#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/73/2017386.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017386_Fobs loop_ _publ_author_name 'Churakov, Andrei V.' 'Lermontova, Elmira Kh.' 'Zaitsev, Kirill V.' 'Huang, Mengmeng' 'Karlov, Sergey S.' 'Zaitseva, Galina S.' 'Howard, Judith A. K.' _publ_section_title ; Crystal packing in the structures of diethanolamine derivatives ; _journal_coeditor_code GD3304 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o587 _journal_page_last o592 _journal_volume 65 _journal_year 2009 _space_group_IT_number 7 _symmetry_space_group_name_Hall 'P -2yc' _symmetry_space_group_name_H-M 'P 1 c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.444 _cell_angle_gamma 90.000 _cell_length_a 5.8366 _cell_length_b 15.3018 _cell_length_c 8.1078 _exptl_crystal_F_000 292.00 _reflns_d_resolution_high 0.7698 _[local]_cod_data_source_file gd3304Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' l in Pc' _shelx_refln_list_code 4 _shelx_f_calc_maximum 80.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2697.37 2504.70 106.30 o 2 0 0 2017.63 2027.75 32.42 o 3 0 0 1421.31 1438.97 31.60 o 4 0 0 301.12 322.52 5.06 o 5 0 0 9.85 10.00 0.63 o 6 0 0 30.91 31.74 1.44 o 7 0 0 95.09 85.08 4.26 o 1 1 0 196.20 189.17 3.52 o 2 1 0 89.37 92.20 2.08 o 3 1 0 228.74 222.32 2.68 o 4 1 0 20.90 21.53 0.83 o 5 1 0 35.74 37.78 1.04 o 6 1 0 31.64 33.48 1.30 o 7 1 0 6.12 7.96 1.07 o 0 2 0 1187.72 1098.89 19.06 o 1 2 0 2187.83 2087.06 47.42 o 2 2 0 732.41 768.54 9.71 o 3 2 0 97.07 108.80 1.71 o 4 2 0 13.11 14.34 0.49 o 5 2 0 4.74 4.54 0.45 o 6 2 0 162.59 160.81 2.76 o 7 2 0 0.55 1.32 0.91 o 0 3 0 35.57 29.16 0.76 o 1 3 0 648.33 646.73 13.18 o 2 3 0 567.04 572.78 8.64 o 3 3 0 293.73 310.73 4.19 o 4 3 0 5.56 4.95 0.41 o 5 3 0 89.11 94.90 1.56 o 6 3 0 133.85 135.96 2.46 o 7 3 0 14.52 13.22 1.28 o 0 4 0 395.68 368.67 6.55 o 1 4 0 565.72 559.22 6.37 o 2 4 0 204.77 197.29 2.94 o 3 4 0 502.13 560.30 7.27 o 4 4 0 15.26 14.88 0.62 o 5 4 0 103.72 107.79 2.60 o 6 4 0 2.61 2.08 0.55 o 7 4 0 8.12 7.85 3.03 o 0 5 0 134.44 124.91 2.50 o 1 5 0 117.77 117.53 1.51 o 2 5 0 10.03 8.92 0.38 o 3 5 0 82.13 87.20 2.19 o 4 5 0 71.72 76.36 1.45 o 5 5 0 204.92 204.83 3.66 o 6 5 0 38.11 37.52 1.15 o 7 5 0 15.55 16.38 1.12 o 0 6 0 1098.02 1039.09 18.01 o 1 6 0 152.08 150.07 1.74 o 2 6 0 183.14 206.52 2.97 o 3 6 0 210.80 200.15 2.89 o 4 6 0 119.34 120.55 2.02 o 5 6 0 58.83 59.72 1.66 o 6 6 0 1.48 0.74 0.54 o 7 6 0 24.69 25.97 1.29 o 0 7 0 38.27 44.33 1.29 o 1 7 0 618.35 667.67 7.00 o 2 7 0 121.37 127.58 1.74 o 3 7 0 92.80 92.52 1.57 o 4 7 0 294.87 295.66 4.21 o 5 7 0 71.42 73.56 1.88 o 6 7 0 87.24 86.44 1.90 o 7 7 0 29.94 34.75 1.52 o 0 8 0 318.83 347.41 6.45 o 1 8 0 7.63 8.27 0.40 o 2 8 0 185.90 183.01 2.37 o 3 8 0 8.07 7.55 0.47 o 4 8 0 62.53 62.54 1.34 o 5 8 0 12.43 15.36 1.03 o 6 8 0 17.04 18.66 0.90 o 0 9 0 368.93 398.41 7.39 o 1 9 0 18.91 22.90 0.68 o 2 9 0 28.73 29.15 0.65 o 3 9 0 113.07 120.18 1.78 o 4 9 0 90.91 88.54 2.49 o 5 9 0 85.17 89.17 2.64 o 6 9 0 17.18 17.76 1.31 o 0 10 0 46.79 41.66 1.45 o 1 10 0 40.96 44.96 1.00 o 2 10 0 37.41 38.75 1.09 o 3 10 0 60.80 59.83 1.26 o 4 10 0 51.92 53.84 1.52 o 5 10 0 6.85 6.61 0.89 o 6 10 0 1.15 1.59 0.94 o 0 11 0 152.01 139.71 3.19 o 1 11 0 246.32 245.42 3.52 o 2 11 0 123.25 121.50 2.36 o 3 11 0 164.69 165.28 2.76 o 4 11 0 217.29 216.56 3.99 o 5 11 0 25.05 26.57 1.21 o 6 11 0 36.86 42.34 1.58 o 0 12 0 11.76 13.69 0.96 o 1 12 0 36.17 34.05 1.07 o 2 12 0 19.52 20.18 0.91 o 3 12 0 20.51 18.27 0.90 o 4 12 0 7.63 9.17 2.59 o 5 12 0 1.29 1.98 0.96 o 6 12 0 0.91 0.38 1.98 o 0 13 0 55.75 49.40 1.73 o 1 13 0 136.58 130.66 2.23 o 2 13 0 66.39 61.41 1.58 o 3 13 0 88.22 87.00 2.60 o 4 13 0 53.02 54.49 1.99 o 5 13 0 51.53 53.95 2.16 o 0 14 0 2.09 2.48 0.99 o 1 14 0 87.70 88.11 1.75 o 2 14 0 33.35 31.08 1.21 o 3 14 0 66.90 61.97 2.59 o 4 14 0 15.29 14.44 1.26 o 5 14 0 21.73 20.57 1.46 o 0 15 0 69.30 58.83 1.94 o 1 15 0 117.62 108.32 2.04 o 2 15 0 68.32 66.69 1.76 o 3 15 0 27.81 32.04 1.53 o 4 15 0 23.42 23.48 1.64 o 0 16 0 22.53 26.74 1.31 o 1 16 0 26.43 24.57 1.52 o 2 16 0 70.24 72.19 3.33 o 3 16 0 20.64 19.57 1.36 o 4 16 0 47.08 52.80 2.16 o 0 17 0 9.44 13.92 1.11 o 1 17 0 67.39 72.52 1.71 o 2 17 0 17.89 19.86 1.33 o 3 17 0 19.10 20.57 1.40 o 0 18 0 108.41 114.29 3.25 o 1 18 0 8.66 11.79 0.95 o 2 18 0 3.31 3.75 1.03 o 3 18 0 30.10 34.10 2.16 o 0 19 0 0.04 2.19 0.96 o 1 19 0 9.33 9.64 0.91 o 2 19 0 21.08 26.37 2.32 o -7 1 1 24.64 23.39 1.64 o -6 1 1 128.15 117.00 3.05 o -5 1 1 69.87 66.14 3.49 o -4 1 1 142.62 141.62 6.61 o -3 1 1 353.99 399.47 7.06 o -2 1 1 5.89 5.57 0.39 o -1 1 1 2086.22 2019.96 86.04 o 0 1 1 684.28 672.56 10.69 o 1 1 1 5974.79 5653.74 82.71 o 2 1 1 477.69 509.67 5.79 o 3 1 1 1243.50 1337.76 16.57 o 4 1 1 15.22 17.51 0.45 o 5 1 1 2.93 3.81 0.41 o 6 1 1 13.60 10.82 1.07 o 7 1 1 0.78 2.02 0.89 o -7 2 1 23.67 25.32 1.29 o -6 2 1 37.16 38.46 0.99 o -5 2 1 106.41 98.72 1.83 o -4 2 1 33.99 31.56 0.83 o -3 2 1 125.94 139.20 3.10 o -2 2 1 305.92 310.78 8.90 o -1 2 1 1114.54 1145.38 28.98 o 0 2 1 105.94 107.96 1.24 o 1 2 1 302.81 302.29 6.14 o 2 2 1 88.31 91.38 1.38 o 3 2 1 136.77 138.52 2.04 o 4 2 1 129.50 134.54 2.11 o 5 2 1 7.88 8.88 0.65 o 6 2 1 91.64 96.13 3.61 o 7 2 1 21.71 23.23 2.41 o -7 3 1 11.01 13.07 1.06 o -6 3 1 31.39 30.22 4.51 o -5 3 1 68.26 65.88 1.26 o -4 3 1 221.31 221.11 3.20 o -3 3 1 106.26 104.40 2.66 o -2 3 1 521.12 515.33 15.72 o -1 3 1 696.06 710.86 16.00 o 0 3 1 1835.91 1723.20 38.94 o 1 3 1 304.83 293.23 3.82 o 2 3 1 295.01 297.92 3.93 o 3 3 1 50.57 49.99 0.96 o 4 3 1 53.86 58.02 1.16 o 5 3 1 27.40 27.67 0.86 o 6 3 1 21.36 25.94 1.16 o 7 3 1 21.10 20.28 2.97 o -7 4 1 7.41 7.81 0.76 o -6 4 1 1.19 1.50 0.50 o -5 4 1 90.44 84.59 1.49 o -4 4 1 65.26 63.26 1.15 o -3 4 1 27.40 25.85 0.96 o -2 4 1 63.29 73.21 2.78 o -1 4 1 910.32 877.23 10.75 o 0 4 1 472.02 457.41 10.30 o 1 4 1 539.81 513.88 5.87 o 2 4 1 39.55 39.49 0.75 o 3 4 1 99.41 88.15 1.45 o 4 4 1 86.62 90.87 1.59 o 5 4 1 46.50 44.94 1.37 o 6 4 1 125.24 125.09 2.77 o 7 4 1 39.88 46.39 2.10 o -7 5 1 8.09 8.38 1.33 o -6 5 1 65.54 59.56 1.85 o -5 5 1 46.47 47.36 1.07 o -4 5 1 231.46 233.14 3.44 o -3 5 1 69.00 71.44 1.79 o -2 5 1 20.84 23.70 1.39 o -1 5 1 1426.56 1451.29 17.64 o 0 5 1 70.62 72.17 2.46 o 1 5 1 34.16 34.23 0.68 o 2 5 1 122.89 126.01 1.85 o 3 5 1 31.24 31.81 0.74 o 4 5 1 32.65 37.36 0.90 o 5 5 1 92.96 85.40 2.02 o 6 5 1 96.77 94.04 2.29 o 7 5 1 30.09 30.99 3.55 o -7 6 1 45.74 49.87 1.49 o -6 6 1 4.41 5.29 0.62 o -5 6 1 435.08 420.84 5.26 o -4 6 1 352.63 353.78 4.96 o -3 6 1 71.46 74.34 1.64 o -2 6 1 946.59 967.28 16.36 o -1 6 1 879.37 911.07 11.24 o 0 6 1 914.66 904.71 17.73 o 1 6 1 45.49 43.43 1.01 o 2 6 1 275.47 294.38 5.11 o 3 6 1 13.38 14.82 0.93 o 4 6 1 127.63 126.05 2.06 o 5 6 1 175.61 173.77 3.41 o 6 6 1 57.54 57.85 1.46 o 7 6 1 21.58 22.39 1.85 o -7 7 1 19.97 21.85 1.05 o -6 7 1 28.66 26.02 1.01 o -5 7 1 15.24 15.65 0.75 o -4 7 1 33.26 31.30 1.13 o -3 7 1 95.68 93.15 1.81 o -2 7 1 141.14 152.21 2.58 o -1 7 1 86.12 89.27 1.46 o 0 7 1 50.44 56.18 1.80 o 1 7 1 71.94 73.85 1.43 o 2 7 1 43.47 38.51 0.73 o 3 7 1 171.82 160.42 2.40 o 4 7 1 35.18 32.07 1.09 o 5 7 1 40.08 38.15 1.32 o 6 7 1 1.83 2.36 0.73 o 7 7 1 33.77 35.53 1.92 o -6 8 1 156.29 154.16 2.83 o -5 8 1 13.02 15.13 0.77 o -4 8 1 90.52 87.44 1.99 o -3 8 1 622.91 621.23 8.15 o -2 8 1 459.85 467.17 6.10 o -1 8 1 50.51 48.98 1.00 o 0 8 1 282.69 303.81 5.59 o 1 8 1 694.72 691.61 14.19 o 2 8 1 49.04 44.24 0.83 o 3 8 1 349.37 340.01 4.20 o 4 8 1 158.23 156.30 2.99 o 5 8 1 17.25 14.94 0.87 o 6 8 1 58.03 62.57 1.85 o -6 9 1 55.45 56.17 1.74 o -5 9 1 11.47 11.78 0.98 o -4 9 1 36.46 38.27 1.51 o -3 9 1 81.78 79.63 1.48 o -2 9 1 243.93 240.78 4.77 o -1 9 1 145.49 142.24 2.19 o 0 9 1 621.63 633.45 10.77 o 1 9 1 255.47 253.72 7.02 o 2 9 1 161.09 157.88 3.07 o 3 9 1 352.79 347.24 4.31 o 4 9 1 81.91 78.51 1.87 o 5 9 1 29.14 29.84 1.44 o 6 9 1 7.58 8.52 1.09 o -6 10 1 1.92 2.78 0.79 o -5 10 1 29.43 33.59 1.55 o -4 10 1 26.21 26.19 0.89 o -3 10 1 370.01 352.94 6.27 o -2 10 1 166.75 160.81 2.47 o -1 10 1 1.47 2.91 0.46 o 0 10 1 5.81 7.29 0.49 o 1 10 1 0.51 1.16 0.46 o 2 10 1 62.92 60.02 1.27 o 3 10 1 288.18 278.34 4.75 o 4 10 1 92.46 94.25 2.17 o 5 10 1 27.00 30.06 1.46 o 6 10 1 1.05 1.36 1.00 o -6 11 1 0.63 2.49 1.32 o -5 11 1 30.61 28.51 1.26 o -4 11 1 19.38 19.27 1.01 o -3 11 1 0.07 0.63 0.46 o -2 11 1 61.97 59.40 1.47 o -1 11 1 151.91 155.44 2.46 o 0 11 1 61.33 67.98 1.34 o 1 11 1 8.38 8.38 0.51 o 2 11 1 27.43 28.93 0.98 o 3 11 1 35.67 34.45 1.15 o 4 11 1 5.52 6.77 0.71 o 5 11 1 2.92 2.88 0.74 o 6 11 1 2.43 3.60 0.87 o -6 12 1 13.10 14.19 1.61 o -5 12 1 31.00 31.02 1.55 o -4 12 1 70.55 76.83 2.40 o -3 12 1 399.46 383.53 9.05 o -2 12 1 311.19 319.16 5.16 o -1 12 1 112.77 114.40 2.02 o 0 12 1 130.64 130.47 2.17 o 1 12 1 106.60 93.78 1.85 o 2 12 1 56.96 61.11 1.51 o 3 12 1 102.12 102.17 2.82 o 4 12 1 24.34 25.37 1.46 o 5 12 1 20.04 20.13 1.39 o -5 13 1 0.68 2.08 0.99 o -4 13 1 18.71 16.94 1.70 o -3 13 1 32.77 30.24 1.20 o -2 13 1 127.33 114.91 2.38 o -1 13 1 161.69 152.19 2.52 o 0 13 1 321.68 301.91 4.31 o 1 13 1 108.68 106.63 1.93 o 2 13 1 26.43 27.48 1.20 o 3 13 1 116.71 113.18 3.18 o 4 13 1 9.48 9.56 1.03 o 5 13 1 1.48 2.14 1.07 o -5 14 1 1.14 1.83 1.03 o -4 14 1 18.86 22.17 1.38 o -3 14 1 64.96 68.65 1.81 o -2 14 1 206.92 209.90 4.19 o -1 14 1 112.31 109.74 2.03 o 0 14 1 53.70 50.50 1.25 o 1 14 1 197.05 195.28 4.79 o 2 14 1 263.03 249.56 5.46 o 3 14 1 25.53 27.12 1.38 o 4 14 1 12.81 14.18 1.18 o 5 14 1 4.25 2.84 1.07 o -4 15 1 4.68 4.43 0.98 o -3 15 1 11.23 11.72 0.91 o -2 15 1 18.66 20.31 0.95 o -1 15 1 25.67 24.09 0.90 o 0 15 1 17.19 17.16 0.81 o 1 15 1 59.43 61.55 1.71 o 2 15 1 91.75 91.37 2.73 o 3 15 1 30.26 33.31 1.85 o 4 15 1 11.59 12.36 2.16 o -4 16 1 10.47 11.32 1.33 o -3 16 1 3.30 3.99 1.20 o -2 16 1 29.39 34.15 1.74 o -1 16 1 2.23 2.96 0.93 o 0 16 1 7.87 7.38 1.05 o 1 16 1 16.39 13.42 0.89 o 2 16 1 1.89 0.63 1.45 o 3 16 1 18.87 22.29 1.42 o 4 16 1 54.76 60.58 2.31 o -3 17 1 2.50 2.83 0.93 o -2 17 1 17.12 18.55 1.15 o -1 17 1 13.48 14.03 1.00 o 0 17 1 22.38 21.71 0.95 o 1 17 1 10.08 9.70 0.98 o 2 17 1 9.60 8.99 1.09 o 3 17 1 34.77 38.25 1.81 o -3 18 1 19.09 17.30 1.31 o -2 18 1 21.49 23.21 1.15 o -1 18 1 3.44 4.31 0.68 o 0 18 1 32.77 33.80 1.14 o 1 18 1 4.61 3.93 0.95 o 2 18 1 10.28 11.48 2.44 o 3 18 1 26.81 30.86 1.73 o -2 19 1 39.08 48.59 2.07 o -1 19 1 12.24 11.91 0.85 o 0 19 1 40.49 51.33 1.44 o 1 19 1 28.03 26.65 1.73 o 2 19 1 1.52 1.84 1.04 o -7 0 2 14.29 12.97 2.04 o -6 0 2 56.14 51.31 1.89 o -5 0 2 764.91 725.91 18.10 o -4 0 2 25.05 30.21 1.95 o -3 0 2 115.90 109.03 4.23 o -2 0 2 366.60 338.76 13.50 o -1 0 2 4077.12 4161.75 153.20 o 0 0 2 6404.62 5961.39 259.56 o 1 0 2 2098.74 2068.17 36.60 o 2 0 2 679.46 709.66 19.46 o 3 0 2 6.59 7.44 0.51 o 4 0 2 571.04 613.24 11.31 o 5 0 2 39.13 37.94 2.29 o 6 0 2 28.94 27.74 2.22 o 7 0 2 15.05 17.36 1.98 o -7 1 2 6.76 7.46 0.73 o -6 1 2 4.91 4.84 0.63 o -5 1 2 101.99 96.25 2.03 o -4 1 2 29.06 26.94 0.88 o -3 1 2 120.51 115.81 2.04 o -2 1 2 146.18 140.95 2.46 o -1 1 2 838.91 804.75 21.32 o 0 1 2 638.73 651.98 7.40 o 1 1 2 2287.54 2219.45 32.54 o 2 1 2 518.45 521.50 7.94 o 3 1 2 4.86 6.44 0.38 o 4 1 2 197.37 196.30 2.89 o 5 1 2 58.02 58.97 2.07 o 6 1 2 1.66 2.21 0.85 o 7 1 2 29.45 34.11 1.83 o -7 2 2 60.07 65.50 1.67 o -6 2 2 10.15 10.51 0.60 o -5 2 2 119.55 111.09 3.64 o -4 2 2 126.37 121.07 2.25 o -3 2 2 16.14 20.61 0.70 o -2 2 2 664.85 694.02 18.92 o -1 2 2 1304.36 1296.39 13.19 o 0 2 2 362.83 369.97 4.28 o 1 2 2 1654.15 1606.10 53.63 o 2 2 2 587.59 612.08 9.27 o 3 2 2 243.62 272.56 7.07 o 4 2 2 77.28 82.79 1.43 o 5 2 2 47.85 38.29 1.24 o 6 2 2 25.63 21.03 1.35 o 7 2 2 18.19 19.47 2.29 o -7 3 2 56.51 56.66 1.56 o -6 3 2 20.29 19.66 0.74 o -5 3 2 70.84 64.36 3.29 o -4 3 2 524.33 511.50 9.99 o -3 3 2 132.64 129.17 2.26 o -2 3 2 462.49 480.34 6.91 o -1 3 2 921.21 953.79 11.83 o 0 3 2 1284.44 1287.29 33.22 o 1 3 2 368.53 373.05 8.17 o 2 3 2 144.13 148.17 2.56 o 3 3 2 0.07 0.51 0.35 o 4 3 2 10.79 11.91 1.09 o 5 3 2 97.17 98.65 2.18 o 6 3 2 6.02 5.32 1.24 o 7 3 2 73.12 75.31 2.80 o -7 4 2 6.33 6.11 0.71 o -6 4 2 58.72 60.46 1.33 o -5 4 2 4.16 5.46 0.55 o -4 4 2 167.90 168.75 2.93 o -3 4 2 479.96 498.20 7.30 o -2 4 2 723.21 759.41 14.33 o -1 4 2 82.89 87.62 1.21 o 0 4 2 75.48 70.30 1.02 o 1 4 2 616.74 610.81 7.89 o 2 4 2 135.68 159.24 3.24 o 3 4 2 99.49 99.98 1.96 o 4 4 2 177.42 168.76 3.10 o 5 4 2 35.39 31.96 1.12 o 6 4 2 29.75 30.57 1.79 o 7 4 2 40.84 42.68 2.03 o -7 5 2 33.18 35.28 2.52 o -6 5 2 10.07 11.14 0.72 o -5 5 2 28.37 30.71 0.96 o -4 5 2 179.91 163.20 4.92 o -3 5 2 76.85 78.78 2.84 o -2 5 2 201.94 214.66 10.26 o -1 5 2 101.21 116.44 1.72 o 0 5 2 209.14 195.81 4.23 o 1 5 2 24.16 29.91 0.58 o 2 5 2 187.98 194.10 4.81 o 3 5 2 64.76 60.27 1.40 o 4 5 2 214.65 205.21 3.67 o 5 5 2 41.30 41.60 1.33 o 6 5 2 35.89 32.36 1.66 o 7 5 2 16.05 14.57 1.54 o -7 6 2 9.07 11.46 0.87 o -6 6 2 39.61 39.39 1.07 o -5 6 2 123.72 121.51 1.97 o -4 6 2 46.37 45.91 1.54 o -3 6 2 32.85 26.81 1.17 o -2 6 2 123.16 148.16 2.48 o -1 6 2 197.43 205.31 4.91 o 0 6 2 503.07 487.57 9.25 o 1 6 2 14.77 15.19 0.57 o 2 6 2 128.28 129.95 3.26 o 3 6 2 180.28 171.46 3.07 o 4 6 2 124.43 113.12 2.32 o 5 6 2 85.51 79.70 1.96 o 6 6 2 40.52 41.37 2.75 o 7 6 2 6.69 8.75 1.18 o -6 7 2 17.12 17.47 0.80 o -5 7 2 20.61 24.49 0.80 o -4 7 2 364.47 348.90 6.66 o -3 7 2 51.82 47.71 1.50 o -2 7 2 59.19 55.94 1.24 o -1 7 2 602.55 625.42 15.08 o 0 7 2 67.45 69.45 0.98 o 1 7 2 207.18 228.23 3.99 o 2 7 2 33.73 37.91 0.74 o 3 7 2 16.01 17.38 0.74 o 4 7 2 35.84 32.04 1.10 o 5 7 2 92.66 89.82 2.13 o 6 7 2 43.47 42.44 1.49 o -6 8 2 35.69 35.61 1.55 o -5 8 2 42.79 43.28 1.08 o -4 8 2 58.42 59.96 1.58 o -3 8 2 110.95 117.18 2.22 o -2 8 2 4.02 5.05 0.49 o -1 8 2 23.01 26.38 1.11 o 0 8 2 51.77 46.63 0.76 o 1 8 2 97.73 94.14 2.00 o 2 8 2 35.25 33.21 0.95 o 3 8 2 12.42 12.48 0.62 o 4 8 2 271.47 264.53 4.64 o 5 8 2 25.25 27.74 1.13 o 6 8 2 14.43 16.56 2.45 o -6 9 2 13.80 15.71 1.02 o -5 9 2 51.87 50.91 1.53 o -4 9 2 37.49 31.94 2.10 o -3 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