#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/75/2017513.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017513_Fobs loop_ _publ_author_name 'Spencer, John' 'Chowdhry, Babur Z.' 'Hamid, Samiyah' 'Mendham, Andrew P.' 'Male, Louise' 'Coles, Simon J.' 'Hursthouse, Michael B.' _publ_section_title ; Seven 3-methylidene-1H-indol-2(3H)-ones related to the multiple-receptor tyrosine kinase inhibitor sunitinib ; _journal_coeditor_code GG3207 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o71 _journal_page_last o78 _journal_volume 66 _journal_year 2010 _space_group_IT_number 60 _symmetry_space_group_name_Hall '-P 2n 2ab' _symmetry_space_group_name_H-M 'P b c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 19.2250 _cell_length_b 5.0503 _cell_length_c 22.1886 _exptl_crystal_F_000 960.00 _reflns_d_resolution_high 0.8403 _[local]_cod_data_source_file gg32073asup4.hkl _[local]_cod_data_source_block 3a #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2007src1419 in Pbcn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 229.62 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y, -z+1/2' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 9343.85 8388.15 257.34 o 6 0 0 4005.69 3590.31 101.98 o 8 0 0 18692.48 18462.14 551.30 o 10 0 0 2512.65 2839.30 97.56 o 12 0 0 798.36 821.42 36.45 o 14 0 0 5.25 23.57 11.45 o 16 0 0 1994.52 1966.07 88.33 o 18 0 0 167.41 114.75 42.49 o 20 0 0 2513.02 2441.59 217.05 o 22 0 0 27.54 63.25 25.49 o 1 1 0 1182.86 1156.10 33.85 o 3 1 0 2145.28 1921.07 48.03 o 5 1 0 2010.14 1736.01 54.51 o 7 1 0 1144.71 1048.95 30.53 o 9 1 0 27.11 34.94 8.64 o 11 1 0 456.38 539.67 23.64 o 13 1 0 91.56 103.25 11.47 o 15 1 0 149.98 167.53 24.48 o 17 1 0 2097.23 1944.10 106.26 o 19 1 0 1019.50 917.95 45.30 o 21 1 0 252.56 213.16 25.75 o 0 2 0 12673.61 11472.54 419.22 o 2 2 0 0.44 -4.04 9.79 o 4 2 0 1244.87 1320.84 37.44 o 6 2 0 3346.87 3293.24 81.88 o 8 2 0 293.93 251.58 13.43 o 10 2 0 72.71 61.01 20.03 o 12 2 0 232.09 173.34 25.85 o 14 2 0 2570.11 2699.73 126.06 o 16 2 0 1278.07 1225.25 70.05 o 18 2 0 232.38 159.53 52.29 o 20 2 0 3.32 -6.55 21.23 o 1 3 0 381.78 361.04 22.92 o 3 3 0 293.71 308.59 23.33 o 5 3 0 1468.39 1485.33 42.56 o 7 3 0 458.84 500.30 24.41 o 9 3 0 461.12 491.88 26.10 o 11 3 0 125.84 116.38 18.71 o 13 3 0 4296.68 4540.00 190.67 o 15 3 0 2556.71 2981.31 175.81 o 17 3 0 195.64 308.03 44.58 o 19 3 0 498.95 553.18 66.15 o 0 4 0 3029.66 2983.29 136.79 o 2 4 0 60.02 83.86 16.61 o 4 4 0 1265.48 1287.47 61.30 o 6 4 0 41.30 33.89 14.28 o 8 4 0 2074.43 2140.02 105.64 o 10 4 0 794.05 734.72 37.82 o 12 4 0 19.23 70.23 41.36 o 14 4 0 73.16 76.78 123.98 o 16 4 0 21.12 28.89 58.19 o 1 5 0 82.95 72.74 27.14 o 3 5 0 144.65 183.98 30.50 o 5 5 0 191.95 258.81 37.36 o 7 5 0 82.56 60.14 21.36 o 9 5 0 280.40 390.89 32.17 o 11 5 0 19.00 -8.55 36.21 o 0 6 0 1539.67 1801.44 155.84 o 1 1 1 205.46 179.16 8.69 o 2 1 1 3.46 12.95 4.49 o 3 1 1 1232.57 1098.20 22.09 o 4 1 1 645.02 544.51 13.66 o 5 1 1 1974.32 1863.80 37.35 o 6 1 1 4227.54 3948.29 67.19 o 7 1 1 153.90 169.85 9.17 o 8 1 1 1455.86 1506.97 31.13 o 9 1 1 177.90 199.47 7.52 o 10 1 1 23.01 30.44 7.53 o 11 1 1 328.69 306.79 11.67 o 12 1 1 1103.40 1031.44 25.37 o 13 1 1 1.63 -6.89 9.99 o 14 1 1 105.23 97.84 7.98 o 15 1 1 797.22 783.00 29.81 o 16 1 1 151.46 145.31 9.36 o 17 1 1 4.32 0.50 8.26 o 18 1 1 612.58 635.96 27.47 o 19 1 1 26.81 27.14 9.40 o 20 1 1 430.21 432.09 24.14 o 21 1 1 8.85 23.92 9.36 o 22 1 1 77.91 70.19 12.70 o 0 2 1 1285.19 1187.88 36.01 o 1 2 1 233.77 324.48 13.07 o 2 2 1 206.30 229.19 10.81 o 3 2 1 15.74 32.41 7.96 o 4 2 1 430.81 484.82 16.37 o 5 2 1 453.60 432.76 13.22 o 6 2 1 42.57 37.36 5.13 o 7 2 1 501.01 463.86 15.59 o 8 2 1 26.94 35.88 5.37 o 9 2 1 2027.77 2004.71 45.83 o 10 2 1 141.70 141.89 6.15 o 11 2 1 711.16 782.82 23.01 o 12 2 1 5.57 -1.58 10.22 o 13 2 1 101.54 110.11 19.75 o 14 2 1 4.84 24.83 15.45 o 15 2 1 310.05 297.39 24.85 o 16 2 1 259.67 273.34 27.85 o 17 2 1 27.24 3.91 18.52 o 18 2 1 53.59 32.11 13.45 o 19 2 1 0.80 2.03 19.85 o 20 2 1 37.71 79.24 23.33 o 21 2 1 37.26 0.89 17.86 o 1 3 1 1554.75 1588.38 35.49 o 2 3 1 1642.39 1513.77 31.42 o 3 3 1 48.13 62.01 9.50 o 4 3 1 77.61 56.05 7.81 o 5 3 1 140.37 178.83 12.30 o 6 3 1 933.36 954.21 26.18 o 7 3 1 74.37 73.05 9.46 o 8 3 1 1686.60 1613.17 40.42 o 9 3 1 2.94 10.39 7.15 o 10 3 1 114.92 120.15 9.41 o 11 3 1 452.76 418.76 18.78 o 12 3 1 47.16 48.92 8.54 o 13 3 1 9.75 43.62 11.46 o 14 3 1 114.70 95.17 50.56 o 15 3 1 41.52 53.99 22.66 o 16 3 1 31.93 16.78 48.06 o 17 3 1 159.09 146.06 31.02 o 18 3 1 602.51 691.78 52.70 o 19 3 1 35.09 82.29 24.44 o 0 4 1 1408.70 1291.55 58.65 o 1 4 1 135.23 133.46 16.43 o 2 4 1 36.05 30.62 21.72 o 3 4 1 93.67 114.02 13.00 o 4 4 1 752.37 730.49 26.56 o 5 4 1 71.22 75.71 11.48 o 6 4 1 138.99 158.98 18.12 o 7 4 1 1003.21 1075.47 37.23 o 8 4 1 287.92 278.26 15.17 o 9 4 1 834.33 827.41 35.40 o 10 4 1 62.71 61.15 11.02 o 11 4 1 606.03 558.44 32.84 o 12 4 1 445.12 420.45 32.49 o 13 4 1 89.36 109.80 24.89 o 14 4 1 0.42 -11.99 32.29 o 15 4 1 154.26 209.34 34.67 o 16 4 1 119.27 186.62 31.20 o 17 4 1 8.29 1.11 54.20 o 1 5 1 67.10 54.22 17.54 o 2 5 1 127.47 103.81 18.24 o 3 5 1 636.32 621.01 33.16 o 4 5 1 247.17 302.56 21.64 o 5 5 1 0.27 24.38 15.28 o 6 5 1 37.15 52.63 16.80 o 7 5 1 222.22 231.15 25.66 o 8 5 1 902.40 939.21 37.73 o 9 5 1 7.16 16.15 14.44 o 10 5 1 70.72 52.83 16.46 o 11 5 1 5.18 2.87 25.61 o 12 5 1 69.71 91.21 44.55 o 0 6 1 69.83 99.21 41.52 o 1 6 1 164.98 143.73 20.92 o 3 0 2 484.12 464.50 17.11 o 4 0 2 23526.96 20609.11 476.60 o 5 0 2 120.41 94.20 7.43 o 6 0 2 1774.74 1916.63 39.88 o 7 0 2 2567.76 2358.68 47.63 o 8 0 2 15.21 31.16 6.83 o 9 0 2 1840.15 1849.01 41.18 o 10 0 2 10.79 -3.18 9.80 o 11 0 2 1516.82 1692.55 38.49 o 12 0 2 1374.78 1417.57 38.99 o 13 0 2 2481.43 2452.56 72.98 o 14 0 2 152.54 124.33 9.77 o 15 0 2 63.56 66.59 11.91 o 16 0 2 1296.31 1343.08 53.28 o 17 0 2 195.78 172.73 15.54 o 18 0 2 550.18 534.96 30.16 o 19 0 2 1187.60 1155.22 50.10 o 20 0 2 408.84 458.28 34.50 o 21 0 2 258.00 262.23 45.48 o 22 0 2 5.35 -7.05 17.43 o 1 1 2 3172.72 3025.35 54.16 o 2 1 2 22569.44 20449.77 370.95 o 3 1 2 308.99 325.12 10.27 o 4 1 2 749.88 665.48 15.62 o 5 1 2 769.81 756.47 17.27 o 6 1 2 47.49 62.54 5.58 o 7 1 2 327.74 316.60 11.20 o 8 1 2 0.40 6.53 7.11 o 9 1 2 18.98 23.89 7.14 o 10 1 2 3780.29 3815.79 56.96 o 11 1 2 158.22 168.95 10.30 o 12 1 2 421.30 444.23 13.74 o 13 1 2 8.06 18.86 4.34 o 14 1 2 125.46 105.15 8.31 o 15 1 2 46.19 77.96 8.60 o 16 1 2 439.81 437.75 18.92 o 17 1 2 14.65 16.27 6.15 o 18 1 2 442.33 453.58 19.69 o 19 1 2 3.44 10.30 9.98 o 20 1 2 119.10 101.92 13.29 o 21 1 2 128.82 140.54 15.56 o 22 1 2 19.68 4.47 9.86 o 0 2 2 11175.00 10474.90 224.50 o 1 2 2 783.54 777.52 19.90 o 2 2 2 356.04 367.13 13.71 o 3 2 2 1911.41 1857.05 38.46 o 4 2 2 1839.76 1722.90 39.85 o 5 2 2 89.57 95.48 7.07 o 6 2 2 1947.89 1885.53 40.17 o 7 2 2 344.57 346.96 15.13 o 8 2 2 1810.47 1816.05 38.97 o 9 2 2 124.56 122.55 8.45 o 10 2 2 88.67 84.19 12.10 o 11 2 2 876.22 812.61 28.31 o 12 2 2 15.53 17.06 10.23 o 13 2 2 547.57 540.11 21.05 o 14 2 2 601.05 605.56 25.95 o 15 2 2 243.16 225.06 12.41 o 16 2 2 2.45 -10.38 8.37 o 17 2 2 287.64 330.08 28.30 o 18 2 2 0.51 29.74 17.07 o 19 2 2 38.90 92.68 26.00 o 20 2 2 522.51 550.38 46.38 o 21 2 2 21.64 71.29 23.41 o 1 3 2 130.47 106.99 10.53 o 2 3 2 127.36 144.07 12.31 o 3 3 2 263.36 277.69 13.49 o 4 3 2 7.65 20.96 8.62 o 5 3 2 17.83 38.49 8.08 o 6 3 2 2739.63 2827.36 65.66 o 7 3 2 368.28 401.06 17.03 o 8 3 2 206.10 226.84 11.55 o 9 3 2 469.76 504.48 15.45 o 10 3 2 95.63 83.41 17.14 o 11 3 2 809.34 759.01 26.20 o 12 3 2 363.44 351.90 17.79 o 13 3 2 110.88 89.88 28.72 o 14 3 2 28.92 58.80 10.69 o 15 3 2 712.12 737.45 63.95 o 16 3 2 575.66 620.86 55.58 o 17 3 2 0.59 -17.25 37.60 o 18 3 2 0.09 1.36 24.77 o 19 3 2 52.84 90.17 32.70 o 0 4 2 1003.73 981.22 55.31 o 1 4 2 20.31 14.83 10.80 o 2 4 2 8.91 4.74 10.05 o 3 4 2 11.73 34.52 10.81 o 4 4 2 16.95 31.97 11.66 o 5 4 2 69.65 69.61 11.11 o 6 4 2 112.02 85.87 11.48 o 7 4 2 370.00 370.30 18.81 o 8 4 2 105.81 82.11 10.10 o 9 4 2 32.69 38.03 10.21 o 10 4 2 6.12 10.05 7.92 o 11 4 2 438.44 404.39 29.11 o 12 4 2 162.29 169.64 24.97 o 13 4 2 7.87 4.87 16.77 o 14 4 2 51.21 111.56 38.64 o 15 4 2 139.68 151.16 29.58 o 16 4 2 134.78 135.99 36.94 o 1 5 2 38.81 23.99 20.71 o 2 5 2 439.79 446.18 26.11 o 3 5 2 35.07 16.33 14.93 o 4 5 2 124.68 139.74 22.56 o 5 5 2 6.44 46.38 16.18 o 6 5 2 5.57 -12.08 19.18 o 7 5 2 110.22 102.16 16.98 o 8 5 2 8.02 17.79 20.87 o 9 5 2 12.91 41.96 14.19 o 10 5 2 1264.44 1280.36 82.48 o 11 5 2 92.09 71.30 18.97 o 12 5 2 688.13 733.78 66.27 o 1 1 3 3732.29 3382.79 67.05 o 2 1 3 382.04 446.49 10.97 o 3 1 3 1490.21 1349.77 25.33 o 4 1 3 9.02 28.82 4.89 o 5 1 3 2012.80 1721.67 29.92 o 6 1 3 1513.14 1441.14 30.96 o 7 1 3 96.21 116.88 6.47 o 8 1 3 5599.10 5776.74 98.27 o 9 1 3 2388.04 2261.35 41.72 o 10 1 3 159.33 179.03 7.61 o 11 1 3 1731.92 1675.62 33.17 o 12 1 3 170.05 167.84 8.29 o 13 1 3 264.73 242.17 11.18 o 14 1 3 274.16 299.28 15.46 o 15 1 3 194.89 181.92 13.22 o 16 1 3 153.96 159.39 10.74 o 17 1 3 293.02 290.05 15.92 o 18 1 3 135.63 141.14 9.40 o 19 1 3 484.57 482.60 29.29 o 20 1 3 50.83 60.13 13.83 o 21 1 3 43.89 61.12 11.10 o 22 1 3 20.51 15.83 16.55 o 0 2 3 431.15 471.02 21.64 o 1 2 3 5.61 19.08 6.75 o 2 2 3 431.89 451.58 16.53 o 3 2 3 729.28 732.49 18.97 o 4 2 3 1585.92 1661.46 34.11 o 5 2 3 13.68 35.92 6.81 o 6 2 3 20.23 9.96 4.17 o 7 2 3 1150.33 1201.46 24.84 o 8 2 3 348.76 404.28 16.00 o 9 2 3 2.42 13.22 5.74 o 10 2 3 120.12 160.96 10.98 o 11 2 3 18.94 13.60 6.42 o 12 2 3 199.49 200.71 17.67 o 13 2 3 1552.94 1502.89 37.39 o 14 2 3 70.50 68.24 13.26 o 15 2 3 6.80 24.35 10.41 o 16 2 3 14.16 10.86 13.10 o 17 2 3 182.02 155.99 13.85 o 18 2 3 23.75 47.33 21.49 o 19 2 3 16.47 10.40 10.49 o 20 2 3 4.56 -5.18 19.30 o 21 2 3 106.40 140.82 21.68 o 1 3 3 1704.39 1581.81 40.82 o 2 3 3 0.03 9.07 7.50 o 3 3 3 317.46 303.68 15.98 o 4 3 3 1.62 3.46 6.74 o 5 3 3 20.05 26.86 8.76 o 6 3 3 224.45 216.36 12.27 o 7 3 3 51.46 63.38 8.62 o 8 3 3 160.27 137.49 16.17 o 9 3 3 1.59 4.46 7.04 o 10 3 3 385.03 442.10 17.38 o 11 3 3 509.02 527.50 24.16 o 12 3 3 686.06 674.08 28.88 o 13 3 3 141.15 130.58 14.03 o 14 3 3 88.38 75.80 8.68 o 15 3 3 142.89 155.45 24.21 o 16 3 3 302.96 215.46 56.20 o 17 3 3 229.88 200.68 34.22 o 18 3 3 88.50 141.72 29.33 o 19 3 3 29.93 33.16 25.36 o 0 4 3 1226.98 1293.27 60.76 o 1 4 3 1.27 11.73 11.63 o 2 4 3 184.98 175.20 13.87 o 3 4 3 394.73 361.29 20.44 o 4 4 3 28.30 30.85 11.22 o 5 4 3 82.80 92.71 14.33 o 6 4 3 90.46 115.67 14.23 o 7 4 3 62.31 61.57 9.85 o 8 4 3 16.37 28.70 8.20 o 9 4 3 262.83 237.48 14.70 o 10 4 3 118.84 88.70 13.16 o 11 4 3 86.40 101.96 14.96 o 12 4 3 1.07 -9.54 16.94 o 13 4 3 157.76 178.14 33.28 o 14 4 3 2.40 39.67 23.19 o 15 4 3 0.35 6.00 25.76 o 16 4 3 112.15 105.76 35.41 o 1 5 3 8.42 -6.54 24.57 o 2 5 3 678.56 697.88 32.22 o 3 5 3 380.94 390.80 28.21 o 4 5 3 81.73 83.76 15.38 o 5 5 3 255.64 255.13 23.13 o 6 5 3 50.06 57.50 16.70 o 7 5 3 25.02 31.17 14.73 o 8 5 3 24.54 71.31 15.93 o 9 5 3 74.29 66.07 17.00 o 10 5 3 114.60 149.93 28.21 o 11 5 3 226.27 261.47 47.10 o 12 5 3 316.66 336.77 47.97 o 0 0 4 19702.45 17924.19 897.85 o 1 0 4 357.27 271.88 13.94 o 2 0 4 3573.93 3300.66 96.71 o 3 0 4 924.84 822.25 26.56 o 4 0 4 7130.26 6543.55 186.19 o 5 0 4 47.49 56.52 7.33 o 6 0 4 4849.57 4844.94 106.60 o 7 0 4 48.61 70.06 9.15 o 8 0 4 235.29 235.23 12.77 o 9 0 4 990.54 1060.30 29.05 o 10 0 4 367.20 389.15 16.18 o 11 0 4 458.82 467.03 16.55 o 12 0 4 208.03 238.88 13.74 o 13 0 4 3.97 14.56 8.66 o 14 0 4 1887.50 1827.08 55.61 o 15 0 4 875.14 899.52 33.49 o 16 0 4 16.07 28.14 7.73 o 17 0 4 1065.28 1005.51 43.11 o 18 0 4 305.32 277.35 19.34 o 19 0 4 126.86 159.82 15.15 o 20 0 4 0.05 46.07 34.58 o 21 0 4 291.84 293.77 78.09 o 22 0 4 70.80 69.50 23.85 o 1 1 4 7053.18 6909.67 133.50 o 2 1 4 21650.87 20594.60 393.91 o 3 1 4 2635.85 2584.31 46.00 o 4 1 4 1598.55 1501.16 33.01 o 5 1 4 0.71 8.50 3.89 o 6 1 4 1811.04 1731.51 34.76 o 7 1 4 423.05 478.33 12.03 o 8 1 4 1217.71 1372.04 23.79 o 9 1 4 431.10 473.38 14.98 o 10 1 4 309.52 293.37 15.24 o 11 1 4 166.73 158.43 9.32 o 12 1 4 16.01 36.63 8.23 o 13 1 4 16.80 20.44 7.18 o 14 1 4 19.68 48.31 6.27 o 15 1 4 104.65 96.18 8.22 o 16 1 4 88.90 96.66 8.58 o 17 1 4 656.39 669.84 22.81 o 18 1 4 193.74 160.51 11.70 o 19 1 4 216.20 189.52 15.05 o 20 1 4 5.46 -0.80 6.94 o 21 1 4 67.70 45.84 9.86 o 22 1 4 51.83 53.26 15.83 o 0 2 4 16483.90 16371.69 373.85 o 1 2 4 11.11 9.41 6.25 o 2 2 4 2.61 -1.70 5.85 o 3 2 4 1892.86 1802.40 40.41 o 4 2 4 2782.95 2986.38 51.94 o 5 2 4 1848.73 1840.74 37.07 o 6 2 4 9.66 28.54 5.11 o 7 2 4 458.55 473.57 14.60 o 8 2 4 1763.75 1859.45 44.14 o 9 2 4 1039.08 1128.85 29.98 o 10 2 4 0.05 0.72 8.08 o 11 2 4 1375.35 1380.74 40.97 o 12 2 4 189.97 199.69 12.54 o 13 2 4 740.16 788.49 29.86 o 14 2 4 617.88 619.76 24.65 o 15 2 4 201.76 211.15 23.05 o 16 2 4 122.43 109.03 14.00 o 17 2 4 919.98 932.35 36.94 o 18 2 4 206.23 208.05 14.99 o 19 2 4 453.88 461.35 31.20 o 20 2 4 886.62 1016.77 60.53 o 21 2 4 74.22 80.68 31.75 o 1 3 4 557.16 508.26 18.03 o 2 3 4 727.85 738.50 19.47 o 3 3 4 1300.74 1388.70 34.50 o 4 3 4 6.81 6.83 11.39 o 5 3 4 1104.99 1280.52 33.43 o 6 3 4 419.67 446.99 19.63 o 7 3 4 612.16 617.33 20.04 o 8 3 4 178.86 186.38 11.62 o 9 3 4 56.66 49.24 9.09 o 10 3 4 1032.59 1050.07 32.37 o 11 3 4 625.83 683.74 27.46 o 12 3 4 333.03 299.72 19.28 o 13 3 4 1913.30 1946.63 59.20 o 14 3 4 149.74 155.24 18.06 o 15 3 4 115.08 112.57 12.51 o 16 3 4 14.95 45.48 29.20 o 17 3 4 38.79 28.03 21.36 o 18 3 4 385.65 509.02 36.58 o 19 3 4 1.22 -7.71 24.83 o 0 4 4 224.71 207.21 21.74 o 1 4 4 37.92 34.69 15.45 o 2 4 4 4.29 4.08 10.86 o 3 4 4 16.83 19.59 9.72 o 4 4 4 35.24 21.65 11.75 o 5 4 4 71.65 46.40 15.35 o 6 4 4 1800.76 1764.00 48.94 o 7 4 4 107.30 59.68 17.01 o 8 4 4 2.21 5.40 11.09 o 9 4 4 80.82 90.92 16.41 o 10 4 4 341.68 334.72 20.79 o 11 4 4 264.45 261.18 16.31 o 12 4 4 13.64 12.15 14.76 o 13 4 4 202.13 234.65 29.37 o 14 4 4 512.69 571.00 45.84 o 15 4 4 6.68 -16.64 26.49 o 16 4 4 4.79 -28.39 84.17 o 1 5 4 829.73 862.10 33.68 o 2 5 4 710.10 779.66 37.45 o 3 5 4 0.29 -4.93 15.14 o 4 5 4 378.69 384.72 24.73 o 5 5 4 343.09 390.61 25.80 o 6 5 4 673.12 694.48 33.98 o 7 5 4 57.10 75.34 18.67 o 8 5 4 370.16 378.32 28.57 o 9 5 4 19.84 33.85 21.64 o 10 5 4 22.16 25.19 26.39 o 11 5 4 25.32 58.42 30.87 o 12 5 4 53.12 118.93 30.95 o 1 1 5 23249.90 21396.86 370.31 o 2 1 5 52725.84 50962.27 833.28 o 3 1 5 4693.26 4433.87 88.02 o 4 1 5 512.40 531.31 13.62 o 5 1 5 1551.16 1631.56 30.24 o 6 1 5 106.20 94.55 8.84 o 7 1 5 2049.71 2164.89 42.36 o 8 1 5 2000.69 1969.72 42.77 o 9 1 5 0.06 -0.17 4.98 o 10 1 5 748.26 745.65 17.95 o 11 1 5 310.15 326.86 12.01 o 12 1 5 1341.73 1335.33 35.31 o 13 1 5 106.80 132.66 6.77 o 14 1 5 1836.57 1859.17 45.79 o 15 1 5 76.28 58.28 7.30 o 16 1 5 470.17 434.24 17.41 o 17 1 5 184.98 141.30 12.89 o 18 1 5 29.16 31.97 7.81 o 19 1 5 187.58 165.84 11.62 o 20 1 5 9.14 9.18 16.14 o 21 1 5 137.09 132.87 16.44 o 22 1 5 128.66 117.53 24.46 o 0 2 5 726.58 774.11 28.95 o 1 2 5 218.32 257.63 11.48 o 2 2 5 52.27 67.78 7.38 o 3 2 5 1625.17 1816.15 35.06 o 4 2 5 513.78 559.20 15.24 o 5 2 5 124.04 117.06 8.20 o 6 2 5 162.15 159.00 11.26 o 7 2 5 189.68 207.47 8.79 o 8 2 5 18.09 29.96 3.74 o 9 2 5 36.23 57.84 9.80 o 10 2 5 291.41 266.44 15.73 o 11 2 5 748.12 709.29 22.85 o 12 2 5 50.70 43.52 8.19 o 13 2 5 285.49 275.55 14.47 o 14 2 5 527.26 514.63 21.06 o 15 2 5 1021.16 1025.39 36.19 o 16 2 5 21.91 23.13 10.25 o 17 2 5 812.95 808.92 43.57 o 18 2 5 297.52 294.67 23.22 o 19 2 5 226.40 207.40 20.43 o 20 2 5 44.35 61.66 22.58 o 21 2 5 82.26 51.73 31.81 o 1 3 5 364.52 346.02 13.45 o 2 3 5 2399.77 2287.19 57.57 o 3 3 5 80.51 90.76 10.26 o 4 3 5 49.18 49.16 8.41 o 5 3 5 266.34 282.99 14.49 o 6 3 5 877.27 910.02 28.30 o 7 3 5 445.58 462.31 19.12 o 8 3 5 238.26 205.13 15.67 o 9 3 5 231.47 241.14 12.23 o 10 3 5 376.73 363.44 18.60 o 11 3 5 112.16 111.00 23.08 o 12 3 5 1080.88 1127.21 39.68 o 13 3 5 43.60 80.06 17.33 o 14 3 5 101.42 81.91 15.87 o 15 3 5 4.50 10.46 11.29 o 16 3 5 37.53 38.11 12.90 o 17 3 5 0.30 4.56 20.64 o 18 3 5 8.51 37.96 23.42 o 19 3 5 344.87 306.63 45.22 o 0 4 5 190.41 208.69 23.59 o 1 4 5 3.06 8.93 11.09 o 2 4 5 51.80 45.19 17.56 o 3 4 5 86.47 85.09 13.33 o 4 4 5 13.27 24.17 18.11 o 5 4 5 65.12 75.85 18.65 o 6 4 5 19.19 37.30 13.86 o 7 4 5 196.77 198.34 16.30 o 8 4 5 85.31 71.72 12.53 o 9 4 5 14.77 -6.65 8.07 o 10 4 5 48.98 28.07 7.93 o 11 4 5 121.29 125.79 16.28 o 12 4 5 256.14 227.17 23.64 o 13 4 5 100.71 117.64 20.55 o 14 4 5 81.23 109.93 21.29 o 15 4 5 229.50 261.22 27.61 o 16 4 5 172.51 139.46 41.86 o 1 5 5 30.26 47.16 15.67 o 2 5 5 545.57 459.01 24.09 o 3 5 5 407.32 496.50 32.46 o 4 5 5 228.98 247.95 20.66 o 5 5 5 0.13 -1.67 14.71 o 6 5 5 215.56 267.18 25.91 o 7 5 5 207.59 244.13 35.68 o 8 5 5 30.48 48.77 20.99 o 9 5 5 32.81 49.91 19.90 o 10 5 5 241.53 228.03 27.98 o 11 5 5 95.97 104.28 26.69 o 0 0 6 20444.54 19160.51 792.54 o 1 0 6 3332.91 3221.60 115.12 o 2 0 6 11231.80 10392.32 353.71 o 3 0 6 2614.78 2718.55 69.65 o 4 0 6 907.45 935.64 29.19 o 5 0 6 1224.27 1146.11 39.10 o 6 0 6 534.86 637.20 27.72 o 7 0 6 418.79 403.49 15.83 o 8 0 6 4880.53 4681.59 133.18 o 9 0 6 655.26 665.31 24.74 o 10 0 6 355.59 321.23 17.63 o 11 0 6 1898.02 1793.29 51.47 o 12 0 6 698.89 778.86 27.72 o 13 0 6 11.21 9.26 10.15 o 14 0 6 1794.10 1747.15 52.20 o 15 0 6 392.57 384.43 18.83 o 16 0 6 2021.51 2053.42 67.21 o 17 0 6 110.64 121.08 13.94 o 18 0 6 1976.45 2008.01 72.38 o 19 0 6 123.02 154.21 23.87 o 20 0 6 723.64 922.44 109.09 o 21 0 6 29.25 8.16 20.24 o 22 0 6 40.79 66.21 19.48 o 1 1 6 5617.67 5598.82 95.52 o 2 1 6 331.90 336.67 11.79 o 3 1 6 1261.10 1275.30 29.08 o 4 1 6 626.61 678.56 17.80 o 5 1 6 742.08 717.99 18.63 o 6 1 6 882.91 922.94 23.53 o 7 1 6 705.20 731.48 20.51 o 8 1 6 1157.28 1226.51 27.71 o 9 1 6 152.33 166.43 10.32 o 10 1 6 273.85 281.81 10.86 o 11 1 6 21.37 24.36 8.05 o 12 1 6 509.19 539.23 17.71 o 13 1 6 37.52 43.62 9.32 o 14 1 6 21.70 40.44 7.42 o 15 1 6 34.49 25.70 7.93 o 16 1 6 576.28 580.31 19.41 o 17 1 6 10.20 43.28 10.80 o 18 1 6 33.66 39.23 9.60 o 19 1 6 5.45 20.18 17.62 o 20 1 6 66.02 56.93 10.77 o 21 1 6 347.55 320.80 28.68 o 0 2 6 0.06 -9.95 10.78 o 1 2 6 1537.15 1538.88 33.77 o 2 2 6 144.33 149.50 9.35 o 3 2 6 92.09 85.06 10.12 o 4 2 6 949.86 867.20 22.79 o 5 2 6 1486.40 1619.29 36.56 o 6 2 6 605.85 609.72 18.01 o 7 2 6 41.71 50.01 5.76 o 8 2 6 209.02 265.07 10.34 o 9 2 6 24.58 19.65 11.43 o 10 2 6 7.98 18.23 9.12 o 11 2 6 63.60 54.59 11.86 o 12 2 6 281.76 273.81 14.60 o 13 2 6 479.29 455.00 21.30 o 14 2 6 731.14 711.78 24.64 o 15 2 6 574.90 548.62 21.87 o 16 2 6 113.10 108.79 12.71 o 17 2 6 16.57 12.08 10.51 o 18 2 6 0.00 0.06 17.40 o 19 2 6 215.61 212.89 21.88 o 20 2 6 93.58 162.39 19.52 o 1 3 6 204.85 220.07 19.19 o 2 3 6 208.80 178.81 14.89 o 3 3 6 402.55 414.25 17.94 o 4 3 6 1310.93 1377.92 32.13 o 5 3 6 43.07 31.54 8.72 o 6 3 6 552.88 541.92 18.09 o 7 3 6 18.46 20.04 8.03 o 8 3 6 161.74 190.62 12.54 o 9 3 6 445.30 416.97 27.49 o 10 3 6 688.39 667.73 29.40 o 11 3 6 652.71 669.27 44.93 o 12 3 6 58.59 87.22 29.18 o 13 3 6 27.08 18.38 14.67 o 14 3 6 41.62 65.15 27.14 o 15 3 6 127.38 113.66 19.76 o 16 3 6 386.76 373.62 33.07 o 17 3 6 8.24 13.58 14.15 o 18 3 6 15.80 38.84 14.51 o 19 3 6 7.08 15.05 33.18 o 0 4 6 1040.73 999.23 72.11 o 1 4 6 219.13 219.65 20.13 o 2 4 6 25.53 15.43 13.07 o 3 4 6 530.26 536.51 30.28 o 4 4 6 6.30 -4.55 21.62 o 5 4 6 35.09 63.53 16.37 o 6 4 6 750.36 743.17 40.24 o 7 4 6 101.71 134.40 12.43 o 8 4 6 1393.57 1359.97 53.28 o 9 4 6 5.57 8.93 9.24 o 10 4 6 39.51 41.52 16.79 o 11 4 6 93.01 134.75 21.19 o 12 4 6 614.15 575.85 34.81 o 13 4 6 248.17 238.01 24.31 o 14 4 6 272.58 324.73 36.17 o 15 4 6 37.52 61.24 18.23 o 16 4 6 58.24 64.96 33.59 o 1 5 6 180.03 187.63 18.24 o 2 5 6 16.19 16.53 15.11 o 3 5 6 58.42 74.26 13.91 o 4 5 6 18.43 6.61 22.74 o 5 5 6 74.02 54.69 18.90 o 6 5 6 275.75 253.21 23.31 o 7 5 6 0.04 25.54 18.56 o 8 5 6 774.63 815.26 47.54 o 9 5 6 82.24 122.32 23.11 o 10 5 6 201.91 229.63 41.30 o 11 5 6 24.06 74.52 28.49 o 1 1 7 785.64 741.14 17.65 o 2 1 7 0.10 7.25 6.03 o 3 1 7 2015.44 1909.77 34.62 o 4 1 7 2061.96 2121.44 39.64 o 5 1 7 1719.07 1719.88 32.65 o 6 1 7 6380.69 6552.02 113.33 o 7 1 7 604.46 600.53 16.63 o 8 1 7 870.48 860.52 20.99 o 9 1 7 29.96 42.23 5.49 o 10 1 7 56.40 76.06 8.02 o 11 1 7 182.74 219.17 10.31 o 12 1 7 2305.30 2400.56 52.70 o 13 1 7 892.36 922.57 25.67 o 14 1 7 2.07 15.82 6.70 o 15 1 7 1994.37 2068.37 55.52 o 16 1 7 360.33 358.14 18.58 o 17 1 7 10.94 9.64 6.95 o 18 1 7 48.57 57.84 10.66 o 19 1 7 12.75 18.63 20.25 o 20 1 7 94.12 55.55 14.15 o 21 1 7 110.44 101.75 20.67 o 0 2 7 555.97 575.83 36.12 o 1 2 7 222.94 249.73 11.88 o 2 2 7 167.01 197.46 11.45 o 3 2 7 1688.45 1771.76 40.09 o 4 2 7 1471.21 1521.88 31.47 o 5 2 7 59.23 75.24 7.04 o 6 2 7 46.49 33.17 6.71 o 7 2 7 2352.61 2542.33 54.75 o 8 2 7 0.14 -1.08 6.08 o 9 2 7 241.34 219.05 10.97 o 10 2 7 566.42 627.05 24.69 o 11 2 7 85.10 91.06 8.93 o 12 2 7 95.95 90.75 12.59 o 13 2 7 100.14 93.02 10.36 o 14 2 7 851.51 848.79 29.10 o 15 2 7 63.45 51.78 11.28 o 16 2 7 63.40 60.61 15.70 o 17 2 7 166.29 179.19 18.73 o 18 2 7 3.05 7.07 14.88 o 19 2 7 6.98 20.17 22.55 o 20 2 7 0.00 -0.22 18.58 o 1 3 7 91.28 89.47 9.62 o 2 3 7 702.33 673.28 25.47 o 3 3 7 52.52 59.78 9.98 o 4 3 7 1.00 1.91 8.24 o 5 3 7 97.30 93.60 8.99 o 6 3 7 141.78 134.88 13.54 o 7 3 7 321.56 289.40 15.94 o 8 3 7 1086.01 1133.46 31.77 o 9 3 7 3.82 17.38 9.14 o 10 3 7 2.34 19.54 7.54 o 11 3 7 9.34 -3.46 10.72 o 12 3 7 31.96 1.11 12.14 o 13 3 7 128.60 138.85 16.86 o 14 3 7 5.32 28.02 17.95 o 15 3 7 26.26 0.64 18.04 o 16 3 7 11.02 80.11 40.39 o 17 3 7 28.69 19.47 26.53 o 18 3 7 124.72 120.70 22.94 o 0 4 7 3642.34 3503.05 137.84 o 1 4 7 129.69 142.30 18.43 o 2 4 7 197.55 207.71 26.02 o 3 4 7 1.48 -20.50 13.66 o 4 4 7 180.72 196.04 16.47 o 5 4 7 665.28 592.52 40.35 o 6 4 7 16.21 16.61 11.72 o 7 4 7 358.46 314.60 20.70 o 8 4 7 579.30 577.60 35.77 o 9 4 7 1358.15 1417.51 57.51 o 10 4 7 954.88 947.57 56.59 o 11 4 7 422.04 422.74 38.83 o 12 4 7 33.25 26.30 27.01 o 13 4 7 174.04 146.61 20.95 o 14 4 7 147.71 194.12 32.76 o 15 4 7 23.49 19.02 17.58 o 1 5 7 319.92 313.02 27.43 o 2 5 7 383.80 360.28 28.73 o 3 5 7 1.13 -5.43 13.59 o 4 5 7 307.68 239.69 28.31 o 5 5 7 26.69 40.01 22.42 o 6 5 7 42.13 53.58 21.95 o 7 5 7 0.02 -15.19 15.23 o 8 5 7 38.29 49.22 19.74 o 9 5 7 50.29 17.91 23.04 o 10 5 7 276.00 289.65 32.32 o 11 5 7 87.73 92.79 30.29 o 0 0 8 5.73 -11.40 11.91 o 1 0 8 6.54 8.13 9.99 o 2 0 8 5335.89 4863.83 151.41 o 3 0 8 45.91 36.71 9.75 o 4 0 8 0.01 2.32 8.52 o 5 0 8 241.45 283.00 16.31 o 6 0 8 1249.20 1459.63 41.63 o 7 0 8 169.56 223.26 17.48 o 8 0 8 270.68 239.45 21.81 o 9 0 8 32.36 53.69 10.28 o 10 0 8 1747.44 1752.60 60.63 o 11 0 8 1286.70 1286.91 49.47 o 12 0 8 6.15 -3.24 22.80 o 13 0 8 392.37 402.70 21.92 o 14 0 8 4.96 12.31 12.82 o 15 0 8 144.33 194.45 19.60 o 16 0 8 304.88 279.95 22.53 o 17 0 8 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13.96 9.93 o 8 4 8 14.60 -1.72 12.39 o 9 4 8 90.31 103.88 23.67 o 10 4 8 97.84 95.70 24.02 o 11 4 8 321.70 417.32 41.87 o 12 4 8 24.77 33.76 20.70 o 13 4 8 7.44 4.25 17.77 o 14 4 8 80.28 116.31 20.90 o 15 4 8 55.80 61.50 18.00 o 1 5 8 305.83 291.09 24.44 o 2 5 8 1.19 10.45 19.62 o 3 5 8 30.32 9.72 17.79 o 4 5 8 10.02 17.04 25.32 o 5 5 8 66.28 83.76 48.98 o 6 5 8 134.83 125.08 25.79 o 7 5 8 30.63 74.61 22.13 o 8 5 8 2.45 -2.88 21.36 o 9 5 8 101.18 83.79 18.19 o 10 5 8 269.45 292.29 29.34 o 1 1 9 584.12 562.90 18.01 o 2 1 9 257.52 295.00 11.33 o 3 1 9 355.65 416.41 13.48 o 4 1 9 254.95 267.37 12.57 o 5 1 9 67.73 92.55 7.85 o 6 1 9 1798.25 1799.53 35.22 o 7 1 9 595.91 635.44 17.52 o 8 1 9 878.60 876.36 22.74 o 9 1 9 119.22 145.35 16.82 o 10 1 9 653.85 678.87 20.95 o 11 1 9 236.54 244.98 12.67 o 12 1 9 77.81 77.31 8.37 o 13 1 9 568.01 622.06 22.81 o 14 1 9 293.82 267.52 15.32 o 15 1 9 447.53 451.81 20.70 o 16 1 9 1537.07 1616.41 39.45 o 17 1 9 110.87 110.13 12.63 o 18 1 9 45.13 34.24 11.99 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3 9 0.00 -0.52 13.82 o 14 3 9 6.45 20.33 17.10 o 15 3 9 2.44 -12.52 58.34 o 16 3 9 0.27 24.41 21.59 o 17 3 9 0.01 -12.16 19.17 o 18 3 9 23.11 62.93 26.12 o 0 4 9 386.70 353.30 47.06 o 1 4 9 1613.69 1544.78 71.08 o 2 4 9 4.55 32.44 14.01 o 3 4 9 1868.54 1821.49 63.76 o 4 4 9 114.59 94.54 16.89 o 5 4 9 272.04 272.26 21.27 o 6 4 9 18.90 35.78 13.51 o 7 4 9 100.53 118.08 20.97 o 8 4 9 0.40 -5.16 15.38 o 9 4 9 0.22 7.85 13.85 o 10 4 9 96.64 60.21 21.15 o 11 4 9 5.52 32.48 21.56 o 12 4 9 0.08 -3.44 21.06 o 13 4 9 125.98 99.18 23.11 o 14 4 9 5.79 -26.71 29.52 o 15 4 9 218.42 211.83 40.27 o 1 5 9 364.11 357.40 28.55 o 2 5 9 422.45 329.71 30.18 o 3 5 9 4.15 33.67 23.05 o 4 5 9 55.32 31.85 32.55 o 5 5 9 24.49 1.45 19.93 o 6 5 9 270.93 324.22 86.34 o 7 5 9 318.39 345.87 29.04 o 8 5 9 37.72 89.57 27.38 o 9 5 9 19.74 36.53 19.22 o 10 5 9 196.76 186.89 34.47 o 0 0 10 7031.51 7440.89 279.77 o 1 0 10 2522.95 2491.94 73.59 o 2 0 10 110.33 91.02 14.62 o 3 0 10 890.66 952.52 45.05 o 4 0 10 1265.28 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