#------------------------------------------------------------------------------ #$Date: 2010-03-05 20:15:21 +0200 (Fri, 05 Mar 2010) $ #$Revision: 1024 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2017504.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017504_Fobs loop_ _publ_author_name 'Lyakhov, Alexander S.' 'Voitekhovich, Sergei V.' 'Ivashkevich, Ludmila S.' 'Gaponik, Pavel N.' _publ_section_title ; A tetrazol-5-yl analogue of glycine, 5-ammoniomethyl-1H-tetrazolide, and its copper(II) complex ; _journal_coeditor_code EG3037 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m22 _journal_page_last m25 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.800 _cell_angle_gamma 90.000 _cell_length_a 7.0452 _cell_length_b 8.9070 _cell_length_c 9.0590 _exptl_crystal_F_000 302.00 _reflns_d_resolution_high 0.7093 _[local]_cod_data_source_file eg3037IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' sj04 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 112.02 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 7668.14 6093.10 95.30 o 2 0 0 120.61 117.69 2.95 o 3 0 0 3850.72 3977.31 19.91 o 4 0 0 3360.10 3386.33 70.00 o 5 0 0 923.34 920.37 13.24 o 6 0 0 5.40 5.46 0.58 o 7 0 0 382.43 388.93 8.15 o 8 0 0 518.72 509.99 6.82 o 9 0 0 116.63 114.16 3.32 o 1 1 0 470.93 577.49 9.61 o 2 1 0 102.57 110.61 3.21 o 3 1 0 375.52 434.76 5.94 o 4 1 0 199.77 244.37 8.97 o 5 1 0 38.46 44.56 0.94 o 6 1 0 48.72 44.95 1.07 o 7 1 0 45.28 40.13 1.16 o 8 1 0 0.84 0.83 0.69 o 9 1 0 1.33 2.06 0.87 o 0 2 0 300.36 311.18 4.73 o 1 2 0 43.99 60.07 0.82 o 2 2 0 2265.38 2227.06 11.95 o 3 2 0 1446.02 1488.13 27.16 o 4 2 0 105.79 96.98 2.80 o 5 2 0 468.34 482.96 6.10 o 6 2 0 392.25 401.96 5.32 o 7 2 0 536.15 544.64 12.92 o 8 2 0 228.32 230.66 3.47 o 9 2 0 46.21 45.69 1.57 o 1 3 0 153.44 182.26 2.42 o 2 3 0 19.82 17.77 0.49 o 3 3 0 228.31 259.51 3.33 o 4 3 0 100.82 98.18 1.51 o 5 3 0 84.28 93.61 1.57 o 6 3 0 3.56 3.89 0.85 o 7 3 0 0.40 1.24 0.63 o 8 3 0 0.04 0.96 0.71 o 9 3 0 10.50 8.57 1.03 o 0 4 0 2329.09 2585.01 20.12 o 1 4 0 2116.11 2296.58 13.77 o 2 4 0 2897.05 3025.44 33.85 o 3 4 0 1417.42 1518.24 23.15 o 4 4 0 1019.50 1026.76 12.24 o 5 4 0 1586.60 1572.38 16.84 o 6 4 0 510.95 509.67 8.55 o 7 4 0 39.37 43.57 1.31 o 8 4 0 50.61 51.47 1.89 o 1 5 0 27.49 29.39 0.68 o 2 5 0 50.88 61.93 2.06 o 3 5 0 319.63 343.63 4.37 o 4 5 0 1.87 2.90 1.07 o 5 5 0 4.54 3.21 0.56 o 6 5 0 19.80 17.64 0.90 o 7 5 0 0.06 0.78 0.68 o 8 5 0 8.44 10.13 0.97 o 0 6 0 4.43 4.09 0.64 o 1 6 0 483.18 468.89 5.49 o 2 6 0 1374.04 1391.49 13.94 o 3 6 0 613.78 640.88 8.32 o 4 6 0 216.44 238.41 3.34 o 5 6 0 444.88 449.08 9.67 o 6 6 0 554.03 571.11 7.66 o 7 6 0 139.71 136.51 2.37 o 8 6 0 66.46 63.71 1.99 o 1 7 0 0.00 0.65 0.62 o 2 7 0 109.72 116.96 1.84 o 3 7 0 44.96 46.24 1.07 o 4 7 0 105.59 110.31 1.87 o 5 7 0 0.05 -0.22 0.57 o 6 7 0 44.79 46.72 2.67 o 7 7 0 0.12 0.11 0.76 o 0 8 0 711.52 759.00 13.55 o 1 8 0 614.68 633.88 15.48 o 2 8 0 245.45 249.24 3.52 o 3 8 0 253.71 254.99 3.51 o 4 8 0 161.39 172.26 3.48 o 5 8 0 46.39 52.75 1.38 o 6 8 0 111.03 121.15 3.51 o 7 8 0 68.81 72.27 1.87 o 1 9 0 4.07 5.41 0.65 o 2 9 0 2.52 2.01 1.04 o 3 9 0 3.81 3.46 0.68 o 4 9 0 22.58 25.55 2.19 o 5 9 0 8.71 9.52 2.07 o 6 9 0 0.48 1.48 1.14 o 0 10 0 648.75 671.60 11.55 o 1 10 0 373.60 385.97 5.31 o 2 10 0 75.08 77.46 1.71 o 3 10 0 198.55 207.32 3.17 o 4 10 0 289.39 299.85 4.32 o 5 10 0 38.87 40.67 1.46 o 1 11 0 57.58 59.66 2.20 o 2 11 0 5.83 6.31 1.06 o 3 11 0 7.18 5.88 0.93 o 4 11 0 0.62 0.05 0.82 o 0 12 0 9.49 9.54 1.43 o 1 12 0 35.66 38.39 1.42 o 2 12 0 47.36 52.57 1.63 o -9 1 1 146.92 152.21 3.62 o -8 1 1 185.27 193.68 4.19 o -7 1 1 257.60 275.53 5.18 o -6 1 1 90.03 94.05 2.26 o -5 1 1 629.89 667.87 11.11 o -4 1 1 2552.53 2569.99 23.07 o -3 1 1 681.49 690.14 10.33 o -2 1 1 5368.11 5382.12 83.94 o -1 1 1 5031.22 4737.29 70.32 o 0 1 1 4896.51 4568.04 63.95 o 1 1 1 3018.86 2895.09 15.53 o 2 1 1 139.61 133.49 2.31 o 3 1 1 3037.85 2947.57 24.06 o 4 1 1 647.45 662.52 10.72 o 5 1 1 538.87 527.58 9.27 o 6 1 1 796.80 742.25 12.29 o 7 1 1 341.44 350.93 6.32 o 8 1 1 285.71 280.31 5.65 o 9 1 1 94.28 90.66 2.94 o -9 2 1 35.05 34.24 1.96 o -8 2 1 71.85 72.77 2.26 o -7 2 1 1.36 3.23 0.85 o -6 2 1 14.25 15.60 1.02 o -5 2 1 0.00 0.28 0.57 o -4 2 1 146.40 130.95 2.62 o -3 2 1 928.54 1037.61 13.27 o -2 2 1 1214.60 1321.86 12.66 o -1 2 1 4785.52 3889.82 18.52 o 0 2 1 1484.77 1608.57 11.41 o 1 2 1 75.92 74.49 1.35 o 2 2 1 10.63 14.22 0.64 o 3 2 1 622.84 713.56 12.48 o 4 2 1 76.89 95.34 2.23 o 5 2 1 432.31 433.48 7.89 o 6 2 1 1.91 2.10 0.85 o 7 2 1 83.02 84.47 2.38 o 8 2 1 10.08 8.54 1.33 o 9 2 1 0.85 0.51 1.19 o -9 3 1 105.20 108.25 3.06 o -8 3 1 175.93 182.71 4.08 o -7 3 1 645.45 664.91 12.24 o -6 3 1 651.61 662.00 11.16 o -5 3 1 794.63 785.29 12.63 o -4 3 1 1696.02 1678.87 20.17 o -3 3 1 1342.52 1396.04 16.47 o -2 3 1 1569.47 1605.39 15.73 o -1 3 1 342.66 301.54 5.02 o 0 3 1 2260.80 2276.45 16.47 o 1 3 1 3531.09 3658.60 22.22 o 2 3 1 257.07 224.00 4.08 o 3 3 1 1283.71 1297.93 17.53 o 4 3 1 1069.79 1131.05 18.51 o 5 3 1 436.70 460.73 8.43 o 6 3 1 180.18 172.44 3.75 o 7 3 1 95.35 103.22 2.66 o 8 3 1 175.12 177.65 4.15 o -9 4 1 3.27 3.71 1.33 o -8 4 1 0.07 -0.42 1.01 o -7 4 1 11.98 12.72 1.18 o -6 4 1 17.82 16.27 1.12 o -5 4 1 202.17 212.94 4.35 o -4 4 1 0.79 0.76 0.57 o -3 4 1 21.73 22.76 0.89 o -2 4 1 108.20 126.61 2.52 o -1 4 1 141.86 121.02 2.35 o 0 4 1 302.71 343.44 6.17 o 1 4 1 29.16 27.66 0.84 o 2 4 1 2.05 1.87 0.52 o 3 4 1 92.96 106.41 2.24 o 4 4 1 82.68 87.89 2.11 o 5 4 1 233.99 233.47 4.65 o 6 4 1 0.38 -0.81 0.81 o 7 4 1 3.02 6.37 1.15 o 8 4 1 23.47 21.94 1.78 o -8 5 1 24.84 24.90 1.71 o -7 5 1 196.96 190.68 4.15 o -6 5 1 528.56 521.86 9.60 o -5 5 1 390.85 404.42 7.79 o -4 5 1 105.25 100.47 2.36 o -3 5 1 532.50 504.88 9.57 o -2 5 1 1292.10 1265.86 17.07 o -1 5 1 441.99 398.51 6.48 o 0 5 1 624.09 588.86 11.04 o 1 5 1 2915.11 3094.20 25.95 o 2 5 1 2957.24 3070.75 27.25 o 3 5 1 1510.85 1539.46 21.22 o 4 5 1 803.63 855.45 14.40 o 5 5 1 552.43 591.43 10.06 o 6 5 1 407.55 409.26 7.87 o 7 5 1 96.92 94.90 2.78 o 8 5 1 35.64 33.96 2.14 o -8 6 1 5.43 3.62 1.27 o -7 6 1 18.26 18.70 1.46 o -6 6 1 85.19 86.60 2.28 o -5 6 1 77.53 75.92 1.99 o -4 6 1 42.27 39.59 1.40 o -3 6 1 11.11 8.07 0.83 o -2 6 1 0.73 0.71 0.57 o -1 6 1 83.32 86.06 1.93 o 0 6 1 157.62 157.94 3.06 o 1 6 1 1.64 0.01 0.55 o 2 6 1 1.31 2.38 0.64 o 3 6 1 31.14 33.36 1.28 o 4 6 1 327.19 327.42 6.09 o 5 6 1 73.12 77.42 2.12 o 6 6 1 29.75 29.35 1.63 o 7 6 1 2.42 2.07 1.20 o 8 6 1 11.88 8.55 1.58 o -8 7 1 128.23 140.19 3.49 o -7 7 1 194.07 204.58 4.48 o -6 7 1 302.44 317.73 6.53 o -5 7 1 443.78 448.49 8.30 o -4 7 1 353.76 361.96 6.97 o -3 7 1 643.02 676.34 12.77 o -2 7 1 674.11 665.91 12.17 o -1 7 1 700.68 642.35 11.45 o 0 7 1 346.22 318.82 5.75 o 1 7 1 222.74 232.32 4.41 o 2 7 1 373.73 371.91 6.59 o 3 7 1 185.35 189.18 3.87 o 4 7 1 179.31 184.65 3.89 o 5 7 1 118.77 123.10 3.00 o 6 7 1 131.71 133.34 3.19 o 7 7 1 93.59 99.25 3.03 o -7 8 1 0.65 0.02 1.17 o -6 8 1 1.06 -0.38 1.07 o -5 8 1 106.43 113.97 2.74 o -4 8 1 3.26 3.00 0.88 o -3 8 1 143.18 147.86 3.16 o -2 8 1 34.42 34.27 1.39 o -1 8 1 200.31 210.01 4.24 o 0 8 1 244.24 249.79 4.56 o 1 8 1 68.27 64.36 1.75 o 2 8 1 2.57 1.96 0.78 o 3 8 1 248.08 244.44 4.93 o 4 8 1 40.53 39.44 1.67 o 5 8 1 9.40 9.50 1.21 o 6 8 1 1.89 -0.16 1.12 o 7 8 1 38.80 41.52 2.21 o -6 9 1 5.30 4.06 1.26 o -5 9 1 118.21 120.05 3.01 o -4 9 1 135.56 132.46 3.15 o -3 9 1 188.19 178.55 3.88 o -2 9 1 289.65 298.81 5.84 o -1 9 1 699.18 628.96 11.57 o 0 9 1 467.89 461.63 8.14 o 1 9 1 243.03 258.70 5.09 o 2 9 1 397.70 425.10 8.09 o 3 9 1 172.99 183.19 3.99 o 4 9 1 125.16 129.14 3.09 o 5 9 1 170.41 179.85 4.08 o 6 9 1 220.48 232.68 5.15 o -5 10 1 1.22 1.08 1.12 o -4 10 1 0.13 -0.79 1.00 o -3 10 1 34.80 36.67 1.79 o -2 10 1 39.66 39.84 1.74 o -1 10 1 5.66 2.20 0.96 o 0 10 1 27.89 32.35 1.57 o 1 10 1 0.57 -0.89 0.89 o 2 10 1 4.29 4.33 1.06 o 3 10 1 8.51 7.57 1.17 o 4 10 1 29.94 33.52 1.84 o 5 10 1 0.13 1.18 1.16 o -4 11 1 109.39 111.69 3.08 o -3 11 1 179.97 201.30 4.55 o -2 11 1 93.47 99.38 2.75 o -1 11 1 127.84 135.82 3.18 o 0 11 1 121.62 125.64 3.05 o 1 11 1 32.58 33.26 1.81 o 2 11 1 30.68 31.27 1.79 o 3 11 1 60.37 61.46 2.39 o 4 11 1 92.15 100.81 3.01 o -2 12 1 0.37 -1.15 1.15 o -1 12 1 9.02 4.21 1.29 o 0 12 1 18.57 18.44 1.63 o 1 12 1 3.94 0.63 1.18 o 2 12 1 3.94 2.98 1.31 o -9 0 2 62.05 59.24 2.27 o -8 0 2 165.51 177.93 3.81 o -7 0 2 138.32 155.56 3.35 o -6 0 2 162.84 163.21 3.43 o -5 0 2 4.19 4.29 0.69 o -4 0 2 2421.90 2422.39 22.15 o -3 0 2 4571.20 4360.06 25.70 o -2 0 2 347.54 395.86 6.53 o -1 0 2 235.11 270.43 4.67 o 0 0 2 224.71 208.48 3.38 o 1 0 2 8476.65 7331.20 103.30 o 2 0 2 183.54 153.26 2.78 o 3 0 2 7.52 25.41 0.93 o 4 0 2 3119.31 3181.48 30.03 o 5 0 2 1812.20 1801.45 25.42 o 6 0 2 503.75 484.12 8.45 o 7 0 2 103.36 99.40 2.58 o 8 0 2 146.13 145.65 3.49 o -9 1 2 16.29 19.33 1.56 o -8 1 2 0.54 -0.76 0.85 o -7 1 2 50.17 51.84 1.70 o -6 1 2 0.03 0.19 0.64 o -5 1 2 61.91 57.35 1.51 o -4 1 2 81.86 97.85 2.10 o -3 1 2 123.31 139.12 2.78 o -2 1 2 10.35 10.96 0.43 o -1 1 2 214.73 197.49 3.38 o 0 1 2 140.74 160.89 2.69 o 1 1 2 720.27 766.20 9.55 o 2 1 2 2.62 8.34 0.60 o 3 1 2 179.28 218.84 3.87 o 4 1 2 52.74 57.30 1.58 o 5 1 2 62.24 51.76 1.61 o 6 1 2 131.64 110.03 2.60 o 7 1 2 25.45 22.32 1.47 o 8 1 2 3.77 2.73 1.19 o -9 2 2 129.04 132.45 3.30 o -8 2 2 137.55 142.26 3.36 o -7 2 2 402.14 418.00 7.73 o -6 2 2 1676.73 1626.44 23.76 o -5 2 2 1368.15 1421.41 20.06 o -4 2 2 2290.58 2383.92 22.95 o -3 2 2 2983.18 2974.88 22.60 o -2 2 2 4712.21 4725.82 24.85 o -1 2 2 12549.55 11236.40 144.38 o 0 2 2 1282.44 1287.26 11.98 o 1 2 2 1194.32 1176.45 12.74 o 2 2 2 1374.39 1446.10 16.35 o 3 2 2 1654.58 1603.26 19.76 o 4 2 2 1414.39 1396.79 20.94 o 5 2 2 139.35 147.60 3.19 o 6 2 2 269.73 282.88 5.54 o 7 2 2 336.50 326.09 6.46 o 8 2 2 206.24 206.93 4.63 o -9 3 2 3.93 4.69 1.27 o -8 3 2 20.10 20.62 1.43 o -7 3 2 149.98 143.00 3.24 o -6 3 2 158.39 150.53 3.26 o -5 3 2 20.33 16.40 0.94 o -4 3 2 26.60 25.77 0.97 o -3 3 2 1.17 -0.21 0.47 o -2 3 2 115.77 136.22 2.58 o -1 3 2 3511.85 3749.33 22.71 o 0 3 2 185.36 196.89 3.39 o 1 3 2 890.39 980.64 12.82 o 2 3 2 361.41 388.80 6.44 o 3 3 2 10.39 10.52 0.79 o 4 3 2 130.41 129.87 2.90 o 5 3 2 222.59 213.94 4.24 o 6 3 2 3.85 4.55 0.97 o 7 3 2 47.98 48.18 2.02 o 8 3 2 8.48 7.98 1.46 o -9 4 2 159.57 159.62 3.85 o -8 4 2 288.02 288.44 6.08 o -7 4 2 222.51 224.42 4.44 o -6 4 2 104.48 112.87 2.65 o -5 4 2 126.59 124.87 2.72 o -4 4 2 474.18 460.01 7.91 o -3 4 2 194.30 159.67 3.10 o -2 4 2 102.71 63.96 1.48 o -1 4 2 1109.46 1080.14 13.84 o 0 4 2 1704.67 1736.43 17.60 o 1 4 2 3046.63 3024.87 24.44 o 2 4 2 1942.14 2082.86 22.25 o 3 4 2 901.23 982.83 16.96 o 4 4 2 493.17 498.95 8.54 o 5 4 2 231.96 238.62 4.85 o 6 4 2 387.98 389.01 7.19 o 7 4 2 193.81 183.32 4.17 o 8 4 2 26.56 28.78 1.97 o -9 5 2 0.06 1.08 1.17 o -8 5 2 1.06 1.63 1.08 o -7 5 2 3.97 2.28 0.96 o -6 5 2 16.03 14.10 1.11 o -5 5 2 29.52 26.51 1.24 o -4 5 2 19.04 18.06 0.98 o -3 5 2 6.04 3.30 0.62 o -2 5 2 509.37 508.22 9.01 o -1 5 2 71.76 69.20 1.62 o 0 5 2 2.87 1.08 0.52 o 1 5 2 202.82 198.57 3.73 o 2 5 2 6.93 6.66 0.74 o 3 5 2 41.25 44.85 1.39 o 4 5 2 41.04 46.03 1.57 o 5 5 2 12.22 11.07 1.07 o 6 5 2 4.35 7.46 1.15 o 7 5 2 4.08 6.19 1.30 o 8 5 2 0.10 -0.61 1.21 o -8 6 2 80.97 82.02 2.63 o -7 6 2 194.38 196.56 4.53 o -6 6 2 418.72 416.43 8.10 o -5 6 2 587.33 600.70 11.02 o -4 6 2 298.86 289.53 5.43 o -3 6 2 313.03 255.44 4.47 o -2 6 2 1331.97 1219.75 18.60 o -1 6 2 1658.20 1645.12 20.90 o 0 6 2 779.48 789.44 11.89 o 1 6 2 417.43 430.87 7.86 o 2 6 2 918.90 908.05 16.80 o 3 6 2 627.66 619.22 10.60 o 4 6 2 137.23 144.69 3.16 o 5 6 2 85.33 96.55 2.43 o 6 6 2 115.09 117.54 3.00 o 7 6 2 113.70 119.07 3.27 o -8 7 2 2.33 1.29 1.20 o -7 7 2 19.62 21.41 1.58 o -6 7 2 7.99 8.33 1.11 o -5 7 2 56.88 61.23 1.91 o -4 7 2 12.67 9.89 0.97 o -3 7 2 160.19 138.09 2.97 o -2 7 2 59.36 52.05 1.53 o -1 7 2 192.13 198.65 4.11 o 0 7 2 0.43 0.38 0.66 o 1 7 2 49.57 57.43 1.57 o 2 7 2 87.89 92.09 2.21 o 3 7 2 1.79 1.97 0.81 o 4 7 2 41.33 45.13 1.74 o 5 7 2 8.22 9.05 1.17 o 6 7 2 25.63 28.22 1.80 o 7 7 2 1.42 4.33 1.29 o -7 8 2 58.85 57.74 2.33 o -6 8 2 162.51 155.89 3.56 o -5 8 2 298.61 294.22 5.88 o -4 8 2 223.80 212.49 4.27 o -3 8 2 495.15 486.48 9.06 o -2 8 2 785.08 678.06 11.47 o -1 8 2 253.00 243.08 4.58 o 0 8 2 282.33 273.40 5.16 o 1 8 2 420.17 405.66 7.29 o 2 8 2 541.36 586.10 9.89 o 3 8 2 287.31 295.66 5.88 o 4 8 2 236.14 236.70 4.79 o 5 8 2 397.90 411.08 7.78 o 6 8 2 193.22 197.35 4.44 o -6 9 2 3.76 3.78 1.18 o -5 9 2 0.20 0.31 0.98 o -4 9 2 3.64 0.63 0.96 o -3 9 2 1.13 1.05 0.82 o -2 9 2 28.19 26.54 1.38 o -1 9 2 13.41 13.05 1.13 o 0 9 2 0.21 -0.73 0.73 o 1 9 2 5.13 3.64 0.91 o 2 9 2 15.40 15.01 1.25 o 3 9 2 34.41 33.70 1.65 o 4 9 2 0.45 0.27 1.00 o 5 9 2 7.18 7.80 1.33 o -6 10 2 28.70 26.85 1.88 o -5 10 2 54.40 58.83 2.28 o -4 10 2 146.15 145.36 3.52 o -3 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1.20 o -1 5 10 8.59 7.10 1.35 o 0 5 10 0.25 0.72 1.18 o 1 5 10 42.09 41.99 2.19 o 2 5 10 30.30 30.39 2.00 o -6 6 10 155.99 154.82 3.94 o -5 6 10 174.59 181.70 4.26 o -4 6 10 133.01 125.82 3.30 o -3 6 10 141.29 141.49 3.67 o -2 6 10 230.61 248.90 5.11 o -1 6 10 148.25 145.20 3.54 o 0 6 10 60.98 52.05 2.35 o 1 6 10 31.77 31.41 1.98 o -4 7 10 21.13 21.35 1.75 o -3 7 10 3.08 3.12 1.25 o -2 7 10 42.83 45.22 2.21 o -1 7 10 1.73 0.37 1.21 o 0 7 10 12.04 11.51 1.60 o -7 1 11 104.29 111.12 3.19 o -6 1 11 56.89 63.03 2.43 o -5 1 11 93.11 100.80 2.87 o -4 1 11 66.07 68.08 2.35 o -3 1 11 348.62 346.54 6.98 o -2 1 11 361.74 369.25 7.17 o -1 1 11 40.52 37.88 1.92 o 0 1 11 148.97 143.59 3.53 o 1 1 11 160.19 168.10 3.94 o 2 1 11 72.69 71.73 2.74 o -7 2 11 1.42 1.13 1.21 o -6 2 11 29.00 33.17 1.96 o -5 2 11 3.59 5.47 1.26 o -4 2 11 0.91 2.18 1.11 o -3 2 11 73.82 70.00 2.45 o -2 2 11 2.43 2.69 1.11 o -1 2 11 13.58 13.32 1.45 o 0 2 11 6.31 4.06 1.28 o 1 2 11 1.16 1.71 1.21 o -6 3 11 98.03 102.16 3.02 o 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