 2 0 404.20 513.44 194.45 o 21 2 0 19.34 0.00 202.48 o 22 2 0 3410.67 3383.70 242.35 o 23 2 0 490.65 549.24 240.07 o 1 3 0 2605.19 3030.19 103.47 o 2 3 0 173.95 219.73 78.61 o 3 3 0 153084.97 152563.92 2013.73 o 4 3 0 27489.67 27552.11 390.73 o 5 3 0 53065.39 49832.77 474.74 o 6 3 0 0.58 0.00 75.07 o 7 3 0 23739.17 23737.61 271.99 o 8 3 0 20839.89 20828.95 251.89 o 9 3 0 36776.13 38546.34 323.34 o 10 3 0 36887.91 36544.16 314.28 o 11 3 0 7205.78 7003.50 182.13 o 12 3 0 2990.28 3208.59 243.42 o 13 3 0 41872.87 42149.39 638.51 o 14 3 0 63875.26 63808.96 737.85 o 15 3 0 10427.20 10720.79 269.10 o 16 3 0 12061.03 11716.58 283.26 o 17 3 0 73.69 54.30 212.55 o 18 3 0 1781.91 1500.14 200.86 o 19 3 0 11.66 255.99 206.56 o 20 3 0 8318.11 8542.99 398.61 o 21 3 0 165.97 137.01 205.76 o 22 3 0 8058.81 8508.14 323.42 o 0 4 0 14938.15 15864.63 301.95 o 1 4 0 20770.91 23168.09 272.35 o 2 4 0 2476.74 2866.14 107.37 o 3 4 0 6808.60 6875.90 161.78 o 4 4 0 5175.45 5252.00 153.88 o 5 4 0 128.13 74.13 94.89 o 6 4 0 2127.46 2314.96 152.54 o 7 4 0 19832.04 20319.16 234.25 o 8 4 0 12190.13 12512.74 236.61 o 9 4 0 790.95 880.44 108.08 o 10 4 0 4398.89 4531.71 163.46 o 11 4 0 30039.19 30280.47 886.49 o 12 4 0 5772.14 5821.36 283.34 o 13 4 0 2450.88 2348.63 211.36 o 14 4 0 1055.85 1034.17 192.87 o 15 4 0 1472.57 1785.47 281.74 o 16 4 0 86.52 0.00 426.20 o 17 4 0 741.96 418.02 215.60 o 18 4 0 29.37 161.52 221.09 o 19 4 0 1357.76 1639.77 218.04 o 20 4 0 1035.54 1081.77 216.81 o 21 4 0 1381.72 1090.44 230.13 o 22 4 0 4250.80 4907.17 273.29 o 1 5 0 1711.39 1595.73 113.90 o 2 5 0 4207.29 4462.11 155.05 o 3 5 0 7744.23 7993.40 184.07 o 4 5 0 12172.13 12546.18 217.40 o 5 5 0 357.15 332.27 108.29 o 6 5 0 19454.96 19870.14 272.70 o 7 5 0 3492.18 3833.74 122.63 o 8 5 0 5173.08 5255.07 186.61 o 9 5 0 62.00 0.00 138.07 o 10 5 0 5757.09 5419.36 279.48 o 11 5 0 1366.90 1579.71 258.41 o 12 5 0 2265.90 2274.69 212.68 o 13 5 0 7727.62 7825.02 328.91 o 14 5 0 277.80 484.51 216.92 o 15 5 0 433.42 676.72 319.87 o 16 5 0 4464.82 4529.39 273.29 o 17 5 0 11.08 334.78 234.78 o 18 5 0 2.98 89.17 240.67 o 19 5 0 737.95 730.26 251.92 o 20 5 0 931.34 1127.16 238.14 o 21 5 0 1699.41 1761.73 248.84 o 0 6 0 115760.73 123285.28 2237.77 o 1 6 0 5826.18 5586.63 177.50 o 2 6 0 136862.59 141262.05 1265.57 o 3 6 0 9.78 13.51 114.24 o 4 6 0 7223.37 6979.70 239.98 o 5 6 0 2201.52 2346.62 134.79 o 6 6 0 4682.46 4656.95 161.88 o 7 6 0 8396.96 8475.08 214.35 o 8 6 0 49815.31 49805.67 533.32 o 9 6 0 6572.49 6972.12 316.56 o 10 6 0 12633.12 12706.74 360.34 o 11 6 0 11713.84 12024.59 368.94 o 12 6 0 6178.15 6255.29 299.19 o 13 6 0 1831.07 1840.86 267.38 o 14 6 0 643.97 421.59 230.28 o 15 6 0 85.53 477.66 243.33 o 16 6 0 4.94 84.15 240.86 o 17 6 0 12178.49 12976.59 422.18 o 18 6 0 9626.30 10697.90 417.47 o 19 6 0 11723.72 11995.63 433.53 o 20 6 0 48.38 103.27 276.31 o 1 7 0 237.11 240.03 131.60 o 2 7 0 792.77 689.70 141.23 o 3 7 0 47.99 0.00 128.15 o 4 7 0 1940.98 2110.08 151.36 o 5 7 0 4.18 62.19 153.80 o 6 7 0 13430.67 13118.15 264.26 o 7 7 0 182.94 267.26 215.02 o 8 7 0 106.14 35.67 166.99 o 9 7 0 1268.93 1213.97 231.43 o 10 7 0 3919.54 4348.97 270.88 o 11 7 0 131.31 642.13 234.32 o 12 7 0 1652.69 1826.06 254.47 o 13 7 0 2738.73 2920.26 271.82 o 14 7 0 108.85 107.71 243.09 o 15 7 0 1750.05 2002.27 272.64 o 16 7 0 625.78 727.29 276.57 o 17 7 0 8.46 2.54 476.89 o 18 7 0 895.15 1052.11 291.24 o 0 8 0 705.91 588.05 214.85 o 1 8 0 33187.21 33816.07 430.53 o 2 8 0 0.15 0.00 145.18 o 3 8 0 2689.75 2707.40 275.27 o 4 8 0 3.00 78.34 170.12 o 5 8 0 12164.70 11981.66 315.80 o 6 8 0 1472.39 1355.28 200.30 o 7 8 0 330.42 211.23 183.44 o 8 8 0 306.30 370.03 191.71 o 9 8 0 7915.71 8435.38 391.49 o 10 8 0 1175.11 1308.93 261.75 o 11 8 0 11871.14 11570.28 403.99 o 12 8 0 235.44 572.08 270.57 o 13 8 0 981.17 1285.61 279.24 o 14 8 0 813.92 902.00 277.68 o 15 8 0 4240.21 4870.31 342.61 o 16 8 0 4336.76 4424.44 346.46 o 1 9 0 194.37 230.82 185.98 o 2 9 0 1196.59 1430.42 206.00 o 3 9 0 19099.09 19445.19 398.51 o 4 9 0 174.98 434.64 193.89 o 5 9 0 25033.56 24397.25 454.32 o 6 9 0 14049.68 13765.93 358.01 o 7 9 0 20037.85 19513.67 613.08 o 8 9 0 147.18 78.54 215.07 o 9 9 0 7.67 0.00 266.24 o 10 9 0 2402.23 2521.04 300.44 o 11 9 0 1317.16 1361.95 332.43 o 12 9 0 24696.42 24134.23 574.61 o 13 9 0 25362.21 25116.17 603.88 o 14 9 0 4821.87 5016.10 354.46 o 0 10 0 13848.77 13730.77 623.60 o 1 10 0 19.69 0.00 328.85 o 2 10 0 6036.15 6568.61 739.34 o 3 10 0 4229.37 3973.50 258.69 o 4 10 0 32.09 30.24 234.61 o 5 10 0 697.60 646.08 223.58 o 6 10 0 9465.96 10071.23 441.78 o 7 10 0 8108.76 8016.68 373.56 o 8 10 0 8179.18 7416.30 390.80 o 9 10 0 7590.48 7511.76 389.59 o 10 10 0 948.59 1072.56 320.40 o 11 10 0 409.44 38.06 441.90 o 1 11 0 127.01 0.00 394.79 o 2 11 0 13315.54 11806.14 636.16 o 3 11 0 393.77 509.64 418.12 o 4 11 0 2846.20 2605.64 435.17 o 5 11 0 1432.71 991.47 403.77 o -23 1 1 4838.37 4464.52 253.81 o -22 1 1 597.81 887.66 218.02 o -21 1 1 7318.45 6904.35 288.75 o -20 1 1 6.75 0.00 192.31 o -19 1 1 980.80 917.82 166.36 o -18 1 1 733.82 693.48 160.33 o -17 1 1 181.53 100.28 192.71 o -16 1 1 71.18 0.00 140.29 o -15 1 1 2466.24 2610.40 178.01 o -14 1 1 28553.46 28059.78 402.49 o -13 1 1 1919.33 1779.50 149.48 o -12 1 1 1142.84 1107.79 99.28 o -11 1 1 9218.94 9138.42 165.84 o -10 1 1 125.88 143.75 90.10 o -9 1 1 1281.23 1314.99 89.14 o -8 1 1 304.84 231.28 80.98 o -7 1 1 15780.61 15279.00 180.95 o -6 1 1 1658.87 1837.33 78.54 o -5 1 1 117.61 197.05 66.84 o -4 1 1 25092.33 26387.77 272.75 o -3 1 1 4186.11 4483.05 122.94 o -2 1 1 3647.35 3826.52 110.89 o -1 1 1 68.01 125.40 56.86 o 0 1 1 7236.13 7838.83 86.37 o 1 1 1 20.38 16.54 20.49 o 2 1 1 107.00 58.93 25.70 o 3 1 1 1416.72 1450.58 47.63 o 4 1 1 18488.28 18333.57 155.69 o 5 1 1 2940.48 2922.56 73.49 o 6 1 1 3370.50 3194.15 82.48 o 7 1 1 7392.94 6971.49 153.18 o 8 1 1 3440.61 3512.35 100.74 o 9 1 1 2038.50 2104.02 84.00 o 10 1 1 28675.99 27577.70 251.85 o 11 1 1 327.90 342.02 83.25 o 12 1 1 1565.65 1526.32 95.10 o 13 1 1 0.44 159.88 122.42 o 14 1 1 11.72 0.00 129.77 o 15 1 1 435.70 455.60 138.53 o 16 1 1 418.76 518.82 142.12 o 17 1 1 9556.12 9705.34 328.86 o 18 1 1 2862.58 3040.36 174.30 o 19 1 1 2837.52 2602.55 196.45 o 20 1 1 2032.44 1984.28 177.32 o 21 1 1 557.69 788.35 173.27 o 22 1 1 207.50 217.19 192.43 o 23 1 1 389.06 395.10 209.50 o -23 2 1 256.78 159.03 372.90 o -22 2 1 1392.66 1274.94 222.90 o -21 2 1 1926.11 2062.74 220.86 o -20 2 1 207.07 68.72 202.06 o -19 2 1 969.78 640.05 281.42 o -18 2 1 10094.64 10133.00 313.77 o -17 2 1 5199.35 5973.02 346.34 o -16 2 1 13925.76 14417.07 400.74 o -15 2 1 15.35 0.00 151.15 o -14 2 1 4587.74 4524.94 182.35 o -13 2 1 25.20 48.24 131.75 o -12 2 1 3063.24 2871.90 127.37 o -11 2 1 26556.10 26695.63 282.80 o -10 2 1 5942.11 6286.07 147.69 o -9 2 1 1239.94 1335.85 89.80 o -8 2 1 287.54 186.30 80.25 o -7 2 1 372.66 238.18 76.58 o -6 2 1 29948.64 30185.91 279.86 o -5 2 1 11914.89 13831.49 349.15 o -4 2 1 6959.65 7311.10 158.52 o -3 2 1 22739.45 23547.42 279.61 o -2 2 1 1923.56 2124.55 89.76 o -1 2 1 10947.90 11732.32 218.10 o 0 2 1 1086.44 1239.59 70.87 o 1 2 1 6636.34 6889.73 117.02 o 2 2 1 2586.00 2781.27 73.35 o 3 2 1 1780.68 1699.77 66.68 o 4 2 1 20098.03 18863.66 184.49 o 5 2 1 13297.89 12551.38 124.02 o 6 2 1 2502.59 2554.94 70.83 o 7 2 1 176.68 327.74 60.26 o 8 2 1 8900.67 8388.25 130.71 o 9 2 1 1232.53 1367.87 97.02 o 10 2 1 36137.30 35378.00 367.96 o 11 2 1 93.81 8.55 72.00 o 12 2 1 186.31 397.01 100.70 o 13 2 1 2118.06 1986.90 133.69 o 14 2 1 13912.72 13857.25 250.59 o 15 2 1 2772.48 2745.14 209.93 o 16 2 1 9649.82 9940.29 241.08 o 17 2 1 124.24 112.90 196.64 o 18 2 1 899.96 1104.22 165.60 o 19 2 1 27.34 11.44 160.77 o 20 2 1 6417.16 6626.88 372.34 o 21 2 1 182.04 172.28 197.07 o 22 2 1 6972.45 7107.37 344.26 o -22 3 1 4714.98 4630.00 338.98 o -21 3 1 3459.90 3409.87 381.80 o -20 3 1 2.92 0.00 204.42 o -19 3 1 5166.36 5016.58 413.64 o -18 3 1 2402.19 2701.23 250.90 o -17 3 1 468.99 651.48 219.15 o -16 3 1 2826.29 2896.15 466.58 o -15 3 1 63.36 238.08 212.23 o -14 3 1 2230.91 2126.28 163.33 o -13 3 1 9573.70 9764.59 247.01 o -12 3 1 288.03 108.81 132.81 o -11 3 1 3046.38 3194.91 123.26 o -10 3 1 2985.82 2898.22 105.73 o -9 3 1 22371.49 22774.68 283.96 o -8 3 1 49.36 0.00 96.83 o -7 3 1 3321.21 3348.26 119.99 o -6 3 1 723.41 884.80 96.11 o -5 3 1 160.42 304.23 103.09 o -4 3 1 1553.66 1757.74 99.68 o -3 3 1 64921.09 65758.59 605.67 o -2 3 1 377.89 334.13 73.30 o -1 3 1 29325.90 30149.57 314.65 o 0 3 1 2349.51 2608.59 96.96 o 1 3 1 3552.17 3541.97 142.07 o 2 3 1 718.59 639.63 82.53 o 3 3 1 21320.53 20044.35 232.28 o 4 3 1 270.56 191.92 72.64 o 5 3 1 34500.05 35405.75 315.03 o 6 3 1 4914.81 4777.74 121.90 o 7 3 1 21952.30 21757.51 222.39 o 8 3 1 15196.48 14773.49 209.01 o 9 3 1 786.68 854.97 87.82 o 10 3 1 437.60 576.86 77.71 o 11 3 1 445.32 203.37 123.63 o 12 3 1 1253.60 1264.50 138.72 o 13 3 1 3647.99 3596.98 164.38 o 14 3 1 1503.02 1639.70 154.80 o 15 3 1 3093.19 3130.29 165.88 o 16 3 1 127.47 183.35 151.03 o 17 3 1 3465.88 3860.27 211.43 o 18 3 1 74.85 226.39 156.95 o 19 3 1 25.73 17.89 185.26 o 20 3 1 2240.62 2388.54 219.26 o 21 3 1 2133.34 2354.41 217.39 o 22 3 1 346.32 186.34 215.46 o -22 4 1 7.32 0.00 322.35 o -21 4 1 6435.37 6529.79 290.81 o -20 4 1 18.65 276.63 264.19 o -19 4 1 712.23 1030.84 255.74 o -18 4 1 9413.73 8943.20 416.78 o -17 4 1 1.84 345.48 240.77 o -16 4 1 284.39 153.55 311.80 o -15 4 1 4552.49 4440.50 261.44 o -14 4 1 10994.71 10989.79 353.02 o -13 4 1 444.47 251.12 201.25 o -12 4 1 3634.22 3747.46 266.04 o -11 4 1 1295.42 1393.35 148.05 o -10 4 1 16994.41 17253.94 292.82 o -9 4 1 45599.11 46291.94 478.48 o -8 4 1 63730.46 64563.32 621.99 o -7 4 1 5675.88 5633.72 169.84 o -6 4 1 10233.56 10785.44 198.39 o -5 4 1 574.38 723.63 103.93 o -4 4 1 9222.39 9370.73 212.00 o -3 4 1 605.65 755.03 91.60 o -2 4 1 5178.55 5478.52 160.46 o -1 4 1 25.39 9.23 92.67 o 0 4 1 7520.48 8650.18 171.23 o 1 4 1 12110.73 12981.62 209.54 o 2 4 1 29772.26 31799.47 337.76 o 3 4 1 13288.10 13149.04 197.65 o 4 4 1 258.53 226.06 86.10 o 5 4 1 1236.35 1409.49 99.07 o 6 4 1 256.17 298.95 89.43 o 7 4 1 12089.36 11953.37 193.98 o 8 4 1 958.80 1025.88 88.68 o 9 4 1 7338.23 7135.32 333.44 o 10 4 1 718.92 973.54 170.03 o 11 4 1 23205.82 22580.74 413.49 o 12 4 1 45858.22 46778.41 688.98 o 13 4 1 6714.82 7017.63 304.17 o 14 4 1 6652.56 6556.57 288.34 o 15 4 1 4247.60 4688.22 244.12 o 16 4 1 1606.51 1600.09 193.62 o 17 4 1 286.96 518.60 190.80 o 18 4 1 2283.23 2753.95 216.45 o 19 4 1 301.23 58.10 201.25 o 20 4 1 2269.77 2447.59 228.03 o 21 4 1 679.94 567.47 217.14 o -21 5 1 13266.30 12915.16 460.93 o -20 5 1 5626.14 5815.45 347.51 o -19 5 1 5287.61 5546.75 325.25 o -18 5 1 1364.22 1456.66 404.22 o -17 5 1 12143.37 12966.94 420.23 o -16 5 1 11.27 93.67 236.91 o -15 5 1 9965.90 10158.32 384.14 o -14 5 1 1784.42 1749.03 232.85 o -13 5 1 7616.34 7330.94 321.76 o -12 5 1 20299.33 20552.62 759.98 o -11 5 1 631.31 404.14 212.65 o -10 5 1 25688.27 26442.19 394.99 o -9 5 1 1948.95 1924.82 163.94 o -8 5 1 13864.01 13952.42 247.52 o -7 5 1 1321.96 1424.23 125.08 o -6 5 1 270.07 135.63 109.33 o -5 5 1 1895.00 2047.29 114.42 o -4 5 1 8397.45 8277.48 217.61 o -3 5 1 3415.66 3553.89 119.04 o -2 5 1 96402.66 101137.66 921.36 o -1 5 1 217.17 244.35 102.66 o 0 5 1 94071.59 97247.61 886.14 o 1 5 1 2447.15 2425.87 183.64 o 2 5 1 15850.18 16297.36 242.00 o 3 5 1 5121.35 5225.93 168.00 o 4 5 1 64629.82 64101.84 613.64 o 5 5 1 188.69 177.98 103.10 o 6 5 1 48252.33 48294.93 488.30 o 7 5 1 29462.42 28650.31 332.64 o 8 5 1 507.86 370.81 125.27 o 9 5 1 263.91 353.10 137.77 o 10 5 1 2613.03 2572.12 166.17 o 11 5 1 1304.71 1134.54 228.80 o 12 5 1 11297.60 11287.38 341.63 o 13 5 1 3785.05 3787.67 229.99 o 14 5 1 9945.18 9867.22 337.71 o 15 5 1 449.24 601.20 216.71 o 16 5 1 9950.62 9937.85 361.15 o 17 5 1 3886.64 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