#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/75/2017511.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017511_Fobs loop_ _publ_author_name 'Spencer, John' 'Chowdhry, Babur Z.' 'Hamid, Samiyah' 'Mendham, Andrew P.' 'Male, Louise' 'Coles, Simon J.' 'Hursthouse, Michael B.' _publ_section_title ; Seven 3-methylidene-1H-indol-2(3H)-ones related to the multiple-receptor tyrosine kinase inhibitor sunitinib ; _journal_coeditor_code GG3207 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o71 _journal_page_last o78 _journal_volume 66 _journal_year 2010 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.6031 _cell_length_b 6.2725 _cell_length_c 22.6997 _exptl_crystal_F_000 880.00 _reflns_d_resolution_high 0.8402 _[local]_cod_data_source_file gg32072asup2.hkl _[local]_cod_data_source_block 2a #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2007src1202 in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 142.01 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 358.31 273.71 14.38 o 8 0 0 502.50 412.99 17.02 o 10 0 0 1049.55 1082.30 41.85 o 12 0 0 786.45 868.17 43.91 o 14 0 0 210.58 186.70 27.52 o 2 1 0 15446.71 13224.55 628.85 o 6 1 0 62.62 70.16 7.39 o 8 1 0 7595.38 7701.62 133.47 o 10 1 0 92.19 111.22 10.94 o 12 1 0 81.71 90.81 13.63 o 14 1 0 15.40 14.91 11.87 o 16 1 0 213.56 179.71 40.93 o 0 2 0 78.97 41.08 13.51 o 2 2 0 1086.33 978.74 32.13 o 4 2 0 1197.66 1277.24 35.93 o 6 2 0 3463.64 3487.79 61.59 o 8 2 0 3597.90 3531.71 91.35 o 10 2 0 1727.22 1808.18 62.59 o 12 2 0 927.21 956.78 41.37 o 14 2 0 562.27 573.29 31.33 o 16 2 0 30.48 46.20 26.98 o 2 3 0 936.78 1026.18 35.17 o 4 3 0 828.64 930.78 28.99 o 6 3 0 3.02 4.29 8.12 o 8 3 0 1260.93 1304.38 42.15 o 10 3 0 44.26 38.87 10.16 o 12 3 0 0.37 27.31 15.52 o 14 3 0 39.63 33.81 21.17 o 0 4 0 5109.64 5635.12 321.64 o 2 4 0 24.77 9.88 16.60 o 4 4 0 1694.45 1806.43 72.51 o 6 4 0 2.44 -1.20 8.36 o 8 4 0 434.43 408.03 33.49 o 10 4 0 61.62 30.37 21.13 o 12 4 0 1397.00 1394.07 69.15 o 14 4 0 32.37 53.42 21.31 o 2 5 0 2756.17 2888.82 127.20 o 4 5 0 4294.17 4401.81 212.31 o 6 5 0 558.79 553.65 32.41 o 8 5 0 2120.53 2016.06 78.29 o 10 5 0 137.50 108.43 17.14 o 12 5 0 0.61 16.18 17.37 o 0 6 0 4635.77 4757.71 436.45 o 2 6 0 543.14 560.03 33.17 o 4 6 0 849.46 843.33 72.46 o 6 6 0 817.80 826.50 68.35 o 8 6 0 185.39 188.28 20.51 o 10 6 0 44.81 46.40 18.76 o 2 7 0 1354.20 1417.59 78.31 o 4 7 0 215.45 210.67 31.44 o 6 7 0 36.37 65.12 18.44 o 1 1 1 8440.46 7373.73 155.26 o 2 1 1 4001.67 3583.24 81.58 o 3 1 1 20168.07 18551.84 307.10 o 4 1 1 12849.50 11977.85 173.44 o 5 1 1 4832.49 4743.43 57.33 o 6 1 1 986.38 981.28 15.30 o 7 1 1 6007.20 6004.14 90.40 o 8 1 1 3567.67 3562.66 49.34 o 9 1 1 1505.18 1508.82 23.27 o 10 1 1 12.37 26.61 5.04 o 11 1 1 50.06 34.83 6.66 o 12 1 1 339.23 355.72 12.05 o 13 1 1 35.67 27.98 8.85 o 14 1 1 26.92 6.58 9.35 o 15 1 1 0.53 -7.42 14.06 o 16 1 1 26.00 3.39 22.18 o 17 1 1 348.75 360.41 60.99 o 0 2 1 52.60 25.46 11.19 o 1 2 1 40.91 33.05 8.63 o 2 2 1 402.06 419.57 12.46 o 3 2 1 436.22 395.14 10.81 o 4 2 1 1285.03 1244.30 23.55 o 5 2 1 674.71 662.11 15.71 o 6 2 1 855.83 844.43 19.60 o 7 2 1 1292.86 1219.10 21.83 o 8 2 1 2381.52 2217.92 34.55 o 9 2 1 309.61 306.38 10.57 o 10 2 1 344.72 336.14 10.95 o 11 2 1 481.55 459.02 16.66 o 12 2 1 493.64 441.61 16.10 o 13 2 1 761.01 765.87 30.55 o 14 2 1 313.56 338.51 18.76 o 15 2 1 23.30 13.68 11.99 o 16 2 1 79.97 70.52 26.09 o 1 3 1 2688.99 2775.87 60.79 o 2 3 1 1665.72 1714.22 35.70 o 3 3 1 819.62 830.44 20.28 o 4 3 1 181.59 217.27 9.02 o 5 3 1 181.60 217.73 12.21 o 6 3 1 467.00 469.84 11.95 o 7 3 1 33.56 34.07 7.69 o 8 3 1 434.60 429.37 18.46 o 9 3 1 232.31 202.01 13.01 o 10 3 1 46.93 53.17 8.77 o 11 3 1 27.21 37.63 10.58 o 12 3 1 147.30 126.49 11.54 o 13 3 1 169.10 152.17 12.11 o 14 3 1 3.62 21.25 9.95 o 15 3 1 7.64 5.40 26.74 o 0 4 1 17.80 20.04 13.54 o 1 4 1 169.15 207.93 13.72 o 2 4 1 117.99 132.93 10.10 o 3 4 1 862.55 929.16 24.47 o 4 4 1 68.92 73.70 8.96 o 5 4 1 0.98 -4.45 7.29 o 6 4 1 170.60 198.16 10.46 o 7 4 1 1240.62 1120.22 31.07 o 8 4 1 313.24 290.16 16.83 o 9 4 1 180.03 186.73 13.14 o 10 4 1 38.17 29.99 9.40 o 11 4 1 181.22 184.47 15.24 o 12 4 1 113.56 106.43 10.48 o 13 4 1 35.13 44.41 10.99 o 14 4 1 52.98 32.49 11.93 o 1 5 1 30.75 422.87 270.42 o 2 5 1 2.69 1.08 10.76 o 3 5 1 6.89 8.27 12.24 o 4 5 1 2.95 -0.95 10.28 o 5 5 1 236.65 234.55 15.68 o 6 5 1 249.75 255.35 21.71 o 7 5 1 128.35 127.43 10.60 o 8 5 1 19.18 31.68 9.39 o 9 5 1 104.83 107.94 12.48 o 10 5 1 187.95 192.51 15.70 o 11 5 1 260.60 250.60 16.91 o 12 5 1 0.05 22.18 17.94 o 0 6 1 330.81 309.35 33.63 o 1 6 1 14.88 24.75 11.60 o 2 6 1 36.84 57.29 13.02 o 3 6 1 48.67 88.34 13.07 o 4 6 1 116.53 111.98 12.53 o 5 6 1 39.35 82.49 23.83 o 6 6 1 43.11 54.38 13.04 o 7 6 1 24.97 34.43 8.62 o 8 6 1 23.71 25.94 8.70 o 9 6 1 25.96 57.75 12.99 o 10 6 1 9.69 15.50 13.11 o 1 7 1 115.64 120.20 15.71 o 2 7 1 84.13 81.82 13.37 o 3 7 1 67.99 53.10 11.75 o 4 7 1 126.41 165.66 19.24 o 5 7 1 4.94 -12.58 12.25 o 6 7 1 80.93 86.12 17.77 o 2 0 2 3683.41 3368.15 108.35 o 3 0 2 1163.07 1170.25 34.26 o 4 0 2 38.58 58.20 4.59 o 5 0 2 35.85 39.75 4.42 o 6 0 2 1003.73 973.89 19.20 o 7 0 2 65.32 73.62 10.20 o 8 0 2 2682.10 2624.79 53.50 o 9 0 2 394.90 451.02 14.07 o 10 0 2 507.98 481.73 16.68 o 11 0 2 235.48 233.66 12.95 o 12 0 2 0.02 -0.42 12.21 o 13 0 2 462.19 440.14 24.68 o 14 0 2 132.01 158.38 14.95 o 15 0 2 46.01 50.08 64.56 o 16 0 2 460.03 487.86 77.83 o 17 0 2 0.07 -25.19 28.93 o 1 1 2 9031.78 7702.87 249.82 o 2 1 2 1291.79 1202.44 24.41 o 3 1 2 5216.88 4728.66 84.58 o 4 1 2 10326.85 9719.93 150.75 o 5 1 2 887.70 845.29 14.14 o 6 1 2 2608.44 2484.68 30.73 o 7 1 2 263.32 267.79 6.75 o 8 1 2 219.80 257.06 7.26 o 9 1 2 15.82 27.11 4.39 o 10 1 2 92.55 100.18 6.11 o 11 1 2 0.36 5.57 4.95 o 12 1 2 686.26 709.08 19.84 o 13 1 2 5.89 6.41 6.34 o 14 1 2 194.79 197.10 13.18 o 15 1 2 0.41 -17.99 13.57 o 16 1 2 170.15 118.57 29.44 o 17 1 2 46.48 55.49 28.48 o 0 2 2 251.20 218.86 15.58 o 1 2 2 2734.61 2594.02 46.38 o 2 2 2 645.57 642.39 14.75 o 3 2 2 656.78 585.46 14.24 o 4 2 2 1204.84 1195.61 24.38 o 5 2 2 4176.13 4152.85 61.61 o 6 2 2 1932.81 1956.60 36.31 o 7 2 2 4580.87 4531.07 70.16 o 8 2 2 4295.50 4331.31 69.37 o 9 2 2 2244.39 2319.50 49.56 o 10 2 2 770.47 785.33 20.51 o 11 2 2 1086.24 1026.73 30.39 o 12 2 2 1030.72 1011.86 32.40 o 13 2 2 559.84 562.78 21.11 o 14 2 2 14.90 38.53 13.20 o 15 2 2 47.52 72.66 16.64 o 16 2 2 48.04 32.48 29.24 o 1 3 2 372.88 383.47 13.76 o 2 3 2 1094.69 1043.91 23.75 o 3 3 2 1087.65 1025.97 22.99 o 4 3 2 5.62 7.47 5.85 o 5 3 2 269.47 303.65 9.34 o 6 3 2 0.03 11.19 4.14 o 7 3 2 126.57 142.87 10.10 o 8 3 2 345.70 337.38 13.69 o 9 3 2 127.76 151.06 9.48 o 10 3 2 152.43 138.66 10.13 o 11 3 2 2917.32 2993.70 76.94 o 12 3 2 2024.73 1990.98 57.48 o 13 3 2 62.61 59.62 9.04 o 14 3 2 175.70 212.92 16.12 o 15 3 2 1339.13 1350.44 54.03 o 0 4 2 389.47 413.50 29.42 o 1 4 2 412.68 442.24 20.05 o 2 4 2 83.72 92.00 9.49 o 3 4 2 467.17 470.63 17.16 o 4 4 2 42.52 38.33 6.80 o 5 4 2 588.92 602.29 24.45 o 6 4 2 425.20 412.07 16.47 o 7 4 2 733.14 704.58 19.40 o 8 4 2 161.48 160.52 12.14 o 9 4 2 74.63 81.48 9.67 o 10 4 2 683.56 730.15 34.96 o 11 4 2 27.97 61.50 9.96 o 12 4 2 24.15 23.67 12.43 o 13 4 2 0.31 3.36 12.32 o 14 4 2 360.60 349.17 23.09 o 1 5 2 66.95 61.52 19.73 o 2 5 2 56.02 58.13 9.94 o 3 5 2 9.08 20.92 9.27 o 4 5 2 623.61 625.50 23.78 o 5 5 2 4.89 -0.67 8.99 o 6 5 2 489.66 449.14 20.25 o 7 5 2 9.88 11.24 6.54 o 8 5 2 82.09 64.01 10.65 o 9 5 2 0.03 -14.32 12.90 o 10 5 2 158.87 151.16 16.15 o 11 5 2 0.01 7.76 11.63 o 12 5 2 47.48 114.58 17.14 o 0 6 2 417.95 394.41 27.86 o 1 6 2 50.46 15.95 14.29 o 2 6 2 124.07 109.30 14.11 o 3 6 2 433.76 408.66 27.96 o 4 6 2 10.39 46.83 12.17 o 5 6 2 34.08 25.91 9.86 o 6 6 2 89.50 76.78 13.03 o 7 6 2 132.39 104.30 11.42 o 8 6 2 470.64 451.62 24.63 o 9 6 2 28.95 16.29 13.78 o 10 6 2 12.99 38.53 13.07 o 1 7 2 160.19 157.84 19.77 o 2 7 2 1.29 8.57 10.91 o 3 7 2 6.78 19.66 13.58 o 4 7 2 297.88 262.40 28.36 o 5 7 2 12.41 -1.58 16.07 o 1 1 3 1141.04 1056.12 21.57 o 2 1 3 5928.45 5605.02 106.74 o 3 1 3 164.33 134.21 5.39 o 4 1 3 3723.80 3664.06 58.18 o 5 1 3 230.35 261.74 9.38 o 6 1 3 96.69 128.51 5.49 o 7 1 3 64.72 61.79 5.10 o 8 1 3 337.19 360.49 8.41 o 9 1 3 821.21 857.09 16.28 o 10 1 3 295.00 308.08 8.52 o 11 1 3 11.47 13.88 6.32 o 12 1 3 7.15 10.75 4.79 o 13 1 3 201.05 193.67 9.34 o 14 1 3 19.43 22.41 10.76 o 15 1 3 24.00 36.39 13.96 o 16 1 3 14.90 22.56 20.69 o 17 1 3 17.37 133.73 42.19 o 0 2 3 4405.67 4218.09 107.58 o 2 2 3 714.76 762.33 20.39 o 3 2 3 120.32 109.30 9.62 o 4 2 3 54.85 50.73 5.83 o 5 2 3 761.67 764.77 15.34 o 6 2 3 432.35 488.72 14.32 o 7 2 3 232.28 242.28 9.36 o 8 2 3 935.90 931.44 20.51 o 9 2 3 4.56 18.54 9.44 o 10 2 3 19.29 30.59 6.31 o 11 2 3 255.22 234.81 10.01 o 12 2 3 235.90 236.16 14.11 o 13 2 3 54.65 60.73 9.27 o 14 2 3 1.76 16.90 8.56 o 15 2 3 30.18 30.92 13.17 o 16 2 3 176.51 251.65 39.38 o 1 3 3 369.68 412.48 13.39 o 2 3 3 24.44 42.42 7.60 o 3 3 3 15.54 28.12 7.60 o 4 3 3 17.55 17.07 5.29 o 5 3 3 293.69 299.68 10.23 o 6 3 3 347.80 347.28 9.55 o 7 3 3 3.76 8.26 6.53 o 8 3 3 175.90 157.82 10.07 o 9 3 3 89.09 101.49 9.09 o 10 3 3 462.37 483.76 17.80 o 11 3 3 360.95 358.62 15.47 o 12 3 3 295.34 270.63 13.89 o 13 3 3 28.72 36.01 7.34 o 14 3 3 79.01 87.33 20.48 o 15 3 3 439.23 350.47 26.37 o 0 4 3 1324.96 1342.12 41.23 o 1 4 3 8.56 11.27 8.04 o 2 4 3 796.23 747.69 23.57 o 3 4 3 0.37 17.01 7.93 o 4 4 3 112.38 102.11 8.30 o 5 4 3 243.38 263.83 11.22 o 6 4 3 1079.43 1064.07 30.24 o 7 4 3 76.70 72.11 7.09 o 8 4 3 31.29 21.90 10.16 o 9 4 3 558.72 498.16 22.54 o 10 4 3 0.69 16.88 8.63 o 11 4 3 53.39 42.57 13.08 o 12 4 3 0.51 -5.11 9.84 o 13 4 3 320.10 269.39 21.26 o 14 4 3 48.03 76.56 15.69 o 1 5 3 274.13 264.96 20.24 o 2 5 3 1515.86 1526.96 43.09 o 3 5 3 1.92 26.18 10.68 o 4 5 3 75.21 68.97 9.72 o 5 5 3 256.77 233.64 15.88 o 6 5 3 0.05 6.93 9.62 o 7 5 3 137.22 136.90 12.75 o 8 5 3 132.09 122.99 7.87 o 9 5 3 2.42 24.76 14.01 o 10 5 3 75.72 68.03 16.67 o 11 5 3 46.85 51.65 12.14 o 12 5 3 86.83 72.04 13.56 o 0 6 3 4.41 3.51 11.48 o 1 6 3 368.06 338.09 17.56 o 2 6 3 8.18 -10.55 12.29 o 3 6 3 616.56 698.64 25.65 o 4 6 3 0.01 2.34 12.64 o 5 6 3 1.58 1.53 12.95 o 6 6 3 1.64 -0.87 9.29 o 7 6 3 53.84 61.81 11.66 o 8 6 3 18.58 28.52 10.98 o 9 6 3 1.98 -6.34 13.94 o 10 6 3 3.51 34.59 13.01 o 1 7 3 16.91 37.42 13.26 o 2 7 3 2.04 29.26 18.75 o 3 7 3 187.30 187.84 16.25 o 4 7 3 75.24 113.70 14.74 o 5 7 3 13.36 33.77 13.48 o 0 0 4 5559.98 4924.59 171.74 o 1 0 4 9337.46 8453.51 242.80 o 2 0 4 302.79 302.13 13.51 o 3 0 4 434.60 347.11 11.78 o 4 0 4 174.71 177.53 9.55 o 5 0 4 2528.02 2536.63 52.46 o 6 0 4 241.81 235.75 10.54 o 7 0 4 79.92 75.32 9.82 o 8 0 4 417.39 399.45 14.44 o 9 0 4 1611.53 1669.10 42.90 o 10 0 4 0.54 -11.32 7.54 o 11 0 4 25.26 34.31 8.59 o 12 0 4 8.31 18.71 11.78 o 13 0 4 2823.21 3063.70 110.30 o 14 0 4 5.04 -1.12 9.40 o 15 0 4 10.09 25.47 12.97 o 16 0 4 208.26 204.90 39.23 o 17 0 4 445.27 385.81 56.63 o 1 1 4 116.09 113.56 5.45 o 2 1 4 6818.91 6199.58 103.65 o 3 1 4 923.76 897.72 16.45 o 4 1 4 2499.63 2402.58 37.78 o 5 1 4 4652.07 4590.00 68.55 o 6 1 4 289.09 289.52 7.98 o 7 1 4 121.79 122.96 5.71 o 8 1 4 88.62 94.67 5.90 o 9 1 4 2148.81 2192.87 37.80 o 10 1 4 4.47 10.65 10.56 o 11 1 4 20.37 21.18 5.05 o 12 1 4 193.33 197.29 9.42 o 13 1 4 17.57 16.28 4.92 o 14 1 4 20.77 25.59 8.24 o 15 1 4 24.40 41.09 12.72 o 16 1 4 92.67 108.19 27.07 o 17 1 4 222.83 266.06 48.81 o 0 2 4 3829.70 3389.02 106.88 o 1 2 4 2211.14 2088.95 42.45 o 2 2 4 1406.22 1377.82 29.72 o 3 2 4 1468.30 1439.28 28.17 o 4 2 4 8.01 9.37 4.95 o 5 2 4 0.20 12.18 5.43 o 6 2 4 1958.55 1965.98 33.62 o 7 2 4 108.89 114.68 6.90 o 8 2 4 1564.40 1599.58 32.91 o 9 2 4 6.46 6.31 4.50 o 10 2 4 41.00 27.59 4.29 o 11 2 4 12.76 5.93 3.88 o 12 2 4 705.97 743.87 25.56 o 13 2 4 0.87 6.15 8.83 o 14 2 4 22.31 44.38 9.75 o 15 2 4 285.07 246.91 18.86 o 16 2 4 161.44 182.58 34.45 o 1 3 4 1342.12 1326.97 28.36 o 2 3 4 947.74 1003.29 23.26 o 3 3 4 420.74 444.24 12.02 o 4 3 4 2211.83 2181.72 38.53 o 5 3 4 547.51 558.55 14.02 o 6 3 4 165.42 150.31 6.99 o 7 3 4 176.62 177.05 7.05 o 8 3 4 265.76 198.81 8.97 o 9 3 4 0.01 -9.94 8.59 o 10 3 4 342.79 358.02 14.76 o 11 3 4 713.63 664.79 21.03 o 12 3 4 74.59 58.36 7.90 o 13 3 4 232.86 203.45 11.73 o 14 3 4 9.20 -7.68 13.96 o 15 3 4 250.35 250.72 21.55 o 0 4 4 848.11 877.14 36.96 o 1 4 4 875.38 966.36 21.87 o 2 4 4 152.78 157.59 10.08 o 3 4 4 432.13 475.93 16.72 o 4 4 4 25.67 30.68 6.64 o 5 4 4 1.29 3.50 6.82 o 6 4 4 145.74 170.53 9.47 o 7 4 4 214.73 218.31 10.38 o 8 4 4 182.47 159.13 12.93 o 9 4 4 12.19 4.38 8.46 o 10 4 4 7.00 5.62 9.80 o 11 4 4 16.66 37.68 9.49 o 12 4 4 8.89 15.82 10.75 o 13 4 4 9.96 -0.66 14.46 o 14 4 4 4.46 28.53 18.79 o 1 5 4 1.68 13.94 10.52 o 2 5 4 382.20 362.19 15.73 o 3 5 4 130.89 139.81 11.77 o 4 5 4 423.22 457.67 21.89 o 5 5 4 327.19 328.17 18.89 o 6 5 4 456.69 414.76 18.33 o 7 5 4 27.88 35.11 10.60 o 8 5 4 143.95 134.32 9.11 o 9 5 4 288.14 272.06 17.89 o 10 5 4 107.45 97.36 13.78 o 11 5 4 1.28 28.83 20.05 o 12 5 4 1.69 -6.33 18.71 o 0 6 4 1385.65 1407.78 70.64 o 1 6 4 169.11 160.96 14.04 o 2 6 4 2.35 1831.82 1218.39 o 3 6 4 18.21 29.42 15.65 o 4 6 4 593.67 673.08 30.61 o 5 6 4 251.39 288.44 21.00 o 6 6 4 3.75 -2.24 10.22 o 7 6 4 76.46 85.11 13.12 o 8 6 4 6.06 12.88 10.86 o 9 6 4 49.88 74.38 16.54 o 10 6 4 56.14 67.08 19.69 o 1 7 4 8.88 -6.12 14.25 o 2 7 4 359.04 334.83 21.62 o 3 7 4 18.51 34.12 11.50 o 4 7 4 144.31 174.66 21.59 o 5 7 4 104.66 138.87 14.34 o 1 1 5 1.49 8.25 4.72 o 2 1 5 60.06 54.60 5.04 o 3 1 5 41.25 56.59 4.64 o 4 1 5 1914.85 1911.77 29.94 o 5 1 5 878.67 901.82 16.86 o 6 1 5 829.39 909.17 18.70 o 7 1 5 13.18 32.15 6.63 o 8 1 5 122.93 132.02 5.73 o 9 1 5 358.70 367.76 10.91 o 10 1 5 271.17 270.33 8.52 o 11 1 5 155.29 174.00 7.58 o 12 1 5 15.81 24.62 4.47 o 13 1 5 97.63 102.06 7.21 o 14 1 5 53.58 36.94 10.73 o 15 1 5 84.23 91.47 16.03 o 16 1 5 0.05 46.49 28.13 o 0 2 5 2348.44 2255.43 65.78 o 1 2 5 614.08 659.22 19.10 o 2 2 5 385.68 406.75 11.64 o 3 2 5 3.30 12.38 4.77 o 4 2 5 138.95 140.93 6.34 o 5 2 5 351.81 403.75 10.95 o 6 2 5 432.45 459.37 11.29 o 7 2 5 0.23 -9.15 6.29 o 8 2 5 231.89 242.68 8.20 o 9 2 5 169.18 157.97 6.24 o 10 2 5 4.72 -0.76 4.63 o 11 2 5 13.61 11.15 11.51 o 12 2 5 55.58 48.30 8.35 o 13 2 5 280.35 244.21 16.08 o 14 2 5 8.66 -1.50 13.02 o 15 2 5 14.16 20.20 16.37 o 16 2 5 59.71 25.21 23.25 o 1 3 5 63.43 64.25 7.09 o 2 3 5 113.41 125.09 7.44 o 3 3 5 0.57 8.89 5.01 o 4 3 5 101.28 83.64 7.19 o 5 3 5 69.11 60.68 5.95 o 6 3 5 54.82 52.18 7.03 o 7 3 5 12.99 12.15 4.61 o 8 3 5 320.35 308.71 9.93 o 9 3 5 38.37 47.14 7.65 o 10 3 5 107.61 112.47 8.30 o 11 3 5 259.29 256.33 13.60 o 12 3 5 289.84 283.17 13.69 o 13 3 5 40.32 30.95 7.61 o 14 3 5 95.12 116.99 16.52 o 15 3 5 379.34 426.20 33.25 o 0 4 5 0.75 7.02 8.59 o 1 4 5 7.77 21.88 6.71 o 2 4 5 188.49 200.94 10.45 o 3 4 5 9.59 10.10 6.57 o 4 4 5 451.69 434.32 13.29 o 5 4 5 356.49 373.82 13.04 o 6 4 5 60.24 59.45 8.69 o 7 4 5 396.74 382.63 13.19 o 8 4 5 875.17 826.00 23.76 o 9 4 5 34.20 44.91 9.43 o 10 4 5 68.59 51.77 10.04 o 11 4 5 240.52 241.65 18.07 o 12 4 5 118.33 132.11 13.05 o 13 4 5 6.10 3.73 12.36 o 14 4 5 0.36 1.23 12.03 o 1 5 5 251.41 243.54 19.75 o 2 5 5 37.17 27.56 9.25 o 3 5 5 241.36 250.32 20.09 o 4 5 5 342.67 360.13 17.86 o 5 5 5 229.62 234.73 12.42 o 6 5 5 290.63 283.66 12.77 o 7 5 5 205.67 209.12 16.54 o 8 5 5 14.04 7.45 9.96 o 9 5 5 13.06 10.57 15.78 o 10 5 5 123.92 112.62 13.41 o 11 5 5 96.89 91.03 17.98 o 12 5 5 0.54 13.31 11.62 o 0 6 5 14.63 18.12 17.65 o 1 6 5 772.30 841.96 33.34 o 2 6 5 31.00 46.38 14.30 o 3 6 5 396.18 485.48 25.50 o 4 6 5 2.01 31.94 12.09 o 5 6 5 35.17 37.58 10.66 o 6 6 5 43.29 72.37 11.70 o 7 6 5 26.39 13.91 12.29 o 8 6 5 14.06 4.63 8.31 o 9 6 5 90.08 59.09 12.02 o 1 7 5 52.06 36.75 12.28 o 2 7 5 154.92 152.40 22.92 o 3 7 5 449.62 442.30 38.19 o 4 7 5 70.76 62.40 11.64 o 5 7 5 98.22 100.00 17.89 o 0 0 6 2065.09 2109.81 63.78 o 1 0 6 1911.68 1890.37 42.33 o 2 0 6 0.81 5.06 6.12 o 3 0 6 3693.47 3644.13 74.46 o 4 0 6 15.24 8.89 5.41 o 5 0 6 53.55 71.54 6.27 o 6 0 6 133.45 120.38 11.49 o 7 0 6 1486.83 1578.68 43.86 o 8 0 6 760.55 774.35 28.96 o 9 0 6 200.10 219.02 14.04 o 10 0 6 19.26 30.24 7.59 o 11 0 6 254.47 249.69 13.74 o 12 0 6 216.08 242.54 14.37 o 13 0 6 0.03 3.31 11.15 o 14 0 6 213.41 192.41 17.12 o 15 0 6 21.77 -22.59 23.63 o 16 0 6 175.56 196.07 40.27 o 1 1 6 299.68 303.79 8.75 o 2 1 6 55.08 49.54 5.07 o 3 1 6 32.65 42.45 5.07 o 4 1 6 1.21 -4.56 3.94 o 5 1 6 208.15 220.55 7.84 o 6 1 6 126.04 136.59 5.92 o 7 1 6 266.99 277.34 11.33 o 8 1 6 22.48 20.88 4.69 o 9 1 6 3.43 9.63 4.78 o 10 1 6 358.15 364.99 9.10 o 11 1 6 592.12 597.01 15.38 o 12 1 6 1.65 12.67 5.74 o 13 1 6 5.34 -2.45 6.16 o 14 1 6 50.49 50.04 9.43 o 15 1 6 124.53 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6 235.72 239.45 10.93 o 4 4 6 87.72 82.10 8.98 o 5 4 6 130.31 116.77 7.25 o 6 4 6 351.46 366.06 13.09 o 7 4 6 818.07 802.99 23.79 o 8 4 6 29.69 35.73 5.90 o 9 4 6 743.51 654.29 18.32 o 10 4 6 25.47 42.21 10.48 o 11 4 6 104.90 100.60 18.20 o 12 4 6 71.82 49.02 10.65 o 13 4 6 613.70 616.32 33.51 o 14 4 6 20.72 32.89 16.21 o 1 5 6 1055.02 1205.41 41.35 o 2 5 6 6.85 10.53 6.83 o 3 5 6 434.74 427.72 15.88 o 4 5 6 14.72 17.70 8.42 o 5 5 6 956.85 891.68 26.89 o 6 5 6 2.56 -0.42 8.39 o 7 5 6 32.00 26.28 7.94 o 8 5 6 29.77 36.37 6.43 o 9 5 6 276.51 230.77 10.85 o 10 5 6 15.89 0.11 17.19 o 11 5 6 0.61 -1.11 10.75 o 12 5 6 20.66 22.83 12.92 o 0 6 6 2.48 23.40 22.65 o 1 6 6 11.42 32.23 14.82 o 2 6 6 56.55 45.93 13.27 o 3 6 6 32.51 40.23 18.78 o 4 6 6 14.81 22.26 11.16 o 5 6 6 75.48 113.24 16.29 o 6 6 6 63.56 56.33 12.79 o 7 6 6 21.03 30.80 13.07 o 8 6 6 1.31 2.15 11.79 o 9 6 6 3.71 10.92 13.11 o 1 7 6 1.86 -9.26 13.92 o 2 7 6 23.84 17.41 14.11 o 3 7 6 11.28 13.38 17.85 o 4 7 6 82.08 117.95 15.76 o 1 1 7 2325.78 2359.36 38.02 o 2 1 7 0.99 -1.41 4.93 o 3 1 7 1.94 -4.57 4.65 o 4 1 7 1326.09 1358.67 21.72 o 5 1 7 489.37 475.61 9.62 o 6 1 7 27.56 39.11 4.62 o 7 1 7 130.09 155.84 11.77 o 8 1 7 458.52 515.78 13.22 o 9 1 7 106.42 91.12 6.23 o 10 1 7 99.31 109.27 6.00 o 11 1 7 1391.73 1396.41 31.16 o 12 1 7 70.64 73.26 9.23 o 13 1 7 4.20 -0.45 7.02 o 14 1 7 117.55 115.80 13.07 o 15 1 7 563.60 588.09 33.76 o 16 1 7 0.00 -4.86 21.94 o 1 2 7 1.96 9.23 5.77 o 2 2 7 7.75 10.95 5.62 o 3 2 7 0.09 5.15 5.96 o 4 2 7 22.09 31.60 6.14 o 5 2 7 831.91 864.64 17.85 o 6 2 7 50.75 46.14 6.25 o 7 2 7 1054.45 1111.38 22.54 o 8 2 7 60.23 68.41 6.99 o 9 2 7 9.66 11.40 5.38 o 10 2 7 12.72 5.94 5.71 o 11 2 7 262.39 283.42 13.56 o 12 2 7 0.50 6.11 6.35 o 13 2 7 24.29 29.93 9.44 o 14 2 7 0.49 10.94 14.94 o 15 2 7 0.25 5.19 14.95 o 16 2 7 13.69 17.34 31.37 o 1 3 7 98.93 107.06 13.06 o 2 3 7 5.94 -0.51 8.87 o 3 3 7 458.44 431.30 11.59 o 4 3 7 7.53 21.98 5.64 o 5 3 7 79.51 89.18 7.62 o 6 3 7 5.40 1.22 5.29 o 7 3 7 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13.62 o 3 6 7 1.47 33.62 12.86 o 4 6 7 1206.45 1257.90 45.40 o 5 6 7 16.74 25.37 10.15 o 6 6 7 22.34 32.31 12.52 o 7 6 7 35.02 13.76 18.68 o 8 6 7 44.55 44.87 12.71 o 9 6 7 16.76 2.41 9.67 o 1 7 7 24.86 33.90 13.24 o 2 7 7 6.48 -18.33 13.67 o 3 7 7 33.14 15.72 11.86 o 4 7 7 70.52 79.24 11.87 o 0 0 8 189.98 189.07 14.58 o 1 0 8 508.52 531.15 16.94 o 2 0 8 1111.18 1061.67 23.77 o 3 0 8 7.59 14.47 7.15 o 4 0 8 1227.68 1207.19 30.43 o 5 0 8 155.40 170.96 8.06 o 6 0 8 911.32 922.45 24.97 o 7 0 8 2641.60 2594.88 46.15 o 8 0 8 1029.55 1023.22 33.31 o 9 0 8 0.51 0.49 9.76 o 10 0 8 204.37 241.87 16.52 o 11 0 8 440.62 437.88 17.67 o 12 0 8 54.04 69.40 11.53 o 13 0 8 0.91 2.48 9.81 o 14 0 8 500.86 497.93 26.70 o 15 0 8 127.88 107.39 19.12 o 16 0 8 0.64 43.85 73.09 o 1 1 8 174.20 134.13 6.41 o 2 1 8 1648.91 1665.08 30.91 o 3 1 8 2766.67 2865.37 45.65 o 4 1 8 192.48 184.78 6.61 o 5 1 8 71.75 65.63 5.35 o 6 1 8 246.79 279.16 7.87 o 7 1 8 687.87 730.14 15.91 o 8 1 8 34.17 33.98 6.33 o 9 1 8 131.50 130.69 6.77 o 10 1 8 173.43 196.03 7.56 o 11 1 8 25.05 22.73 6.22 o 12 1 8 0.66 12.15 5.97 o 13 1 8 39.82 46.43 7.11 o 14 1 8 47.84 54.79 13.73 o 15 1 8 0.53 16.70 14.81 o 16 1 8 4.74 0.65 22.26 o 0 2 8 0.95 15.57 11.60 o 1 2 8 33.45 26.86 5.23 o 2 2 8 157.82 189.72 7.23 o 3 2 8 56.65 89.51 5.90 o 4 2 8 325.73 367.82 10.91 o 5 2 8 180.98 215.77 8.85 o 6 2 8 33.64 38.58 5.45 o 7 2 8 112.00 125.51 7.76 o 8 2 8 261.87 271.74 9.51 o 9 2 8 15.35 23.31 5.02 o 10 2 8 49.76 40.19 6.85 o 11 2 8 166.07 166.13 8.91 o 12 2 8 63.47 63.02 7.04 o 13 2 8 199.57 190.68 10.96 o 14 2 8 8.97 -7.69 12.43 o 15 2 8 125.41 112.50 39.97 o 1 3 8 478.52 483.41 17.30 o 2 3 8 1125.25 1245.77 29.87 o 3 3 8 1654.78 1645.67 31.76 o 4 3 8 652.10 630.52 15.36 o 5 3 8 14.68 16.24 5.98 o 6 3 8 17.95 23.35 5.85 o 7 3 8 1445.02 1501.89 36.83 o 8 3 8 42.87 31.35 7.47 o 9 3 8 52.98 46.43 6.36 o 10 3 8 71.65 60.49 7.54 o 11 3 8 638.64 637.70 21.37 o 12 3 8 159.77 162.80 10.11 o 13 3 8 29.67 28.75 11.63 o 14 3 8 347.92 398.23 26.84 o 15 3 8 151.98 165.29 17.75 o 0 4 8 109.90 105.54 14.71 o 1 4 8 141.41 131.37 15.37 o 2 4 8 226.85 231.23 12.27 o 3 4 8 118.01 106.25 9.34 o 4 4 8 37.91 38.11 6.03 o 5 4 8 455.01 484.49 15.68 o 6 4 8 148.91 151.98 9.45 o 7 4 8 505.90 439.58 15.83 o 8 4 8 179.98 151.55 11.62 o 9 4 8 213.64 200.66 10.92 o 10 4 8 4.44 12.70 6.10 o 11 4 8 192.10 167.36 20.92 o 12 4 8 14.87 20.13 10.81 o 13 4 8 37.11 24.13 14.81 o 1 5 8 741.69 772.02 29.43 o 2 5 8 97.17 98.98 13.06 o 3 5 8 1614.61 1699.91 45.85 o 4 5 8 11.20 26.60 8.19 o 5 5 8 90.76 71.27 13.05 o 6 5 8 47.30 49.20 9.16 o 7 5 8 599.25 448.57 25.86 o 8 5 8 4.01 16.11 10.64 o 9 5 8 7.92 31.18 16.36 o 10 5 8 32.61 50.74 15.03 o 11 5 8 3.18 -5.80 11.22 o 0 6 8 849.53 836.33 71.07 o 1 6 8 63.89 58.29 14.12 o 2 6 8 123.87 120.60 15.45 o 3 6 8 5.94 9.25 13.69 o 4 6 8 213.02 254.96 19.24 o 5 6 8 300.14 317.87 25.15 o 6 6 8 184.20 163.76 17.72 o 7 6 8 85.00 81.82 13.44 o 8 6 8 2.42 13.59 15.70 o 1 7 8 229.72 267.81 27.96 o 2 7 8 3.04 9.98 12.96 o 3 7 8 92.82 100.73 13.67 o 1 1 9 893.92 810.27 16.42 o 3 1 9 10.87 16.13 5.03 o 4 1 9 1464.64 1524.60 24.41 o 5 1 9 120.87 141.46 6.00 o 6 1 9 192.91 184.60 7.46 o 7 1 9 83.39 55.14 5.04 o 8 1 9 4.95 10.87 5.61 o 9 1 9 990.14 1030.83 24.77 o 10 1 9 66.02 74.27 6.22 o 11 1 9 4.13 9.38 4.23 o 12 1 9 95.43 95.50 11.05 o 13 1 9 141.66 134.13 9.76 o 14 1 9 178.90 191.75 14.64 o 15 1 9 19.99 36.31 14.53 o 16 1 9 2.25 43.58 25.09 o 0 2 9 7693.89 8005.83 146.36 o 1 2 9 2295.27 2530.42 40.94 o 2 2 9 23.49 34.40 5.57 o 3 2 9 446.00 609.21 12.52 o 4 2 9 1328.46 1387.78 25.22 o 5 2 9 3939.21 4121.33 71.60 o 6 2 9 772.96 803.90 17.62 o 7 2 9 522.65 581.11 14.19 o 8 2 9 3.90 15.29 5.95 o 9 2 9 631.53 646.96 17.11 o 10 2 9 966.02 989.12 25.11 o 11 2 9 37.15 43.52 6.16 o 12 2 9 142.42 145.87 9.89 o 13 2 9 31.55 29.97 10.47 o 14 2 9 90.45 88.02 14.38 o 15 2 9 46.09 48.66 13.56 o 1 3 9 415.50 390.90 14.24 o 2 3 9 178.08 171.02 7.99 o 3 3 9 375.65 399.83 12.56 o 4 3 9 39.86 48.56 6.87 o 5 3 9 45.69 53.80 7.42 o 6 3 9 63.16 54.32 6.24 o 7 3 9 0.51 2.75 6.75 o 8 3 9 36.24 50.02 6.98 o 9 3 9 55.04 46.36 8.87 o 10 3 9 0.07 18.17 6.49 o 11 3 9 199.73 201.99 16.09 o 12 3 9 77.56 88.97 14.43 o 13 3 9 120.80 121.00 21.79 o 14 3 9 0.06 48.23 14.99 o 0 4 9 490.42 478.50 25.14 o 1 4 9 875.34 925.15 30.02 o 2 4 9 57.72 51.81 10.63 o 3 4 9 10.33 9.88 8.90 o 4 4 9 256.10 266.90 13.00 o 5 4 9 2520.09 2447.13 67.84 o 6 4 9 10.20 24.40 7.91 o 7 4 9 5.03 2.84 8.48 o 8 4 9 151.24 132.03 10.04 o 9 4 9 841.87 815.47 25.42 o 10 4 9 118.05 111.19 8.38 o 11 4 9 1.63 -1.63 11.17 o 12 4 9 78.42 63.63 15.02 o 13 4 9 75.19 85.60 25.32 o 1 5 9 78.36 106.70 15.47 o 2 5 9 968.94 1022.66 35.48 o 3 5 9 621.53 687.89 27.53 o 4 5 9 178.74 142.23 14.56 o 5 5 9 82.77 97.39 9.33 o 6 5 9 16.18 -5.86 8.67 o 7 5 9 286.64 291.92 17.03 o 8 5 9 299.65 248.12 13.95 o 9 5 9 69.82 40.57 8.68 o 10 5 9 44.57 44.91 12.68 o 11 5 9 7.62 10.04 19.97 o 0 6 9 672.02 681.92 46.88 o 1 6 9 297.97 281.05 20.93 o 2 6 9 86.71 96.29 13.53 o 3 6 9 24.86 26.61 13.92 o 4 6 9 139.43 134.44 15.09 o 5 6 9 445.19 537.48 27.98 o 6 6 9 317.97 319.78 22.38 o 7 6 9 58.90 38.43 22.31 o 8 6 9 81.17 81.79 16.09 o 1 7 9 183.22 168.47 17.57 o 0 0 10 1364.64 1329.37 49.08 o 1 0 10 3851.74 3980.47 67.16 o 2 0 10 2989.41 3208.90 58.23 o 3 0 10 8257.71 8388.26 181.73 o 4 0 10 961.63 986.25 25.02 o 5 0 10 177.58 157.35 9.61 o 6 0 10 3210.44 3205.36 74.16 o 7 0 10 3.07 10.67 6.54 o 8 0 10 587.27 605.91 19.67 o 9 0 10 444.87 427.57 15.86 o 10 0 10 101.88 95.18 12.12 o 11 0 10 95.11 85.03 16.19 o 12 0 10 333.85 361.61 20.60 o 13 0 10 1101.18 1096.31 42.51 o 14 0 10 38.60 18.36 39.57 o 15 0 10 56.27 57.01 23.44 o 16 0 10 75.15 -3.35 39.09 o 1 1 10 1230.83 1237.64 20.90 o 2 1 10 6643.65 6972.88 101.84 o 3 1 10 442.78 460.74 11.07 o 4 1 10 14.78 14.77 4.65 o 5 1 10 43.37 36.84 4.97 o 6 1 10 160.09 187.59 7.52 o 7 1 10 606.30 558.06 13.24 o 8 1 10 3.94 13.09 4.82 o 9 1 10 330.46 357.39 15.68 o 10 1 10 74.46 88.43 9.52 o 11 1 10 61.41 59.56 6.44 o 12 1 10 1.19 0.47 8.79 o 13 1 10 0.00 10.49 11.19 o 14 1 10 46.64 57.89 13.46 o 15 1 10 0.99 3.82 19.53 o 0 2 10 648.24 661.45 24.24 o 1 2 10 3.07 3.86 4.86 o 2 2 10 7.94 -1.89 5.15 o 3 2 10 136.41 152.36 7.83 o 4 2 10 245.11 273.34 8.44 o 5 2 10 11.42 1.67 5.29 o 6 2 10 42.30 37.41 5.93 o 7 2 10 253.78 279.07 10.14 o 8 2 10 41.11 40.58 6.13 o 9 2 10 15.32 14.96 5.35 o 10 2 10 11.60 14.77 6.62 o 11 2 10 7.10 9.44 5.84 o 12 2 10 346.34 363.82 13.81 o 13 2 10 47.31 39.92 12.41 o 14 2 10 13.57 10.93 11.91 o 15 2 10 169.54 170.08 22.53 o 1 3 10 516.27 472.35 15.88 o 2 3 10 2612.06 2717.33 55.86 o 3 3 10 54.53 82.25 11.57 o 4 3 10 203.14 206.83 10.94 o 5 3 10 27.76 31.55 7.74 o 6 3 10 771.60 748.57 19.40 o 7 3 10 27.94 20.49 7.15 o 8 3 10 675.87 627.69 19.08 o 9 3 10 415.79 418.68 18.77 o 10 3 10 453.45 412.55 23.23 o 11 3 10 29.16 31.22 7.00 o 12 3 10 333.91 360.91 20.46 o 13 3 10 79.29 116.21 15.83 o 14 3 10 149.41 150.30 21.66 o 0 4 10 1245.90 1328.88 64.99 o 1 4 10 7.21 1.60 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o 3 3 24 150.11 166.93 26.64 o 1 1 25 13.04 12.45 13.77 o 2 1 25 97.48 99.09 18.70 o 3 1 25 48.26 86.36 25.44 o 4 1 25 30.13 33.00 15.60 o 5 1 25 14.45 16.45 33.37 o 6 1 25 101.02 79.40 18.19 o 0 2 25 302.34 276.38 44.68 o 1 2 25 1.42 19.15 13.92 o 2 2 25 69.30 79.28 24.29 o 3 2 25 5.56 18.45 20.28 o 4 2 25 116.17 104.30 34.94 o 0 0 26 97.77 114.27 28.36 o 1 0 26 159.84 147.23 28.86 o 2 0 26 70.63 1757.94 818.25 o 3 0 26 97.71 52.16 28.87 o 4 0 26 45.22 54.59 25.85 o 1 1 26 8.82 24.25 15.78 o 2 1 26 56.32 80.63 17.20 o 3 1 26 39.58 52.50 20.26 o 4 1 26 15.91 36.30 16.80 o 0 2 26 4.04 -45.70 30.47 o