#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/74/2017428.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017428_Fobs loop_ _publ_author_name 'Hendsbee, Arthur D.' 'Masuda, Jason D.' 'Pi\'orko, Adam' _publ_section_title ; (\h^5^-Cyclopentadienyl)[(1,2,3,4,4a,10a-\h)-1-methylthianthrene]iron(II) hexafluoridophosphate acetone 0.33-solvate ; _journal_coeditor_code FN3032 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m466 _journal_page_last m468 _journal_volume 65 _journal_year 2009 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 83.508 _cell_angle_beta 75.251 _cell_angle_gamma 84.088 _cell_length_a 10.5598 _cell_length_b 15.4984 _cell_length_c 19.4769 _exptl_crystal_F_000 1564.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file fn3032Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' AP03_0m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 307.57 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1610.91 1247.49 29.20 o 2 0 0 78945.88 81772.69 767.68 o 3 0 0 13156.01 13684.79 118.67 o 4 0 0 762.84 613.81 32.19 o 5 0 0 708.42 592.63 34.90 o 6 0 0 154.80 84.52 31.56 o 7 0 0 3.69 29.92 42.34 o 8 0 0 1436.95 1339.94 75.08 o 9 0 0 7.63 -17.76 48.07 o 10 0 0 434.56 255.51 103.72 o 11 0 0 10.85 45.21 54.36 o 12 0 0 7.68 -57.30 55.86 o -12 1 0 542.94 536.18 76.04 o -11 1 0 310.85 306.59 65.83 o -10 1 0 1283.04 1233.61 84.22 o -9 1 0 0.45 48.45 67.28 o -8 1 0 1809.43 2039.64 92.13 o -7 1 0 24.15 -5.77 49.56 o -6 1 0 59.31 28.39 36.98 o -5 1 0 2917.81 3264.39 78.26 o -4 1 0 1278.67 1266.18 74.11 o -3 1 0 686.86 557.30 33.97 o -2 1 0 2356.37 2294.91 43.63 o -1 1 0 2184.00 2481.88 33.49 o 2 1 0 36819.41 37229.82 215.97 o 3 1 0 12164.29 13819.94 99.81 o 4 1 0 283.14 444.18 28.09 o 5 1 0 3009.36 3303.88 76.96 o 6 1 0 76.52 44.76 29.17 o 7 1 0 5178.43 4541.34 113.40 o 8 1 0 1038.69 1147.54 70.13 o 9 1 0 461.40 429.71 60.03 o 10 1 0 670.13 962.94 165.89 o 11 1 0 902.69 775.89 131.59 o 12 1 0 93.28 7.08 81.48 o -11 2 0 110.99 131.91 121.09 o -10 2 0 0.03 -44.79 51.54 o -9 2 0 536.40 528.49 64.68 o -8 2 0 270.10 414.68 81.47 o -7 2 0 208.99 90.93 48.07 o -6 2 0 1223.09 978.64 58.75 o -5 2 0 4289.09 3632.72 84.15 o -4 2 0 4484.23 4255.07 81.39 o -3 2 0 2385.41 1970.97 58.37 o -2 2 0 11494.30 11240.03 119.61 o -1 2 0 16084.21 17598.07 126.40 o 0 2 0 4220.85 4553.37 39.41 o 2 2 0 2856.46 3424.48 35.62 o 3 2 0 5056.98 5175.17 53.40 o 4 2 0 233.07 353.24 21.36 o 5 2 0 860.74 1054.51 45.55 o 6 2 0 174.28 192.34 32.33 o 7 2 0 14690.27 14526.68 160.44 o 8 2 0 708.30 518.99 57.80 o 9 2 0 1576.89 1619.36 82.07 o 10 2 0 106.65 85.81 52.52 o 11 2 0 562.17 478.70 93.94 o 12 2 0 15.41 -8.02 79.64 o -11 3 0 381.71 406.17 72.32 o -10 3 0 62.71 -6.13 53.40 o -9 3 0 291.09 375.15 62.67 o -8 3 0 197.03 176.75 56.94 o -7 3 0 2.56 -8.87 46.64 o -6 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8359.54 104.91 o 4 4 0 5699.50 4891.06 65.78 o 5 4 0 684.23 926.33 33.80 o 6 4 0 9192.93 8791.59 94.45 o 7 4 0 2747.60 2863.52 96.40 o 8 4 0 370.47 382.17 51.61 o 9 4 0 152.24 205.40 70.49 o 10 4 0 291.58 238.04 78.38 o 11 4 0 5.94 -98.02 65.35 o 12 4 0 16.63 -26.31 79.60 o -11 5 0 199.63 302.08 68.67 o -10 5 0 807.19 814.62 80.56 o -9 5 0 2150.30 2162.54 104.92 o -8 5 0 143.49 114.20 68.13 o -7 5 0 1514.60 1472.60 118.38 o -6 5 0 1734.08 1875.33 86.53 o -5 5 0 1527.76 1271.85 48.30 o -4 5 0 3825.88 3750.10 53.84 o -3 5 0 1498.88 1158.64 33.24 o -2 5 0 1986.40 2143.09 46.75 o -1 5 0 1522.19 1910.23 38.82 o 0 5 0 751.32 993.41 29.45 o 1 5 0 2828.18 2360.01 90.68 o 2 5 0 2024.46 1949.78 61.99 o 3 5 0 5496.77 5354.85 81.09 o 4 5 0 39.20 102.60 17.78 o 5 5 0 5384.80 5148.80 66.91 o 6 5 0 3257.31 3047.35 57.61 o 7 5 0 2254.82 2043.13 62.26 o 8 5 0 227.01 268.01 55.33 o 9 5 0 21.89 -88.18 59.08 o 10 5 0 35.14 -42.68 65.62 o 11 5 0 275.87 319.41 85.24 o -11 6 0 18.09 56.09 60.42 o -10 6 0 29.24 -32.84 55.91 o -9 6 0 628.01 690.63 73.46 o -8 6 0 21.12 -30.78 56.24 o -7 6 0 384.33 323.29 38.35 o -6 6 0 110.35 56.92 30.44 o -5 6 0 269.19 356.50 29.13 o -4 6 0 1577.72 1177.28 37.40 o -3 6 0 518.87 575.64 32.87 o -2 6 0 3965.98 3941.62 54.29 o -1 6 0 11768.92 10940.77 93.67 o 0 6 0 6402.64 5927.01 63.11 o 1 6 0 11438.96 12060.23 150.35 o 2 6 0 5790.16 6359.14 170.68 o 3 6 0 9989.04 10175.54 142.38 o 4 6 0 90.80 68.28 17.52 o 5 6 0 46.79 100.28 22.16 o 6 6 0 257.57 229.62 28.63 o 7 6 0 1565.28 1574.64 64.90 o 8 6 0 298.07 219.61 42.92 o 9 6 0 46.78 26.89 60.86 o 10 6 0 162.39 185.47 76.60 o 11 6 0 3.37 -71.22 71.29 o -10 7 0 172.75 231.46 94.54 o -9 7 0 664.31 821.78 78.64 o -8 7 0 16.69 -27.56 47.59 o -7 7 0 2238.80 2055.85 67.17 o -6 7 0 222.41 244.08 37.36 o -5 7 0 55.76 37.40 26.55 o -4 7 0 57.70 0.00 23.54 o -3 7 0 241.15 244.51 25.29 o -2 7 0 1039.19 910.95 32.92 o -1 7 0 83.17 64.19 26.25 o 0 7 0 120.95 182.34 23.75 o 1 7 0 18.03 12.26 38.42 o 2 7 0 447.65 497.89 46.09 o 3 7 0 0.99 -47.48 31.66 o 4 7 0 1010.71 997.38 58.74 o 5 7 0 364.67 401.58 48.89 o 6 7 0 147.91 171.40 36.18 o 7 7 0 19.86 19.68 35.30 o 8 7 0 668.58 900.58 65.26 o 9 7 0 145.29 238.03 48.00 o 10 7 0 636.85 672.46 90.57 o 11 7 0 246.21 309.51 86.82 o -10 8 0 33.63 48.78 59.32 o -9 8 0 8.23 3.00 53.88 o -8 8 0 14.47 13.45 51.85 o -7 8 0 138.27 143.80 54.28 o -6 8 0 496.98 558.19 45.10 o -5 8 0 9.31 -5.35 28.08 o -4 8 0 398.97 486.24 37.87 o -3 8 0 4154.28 3906.91 78.35 o -2 8 0 1566.82 1497.19 44.84 o -1 8 0 343.51 250.34 25.48 o 0 8 0 5255.66 4842.04 76.99 o 1 8 0 6908.18 6265.86 242.06 o 2 8 0 15562.92 13799.45 184.98 o 3 8 0 2836.48 2508.33 135.12 o 4 8 0 5990.34 6051.37 124.46 o 5 8 0 1.61 14.40 29.68 o 6 8 0 3131.37 3023.91 75.66 o 7 8 0 9.00 -33.96 33.91 o 8 8 0 166.86 196.07 42.24 o 9 8 0 18.51 46.05 43.10 o 10 8 0 856.22 917.20 99.28 o 11 8 0 133.27 104.79 79.88 o -10 9 0 231.28 305.74 68.11 o -9 9 0 91.48 93.46 92.22 o -8 9 0 456.23 313.56 63.92 o -7 9 0 109.85 151.07 55.04 o 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1065.73 57.26 o 8 10 0 937.34 1053.18 60.51 o 9 10 0 430.31 444.37 52.37 o 10 10 0 234.38 287.19 77.00 o -9 11 0 54.90 94.08 61.62 o -8 11 0 527.55 615.31 73.74 o -7 11 0 282.16 331.73 76.47 o -6 11 0 43.52 86.48 51.28 o -5 11 0 149.25 190.23 52.17 o -4 11 0 3.63 -47.21 31.48 o -3 11 0 640.01 612.45 42.85 o -2 11 0 1100.56 1298.12 50.15 o -1 11 0 649.17 750.09 42.42 o 0 11 0 2031.78 2154.78 70.28 o 1 11 0 1806.66 1335.34 79.08 o 2 11 0 832.34 882.13 75.31 o 3 11 0 2756.19 2966.92 109.74 o 4 11 0 1440.58 1299.48 82.92 o 5 11 0 1011.12 1130.07 81.22 o 6 11 0 619.67 686.61 49.45 o 7 11 0 78.42 90.22 36.13 o 8 11 0 1412.16 1345.17 66.71 o 9 11 0 53.81 -37.76 39.52 o 10 11 0 139.23 175.69 52.63 o -8 12 0 550.63 553.85 75.68 o -7 12 0 20.13 -48.97 49.94 o -6 12 0 590.62 702.13 99.70 o -5 12 0 56.54 31.45 48.23 o -4 12 0 217.81 183.92 37.35 o -3 12 0 23.43 36.75 34.24 o -2 12 0 357.41 469.91 41.49 o -1 12 0 743.78 767.11 53.66 o 0 12 0 1518.76 1903.59 96.82 o 1 12 0 785.47 817.37 75.17 o 2 12 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