#------------------------------------------------------------------------------ #$Date: 2010-03-05 20:15:21 +0200 (Fri, 05 Mar 2010) $ #$Revision: 1024 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2017524.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017524_Fobs loop_ _publ_author_name 'Gautier, Romain' 'Colin, Jean-Fran\,cois' 'Le Fur, Eric' _publ_section_title ; Two caesium vanadium hydrogenphosphates with tunnelled structures: Cs~2~V~2~O~3~(PO~4~)(HPO~4~) and Cs~2~[(VO)~3~(HPO~4~)~4~(H~2~O)]·H~2~O ; _journal_coeditor_code SQ3221 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i12 _journal_page_last i15 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.786 _cell_angle_gamma 90.000 _cell_length_a 12.5460 _cell_length_b 11.9180 _cell_length_c 12.6530 _exptl_crystal_F_000 1628.00 _reflns_d_resolution_high 0.5311 _[local]_cod_data_source_file sq3221IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' import in P 21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 456.41 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 906.01 609.74 32.32 o 3 0 0 44555.50 47029.60 1496.62 o 4 0 0 208305.67 171596.00 10004.89 o 5 0 0 716.96 556.31 34.56 o 6 0 0 126.39 87.08 14.10 o 7 0 0 26636.23 28220.41 901.47 o 8 0 0 2081.16 2220.61 109.01 o 9 0 0 54799.00 52848.04 3261.17 o 10 0 0 828.90 915.12 68.07 o 11 0 0 1564.06 1432.92 52.79 o 12 0 0 0.17 50.47 25.22 o 13 0 0 5423.12 5455.51 169.54 o 14 0 0 6674.54 6560.75 202.70 o 15 0 0 13691.86 14146.47 424.64 o 16 0 0 923.57 962.79 46.79 o 17 0 0 1496.58 1395.18 60.14 o 18 0 0 2200.36 2232.95 83.57 o 19 0 0 407.63 419.71 62.20 o 20 0 0 3635.27 3938.17 235.12 o 21 0 0 9.89 201.88 73.69 o 22 0 0 238.20 135.25 111.24 o 2 1 0 10594.71 10754.22 263.69 o 3 1 0 32889.79 32748.58 1208.99 o 4 1 0 124859.60 120745.90 13765.95 o 5 1 0 4674.09 4675.45 97.66 o 6 1 0 21088.17 20716.40 404.60 o 7 1 0 1333.18 1205.01 42.03 o 8 1 0 46690.48 48532.74 1069.57 o 9 1 0 246.69 267.05 116.79 o 10 1 0 7645.66 7101.35 189.83 o 11 1 0 6941.51 7009.27 187.66 o 12 1 0 13177.20 12853.17 272.08 o 13 1 0 6.85 43.41 13.33 o 14 1 0 709.44 719.18 26.10 o 15 1 0 187.25 222.42 35.31 o 16 1 0 3946.02 3909.09 90.48 o 17 1 0 473.30 501.79 27.39 o 18 1 0 2709.56 2736.58 74.17 o 19 1 0 2104.45 2278.01 63.33 o 20 1 0 0.32 -15.83 48.00 o 21 1 0 2.41 33.08 43.17 o 22 1 0 44.27 291.51 114.88 o 0 2 0 14776.30 14022.61 548.05 o 1 2 0 8282.39 7579.76 171.42 o 2 2 0 4273.42 4269.23 72.55 o 3 2 0 23788.56 23161.87 424.10 o 4 2 0 60.17 4.18 6.29 o 5 2 0 2145.53 2028.57 50.79 o 6 2 0 87011.75 91004.66 2870.97 o 7 2 0 1670.54 1585.67 48.13 o 8 2 0 288.97 322.24 14.55 o 9 2 0 30852.14 29567.77 705.90 o 10 2 0 3277.56 3411.92 95.58 o 11 2 0 651.96 661.32 32.89 o 12 2 0 1904.52 1856.91 52.40 o 13 2 0 1844.29 1827.84 46.34 o 14 2 0 4188.51 3982.76 90.91 o 15 2 0 1752.06 1765.29 50.80 o 16 2 0 418.85 335.24 23.15 o 17 2 0 114.30 177.30 21.99 o 18 2 0 3659.54 3617.07 86.95 o 19 2 0 1027.58 921.44 43.55 o 20 2 0 7008.71 7135.19 224.08 o 21 2 0 2.79 -22.38 63.90 o 22 2 0 86.23 -26.21 129.36 o 1 3 0 13784.81 13791.91 339.33 o 2 3 0 61452.39 61257.76 2901.24 o 3 3 0 16878.94 15557.85 280.86 o 4 3 0 16750.04 17447.10 312.23 o 5 3 0 8928.84 8139.67 165.32 o 6 3 0 536.72 802.68 21.15 o 7 3 0 2775.84 2885.85 84.34 o 8 3 0 2124.70 1899.91 47.53 o 9 3 0 4258.42 4229.00 107.00 o 10 3 0 1582.78 1384.92 43.83 o 11 3 0 3737.66 3606.20 104.10 o 12 3 0 24396.22 23221.16 606.64 o 13 3 0 6426.27 6343.17 151.61 o 14 3 0 90.99 163.04 23.46 o 15 3 0 308.29 309.60 20.96 o 16 3 0 3136.74 3009.94 72.87 o 17 3 0 1139.75 1191.14 43.94 o 18 3 0 367.81 396.11 27.97 o 19 3 0 463.61 487.03 41.97 o 20 3 0 415.19 393.37 53.95 o 21 3 0 760.60 941.10 122.95 o 0 4 0 59299.71 64381.86 3544.91 o 1 4 0 60989.82 65570.90 1803.16 o 2 4 0 37223.73 37360.05 854.19 o 3 4 0 3099.89 3446.69 74.20 o 4 4 0 9876.79 9915.83 216.11 o 5 4 0 21239.34 21039.12 426.32 o 6 4 0 14846.30 14901.85 345.08 o 7 4 0 17081.57 15607.80 330.83 o 8 4 0 28522.18 27171.76 632.60 o 9 4 0 1660.03 1664.08 46.71 o 10 4 0 7038.52 6563.42 158.19 o 11 4 0 339.59 342.54 29.30 o 12 4 0 2176.12 2186.28 79.85 o 13 4 0 335.80 329.42 28.05 o 14 4 0 200.11 256.71 19.25 o 15 4 0 1186.44 1102.54 36.84 o 16 4 0 4435.83 4532.35 103.66 o 17 4 0 5315.97 5362.42 121.57 o 18 4 0 238.14 191.93 36.26 o 19 4 0 289.54 370.60 70.35 o 20 4 0 1760.83 1875.23 105.81 o 21 4 0 868.10 771.34 74.49 o 22 4 0 0.60 367.28 111.63 o 1 5 0 12.84 26.01 27.35 o 2 5 0 38942.16 42564.77 1058.48 o 3 5 0 329.65 332.95 13.62 o 4 5 0 722.58 758.17 21.31 o 5 5 0 3145.22 3144.26 82.09 o 6 5 0 3076.28 3181.22 92.27 o 7 5 0 87.27 168.10 13.83 o 8 5 0 1066.52 1082.31 36.05 o 9 5 0 155.51 200.71 17.33 o 10 5 0 1396.89 1490.45 47.86 o 11 5 0 46.66 76.69 13.19 o 12 5 0 943.57 944.90 33.74 o 13 5 0 2319.14 2232.10 59.67 o 14 5 0 272.56 367.52 20.98 o 15 5 0 449.00 415.30 23.57 o 16 5 0 42.08 40.81 28.10 o 17 5 0 64.82 87.83 20.98 o 18 5 0 3101.83 3129.49 128.53 o 19 5 0 300.28 263.36 95.02 o 20 5 0 241.91 154.44 125.66 o 21 5 0 194.19 132.52 81.04 o 22 5 0 602.75 874.44 88.73 o 0 6 0 1756.80 2720.27 181.55 o 1 6 0 49938.41 53908.93 1329.54 o 2 6 0 599.31 789.90 46.21 o 3 6 0 13249.80 14305.28 318.68 o 4 6 0 3140.52 2936.71 70.46 o 5 6 0 6393.08 6721.48 210.40 o 6 6 0 33882.02 35490.71 995.52 o 7 6 0 2351.27 2112.27 91.26 o 8 6 0 25842.34 25958.85 784.29 o 9 6 0 10366.38 10016.63 263.37 o 10 6 0 17078.29 16896.53 441.46 o 11 6 0 3074.59 2892.91 82.07 o 12 6 0 2101.75 1985.97 60.90 o 13 6 0 45.20 76.88 15.53 o 14 6 0 11878.34 11804.83 304.59 o 15 6 0 536.37 498.92 26.13 o 16 6 0 1127.22 1210.95 55.41 o 17 6 0 270.52 251.57 42.96 o 18 6 0 3404.04 3336.69 184.41 o 19 6 0 75.00 67.39 78.13 o 20 6 0 778.45 810.95 95.47 o 21 6 0 115.07 251.07 117.41 o 22 6 0 645.54 503.16 145.59 o 1 7 0 1747.31 1746.33 88.95 o 2 7 0 310.79 286.79 31.64 o 3 7 0 2911.48 2950.19 129.59 o 4 7 0 25516.48 26237.65 711.84 o 5 7 0 20318.08 19449.29 571.15 o 6 7 0 785.47 874.31 68.17 o 7 7 0 2736.44 2474.02 97.06 o 8 7 0 586.16 612.29 48.72 o 9 7 0 3459.36 3129.71 141.48 o 10 7 0 1479.30 1469.35 162.22 o 11 7 0 7278.97 6791.94 211.12 o 12 7 0 3347.08 3482.63 97.41 o 13 7 0 7.11 8.64 15.47 o 14 7 0 3012.09 2958.26 107.00 o 15 7 0 162.08 177.25 36.58 o 16 7 0 561.16 553.55 58.88 o 17 7 0 335.36 302.67 53.25 o 18 7 0 5254.95 5721.99 192.85 o 19 7 0 1255.33 1354.39 109.45 o 20 7 0 20.38 76.11 89.45 o 21 7 0 125.85 153.37 111.96 o 22 7 0 153.79 252.02 140.16 o 0 8 0 50811.72 53870.17 2091.93 o 1 8 0 167.92 153.62 112.41 o 2 8 0 60.46 56.72 15.84 o 3 8 0 67.52 27.74 28.85 o 4 8 0 1637.92 1558.22 96.10 o 5 8 0 7821.13 8031.31 268.78 o 6 8 0 10065.25 9397.59 353.74 o 7 8 0 934.04 739.79 48.18 o 8 8 0 965.82 826.02 43.84 o 9 8 0 24964.96 24009.54 944.49 o 10 8 0 3153.61 2972.48 133.47 o 11 8 0 100.99 74.72 36.59 o 12 8 0 1004.24 904.09 47.19 o 13 8 0 2511.82 2431.07 92.08 o 14 8 0 1156.87 1075.53 55.02 o 15 8 0 5679.81 5932.75 195.71 o 16 8 0 191.40 207.26 59.21 o 17 8 0 1731.84 1504.33 157.44 o 18 8 0 2107.22 2048.41 187.76 o 19 8 0 101.22 71.10 109.18 o 20 8 0 389.98 473.85 115.36 o 21 8 0 22.97 106.92 114.46 o 1 9 0 6091.45 6419.90 176.03 o 2 9 0 81.49 119.51 22.21 o 3 9 0 890.65 830.53 58.62 o 4 9 0 3237.89 3332.82 116.53 o 5 9 0 368.67 423.78 34.54 o 6 9 0 282.28 311.66 40.66 o 7 9 0 329.06 275.25 37.89 o 8 9 0 6212.87 6252.89 186.27 o 9 9 0 301.70 276.31 44.99 o 11 9 0 59.06 7.89 23.84 o 12 9 0 2641.47 2346.78 89.10 o 13 9 0 3757.86 3650.88 127.99 o 14 9 0 4.26 29.34 42.54 o 15 9 0 1018.69 817.48 59.89 o 16 9 0 221.88 204.68 55.95 o 17 9 0 28.16 148.53 129.03 o 18 9 0 633.86 782.70 164.99 o 19 9 0 135.58 337.04 124.54 o 20 9 0 130.29 56.32 124.28 o 21 9 0 190.91 336.53 128.11 o 0 10 0 75087.46 74240.39 2684.62 o 1 10 0 2020.73 2102.30 79.21 o 2 10 0 1876.64 1936.38 110.75 o 3 10 0 19565.04 20364.49 669.04 o 4 10 0 29745.65 30541.83 973.84 o 5 10 0 1278.10 1314.82 89.27 o 6 10 0 18753.31 19900.27 639.91 o 7 10 0 513.66 615.05 59.72 o 8 10 0 1500.21 1542.64 82.80 o 9 10 0 22747.85 24727.00 970.87 o 10 10 0 20.14 6.05 38.23 o 11 10 0 147.89 174.33 36.07 o 12 10 0 0.42 35.12 27.48 o 13 10 0 2168.95 2168.36 77.04 o 14 10 0 149.37 173.20 32.07 o 15 10 0 3250.25 3313.92 122.33 o 16 10 0 512.63 328.80 121.35 o 17 10 0 333.51 290.24 156.66 o 18 10 0 1935.42 1942.44 198.00 o 19 10 0 1034.11 1129.00 183.01 o 20 10 0 189.48 40.83 153.22 o 21 10 0 9.29 -162.68 162.68 o 1 11 0 168.36 151.80 12.70 o 2 11 0 1829.89 1713.60 58.03 o 3 11 0 3463.58 3282.42 154.17 o 4 11 0 4467.97 4619.89 161.26 o 5 11 0 2138.07 2043.72 89.35 o 6 11 0 6979.70 7425.96 248.60 o 7 11 0 500.76 611.26 42.01 o 8 11 0 4317.02 4674.30 163.91 o 9 11 0 849.97 744.42 50.22 o 10 11 0 1656.12 1707.33 121.87 o 11 11 0 1670.77 1980.13 156.80 o 12 11 0 76.70 46.64 41.31 o 13 11 0 1958.11 2172.90 122.72 o 14 11 0 79.83 88.78 68.14 o 15 11 0 48.83 126.03 65.23 o 16 11 0 6.59 93.71 152.72 o 17 11 0 336.08 300.62 167.25 o 18 11 0 222.22 190.50 150.97 o 19 11 0 24.46 -127.98 157.33 o 20 11 0 215.03 227.49 154.01 o 0 12 0 18085.43 18449.75 565.97 o 1 12 0 3972.38 3765.51 95.05 o 2 12 0 605.35 600.46 25.45 o 3 12 0 278.17 333.58 19.85 o 4 12 0 555.42 460.21 31.92 o 5 12 0 1931.22 1814.92 61.44 o 6 12 0 1890.42 1922.57 65.94 o 7 12 0 723.20 609.08 35.24 o 8 12 0 1731.13 1721.81 61.75 o 9 12 0 5288.30 5431.17 244.89 o 10 12 0 9448.10 9711.22 317.52 o 11 12 0 48.52 58.14 41.94 o 12 12 0 1605.89 1560.54 70.49 o 13 12 0 50.27 8.88 46.94 o 14 12 0 872.29 905.94 86.07 o 16 12 0 23.62 54.11 51.29 o 17 12 0 1519.83 1389.89 169.67 o 18 12 0 695.45 919.73 167.73 o 19 12 0 47.67 154.72 193.50 o 1 13 0 120.92 169.36 29.62 o 2 13 0 3914.99 4114.19 108.98 o 3 13 0 6751.25 6783.42 191.38 o 4 13 0 1190.23 1258.72 49.87 o 5 13 0 1027.30 1081.65 45.65 o 6 13 0 138.53 187.18 53.52 o 7 13 0 1158.79 1133.41 61.99 o 8 13 0 1.18 -10.59 23.38 o 9 13 0 39.07 21.71 35.01 o 10 13 0 902.23 831.26 79.33 o 11 13 0 4.46 56.77 44.81 o 12 13 0 1821.08 1693.13 113.89 o 13 13 0 14.86 -2.17 71.78 o 14 13 0 1777.65 1693.31 177.82 o 15 13 0 713.83 739.13 153.26 o 16 13 0 5.42 200.83 150.52 o 17 13 0 461.43 88.09 152.90 o 18 13 0 388.14 362.61 213.81 o 19 13 0 171.10 269.11 226.13 o 0 14 0 345.22 495.99 84.71 o 1 14 0 10953.02 10922.84 241.08 o 2 14 0 3065.51 3099.35 107.31 o 3 14 0 2422.22 2465.20 73.22 o 4 14 0 1671.88 1741.83 62.68 o 5 14 0 1014.13 935.96 52.87 o 6 14 0 1676.98 1763.94 63.74 o 7 14 0 5544.74 5417.18 165.73 o 8 14 0 6673.34 6970.94 200.30 o 9 14 0 573.74 555.54 57.66 o 10 14 0 804.45 784.39 61.85 o 11 14 0 46.06 45.89 40.28 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84.17 o 10 16 0 8053.45 8416.62 400.58 o 11 16 0 266.37 258.74 62.12 o 12 16 0 1843.68 1738.14 138.38 o 13 16 0 30.38 -127.78 172.74 o 14 16 0 1298.27 1080.83 185.16 o 15 16 0 217.04 22.12 172.15 o 1 17 0 10.59 74.47 36.14 o 2 17 0 172.17 192.30 41.36 o 3 17 0 227.48 196.62 33.57 o 4 17 0 670.99 527.70 33.92 o 5 17 0 5160.27 5318.02 142.98 o 6 17 0 522.97 601.23 41.43 o 7 17 0 39.96 -17.95 36.68 o 8 17 0 146.46 -14.59 57.09 o 9 17 0 1970.14 1976.92 111.53 o 10 17 0 128.60 57.82 71.66 o 11 17 0 4.33 22.84 60.85 o 12 17 0 3.54 90.98 198.10 o 13 17 0 75.78 106.92 172.02 o 14 17 0 1464.38 1233.75 242.09 o 15 17 0 82.79 110.70 150.22 o 0 18 0 4665.73 4175.01 195.25 o 1 18 0 10.62 46.90 91.58 o 2 18 0 223.06 247.83 45.97 o 3 18 0 429.16 372.54 44.07 o 4 18 0 863.25 750.22 65.13 o 5 18 0 2.13 13.17 37.28 o 6 18 0 1540.46 1494.26 59.17 o 7 18 0 276.03 330.39 46.41 o 8 18 0 170.02 218.81 58.73 o 9 18 0 4165.76 4396.37 170.09 o 10 18 0 20.33 17.57 68.81 o 11 18 0 52.11 123.76 81.59 o 12 18 0 33.24 -17.19 222.12 o 13 18 0 703.26 717.38 199.62 o 14 18 0 19.59 -364.98 364.98 o 1 19 0 4.67 -39.62 130.60 o 2 19 0 3.58 115.33 153.98 o 3 19 0 678.03 521.44 135.63 o 4 19 0 65.42 82.89 105.24 o 5 19 0 0.99 -155.97 166.14 o 6 19 0 800.57 695.97 97.35 o 7 19 0 112.55 166.22 125.85 o 8 19 0 532.46 497.15 114.69 o 9 19 0 697.33 470.75 129.73 o 10 19 0 68.74 131.66 179.25 o 11 19 0 294.53 360.32 161.02 o 12 19 0 4.71 -141.50 141.50 o 0 20 0 2098.94 2146.60 227.88 o 1 20 0 1148.14 1053.26 126.93 o 2 20 0 14.31 -181.76 181.76 o 3 20 0 1020.47 912.13 126.50 o 4 20 0 4.38 50.55 115.68 o 5 20 0 1142.23 1183.56 140.33 o 6 20 0 1407.31 1440.77 146.20 o 7 20 0 371.43 496.22 114.13 o 8 20 0 3.14 -71.21 129.52 o 9 20 0 2253.75 2228.76 287.47 o 10 20 0 539.68 572.74 247.41 o 1 21 0 22.39 -0.48 111.79 o 2 21 0 35.98 -124.04 133.22 o 3 21 0 1114.74 1123.69 156.10 o 4 21 0 77.38 163.92 124.35 o 5 21 0 186.96 322.41 146.47 o 6 21 0 237.40 354.54 144.03 o 7 21 0 158.56 303.50 220.78 o 8 21 0 1.60 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