#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:17:04 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180843 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/74/2017497.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017497_Fobs loop_ _publ_author_name 'Ravikumar, Krishnan' 'Sridhar, Balasubramanian' _publ_section_title ; Granisetron, an antiemetic drug, and its cobalt complex ; _journal_coeditor_code DN3133 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m35 _journal_page_last m39 _journal_volume 66 _journal_year 2010 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.7930 _cell_length_b 13.5544 _cell_length_c 17.9574 _exptl_crystal_F_000 1344.00 _reflns_d_resolution_high 0.8410 _cod_data_source_file dn3133Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' AE79 in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 221.83 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4823.71 5364.22 140.26 o 4 0 0 6867.37 7817.94 204.17 o 6 0 0 639.15 614.33 16.34 o 8 0 0 1611.68 1676.50 50.27 o 10 0 0 115.54 124.90 4.52 o 12 0 0 2020.68 1976.45 166.92 o 14 0 0 21.52 19.59 2.76 o 16 0 0 110.84 124.09 6.70 o 2 1 0 12012.92 14443.54 332.10 o 4 1 0 15.84 9.14 0.52 o 6 1 0 638.04 720.14 15.43 o 8 1 0 175.13 226.27 4.48 o 10 1 0 937.05 960.99 21.02 o 12 1 0 311.92 299.36 7.81 o 14 1 0 4.91 2.59 1.52 o 16 1 0 6.59 5.01 1.78 o 0 2 0 1488.09 1413.09 42.84 o 4 2 0 16734.67 19934.51 458.06 o 6 2 0 538.58 681.46 14.65 o 8 2 0 2293.10 2576.08 54.39 o 10 2 0 170.44 193.49 4.70 o 12 2 0 10.74 7.36 1.19 o 14 2 0 0.26 0.99 1.44 o 16 2 0 19.37 23.36 2.19 o 2 3 0 9092.70 8480.51 167.34 o 4 3 0 628.12 600.65 11.97 o 6 3 0 2128.76 2384.32 55.04 o 8 3 0 255.24 296.68 6.22 o 10 3 0 341.47 331.56 11.15 o 12 3 0 0.46 -0.25 1.10 o 14 3 0 0.19 2.94 1.59 o 16 3 0 1.02 3.58 1.76 o 0 4 0 64.79 50.39 1.55 o 2 4 0 9070.95 8579.34 169.34 o 4 4 0 12831.52 13611.13 268.48 o 6 4 0 1981.22 2463.75 48.48 o 8 4 0 290.84 330.65 6.86 o 10 4 0 11.38 13.20 1.27 o 12 4 0 121.04 124.14 5.20 o 14 4 0 236.29 249.73 9.34 o 2 5 0 1059.81 1032.09 19.17 o 4 5 0 1413.78 1541.10 30.65 o 6 5 0 432.05 406.35 7.78 o 8 5 0 1546.78 1683.13 39.16 o 10 5 0 132.94 127.35 5.07 o 12 5 0 791.24 803.43 33.84 o 14 5 0 134.97 146.67 7.64 o 0 6 0 2018.98 2005.81 59.60 o 2 6 0 4116.32 4136.30 76.38 o 4 6 0 1374.49 1442.26 28.71 o 6 6 0 517.34 594.75 11.25 o 8 6 0 114.02 108.59 3.63 o 10 6 0 78.21 63.82 2.47 o 12 6 0 1084.92 1023.86 35.91 o 14 6 0 10.56 13.44 1.76 o 2 7 0 46.50 37.61 1.03 o 4 7 0 875.25 927.67 17.35 o 6 7 0 74.15 64.05 1.71 o 8 7 0 6.18 2.65 0.90 o 10 7 0 863.16 867.86 25.22 o 12 7 0 17.70 23.85 2.55 o 14 7 0 28.50 32.58 2.41 o 0 8 0 2569.28 2563.45 67.28 o 2 8 0 263.46 224.21 4.77 o 4 8 0 4.82 6.30 0.93 o 6 8 0 2.75 5.49 0.78 o 8 8 0 9.77 4.28 1.34 o 10 8 0 13.16 7.72 1.47 o 12 8 0 3.98 3.59 1.53 o 14 8 0 33.04 32.76 2.41 o 2 9 0 478.79 499.11 11.40 o 4 9 0 34.00 38.41 1.40 o 6 9 0 34.99 34.08 1.61 o 8 9 0 687.42 696.20 15.38 o 10 9 0 177.10 176.28 5.71 o 12 9 0 11.83 15.42 2.22 o 0 10 0 85.76 99.19 3.82 o 2 10 0 9.78 6.63 0.99 o 4 10 0 60.95 43.43 1.66 o 6 10 0 1829.42 2004.57 43.11 o 8 10 0 111.97 104.51 3.11 o 10 10 0 155.37 151.77 5.14 o 12 10 0 8.77 12.17 1.76 o 2 11 0 1.06 1.09 0.80 o 4 11 0 41.78 34.65 1.57 o 6 11 0 52.24 53.35 2.24 o 8 11 0 157.33 136.66 5.20 o 10 11 0 3.38 2.52 1.67 o 0 12 0 34.45 46.15 2.57 o 2 12 0 113.33 118.31 3.26 o 4 12 0 158.57 153.30 4.02 o 6 12 0 50.40 45.55 2.34 o 8 12 0 11.58 17.95 1.64 o 10 12 0 9.92 13.60 2.03 o 2 13 0 286.41 288.62 6.79 o 4 13 0 175.51 218.11 5.37 o 6 13 0 10.32 6.66 1.55 o 8 13 0 0.71 -1.17 1.55 o 0 14 0 187.19 214.85 7.64 o 2 14 0 138.22 131.33 5.27 o 4 14 0 0.02 -1.72 1.31 o 6 14 0 18.94 20.11 2.06 o 8 14 0 7.09 0.36 1.68 o 2 15 0 24.71 46.40 2.83 o 4 15 0 14.64 2.69 2.03 o 6 15 0 65.59 95.98 6.49 o 0 16 0 99.52 123.65 6.84 o 1 1 1 190.03 158.67 3.19 o 2 1 1 13.34 19.83 0.68 o 3 1 1 11014.97 12206.31 182.34 o 4 1 1 12711.61 14526.95 217.26 o 5 1 1 391.05 468.28 6.85 o 6 1 1 899.81 1018.10 13.41 o 7 1 1 255.76 269.89 3.82 o 8 1 1 8.09 2.82 0.39 o 9 1 1 79.41 84.26 1.48 o 10 1 1 207.17 229.37 3.53 o 11 1 1 1.04 -0.63 0.60 o 12 1 1 6.41 4.43 0.86 o 13 1 1 54.61 60.50 2.06 o 14 1 1 16.62 20.05 1.36 o 15 1 1 134.78 134.57 3.49 o 16 1 1 1.31 2.77 1.20 o 0 2 1 23947.60 22722.10 594.32 o 1 2 1 9768.18 9487.35 155.00 o 2 2 1 49206.46 44460.92 819.64 o 3 2 1 6511.49 6975.46 96.54 o 4 2 1 36.84 38.99 1.15 o 5 2 1 424.88 534.79 7.99 o 6 2 1 2889.29 3273.56 48.97 o 7 2 1 779.53 957.82 13.07 o 8 2 1 180.78 173.71 2.50 o 9 2 1 0.09 0.01 0.35 o 10 2 1 325.05 330.68 5.32 o 11 2 1 21.19 19.37 0.90 o 12 2 1 70.35 67.72 2.21 o 13 2 1 375.08 380.49 7.32 o 14 2 1 15.83 15.49 1.31 o 15 2 1 2.11 2.88 1.13 o 16 2 1 49.88 56.25 2.13 o 1 3 1 9715.30 9216.86 144.28 o 2 3 1 414.17 348.44 4.95 o 3 3 1 21748.18 23478.19 338.79 o 4 3 1 874.37 915.04 12.76 o 5 3 1 370.01 399.47 5.89 o 6 3 1 1809.02 2094.97 34.21 o 7 3 1 61.02 85.35 1.42 o 8 3 1 650.85 817.26 12.46 o 9 3 1 253.57 276.98 4.52 o 10 3 1 3.05 2.93 0.53 o 11 3 1 496.64 512.39 10.28 o 12 3 1 124.63 118.20 3.43 o 13 3 1 110.44 111.15 3.44 o 14 3 1 299.36 306.48 6.91 o 15 3 1 197.24 180.48 6.14 o 16 3 1 6.05 8.32 1.34 o 0 4 1 415.09 395.93 7.99 o 1 4 1 906.80 887.91 13.39 o 2 4 1 3252.37 3098.11 43.30 o 3 4 1 0.56 1.08 0.26 o 4 4 1 241.49 194.68 3.53 o 5 4 1 906.51 1172.07 16.49 o 6 4 1 4022.13 4531.73 65.19 o 7 4 1 50.80 72.55 1.42 o 8 4 1 213.75 219.64 3.19 o 9 4 1 314.58 290.07 4.87 o 10 4 1 167.15 167.05 3.76 o 11 4 1 192.99 193.01 5.39 o 12 4 1 32.28 27.54 1.16 o 13 4 1 295.78 273.02 6.80 o 14 4 1 33.24 30.13 1.54 o 15 4 1 14.05 11.57 1.46 o 1 5 1 3448.56 3255.16 45.31 o 2 5 1 266.29 262.68 3.70 o 3 5 1 158.86 130.60 2.07 o 4 5 1 54.02 33.76 0.72 o 5 5 1 116.29 143.34 2.30 o 6 5 1 0.28 3.27 0.53 o 7 5 1 996.66 1013.41 13.42 o 8 5 1 131.82 118.77 2.43 o 9 5 1 45.39 54.04 1.15 o 10 5 1 139.63 137.13 3.06 o 11 5 1 7.39 6.90 0.90 o 12 5 1 178.80 172.45 4.33 o 13 5 1 23.65 29.17 1.81 o 14 5 1 41.92 48.02 2.30 o 15 5 1 1.19 1.56 1.28 o 0 6 1 18.97 9.97 0.51 o 1 6 1 13.35 17.96 0.45 o 2 6 1 9.46 9.42 0.44 o 3 6 1 330.56 331.64 4.50 o 4 6 1 1215.02 1350.59 18.35 o 5 6 1 14.44 17.51 0.53 o 6 6 1 132.87 102.36 1.68 o 7 6 1 335.38 301.61 4.19 o 8 6 1 325.76 334.13 5.05 o 9 6 1 62.20 60.33 1.62 o 10 6 1 1.19 -0.06 0.66 o 11 6 1 229.09 234.90 5.79 o 12 6 1 44.05 48.70 1.90 o 13 6 1 8.86 13.86 1.62 o 14 6 1 26.46 25.95 1.72 o 15 6 1 83.66 71.79 2.78 o 1 7 1 725.48 665.07 9.11 o 2 7 1 24.79 25.65 0.63 o 3 7 1 1035.26 1088.58 16.56 o 4 7 1 342.79 345.29 4.88 o 5 7 1 661.52 688.96 9.19 o 6 7 1 175.47 174.97 2.73 o 7 7 1 11.63 18.96 0.71 o 8 7 1 112.12 112.10 1.98 o 9 7 1 74.32 90.76 2.14 o 10 7 1 35.91 38.42 2.13 o 11 7 1 452.31 449.23 10.31 o 12 7 1 78.84 91.12 3.99 o 13 7 1 0.02 -0.24 1.03 o 14 7 1 24.75 26.75 1.54 o 0 8 1 1828.61 2022.94 37.55 o 1 8 1 1117.14 1158.28 15.74 o 2 8 1 18.48 8.51 0.40 o 3 8 1 224.75 211.10 3.19 o 4 8 1 868.01 835.24 11.81 o 5 8 1 748.26 697.42 10.75 o 6 8 1 1234.51 1221.98 17.23 o 7 8 1 3.79 7.77 0.65 o 8 8 1 215.03 223.84 3.82 o 9 8 1 534.41 490.18 7.78 o 10 8 1 24.94 17.78 1.06 o 11 8 1 5.25 2.97 1.02 o 12 8 1 93.05 79.07 2.38 o 13 8 1 3.77 3.71 1.08 o 14 8 1 27.11 18.70 1.41 o 1 9 1 137.18 135.60 2.26 o 2 9 1 20.77 17.63 0.80 o 3 9 1 19.53 16.81 0.61 o 4 9 1 534.85 519.61 7.79 o 5 9 1 4.00 3.60 0.56 o 6 9 1 129.97 119.48 2.08 o 7 9 1 85.34 107.77 2.09 o 8 9 1 0.26 -1.12 0.75 o 9 9 1 189.57 202.87 4.18 o 10 9 1 77.10 80.90 2.11 o 11 9 1 18.47 19.37 1.32 o 12 9 1 15.71 17.24 1.34 o 13 9 1 15.42 13.33 1.34 o 0 10 1 7.80 7.35 0.89 o 1 10 1 509.90 488.02 7.57 o 2 10 1 8.66 7.05 0.62 o 3 10 1 69.79 54.49 1.35 o 4 10 1 52.10 49.71 1.26 o 5 10 1 77.39 63.41 1.45 o 6 10 1 359.88 341.37 6.14 o 7 10 1 444.69 426.58 6.56 o 8 10 1 22.44 23.27 1.05 o 9 10 1 7.57 6.98 0.83 o 10 10 1 0.06 -1.29 0.86 o 11 10 1 4.04 9.14 1.15 o 12 10 1 1.59 0.79 1.09 o 1 11 1 1.85 3.22 0.62 o 2 11 1 1.94 1.88 0.62 o 3 11 1 34.65 39.06 1.19 o 4 11 1 128.77 131.01 2.61 o 5 11 1 59.42 61.57 1.54 o 6 11 1 48.04 39.40 1.30 o 7 11 1 5.73 1.72 0.84 o 8 11 1 42.46 50.25 1.52 o 9 11 1 10.48 9.65 0.95 o 10 11 1 22.40 22.81 1.31 o 11 11 1 1.19 -0.61 1.13 o 0 12 1 54.82 46.77 1.87 o 1 12 1 49.84 55.81 1.46 o 2 12 1 0.74 -0.85 0.65 o 3 12 1 111.41 111.82 2.23 o 4 12 1 41.64 45.54 1.63 o 5 12 1 334.39 361.54 6.16 o 6 12 1 4.32 3.29 0.86 o 7 12 1 57.19 50.12 2.12 o 8 12 1 0.83 -0.63 0.89 o 9 12 1 4.41 7.68 1.08 o 10 12 1 0.06 -0.38 1.17 o 1 13 1 47.41 47.28 1.37 o 2 13 1 1.05 -0.11 0.77 o 3 13 1 84.59 86.28 2.12 o 4 13 1 1.58 1.03 0.86 o 5 13 1 68.35 72.55 1.99 o 6 13 1 26.17 28.39 1.45 o 7 13 1 9.03 10.41 1.12 o 8 13 1 29.97 32.84 1.50 o 9 13 1 22.60 21.16 1.36 o 0 14 1 137.60 153.32 4.58 o 1 14 1 20.19 27.69 1.32 o 2 14 1 33.54 30.78 1.35 o 3 14 1 33.56 29.15 1.33 o 4 14 1 59.60 75.01 2.19 o 5 14 1 0.00 -1.38 1.01 o 6 14 1 57.31 63.39 2.65 o 7 14 1 5.32 10.39 1.31 o 8 14 1 58.13 70.71 3.58 o 1 15 1 6.06 8.33 1.19 o 2 15 1 3.47 4.71 1.13 o 3 15 1 3.80 3.59 1.15 o 4 15 1 6.11 5.24 1.18 o 5 15 1 2.42 3.12 1.29 o 0 16 1 3.24 0.04 1.88 o 1 16 1 72.67 88.31 2.78 o 0 0 2 4421.41 4140.44 108.27 o 2 0 2 46706.88 40454.30 2517.25 o 3 0 2 23897.83 25956.35 602.60 o 4 0 2 215.62 233.85 6.29 o 5 0 2 390.76 486.79 11.07 o 6 0 2 282.75 325.42 6.71 o 7 0 2 0.01 -0.52 0.52 o 8 0 2 367.22 397.18 7.61 o 9 0 2 327.98 347.64 7.30 o 10 0 2 1198.32 1176.80 23.61 o 11 0 2 76.20 69.37 2.51 o 12 0 2 153.70 133.75 4.00 o 13 0 2 325.27 321.39 11.62 o 14 0 2 97.56 89.85 5.21 o 15 0 2 409.98 418.89 12.30 o 16 0 2 58.27 63.40 3.28 o 1 1 2 513.34 347.14 5.07 o 2 1 2 957.11 986.31 18.22 o 3 1 2 1201.39 1230.85 18.57 o 4 1 2 10.01 22.33 0.51 o 5 1 2 77.05 104.44 1.79 o 6 1 2 8.04 8.60 0.39 o 7 1 2 1525.76 1671.84 22.61 o 8 1 2 35.95 43.10 0.84 o 9 1 2 1240.48 1402.04 20.52 o 10 1 2 413.68 412.28 6.32 o 11 1 2 37.04 37.97 1.25 o 12 1 2 6.72 5.18 0.84 o 13 1 2 0.96 1.16 0.90 o 14 1 2 22.52 18.88 1.34 o 15 1 2 158.72 156.54 4.33 o 16 1 2 0.31 1.51 1.18 o 0 2 2 21920.82 21784.64 504.15 o 1 2 2 2329.80 2204.76 33.07 o 2 2 2 9922.41 10179.06 146.52 o 3 2 2 5037.12 5163.78 81.11 o 4 2 2 480.20 443.75 6.31 o 5 2 2 70.81 87.12 1.72 o 6 2 2 330.88 387.08 5.95 o 7 2 2 19.05 21.96 0.65 o 8 2 2 4.28 3.94 0.43 o 9 2 2 1.35 0.69 0.46 o 10 2 2 38.79 31.41 0.90 o 11 2 2 44.23 49.97 1.51 o 12 2 2 192.68 166.30 3.97 o 13 2 2 108.98 103.16 2.73 o 14 2 2 6.29 7.84 1.20 o 15 2 2 40.75 48.68 1.98 o 16 2 2 21.19 18.06 1.56 o 1 3 2 675.06 466.02 6.80 o 2 3 2 4.70 3.96 0.24 o 3 3 2 17256.25 18717.23 260.29 o 4 3 2 3720.88 3850.46 57.71 o 5 3 2 159.06 182.09 3.10 o 6 3 2 7.26 8.00 0.50 o 7 3 2 1496.01 1834.17 27.51 o 8 3 2 633.16 732.68 11.20 o 9 3 2 2.82 1.82 0.47 o 10 3 2 0.71 0.81 0.49 o 11 3 2 3.97 3.50 0.83 o 12 3 2 116.25 103.92 3.25 o 13 3 2 296.98 296.42 8.98 o 14 3 2 4.34 3.84 0.98 o 15 3 2 42.16 44.43 2.86 o 16 3 2 2.64 1.73 1.18 o 0 4 2 1196.09 1203.73 25.62 o 1 4 2 289.46 261.97 4.08 o 2 4 2 4990.82 4813.55 69.24 o 3 4 2 3596.44 3533.69 47.50 o 4 4 2 5742.89 6013.66 86.50 o 5 4 2 5507.91 6062.17 81.35 o 6 4 2 1177.04 1271.35 17.76 o 7 4 2 208.38 208.76 3.67 o 8 4 2 337.80 327.76 4.74 o 9 4 2 7.97 10.60 0.64 o 10 4 2 2.87 5.67 0.60 o 11 4 2 132.71 128.72 3.34 o 12 4 2 234.08 225.97 6.00 o 13 4 2 61.17 62.18 1.97 o 14 4 2 6.99 5.92 1.09 o 15 4 2 0.19 0.64 1.12 o 1 5 2 1437.57 1517.13 23.89 o 2 5 2 116.05 115.14 1.72 o 3 5 2 13.41 19.27 0.45 o 4 5 2 1123.22 1250.00 17.62 o 5 5 2 8192.30 8657.06 116.52 o 6 5 2 60.73 34.49 0.79 o 7 5 2 13.09 8.74 0.48 o 8 5 2 5.39 3.00 0.47 o 9 5 2 95.16 77.25 1.84 o 10 5 2 228.88 226.62 3.76 o 11 5 2 856.71 888.03 19.39 o 12 5 2 23.80 26.33 1.21 o 13 5 2 14.89 15.99 1.92 o 14 5 2 17.59 22.17 1.32 o 15 5 2 57.81 57.65 2.29 o 0 6 2 4652.76 4448.74 87.30 o 1 6 2 2443.92 2325.30 31.36 o 2 6 2 109.19 106.16 1.65 o 3 6 2 1594.48 1559.00 21.08 o 4 6 2 1818.86 1940.44 26.32 o 5 6 2 793.26 765.16 10.89 o 6 6 2 1977.11 2047.91 27.80 o 7 6 2 36.90 38.49 0.94 o 8 6 2 350.73 335.85 5.49 o 9 6 2 185.04 179.35 4.74 o 10 6 2 0.39 1.23 0.69 o 11 6 2 185.57 178.27 4.66 o 12 6 2 7.44 5.01 1.09 o 13 6 2 54.14 59.57 1.93 o 14 6 2 122.78 111.58 4.04 o 15 6 2 59.47 54.72 2.26 o 1 7 2 117.03 89.60 1.50 o 2 7 2 347.88 415.08 5.95 o 3 7 2 163.12 157.93 2.45 o 4 7 2 778.69 784.36 11.13 o 5 7 2 264.06 226.78 3.33 o 6 7 2 54.61 38.84 0.96 o 7 7 2 661.64 680.77 10.59 o 8 7 2 515.88 556.70 8.06 o 9 7 2 893.07 922.11 14.93 o 10 7 2 102.50 87.21 2.10 o 11 7 2 0.05 -1.46 0.97 o 12 7 2 238.99 230.47 5.04 o 13 7 2 19.28 21.69 1.36 o 14 7 2 28.15 28.12 1.68 o 0 8 2 66.45 47.69 1.40 o 1 8 2 9.20 14.50 0.54 o 2 8 2 561.71 515.21 7.14 o 3 8 2 87.25 80.86 1.49 o 4 8 2 4.00 3.34 0.56 o 5 8 2 69.22 66.10 1.42 o 6 8 2 447.26 417.10 6.33 o 7 8 2 352.28 336.15 5.65 o 8 8 2 388.92 405.60 6.23 o 9 8 2 7.37 6.60 0.90 o 10 8 2 13.04 17.33 1.06 o 11 8 2 2.15 1.34 0.99 o 12 8 2 51.17 61.26 2.09 o 13 8 2 40.03 41.33 1.71 o 14 8 2 32.60 33.94 1.88 o 1 9 2 8.01 3.66 0.45 o 2 9 2 204.11 179.60 2.90 o 3 9 2 88.06 81.64 1.58 o 4 9 2 0.40 0.89 0.51 o 5 9 2 64.54 63.57 1.35 o 6 9 2 0.89 1.30 0.59 o 7 9 2 18.31 20.31 0.90 o 8 9 2 754.47 707.71 11.03 o 9 9 2 492.59 507.35 9.39 o 10 9 2 6.58 9.79 0.96 o 11 9 2 3.89 1.13 1.05 o 12 9 2 11.47 9.87 1.21 o 13 9 2 1.85 4.16 1.18 o 0 10 2 154.34 154.77 4.48 o 1 10 2 213.95 240.36 3.94 o 2 10 2 29.73 28.65 0.92 o 3 10 2 1218.85 1319.83 19.23 o 4 10 2 743.22 702.97 10.42 o 5 10 2 395.04 398.36 6.11 o 6 10 2 277.07 266.83 4.46 o 7 10 2 48.62 46.55 1.30 o 8 10 2 76.88 69.99 1.77 o 9 10 2 34.13 39.02 1.40 o 10 10 2 2.24 1.03 0.99 o 11 10 2 14.53 19.18 1.43 o 12 10 2 3.20 5.99 1.29 o 1 11 2 7.87 12.46 0.76 o 2 11 2 160.85 154.77 2.75 o 3 11 2 363.65 354.25 5.69 o 4 11 2 34.55 36.87 1.14 o 5 11 2 1.86 -0.63 0.72 o 6 11 2 466.25 440.61 7.34 o 7 11 2 202.97 195.63 4.19 o 8 11 2 5.56 3.88 0.90 o 9 11 2 15.16 12.04 1.48 o 10 11 2 1.42 -0.77 1.00 o 11 11 2 11.70 17.80 1.59 o 0 12 2 136.64 104.35 3.01 o 1 12 2 22.85 22.68 0.97 o 2 12 2 32.31 24.27 1.08 o 3 12 2 24.49 20.79 1.02 o 4 12 2 25.43 19.51 1.02 o 5 12 2 31.39 24.44 1.18 o 6 12 2 4.81 5.10 0.91 o 7 12 2 35.45 39.94 1.79 o 8 12 2 21.53 20.25 1.28 o 9 12 2 17.22 12.51 1.31 o 10 12 2 8.24 10.46 1.34 o 1 13 2 13.18 5.64 0.92 o 2 13 2 27.99 26.58 1.28 o 3 13 2 1.15 0.47 0.89 o 4 13 2 469.96 517.55 11.99 o 5 13 2 100.39 81.98 2.18 o 6 13 2 11.67 6.89 0.98 o 7 13 2 21.49 25.44 1.31 o 8 13 2 10.07 10.11 1.17 o 9 13 2 23.73 26.60 1.67 o 0 14 2 27.57 35.43 2.99 o 1 14 2 82.61 88.89 2.33 o 2 14 2 91.34 81.86 2.19 o 3 14 2 2.39 1.30 0.93 o 4 14 2 28.54 29.61 1.57 o 5 14 2 0.67 -0.80 0.98 o 6 14 2 58.22 65.65 2.36 o 7 14 2 1.21 1.45 1.10 o 1 15 2 0.68 -0.96 0.99 o 2 15 2 33.57 38.43 1.56 o 3 15 2 4.49 5.08 1.12 o 4 15 2 16.13 12.78 1.24 o 5 15 2 11.10 13.87 1.37 o 0 16 2 13.74 17.90 2.23 o 1 16 2 5.07 8.35 1.31 o 1 1 3 16408.52 16372.00 220.55 o 2 1 3 545.20 529.28 7.74 o 3 1 3 263.23 255.28 3.55 o 4 1 3 5860.17 6337.63 103.57 o 5 1 3 632.37 668.82 9.48 o 6 1 3 564.41 551.16 8.18 o 7 1 3 0.22 0.51 0.33 o 8 1 3 201.84 255.65 3.81 o 9 1 3 180.06 169.87 4.71 o 10 1 3 46.01 43.39 1.18 o 11 1 3 49.26 40.24 1.19 o 12 1 3 3.21 0.21 0.78 o 13 1 3 246.65 238.76 6.37 o 14 1 3 5.91 2.22 1.03 o 15 1 3 0.70 -1.23 1.07 o 16 1 3 50.42 45.22 1.97 o 0 2 3 183.89 151.98 3.72 o 1 2 3 17122.99 16484.17 221.76 o 2 2 3 4157.41 4028.47 60.35 o 3 2 3 2680.49 2673.64 40.41 o 4 2 3 29.10 32.02 0.90 o 5 2 3 1849.76 1990.97 33.45 o 6 2 3 2807.60 3052.01 45.82 o 7 2 3 772.42 858.24 13.10 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8 8 67.71 51.88 1.36 o 6 8 8 0.01 -0.90 0.60 o 7 8 8 131.05 135.07 2.86 o 8 8 8 352.15 354.49 6.43 o 9 8 8 0.58 0.94 0.88 o 10 8 8 85.55 75.75 2.07 o 11 8 8 53.53 51.77 1.95 o 12 8 8 2.01 -0.57 1.17 o 1 9 8 546.45 546.94 8.56 o 2 9 8 156.45 149.47 2.69 o 3 9 8 13.35 14.82 0.81 o 4 9 8 556.33 573.23 9.41 o 5 9 8 0.11 -0.95 0.64 o 6 9 8 3.72 4.20 0.73 o 7 9 8 1.12 1.49 0.85 o 8 9 8 44.76 39.29 1.50 o 9 9 8 34.02 32.60 1.42 o 10 9 8 64.99 66.79 2.06 o 11 9 8 39.40 42.11 1.66 o 12 9 8 1.07 1.38 1.19 o 0 10 8 260.28 242.40 5.78 o 1 10 8 175.30 162.91 2.95 o 2 10 8 11.48 13.58 0.85 o 3 10 8 82.51 63.81 1.89 o 4 10 8 7.64 4.48 0.82 o 5 10 8 14.28 13.40 0.94 o 6 10 8 247.07 242.40 4.56 o 7 10 8 6.28 4.57 0.95 o 8 10 8 2.60 2.52 1.00 o 9 10 8 22.76 21.97 1.40 o 10 10 8 3.07 6.67 1.16 o 11 10 8 31.13 33.58 1.79 o 1 11 8 18.36 18.19 1.02 o 2 11 8 40.10 42.02 1.40 o 3 11 8 26.41 20.55 1.09 o 4 11 8 16.77 15.05 1.00 o 5 11 8 0.01 -1.19 0.79 o 6 11 8 62.71 56.55 1.85 o 7 11 8 19.38 15.87 1.24 o 8 11 8 31.80 36.92 1.63 o 9 11 8 31.48 24.97 1.49 o 10 11 8 0.76 1.17 1.16 o 0 12 8 81.01 66.09 2.68 o 1 12 8 16.97 15.29 1.14 o 2 12 8 27.18 37.36 1.99 o 3 12 8 204.38 220.91 4.52 o 4 12 8 181.94 178.15 3.80 o 5 12 8 0.26 -1.31 0.87 o 6 12 8 0.02 -1.04 0.95 o 7 12 8 1.42 1.01 0.98 o 8 12 8 32.90 46.76 1.87 o 9 12 8 15.70 17.37 1.43 o 1 13 8 157.77 168.56 3.71 o 2 13 8 3.40 0.45 0.93 o 3 13 8 6.35 6.56 1.04 o 4 13 8 13.43 22.05 1.31 o 5 13 8 59.72 61.82 2.02 o 6 13 8 1.47 -1.44 1.07 o 7 13 8 4.06 4.00 1.24 o 0 14 8 36.92 60.53 3.06 o 1 14 8 16.32 19.57 1.36 o 2 14 8 119.91 128.14 3.11 o 3 14 8 30.62 39.08 1.64 o 4 14 8 0.83 -0.68 1.00 o 5 14 8 47.61 51.67 1.91 o 1 1 9 110.88 127.87 1.87 o 2 1 9 33.65 52.16 0.93 o 3 1 9 18.18 24.09 0.56 o 4 1 9 3.83 5.46 0.34 o 5 1 9 1.79 2.03 0.36 o 6 1 9 342.37 330.58 5.12 o 7 1 9 6.60 6.85 0.62 o 8 1 9 60.17 53.43 1.42 o 9 1 9 211.58 217.26 3.80 o 10 1 9 19.63 18.56 0.97 o 11 1 9 23.68 25.45 1.12 o 12 1 9 50.75 44.44 1.42 o 13 1 9 82.30 86.06 2.10 o 14 1 9 41.70 37.79 1.72 o 0 2 9 3332.35 3471.54 64.08 o 1 2 9 4051.77 4340.75 58.37 o 2 2 9 745.06 698.69 9.29 o 3 2 9 136.20 143.45 2.08 o 4 2 9 90.10 105.03 1.61 o 5 2 9 103.61 107.66 1.74 o 6 2 9 22.55 18.12 0.69 o 7 2 9 16.15 18.05 1.07 o 8 2 9 456.32 444.58 7.14 o 9 2 9 402.80 373.03 6.11 o 10 2 9 159.26 175.88 3.23 o 11 2 9 368.38 344.16 6.15 o 12 2 9 0.03 0.33 0.85 o 13 2 9 22.80 26.87 1.23 o 14 2 9 63.73 58.51 2.68 o 1 3 9 58.05 70.87 1.20 o 2 3 9 6.04 9.73 0.41 o 3 3 9 161.25 163.93 2.45 o 4 3 9 888.06 874.28 11.61 o 5 3 9 229.01 246.01 3.59 o 6 3 9 15.75 15.28 0.66 o 7 3 9 626.07 602.65 9.44 o 8 3 9 646.47 637.90 10.10 o 9 3 9 49.92 52.83 1.44 o 10 3 9 211.17 183.47 3.53 o 11 3 9 646.24 605.41 10.63 o 12 3 9 149.80 141.08 3.90 o 13 3 9 0.87 0.14 0.91 o 14 3 9 46.00 44.31 1.81 o 0 4 9 24.22 8.13 0.66 o 1 4 9 1266.03 1496.02 21.89 o 2 4 9 177.58 198.45 2.91 o 3 4 9 416.63 444.94 6.22 o 4 4 9 47.55 50.38 1.06 o 5 4 9 18.75 22.48 1.09 o 6 4 9 339.16 312.86 5.11 o 7 4 9 243.87 254.74 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7 9 20.53 19.10 0.86 o 6 7 9 0.05 -0.30 0.70 o 7 7 9 140.60 136.97 2.90 o 8 7 9 229.29 215.23 4.16 o 9 7 9 59.75 49.94 1.58 o 10 7 9 2.07 0.95 0.95 o 11 7 9 42.17 45.68 1.70 o 12 7 9 2.19 2.32 1.06 o 13 7 9 0.08 0.58 1.15 o 0 8 9 0.09 1.32 0.78 o 1 8 9 2.93 1.79 0.55 o 2 8 9 28.02 32.87 1.03 o 3 8 9 759.55 772.61 13.04 o 4 8 9 258.47 245.23 4.33 o 5 8 9 5.81 5.67 0.73 o 6 8 9 72.61 76.01 1.94 o 7 8 9 0.31 -1.15 0.77 o 8 8 9 8.49 5.82 0.94 o 9 8 9 159.04 144.56 3.11 o 10 8 9 0.46 -0.85 0.85 o 11 8 9 5.01 3.21 1.01 o 12 8 9 1.43 -1.60 1.09 o 1 9 9 413.93 422.16 6.74 o 2 9 9 11.10 13.49 0.83 o 3 9 9 26.53 28.57 1.09 o 4 9 9 357.69 348.02 5.91 o 5 9 9 100.06 86.42 1.96 o 6 9 9 21.05 14.42 1.02 o 7 9 9 0.69 -0.19 0.83 o 8 9 9 0.41 -0.06 0.95 o 9 9 9 28.26 36.10 2.21 o 10 9 9 20.92 24.23 1.38 o 11 9 9 1.06 1.85 1.11 o 0 10 9 25.13 28.19 1.44 o 1 10 9 0.12 0.00 0.69 o 2 10 9 70.64 56.63 1.58 o 3 10 9 144.10 143.83 2.81 o 4 10 9 70.77 53.53 1.59 o 5 10 9 0.76 -0.48 0.77 o 6 10 9 18.12 16.07 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9 5 10 12.30 5.87 0.93 o 10 5 10 0.12 -1.32 0.88 o 11 5 10 236.58 228.00 4.48 o 12 5 10 34.84 36.17 1.49 o 13 5 10 1.06 -0.02 0.99 o 0 6 10 80.33 69.17 1.89 o 1 6 10 67.54 66.02 1.30 o 2 6 10 35.91 26.07 0.76 o 3 6 10 1070.86 1050.08 16.79 o 4 6 10 1055.87 1023.72 16.46 o 5 6 10 54.36 42.10 1.18 o 6 6 10 144.53 154.57 3.09 o 7 6 10 5.96 3.11 0.79 o 8 6 10 223.17 191.53 3.76 o 9 6 10 214.28 181.21 3.88 o 10 6 10 2.11 7.85 1.05 o 11 6 10 27.01 27.88 1.51 o 12 6 10 48.62 51.67 1.98 o 13 6 10 14.37 19.60 1.39 o 1 7 10 419.78 426.08 6.75 o 2 7 10 1071.61 1020.88 15.71 o 3 7 10 36.78 26.02 0.96 o 4 7 10 437.68 431.46 6.89 o 5 7 10 291.23 265.24 4.46 o 6 7 10 4.30 7.18 0.85 o 7 7 10 16.92 12.54 0.95 o 8 7 10 26.41 23.89 1.18 o 9 7 10 1.26 1.35 0.85 o 10 7 10 53.00 50.04 1.75 o 11 7 10 22.94 21.89 1.35 o 12 7 10 21.60 24.12 1.45 o 0 8 10 90.47 84.78 2.48 o 1 8 10 40.78 38.29 1.10 o 2 8 10 473.77 471.10 7.79 o 3 8 10 552.81 518.22 8.93 o 4 8 10 52.87 51.63 1.45 o 5 8 10 123.21 121.90 2.49 o 6 8 10 128.34 116.08 2.58 o 7 8 10 459.64 454.75 8.08 o 8 8 10 19.41 26.56 1.24 o 9 8 10 20.58 19.06 1.18 o 10 8 10 2.95 4.89 1.01 o 11 8 10 4.83 7.67 1.15 o 1 9 10 160.10 143.86 2.69 o 2 9 10 11.01 11.84 0.85 o 3 9 10 259.88 240.01 4.49 o 4 9 10 0.81 -0.65 0.69 o 5 9 10 100.29 107.46 2.32 o 6 9 10 1.58 -0.96 0.86 o 7 9 10 24.49 21.81 1.23 o 8 9 10 1.75 2.10 0.89 o 9 9 10 3.27 7.17 1.14 o 10 9 10 1.00 0.78 1.11 o 11 9 10 3.81 4.62 1.18 o 0 10 10 157.89 154.22 4.02 o 1 10 10 1007.49 1028.56 17.43 o 2 10 10 0.25 0.23 0.76 o 3 10 10 51.01 58.63 1.62 o 4 10 10 87.21 85.41 2.01 o 5 10 10 231.33 248.64 4.69 o 6 10 10 120.64 117.75 2.94 o 7 10 10 10.77 13.92 1.18 o 8 10 10 8.03 14.04 1.21 o 9 10 10 7.91 9.33 1.18 o 10 10 10 41.26 50.37 1.96 o 1 11 10 15.91 16.76 1.03 o 2 11 10 4.11 2.77 0.88 o 3 11 10 15.42 16.12 1.08 o 4 11 10 0.85 1.33 0.87 o 5 11 10 15.38 20.21 1.16 o 6 11 10 0.11 -1.42 0.95 o 7 11 10 4.62 5.70 1.11 o 8 11 10 16.50 22.02 1.46 o 9 11 10 69.27 76.78 2.56 o 0 12 10 176.43 187.90 6.07 o 1 12 10 137.86 142.10 3.23 o 2 12 10 39.86 39.18 1.53 o 3 12 10 135.24 145.28 3.25 o 4 12 10 0.00 -0.29 0.89 o 5 12 10 9.07 9.02 1.12 o 6 12 10 16.84 18.45 1.36 o 7 12 10 65.12 68.00 2.28 o 1 13 10 0.22 0.23 1.11 o 2 13 10 48.35 56.82 1.93 o 3 13 10 28.74 29.78 1.45 o 4 13 10 15.22 21.65 1.35 o 5 13 10 5.43 2.68 1.18 o 0 14 10 26.40 23.00 2.11 o 1 14 10 15.35 17.44 1.46 o 2 14 10 27.37 37.71 1.72 o 1 1 11 998.84 948.15 13.02 o 2 1 11 4.05 0.14 0.32 o 3 1 11 1569.32 1497.24 19.70 o 4 1 11 1029.31 947.22 12.56 o 5 1 11 70.95 94.74 1.74 o 6 1 11 7.95 6.88 0.58 o 7 1 11 89.89 84.42 2.28 o 8 1 11 92.24 70.38 1.75 o 9 1 11 4.82 6.71 0.89 o 10 1 11 0.26 -0.98 0.79 o 11 1 11 20.56 15.30 1.14 o 12 1 11 0.24 -0.59 0.94 o 13 1 11 0.38 0.32 0.92 o 14 1 11 1.61 2.35 1.00 o 0 2 11 1867.84 1818.12 36.11 o 1 2 11 60.89 46.80 0.98 o 2 2 11 753.56 746.22 10.29 o 3 2 11 560.31 579.67 8.04 o 4 2 11 46.67 43.92 1.01 o 5 2 11 3.97 9.59 0.60 o 6 2 11 397.59 365.98 6.22 o 7 2 11 842.39 880.83 14.36 o 8 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1.17 2.11 0.88 o 5 8 11 759.23 773.08 13.93 o 6 8 11 39.26 26.61 1.28 o 7 8 11 131.74 118.57 2.70 o 8 8 11 59.67 49.95 1.63 o 9 8 11 1.63 2.39 0.96 o 10 8 11 0.32 -1.46 0.97 o 11 8 11 0.59 -0.58 1.05 o 1 9 11 21.43 18.36 1.05 o 2 9 11 403.79 387.72 6.57 o 3 9 11 588.53 566.80 9.79 o 4 9 11 21.55 20.15 1.07 o 5 9 11 0.31 1.44 0.90 o 6 9 11 194.56 193.24 4.06 o 7 9 11 1.53 0.35 0.89 o 8 9 11 0.67 0.52 0.95 o 9 9 11 23.28 21.22 1.29 o 10 9 11 3.48 2.00 1.21 o 0 10 11 78.25 78.81 2.77 o 1 10 11 0.82 1.16 0.78 o 2 10 11 5.54 5.83 0.87 o 3 10 11 284.04 305.68 5.32 o 4 10 11 14.41 15.22 1.00 o 5 10 11 195.12 179.95 3.87 o 6 10 11 9.73 7.63 1.07 o 7 10 11 13.98 12.57 1.24 o 8 10 11 0.02 0.23 1.00 o 9 10 11 89.57 97.00 2.79 o 1 11 11 0.21 1.42 0.79 o 2 11 11 28.10 30.04 1.27 o 3 11 11 23.13 20.80 1.15 o 4 11 11 8.17 5.97 0.94 o 5 11 11 2.30 3.08 1.03 o 6 11 11 40.16 38.51 1.65 o 7 11 11 25.56 31.85 1.58 o 8 11 11 2.27 4.32 1.16 o 0 12 11 17.00 21.06 1.95 o 1 12 11 24.70 30.37 1.55 o 2 12 11 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12 76.86 92.53 2.84 o 1 8 12 1.56 -0.14 0.66 o 2 8 12 6.08 5.99 0.79 o 3 8 12 1.66 1.05 0.78 o 4 8 12 212.17 200.28 3.87 o 5 8 12 0.11 0.00 0.82 o 6 8 12 124.16 117.08 2.77 o 7 8 12 0.05 -1.25 0.83 o 8 8 12 62.95 61.63 1.87 o 9 8 12 5.01 6.71 1.10 o 10 8 12 18.50 18.61 1.31 o 1 9 12 6.21 2.29 0.75 o 2 9 12 81.23 68.69 1.78 o 3 9 12 0.12 0.66 0.82 o 4 9 12 91.82 93.83 2.16 o 5 9 12 0.01 -0.90 0.89 o 6 9 12 2.72 3.84 0.95 o 7 9 12 4.36 5.40 1.01 o 8 9 12 97.25 96.32 2.55 o 9 9 12 13.61 12.71 1.25 o 10 9 12 2.29 2.42 1.23 o 0 10 12 5.77 4.07 1.19 o 1 10 12 4.34 5.17 0.82 o 2 10 12 296.75 299.84 5.27 o 3 10 12 138.06 142.51 2.89 o 4 10 12 17.65 15.19 1.00 o 5 10 12 3.34 2.97 0.94 o 6 10 12 8.30 8.52 1.05 o 7 10 12 0.00 -0.23 0.97 o 8 10 12 7.70 6.49 1.20 o 1 11 12 76.31 88.41 2.23 o 2 11 12 39.64 43.56 1.53 o 3 11 12 62.13 65.56 1.89 o 4 11 12 0.69 0.01 0.88 o 5 11 12 27.49 27.58 1.62 o 6 11 12 4.57 7.38 1.20 o 7 11 12 1.24 0.25 1.02 o 0 12 12 36.89 38.28 2.29 o 1 12 12 229.21 264.68 5.66 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13 8.54 8.72 1.06 o 8 6 13 6.64 4.93 1.00 o 9 6 13 7.13 5.36 1.04 o 10 6 13 31.84 34.18 1.58 o 11 6 13 11.01 14.23 1.35 o 1 7 13 9.41 10.35 0.84 o 2 7 13 242.76 254.22 4.46 o 3 7 13 10.99 8.20 0.86 o 4 7 13 39.84 39.20 1.42 o 5 7 13 1.63 0.69 0.85 o 6 7 13 21.70 13.68 1.04 o 7 7 13 8.81 11.13 1.07 o 8 7 13 23.28 28.50 1.48 o 9 7 13 48.69 53.41 1.98 o 10 7 13 34.15 39.55 1.67 o 0 8 13 666.79 656.53 15.99 o 1 8 13 16.91 20.68 1.07 o 2 8 13 197.33 206.62 3.79 o 3 8 13 3.79 1.75 0.81 o 4 8 13 51.28 47.10 1.69 o 5 8 13 108.19 100.02 2.51 o 6 8 13 25.54 24.03 1.29 o 7 8 13 69.82 66.30 2.14 o 8 8 13 24.11 21.31 1.38 o 9 8 13 0.76 -1.50 1.05 o 10 8 13 0.19 0.35 1.02 o 1 9 13 34.48 30.76 1.19 o 2 9 13 37.01 34.62 1.24 o 3 9 13 36.33 40.39 1.34 o 4 9 13 8.23 9.10 1.10 o 5 9 13 207.30 210.31 4.36 o 6 9 13 66.27 68.83 2.06 o 7 9 13 60.70 60.83 1.98 o 8 9 13 0.02 -0.85 1.00 o 9 9 13 2.59 2.37 1.16 o 0 10 13 72.53 72.49 2.81 o 1 10 13 16.02 16.80 1.05 o 2 10 13 16.75 17.90 1.06 o 3 10 13 9.85 16.52 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14 30.11 31.29 1.34 o 10 1 14 93.53 99.36 2.50 o 11 1 14 34.29 31.37 1.49 o 12 1 14 17.49 20.53 1.50 o 0 2 14 71.34 61.55 2.00 o 1 2 14 593.25 516.21 8.12 o 2 2 14 263.99 263.97 4.03 o 3 2 14 106.60 106.03 2.00 o 4 2 14 189.75 177.32 3.31 o 5 2 14 464.85 447.09 7.95 o 6 2 14 194.70 190.95 3.76 o 7 2 14 71.08 66.51 1.82 o 8 2 14 35.15 24.97 1.29 o 9 2 14 0.00 -1.13 0.96 o 10 2 14 60.53 72.08 2.43 o 11 2 14 1.33 1.94 1.05 o 12 2 14 0.62 -0.07 1.12 o 1 3 14 122.23 106.64 1.91 o 2 3 14 167.92 179.12 3.03 o 3 3 14 15.81 22.60 0.90 o 4 3 14 457.67 448.20 7.53 o 5 3 14 5.83 6.32 0.85 o 6 3 14 26.88 24.26 1.16 o 7 3 14 51.39 48.27 1.54 o 8 3 14 158.80 164.78 3.44 o 9 3 14 301.47 289.75 5.52 o 10 3 14 0.45 0.28 0.93 o 11 3 14 5.65 7.30 1.17 o 12 3 14 4.91 2.35 1.22 o 0 4 14 87.51 93.71 3.27 o 1 4 14 61.49 56.13 1.43 o 2 4 14 1346.65 1327.36 19.58 o 3 4 14 1018.45 1000.73 14.88 o 4 4 14 112.50 105.60 2.26 o 5 4 14 32.49 28.06 1.11 o 6 4 14 0.04 -0.89 0.72 o 7 4 14 18.85 20.67 1.13 o 8 4 14 5.01 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