#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/74/2017433.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017433_Fobs loop_ _publ_author_name 'Goodreid, Jordan D.' 'Jennings, Michael C.' 'Tam, William' _publ_section_title ; Asymmetric ruthenium-catalysed [2+2] cycloadditions between bicyclic alkenes and chiral aryl-substituted acetylenic acyl camphorsultam alkynes ; _journal_coeditor_code GA3134 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o649 _journal_page_last o652 _journal_volume 65 _journal_year 2009 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.6868 _cell_length_b 12.8492 _cell_length_c 31.5467 _exptl_crystal_F_000 1936.00 _reflns_d_resolution_high 0.8000 _[local]_cod_data_source_file ga3134VIIsup3.hkl _[local]_cod_data_source_block VII #BEGIN Tags that were not found in dictionaries: _shelx_title ' N09023 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 213.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 7898.76 8478.21 143.99 o 6 0 0 961.79 1050.16 27.31 o 8 0 0 1256.16 1442.41 47.17 o 10 0 0 1398.70 1348.07 89.38 o 12 0 0 169.40 203.58 37.24 o 14 0 0 238.61 273.09 42.20 o 2 1 0 45059.14 41249.05 662.86 o 3 1 0 7998.81 7435.50 96.82 o 4 1 0 2837.17 2758.21 39.72 o 5 1 0 656.87 640.52 14.90 o 6 1 0 610.31 754.72 17.38 o 7 1 0 853.50 836.65 17.38 o 8 1 0 462.49 464.25 14.90 o 9 1 0 354.09 382.33 17.38 o 10 1 0 108.30 109.24 17.38 o 11 1 0 120.93 143.99 22.34 o 12 1 0 345.62 359.98 29.79 o 13 1 0 472.94 479.15 29.79 o 14 1 0 99.25 139.03 39.72 o 0 2 0 27748.65 24674.95 777.07 o 1 2 0 1661.38 1405.17 24.83 o 2 2 0 5036.15 4528.33 69.51 o 3 2 0 4212.53 4424.06 54.62 o 4 2 0 128.06 146.48 7.45 o 5 2 0 1.54 -9.93 9.93 o 6 2 0 410.38 384.81 12.41 o 7 2 0 3.16 12.41 7.45 o 8 2 0 298.69 280.54 14.90 o 9 2 0 1097.37 1084.91 32.27 o 10 2 0 30.00 12.41 17.38 o 11 2 0 797.12 829.20 39.72 o 12 2 0 80.55 84.41 24.83 o 13 2 0 2.03 24.83 37.24 o 14 2 0 167.44 126.61 29.79 o 1 3 0 14908.19 13589.97 223.44 o 2 3 0 15.72 9.93 2.48 o 3 3 0 2667.46 2718.49 42.20 o 4 3 0 3979.88 4553.16 69.51 o 5 3 0 9355.13 9928.07 151.44 o 6 3 0 949.95 908.65 22.34 o 7 3 0 105.30 109.24 9.93 o 8 3 0 91.86 89.38 12.41 o 9 3 0 0.40 0.00 12.41 o 10 3 0 74.30 54.62 19.86 o 11 3 0 77.25 81.93 22.34 o 12 3 0 59.94 44.69 22.34 o 13 3 0 486.50 461.77 34.76 o 14 3 0 58.40 86.89 47.17 o 0 4 0 10251.90 10178.82 198.61 o 1 4 0 249.16 258.19 9.93 o 2 4 0 218.01 218.47 7.45 o 3 4 0 7900.98 7713.56 116.68 o 4 4 0 1731.48 1722.95 27.31 o 5 4 0 207.81 230.89 9.93 o 6 4 0 69.35 72.00 4.97 o 7 4 0 3763.66 3994.57 74.48 o 8 4 0 523.19 551.15 22.34 o 9 4 0 270.29 258.19 19.86 o 10 4 0 2297.74 2274.10 62.07 o 11 4 0 133.53 136.55 34.76 o 12 4 0 16.47 29.79 27.31 o 13 4 0 38.21 37.24 54.62 o 14 4 0 69.00 106.75 47.17 o 1 5 0 2350.16 2497.54 47.17 o 2 5 0 206.74 166.34 9.93 o 3 5 0 1162.87 1370.42 24.83 o 4 5 0 12.25 12.41 7.45 o 5 5 0 5269.92 5705.11 76.96 o 6 5 0 907.85 839.13 19.86 o 7 5 0 576.18 613.21 22.34 o 8 5 0 101.10 86.89 17.38 o 9 5 0 1311.66 1142.01 42.20 o 10 5 0 179.22 178.75 27.31 o 11 5 0 979.21 1067.53 49.65 o 12 5 0 85.55 79.44 37.24 o 13 5 0 95.55 2.48 42.20 o 0 6 0 25.80 19.86 12.41 o 1 6 0 0.03 12.41 7.45 o 2 6 0 3.76 7.45 7.45 o 3 6 0 7092.97 7301.44 114.20 o 4 6 0 2375.06 2673.80 49.65 o 5 6 0 2640.57 2651.46 44.69 o 6 6 0 328.67 379.84 19.86 o 7 6 0 283.00 218.47 17.38 o 8 6 0 178.15 196.13 19.86 o 9 6 0 807.39 680.24 32.27 o 10 6 0 475.61 546.18 32.27 o 11 6 0 71.42 79.44 32.27 o 12 6 0 9.67 17.38 72.00 o 13 6 0 281.79 345.09 57.10 o 1 7 0 3041.46 3393.77 59.58 o 2 7 0 219.49 211.02 12.41 o 3 7 0 652.97 710.03 19.86 o 4 7 0 452.75 431.98 19.86 o 5 7 0 486.81 511.42 17.38 o 6 7 0 164.59 163.85 19.86 o 7 7 0 324.81 374.88 27.31 o 8 7 0 78.04 62.07 32.27 o 9 7 0 416.56 484.11 32.27 o 10 7 0 13.14 7.45 22.34 o 11 7 0 46.63 49.65 34.76 o 12 7 0 40.25 79.44 37.24 o 13 7 0 167.99 230.89 44.69 o 0 8 0 0.25 0.00 17.38 o 1 8 0 244.14 240.82 14.90 o 2 8 0 17.77 29.79 9.93 o 3 8 0 589.52 583.42 17.38 o 4 8 0 1955.05 1869.43 44.69 o 5 8 0 136.41 106.75 17.38 o 6 8 0 746.67 719.97 34.76 o 7 8 0 1809.90 1837.15 74.48 o 8 8 0 443.64 377.36 44.69 o 9 8 0 1.56 34.76 22.34 o 10 8 0 121.45 72.00 29.79 o 11 8 0 102.94 158.89 47.17 o 12 8 0 45.91 76.96 47.17 o 1 9 0 302.62 292.95 22.34 o 2 9 0 1.94 4.97 12.41 o 3 9 0 405.01 374.88 17.38 o 4 9 0 318.77 320.26 22.34 o 5 9 0 100.35 86.89 17.38 o 6 9 0 614.61 583.42 29.79 o 7 9 0 10.72 14.90 27.31 o 8 9 0 11.38 34.76 27.31 o 9 9 0 581.90 573.49 42.20 o 10 9 0 66.23 72.00 24.83 o 11 9 0 19.48 59.58 44.69 o 12 9 0 121.28 106.75 52.14 o 0 10 0 2223.23 2326.23 81.93 o 1 10 0 630.35 583.42 34.76 o 2 10 0 0.04 7.45 14.90 o 3 10 0 807.50 799.41 34.76 o 4 10 0 2021.12 1906.67 57.10 o 5 10 0 1.52 -9.93 19.86 o 6 10 0 326.54 347.57 37.24 o 7 10 0 52.09 69.51 27.31 o 8 10 0 116.88 183.72 32.27 o 9 10 0 104.36 54.62 39.72 o 10 10 0 55.25 67.03 37.24 o 11 10 0 128.70 84.41 44.69 o 1 11 0 1089.91 881.34 47.17 o 2 11 0 110.09 91.86 24.83 o 3 11 0 100.99 131.58 24.83 o 4 11 0 39.98 7.45 17.38 o 5 11 0 2.20 4.97 24.83 o 6 11 0 0.22 9.93 22.34 o 7 11 0 137.38 89.38 34.76 o 8 11 0 130.22 121.65 37.24 o 9 11 0 81.94 96.82 34.76 o 10 11 0 8.33 -32.27 34.76 o 0 12 0 304.23 233.37 54.62 o 1 12 0 254.33 245.78 39.72 o 2 12 0 379.11 359.98 37.24 o 3 12 0 382.27 332.67 34.76 o 4 12 0 388.47 352.53 24.83 o 5 12 0 22.89 -2.48 24.83 o 6 12 0 46.54 54.62 39.72 o 7 12 0 0.00 4.97 27.31 o 8 12 0 34.06 111.72 44.69 o 9 12 0 39.24 39.72 39.72 o 1 13 0 178.10 213.51 39.72 o 2 13 0 54.31 76.96 37.24 o 3 13 0 74.10 111.72 29.79 o 4 13 0 831.98 881.34 62.07 o 5 13 0 1.72 32.27 27.31 o 6 13 0 751.70 819.27 62.07 o 7 13 0 325.44 332.67 52.14 o 8 13 0 190.06 240.82 42.20 o 0 14 0 542.01 538.73 67.03 o 1 14 0 41.27 114.20 34.76 o 2 14 0 148.08 89.38 32.27 o 3 14 0 186.84 213.51 34.76 o 4 14 0 39.46 12.41 49.65 o 5 14 0 204.88 238.33 57.10 o 6 14 0 74.97 47.17 37.24 o 7 14 0 123.19 136.55 67.03 o 1 15 0 501.48 573.49 49.65 o 2 15 0 48.55 24.83 54.62 o 3 15 0 52.08 27.31 29.79 o 4 15 0 367.87 345.09 57.10 o 5 15 0 0.75 12.41 54.62 o 0 16 0 366.59 248.26 99.31 o 1 16 0 62.57 67.03 47.17 o 2 0 1 24305.11 21949.01 315.30 o 3 0 1 2573.29 2192.17 29.79 o 4 0 1 23.42 32.27 4.97 o 5 0 1 184.58 198.61 7.45 o 6 0 1 0.30 4.97 4.97 o 7 0 1 762.21 732.38 17.38 o 8 0 1 11714.97 11966.32 188.68 o 9 0 1 1103.68 1127.12 29.79 o 10 0 1 564.99 536.25 24.83 o 11 0 1 2.00 0.00 17.38 o 12 0 1 22.02 27.31 22.34 o 13 0 1 139.11 121.65 29.79 o 14 0 1 4.60 -9.93 27.31 o -14 1 1 15.62 27.31 47.17 o -13 1 1 214.36 171.30 32.27 o -12 1 1 60.57 44.69 24.83 o -11 1 1 2862.76 3031.30 67.03 o -10 1 1 1264.77 1308.35 34.76 o -9 1 1 97.44 86.89 12.41 o -8 1 1 338.67 305.36 12.41 o -7 1 1 1698.42 1767.64 29.79 o -6 1 1 1413.60 1454.83 27.31 o -5 1 1 3479.66 3344.11 49.65 o -4 1 1 1711.42 1792.47 29.79 o -3 1 1 362.07 312.81 7.45 o -2 1 1 1140.30 1007.95 14.90 o 2 1 1 1122.58 935.96 14.90 o 3 1 1 353.49 320.26 7.45 o 4 1 1 1760.19 1812.33 34.76 o 5 1 1 3494.75 3237.36 44.69 o 6 1 1 1425.67 1449.86 24.83 o 7 1 1 1711.42 1797.43 37.24 o 8 1 1 341.66 362.47 17.38 o 9 1 1 99.88 79.44 12.41 o 10 1 1 1277.91 1308.35 34.76 o 11 1 1 2835.00 2909.65 74.48 o 12 1 1 65.06 27.31 19.86 o 13 1 1 216.91 111.72 32.27 o 14 1 1 14.94 12.41 27.31 o -14 2 1 12.36 14.90 27.31 o -13 2 1 741.75 762.17 44.69 o -12 2 1 215.17 203.58 32.27 o -11 2 1 75.04 74.48 24.83 o -10 2 1 587.53 595.83 24.83 o -9 2 1 354.34 312.81 24.83 o -8 2 1 267.77 263.16 14.90 o -7 2 1 104.55 91.86 9.93 o -6 2 1 605.35 580.94 19.86 o -5 2 1 615.83 655.42 14.90 o -4 2 1 5506.07 5518.91 74.48 o -3 2 1 4025.55 3694.17 47.17 o -2 2 1 757.63 757.21 12.41 o -1 2 1 9620.22 8714.06 143.99 o 0 2 1 7810.88 7311.37 99.31 o 1 2 1 9692.82 8701.65 111.72 o 2 2 1 776.80 796.93 12.41 o 3 2 1 4015.64 3659.41 54.62 o 4 2 1 5531.53 5265.68 84.41 o 5 2 1 648.26 732.38 14.90 o 6 2 1 608.21 593.35 14.90 o 7 2 1 103.73 81.93 7.45 o 8 2 1 271.61 275.57 12.41 o 9 2 1 352.21 330.19 19.86 o 10 2 1 591.05 580.94 27.31 o 11 2 1 74.12 49.65 24.83 o 12 2 1 218.26 211.02 24.83 o 13 2 1 733.52 787.00 47.17 o 14 2 1 13.91 27.31 34.76 o -14 3 1 91.30 104.27 37.24 o -13 3 1 107.40 94.34 27.31 o -12 3 1 76.80 101.79 27.31 o -11 3 1 535.18 533.77 27.31 o -10 3 1 1224.42 1251.25 42.20 o -9 3 1 83.55 86.89 14.90 o -8 3 1 205.55 198.61 19.86 o -7 3 1 368.30 364.95 17.38 o -6 3 1 1886.56 1814.81 29.79 o -5 3 1 5402.17 5722.48 79.44 o -4 3 1 834.79 873.89 19.86 o -3 3 1 175.03 178.75 7.45 o -2 3 1 678.68 608.25 12.41 o -1 3 1 6744.84 6320.80 86.89 o 0 3 1 2588.46 2522.36 44.69 o 1 3 1 6823.37 6286.04 124.13 o 2 3 1 684.35 625.63 14.90 o 3 3 1 154.70 158.89 7.45 o 4 3 1 818.08 824.24 19.86 o 5 3 1 5490.99 5841.65 84.41 o 6 3 1 1866.71 1824.74 39.72 o 7 3 1 384.58 374.88 14.90 o 8 3 1 206.33 188.68 12.41 o 9 3 1 77.05 91.86 17.38 o 10 3 1 1229.55 1283.52 39.72 o 11 3 1 523.53 556.11 34.76 o 12 3 1 72.18 104.27 27.31 o 13 3 1 109.35 119.17 37.24 o 14 3 1 93.00 84.41 42.20 o -14 4 1 54.95 54.62 39.72 o -13 4 1 36.67 52.14 32.27 o -12 4 1 287.27 275.57 37.24 o -11 4 1 323.13 322.74 42.20 o -10 4 1 585.26 543.70 37.24 o -9 4 1 202.11 213.51 19.86 o -8 4 1 1512.54 1645.99 49.65 o -7 4 1 410.80 409.64 19.86 o -6 4 1 1545.55 1502.00 24.83 o -5 4 1 5889.25 6348.11 91.86 o -4 4 1 2630.57 2730.90 47.17 o -3 4 1 3753.37 3758.72 62.07 o -2 4 1 240.64 196.13 7.45 o -1 4 1 2.75 4.97 4.97 o 0 4 1 6969.02 6747.81 104.27 o 1 4 1 2.23 7.45 4.97 o 2 4 1 240.20 208.54 7.45 o 3 4 1 3743.74 3932.50 64.55 o 4 4 1 2646.39 2750.76 44.69 o 5 4 1 5837.37 6295.97 111.72 o 6 4 1 1544.84 1474.69 29.79 o 7 4 1 393.63 374.88 19.86 o 8 4 1 1535.45 1618.68 39.72 o 9 4 1 198.08 186.20 19.86 o 10 4 1 586.19 513.91 49.65 o 11 4 1 319.74 310.33 27.31 o 12 4 1 282.33 310.33 37.24 o 13 4 1 38.65 9.93 44.69 o 14 4 1 55.88 19.86 34.76 o -13 5 1 114.87 168.82 44.69 o -12 5 1 122.16 94.34 32.27 o -11 5 1 38.10 52.14 32.27 o -10 5 1 275.23 278.06 37.24 o -9 5 1 410.92 362.47 22.34 o -8 5 1 836.46 836.65 27.31 o -7 5 1 855.72 816.79 29.79 o -6 5 1 944.03 933.47 22.34 o -5 5 1 39.13 54.62 9.93 o -4 5 1 674.45 662.86 14.90 o -3 5 1 7531.35 7646.53 116.68 o -2 5 1 120.49 141.51 9.93 o -1 5 1 1862.06 1814.81 37.24 o 0 5 1 1571.99 1618.68 34.76 o 1 5 1 1818.12 1713.02 42.20 o 2 5 1 110.79 126.61 9.93 o 3 5 1 7572.05 7641.56 109.24 o 4 5 1 664.90 615.69 17.38 o 5 5 1 44.84 62.07 9.93 o 6 5 1 941.75 940.92 27.31 o 7 5 1 845.62 767.14 29.79 o 8 5 1 834.43 868.92 32.27 o 9 5 1 412.26 392.26 24.83 o 10 5 1 281.31 297.92 27.31 o 11 5 1 36.08 47.17 29.79 o 12 5 1 125.26 116.68 32.27 o 13 5 1 119.20 74.48 39.72 o -13 6 1 47.79 24.83 32.27 o -12 6 1 20.54 -4.97 34.76 o -11 6 1 1492.85 1710.54 67.03 o -10 6 1 546.52 531.28 32.27 o -9 6 1 2786.14 2763.18 67.03 o -8 6 1 574.73 551.15 29.79 o -7 6 1 1338.45 1290.97 42.20 o -6 6 1 867.18 893.75 24.83 o -5 6 1 1266.45 1308.35 29.79 o -4 6 1 1394.43 1385.31 29.79 o -3 6 1 426.78 419.57 14.90 o -2 6 1 5317.95 5223.47 86.89 o -1 6 1 4085.78 3994.57 72.00 o 0 6 1 10269.26 9794.01 166.34 o 1 6 1 4090.72 4026.84 84.41 o 2 6 1 5360.33 5119.20 84.41 o 3 6 1 417.58 417.08 12.41 o 4 6 1 1347.29 1315.80 29.79 o 5 6 1 1238.45 1276.08 24.83 o 6 6 1 855.21 836.65 27.31 o 7 6 1 1367.15 1412.62 44.69 o 8 6 1 570.14 575.97 24.83 o 9 6 1 2840.59 2725.94 69.51 o 10 6 1 538.42 561.08 42.20 o 11 6 1 1502.86 1524.34 106.75 o 12 6 1 20.07 14.90 32.27 o 13 6 1 45.37 91.86 44.69 o -13 7 1 183.06 158.89 42.20 o -12 7 1 27.61 34.76 34.76 o -11 7 1 210.28 213.51 44.69 o -10 7 1 616.52 571.01 37.24 o -9 7 1 87.33 91.86 22.34 o -8 7 1 717.97 759.69 47.17 o -7 7 1 1386.88 1313.32 47.17 o -6 7 1 1632.71 1680.75 47.17 o -5 7 1 1318.46 1358.00 29.79 o -4 7 1 1384.99 1444.90 27.31 o -3 7 1 337.11 285.50 12.41 o -2 7 1 1115.68 1233.87 32.27 o -1 7 1 243.39 263.16 14.90 o 0 7 1 172.52 129.10 9.93 o 1 7 1 258.21 292.95 14.90 o 2 7 1 1139.45 1273.59 27.31 o 3 7 1 320.43 305.36 12.41 o 4 7 1 1424.82 1469.72 37.24 o 5 7 1 1291.63 1375.38 29.79 o 6 7 1 1633.76 1571.51 44.69 o 7 7 1 1391.11 1447.38 42.20 o 8 7 1 739.62 809.34 39.72 o 9 7 1 85.82 89.38 19.86 o 10 7 1 617.86 647.97 44.69 o 11 7 1 215.16 213.51 42.20 o 12 7 1 26.78 47.17 34.76 o 13 7 1 180.18 198.61 69.51 o -12 8 1 318.63 345.09 47.17 o -11 8 1 324.34 283.02 57.10 o -10 8 1 535.91 506.46 37.24 o -9 8 1 1141.55 1156.91 49.65 o -8 8 1 264.35 280.54 34.76 o -7 8 1 468.89 481.63 32.27 o -6 8 1 265.75 260.68 27.31 o -5 8 1 355.81 362.47 22.34 o -4 8 1 135.84 136.55 14.90 o -3 8 1 643.40 613.21 22.34 o -2 8 1 2782.48 2770.63 57.10 o -1 8 1 972.16 1062.57 29.79 o 0 8 1 263.37 243.30 14.90 o 1 8 1 997.50 1047.67 27.31 o 2 8 1 2794.29 2879.86 59.58 o 3 8 1 648.78 652.93 19.86 o 4 8 1 133.34 126.61 12.41 o 5 8 1 347.80 335.16 22.34 o 6 8 1 261.92 273.09 37.24 o 7 8 1 458.80 486.60 32.27 o 8 8 1 272.86 270.61 29.79 o 9 8 1 1152.17 1216.49 44.69 o 10 8 1 526.71 508.94 39.72 o 11 8 1 326.21 263.16 39.72 o 12 8 1 314.56 176.27 39.72 o -12 9 1 5.09 -7.45 42.20 o -11 9 1 43.33 62.07 37.24 o -10 9 1 59.41 89.38 27.31 o -9 9 1 99.46 64.55 29.79 o -8 9 1 692.09 700.10 42.20 o -7 9 1 383.09 342.60 27.31 o -6 9 1 265.12 213.51 22.34 o -5 9 1 966.26 950.85 34.76 o -4 9 1 489.13 464.25 24.83 o -3 9 1 1619.16 1531.79 39.72 o -2 9 1 373.58 392.26 24.83 o -1 9 1 1733.15 1685.71 44.69 o 0 9 1 151.96 134.06 14.90 o 1 9 1 1738.85 1695.64 42.20 o 2 9 1 365.84 374.88 19.86 o 3 9 1 1644.79 1631.09 42.20 o 4 9 1 480.88 486.60 19.86 o 5 9 1 940.56 948.37 32.27 o 6 9 1 269.14 223.44 29.79 o 7 9 1 381.13 327.71 37.24 o 8 9 1 700.97 774.58 44.69 o 9 9 1 103.61 136.55 44.69 o 10 9 1 59.70 69.51 24.83 o 11 9 1 44.02 49.65 32.27 o 12 9 1 6.51 22.34 34.76 o -11 10 1 64.58 81.93 54.62 o -10 10 1 93.99 148.96 34.76 o -9 10 1 42.65 44.69 39.72 o -8 10 1 567.39 625.63 47.17 o -7 10 1 547.56 546.18 42.20 o -6 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557.62 625.63 44.69 o 7 11 1 274.44 317.78 52.14 o 8 11 1 234.57 355.02 52.14 o 9 11 1 140.26 116.68 42.20 o 10 11 1 19.89 -37.24 37.24 o -9 12 1 8.85 -2.48 57.10 o -8 12 1 35.74 74.48 42.20 o -7 12 1 13.78 -2.48 39.72 o -6 12 1 410.08 350.05 34.76 o -5 12 1 589.06 551.15 37.24 o -4 12 1 664.34 655.42 44.69 o -3 12 1 155.80 79.44 27.31 o -2 12 1 114.19 99.31 57.10 o -1 12 1 386.69 332.67 42.20 o 0 12 1 328.38 374.88 42.20 o 1 12 1 390.01 434.46 44.69 o 2 12 1 111.81 101.79 29.79 o 3 12 1 152.42 104.27 22.34 o 4 12 1 654.21 692.66 37.24 o 5 12 1 587.94 556.11 47.17 o 6 12 1 410.20 322.74 44.69 o 7 12 1 13.85 62.07 39.72 o 8 12 1 31.12 39.72 34.76 o 9 12 1 8.43 0.00 42.20 o -8 13 1 15.30 -27.31 57.10 o -7 13 1 68.92 72.00 34.76 o -6 13 1 82.79 81.93 29.79 o -5 13 1 72.78 116.68 32.27 o -4 13 1 627.77 707.55 47.17 o -3 13 1 54.88 64.55 24.83 o -2 13 1 271.02 332.67 34.76 o -1 13 1 2.82 7.45 32.27 o 0 13 1 239.90 275.57 37.24 o 1 13 1 2.57 17.38 32.27 o 2 13 1 268.64 292.95 37.24 o 3 13 1 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