#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/75/2017536.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017536_Fobs loop_ _publ_author_name 'Becker, Clifford A. L.' 'Black, Robert S.' 'Forbes, Roy P.' _publ_section_title ; Tris(tert-butyl isocyanide)bis[tris(4-methoxyphenyl)phosphine]cobalt(I) perchlorate dichloromethane disolvate and tris(tert-butyl isocyanide)bis[tris(4-methoxyphenyl)phosphine]cobalt(II) bis(perchlorate) dichloromethane disolvate: modification of a trigonal--bipyramidal structure with change of metal oxidation state ; _journal_coeditor_code TR3058 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m40 _journal_page_last m43 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.818 _cell_angle_gamma 90.000 _cell_length_a 12.3461 _cell_length_b 19.7566 _cell_length_c 28.4452 _exptl_crystal_F_000 2876.00 _reflns_d_resolution_high 0.7570 _[local]_cod_data_source_file tr3058IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' 8p_Co_II_red_s in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 466.20 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3411.32 3210.44 66.02 o 4 0 0 5449.12 5913.69 141.26 o 6 0 0 385.56 175.25 33.49 o 8 0 0 1513.84 1723.43 71.58 o 10 0 0 442.87 424.18 48.21 o 12 0 0 1730.08 1863.19 94.56 o 14 0 0 47.94 -46.93 46.93 o 16 0 0 67.14 51.88 81.49 o 1 1 0 2243.22 2468.41 34.85 o 2 1 0 38.93 102.44 4.53 o 3 1 0 2.24 185.18 17.18 o 4 1 0 18804.00 21197.96 306.56 o 5 1 0 3219.56 3121.27 64.76 o 6 1 0 18097.88 17409.39 311.41 o 7 1 0 433.31 472.92 26.29 o 8 1 0 2658.72 2811.10 68.38 o 9 1 0 295.21 286.96 27.62 o 10 1 0 51.95 98.31 28.03 o 11 1 0 1988.95 1956.74 64.31 o 12 1 0 3152.41 3613.39 93.56 o 13 1 0 63.89 27.48 31.80 o 14 1 0 7.47 -4.14 32.15 o 15 1 0 1.73 -36.27 36.27 o 16 1 0 169.55 9.86 55.70 o 0 2 0 90811.80 84952.23 1519.87 o 1 2 0 1730.96 1949.66 40.30 o 2 2 0 9187.78 10580.05 146.03 o 3 2 0 3729.97 4119.29 56.76 o 4 2 0 2187.23 2407.92 38.50 o 5 2 0 795.45 1008.62 22.38 o 6 2 0 7887.25 7703.98 132.43 o 7 2 0 942.89 1009.76 49.69 o 8 2 0 616.61 515.61 28.05 o 9 2 0 1402.11 1472.39 50.23 o 10 2 0 743.00 795.36 39.69 o 11 2 0 60.12 -3.30 27.46 o 12 2 0 2710.81 2676.95 79.50 o 13 2 0 47.44 18.12 30.91 o 14 2 0 167.70 155.70 41.66 o 15 2 0 4.07 -38.80 38.80 o 16 2 0 8.30 -41.43 41.43 o 1 3 0 795.55 1031.17 17.10 o 2 3 0 40171.04 43397.75 618.56 o 3 3 0 10787.30 12235.24 180.13 o 4 3 0 3526.13 3009.48 46.66 o 5 3 0 4915.92 5558.15 83.93 o 6 3 0 102.59 66.52 14.46 o 7 3 0 2593.66 2400.55 52.09 o 8 3 0 308.75 266.67 17.66 o 9 3 0 768.39 706.00 35.59 o 10 3 0 42.84 34.88 26.09 o 11 3 0 51.75 82.23 29.52 o 12 3 0 2832.78 2792.89 80.90 o 13 3 0 265.36 190.53 34.64 o 14 3 0 41.09 -5.96 38.25 o 15 3 0 23.21 -39.38 39.38 o 16 3 0 278.21 162.45 73.20 o 0 4 0 28517.86 34683.86 615.84 o 1 4 0 45014.48 46983.58 718.58 o 2 4 0 1537.08 1035.48 43.84 o 3 4 0 3398.78 3044.74 62.99 o 4 4 0 1369.28 1068.02 22.65 o 5 4 0 3610.53 3923.36 61.97 o 6 4 0 1293.08 1210.28 27.11 o 7 4 0 36.05 48.34 13.63 o 8 4 0 5945.55 5707.24 106.00 o 9 4 0 799.32 908.86 40.10 o 10 4 0 1287.97 1476.83 57.12 o 11 4 0 4.91 -16.97 27.69 o 12 4 0 3013.07 3023.37 86.64 o 13 4 0 1093.15 1044.66 59.93 o 14 4 0 61.32 14.66 40.40 o 15 4 0 3.46 -0.22 41.53 o 16 4 0 307.54 308.25 55.36 o 1 5 0 45653.39 47707.61 672.07 o 2 5 0 5836.03 5016.39 77.12 o 3 5 0 9328.77 8969.08 166.20 o 4 5 0 307.95 224.30 12.01 o 5 5 0 591.63 514.52 16.56 o 6 5 0 10862.71 10880.42 159.58 o 7 5 0 2261.38 2359.60 47.90 o 8 5 0 924.45 1095.31 32.64 o 9 5 0 165.88 220.16 21.33 o 10 5 0 1084.36 1225.81 49.33 o 11 5 0 72.11 58.84 33.55 o 12 5 0 4693.77 4673.25 111.50 o 13 5 0 2.72 -35.53 35.53 o 14 5 0 21.87 23.35 39.54 o 15 5 0 28.20 40.71 55.73 o 0 6 0 17919.87 16800.86 318.02 o 1 6 0 2658.89 2591.00 52.16 o 2 6 0 7.80 38.87 6.68 o 3 6 0 784.00 963.15 30.01 o 4 6 0 6234.82 6522.74 132.82 o 5 6 0 807.29 891.73 30.56 o 6 6 0 4610.02 4495.66 72.17 o 7 6 0 344.01 485.73 18.60 o 8 6 0 1831.18 1693.77 41.72 o 9 6 0 95.17 81.99 18.32 o 10 6 0 193.02 191.37 27.56 o 11 6 0 5.57 -25.97 25.97 o 12 6 0 483.53 465.18 46.60 o 13 6 0 354.16 283.46 45.08 o 14 6 0 382.51 269.38 47.41 o 15 6 0 57.25 29.73 44.55 o 1 7 0 367.32 418.74 14.42 o 2 7 0 7540.12 8411.87 126.32 o 3 7 0 1364.89 1586.16 42.03 o 4 7 0 3406.25 4096.25 79.80 o 5 7 0 18.25 190.89 18.64 o 6 7 0 1105.62 962.39 24.45 o 7 7 0 3004.69 2914.57 52.29 o 8 7 0 1178.95 1266.54 32.65 o 9 7 0 144.46 108.77 19.49 o 10 7 0 216.05 189.63 26.71 o 11 7 0 7.23 -31.67 31.67 o 12 7 0 10.93 -13.48 34.30 o 13 7 0 0.20 -36.64 36.64 o 14 7 0 197.42 88.50 43.87 o 15 7 0 3.99 -1.57 62.40 o 0 8 0 8644.01 9870.41 238.42 o 1 8 0 8329.03 8382.71 126.76 o 2 8 0 5505.04 5596.19 86.66 o 3 8 0 69.11 124.58 13.85 o 4 8 0 65.54 17.84 10.67 o 5 8 0 1133.54 1117.12 38.92 o 6 8 0 108.93 130.98 21.11 o 7 8 0 84.35 83.61 12.20 o 8 8 0 1449.79 1442.33 45.39 o 9 8 0 1142.34 1096.86 35.22 o 10 8 0 90.30 138.26 34.60 o 11 8 0 72.82 18.14 32.66 o 12 8 0 1.02 -35.85 35.85 o 13 8 0 744.25 855.44 58.57 o 14 8 0 222.04 151.27 49.73 o 15 8 0 26.83 -45.01 53.59 o 1 9 0 6946.07 8001.06 121.62 o 2 9 0 2382.54 2251.96 43.98 o 3 9 0 1910.74 2482.46 43.87 o 4 9 0 1694.46 1812.12 45.66 o 5 9 0 14587.68 13529.03 249.80 o 6 9 0 2585.61 2244.31 63.87 o 7 9 0 2158.79 2195.07 55.14 o 8 9 0 233.22 206.22 24.61 o 9 9 0 170.64 152.03 25.05 o 10 9 0 3480.00 3782.47 104.57 o 11 9 0 5.94 -32.72 32.72 o 12 9 0 395.32 363.68 45.01 o 13 9 0 22.48 -3.57 50.22 o 14 9 0 525.36 556.58 56.60 o 15 9 0 0.93 1.33 49.33 o 0 10 0 87.09 104.95 27.39 o 1 10 0 732.95 950.50 22.55 o 2 10 0 17873.42 16837.15 239.86 o 3 10 0 4807.36 5242.52 83.48 o 4 10 0 50.03 55.56 15.76 o 5 10 0 1.11 -13.33 13.33 o 6 10 0 12.52 -3.28 19.80 o 7 10 0 903.22 838.01 37.84 o 8 10 0 915.58 1057.38 41.99 o 9 10 0 594.31 711.20 35.13 o 10 10 0 270.65 284.75 36.07 o 11 10 0 435.15 560.38 47.48 o 12 10 0 0.78 -43.07 43.07 o 13 10 0 147.08 41.82 39.09 o 14 10 0 143.36 108.24 50.35 o 15 10 0 17.80 66.77 60.84 o 1 11 0 2030.82 1876.44 41.94 o 2 11 0 78.30 123.00 11.78 o 3 11 0 221.60 184.50 12.54 o 4 11 0 400.86 403.79 20.90 o 5 11 0 11058.73 11277.63 241.51 o 6 11 0 12.04 12.48 22.25 o 7 11 0 7181.41 7102.09 209.07 o 8 11 0 960.34 895.33 38.52 o 9 11 0 85.89 159.07 27.97 o 10 11 0 1060.80 994.33 67.25 o 11 11 0 1232.15 1176.24 64.43 o 12 11 0 346.66 431.87 82.08 o 13 11 0 30.42 19.84 42.26 o 14 11 0 184.58 263.51 54.90 o 0 12 0 2364.74 2513.88 78.40 o 1 12 0 2735.30 2704.29 65.03 o 2 12 0 1233.56 1051.14 27.98 o 3 12 0 368.45 413.71 17.42 o 4 12 0 2690.35 2588.49 64.05 o 5 12 0 956.43 989.47 41.43 o 6 12 0 820.47 724.50 67.84 o 7 12 0 796.44 903.13 42.26 o 8 12 0 1177.04 1152.84 48.67 o 9 12 0 637.68 638.47 48.40 o 10 12 0 566.51 370.54 37.48 o 11 12 0 2.66 -43.11 43.11 o 12 12 0 22.58 -20.47 41.45 o 13 12 0 231.93 208.95 76.43 o 14 12 0 39.92 92.11 59.63 o 1 13 0 6806.14 6474.51 131.68 o 2 13 0 4660.37 4447.99 84.60 o 3 13 0 13.63 39.12 11.19 o 4 13 0 1460.35 1438.75 48.57 o 5 13 0 5467.53 5141.74 147.89 o 6 13 0 1385.69 1352.85 86.24 o 7 13 0 2822.21 3030.59 92.69 o 8 13 0 41.58 0.83 28.63 o 9 13 0 111.69 152.22 30.95 o 10 13 0 1261.11 1281.86 56.86 o 11 13 0 512.27 471.43 49.14 o 12 13 0 419.95 342.63 63.32 o 13 13 0 2.58 40.03 53.01 o 14 13 0 164.08 271.88 53.67 o 0 14 0 6178.49 5935.60 197.28 o 1 14 0 2060.21 1998.28 55.56 o 2 14 0 2093.62 2231.84 54.40 o 3 14 0 162.87 170.14 14.62 o 4 14 0 2544.06 2406.46 59.14 o 5 14 0 3156.52 3054.92 104.47 o 6 14 0 4215.53 4311.35 120.27 o 7 14 0 139.06 91.85 28.99 o 8 14 0 49.63 22.05 31.78 o 9 14 0 7.95 -5.88 35.81 o 10 14 0 106.53 71.70 45.28 o 11 14 0 193.58 154.60 49.94 o 12 14 0 0.90 35.56 43.12 o 13 14 0 137.68 237.47 52.66 o 1 15 0 570.70 536.34 30.29 o 2 15 0 65.63 97.38 21.49 o 3 15 0 1526.42 1567.06 42.33 o 4 15 0 772.08 780.82 36.52 o 5 15 0 5251.11 5583.93 125.19 o 6 15 0 428.52 361.77 33.36 o 7 15 0 1237.20 1038.04 78.99 o 8 15 0 645.36 657.10 58.78 o 9 15 0 7.73 6.10 31.54 o 10 15 0 133.88 207.01 39.50 o 11 15 0 74.05 154.83 42.88 o 12 15 0 228.49 238.44 49.27 o 13 15 0 102.27 266.39 53.43 o 0 16 0 3074.88 2597.49 198.52 o 1 16 0 178.99 265.92 26.93 o 2 16 0 1477.85 1482.58 50.95 o 3 16 0 1688.18 1818.99 50.56 o 4 16 0 271.89 206.37 24.58 o 5 16 0 549.57 622.02 35.64 o 6 16 0 260.96 347.97 58.63 o 7 16 0 289.07 342.06 35.68 o 8 16 0 273.57 217.16 34.18 o 9 16 0 3085.85 3083.93 114.37 o 10 16 0 18.79 46.22 55.16 o 11 16 0 18.56 131.08 58.67 o 12 16 0 0.05 81.69 102.31 o 1 17 0 683.74 571.38 33.53 o 2 17 0 1.66 9.14 21.17 o 3 17 0 5314.63 5263.83 116.82 o 4 17 0 86.27 138.46 35.68 o 5 17 0 2667.18 2675.46 195.32 o 6 17 0 159.66 185.78 70.16 o 7 17 0 437.30 402.10 45.35 o 8 17 0 218.74 298.11 74.65 o 9 17 0 129.99 204.48 62.09 o 10 17 0 134.58 199.58 55.04 o 11 17 0 170.41 375.78 106.02 o 12 17 0 136.63 303.98 96.14 o 0 18 0 219.83 302.52 46.20 o 1 18 0 232.06 211.05 30.46 o 2 18 0 808.05 915.73 41.87 o 3 18 0 244.07 351.28 72.91 o 4 18 0 32.59 62.26 41.51 o 5 18 0 4.99 -34.60 38.70 o 6 18 0 367.82 357.44 70.27 o 7 18 0 88.96 24.46 84.49 o 8 18 0 656.39 632.57 87.26 o 9 18 0 1490.78 1642.31 132.12 o 10 18 0 1.36 93.34 88.52 o 11 18 0 13.72 68.90 78.74 o 1 19 0 11.13 -22.66 27.02 o 2 19 0 107.05 111.59 33.87 o 3 19 0 2168.82 2300.46 82.43 o 4 19 0 106.82 111.47 48.23 o 5 19 0 9.33 31.32 36.57 o 6 19 0 4.54 -6.66 47.57 o 7 19 0 275.76 267.41 87.71 o 8 19 0 72.73 38.40 83.74 o 9 19 0 562.59 675.29 92.56 o 10 19 0 646.32 789.74 69.25 o 11 19 0 145.54 224.08 120.86 o 0 20 0 0.22 -39.01 39.01 o 1 20 0 2.78 -24.24 27.61 o 2 20 0 845.15 803.77 54.56 o 3 20 0 207.17 201.16 39.59 o 4 20 0 1117.50 1097.52 60.15 o 5 20 0 222.03 299.90 67.01 o 6 20 0 33.83 -44.25 44.25 o 7 20 0 34.70 21.90 84.25 o 8 20 0 151.24 105.01 61.75 o 9 20 0 666.11 900.61 151.74 o 10 20 0 14.54 -24.16 47.21 o 1 21 0 174.54 175.46 45.70 o 2 21 0 70.89 46.28 44.82 o 3 21 0 5145.95 5028.48 137.96 o 4 21 0 7.57 -29.61 55.14 o 5 21 0 183.29 199.26 59.38 o 6 21 0 76.92 38.67 94.36 o 7 21 0 0.16 -29.71 78.07 o 8 21 0 0.24 -11.81 105.79 o 9 21 0 677.57 842.24 119.45 o 0 22 0 377.11 208.75 109.08 o 1 22 0 348.75 472.00 123.05 o 2 22 0 454.44 470.78 56.62 o 3 22 0 328.33 398.07 47.43 o 4 22 0 229.34 286.97 46.66 o 5 22 0 137.09 58.73 42.77 o 6 22 0 162.01 111.24 54.66 o 7 22 0 493.89 585.37 97.25 o 8 22 0 7.18 -59.68 104.44 o 1 23 0 4.14 -77.58 89.68 o 2 23 0 498.63 471.58 59.59 o 3 23 0 2373.78 2298.53 134.76 o 4 23 0 15.90 -25.87 49.30 o 5 23 0 33.87 -19.89 42.84 o 6 23 0 0.04 -39.25 39.25 o 7 23 0 56.88 -31.96 62.02 o 0 24 0 292.51 24.45 97.09 o 1 24 0 118.68 -56.21 72.63 o 2 24 0 54.78 -15.99 81.12 o 3 24 0 185.82 87.69 57.33 o 4 24 0 97.73 30.78 44.17 o 5 24 0 57.54 29.35 45.31 o 6 24 0 74.85 -24.78 47.13 o 1 25 0 60.67 -69.68 80.93 o 2 25 0 43.67 -100.73 102.61 o 3 25 0 395.05 287.56 95.66 o 4 25 0 83.57 -46.67 54.39 o 0 26 0 422.92 315.47 141.28 o 1 26 0 94.08 -48.53 87.51 o -15 0 1 771.67 735.63 69.87 o -13 0 1 95.18 -22.42 45.31 o -11 0 1 2591.48 2693.07 123.23 o -9 0 1 896.16 1127.17 62.48 o -7 0 1 33570.00 32750.75 819.98 o -5 0 1 7151.33 7275.00 193.01 o -3 0 1 8549.59 10491.32 240.21 o -1 0 1 78385.54 76138.17 1717.92 o 3 0 1 43429.40 42531.59 1039.08 o 5 0 1 22026.38 19947.37 497.57 o 7 0 1 335.60 247.89 29.90 o 9 0 1 902.89 886.28 57.25 o 11 0 1 2000.79 2022.45 91.86 o 13 0 1 5.90 -13.51 41.54 o 15 0 1 39.31 11.92 49.88 o -16 1 1 22.96 -25.12 54.91 o -15 1 1 8.48 -39.05 39.05 o -14 1 1 9.96 -29.40 29.40 o -13 1 1 9.85 -29.96 29.96 o -12 1 1 1.40 -14.46 29.90 o -11 1 1 3243.26 3324.29 86.78 o -10 1 1 15.40 40.72 26.93 o -9 1 1 224.42 174.78 25.54 o -8 1 1 1462.44 1737.09 52.43 o -7 1 1 6612.09 5850.42 117.10 o -6 1 1 38.66 211.04 21.56 o -5 1 1 24419.60 26379.44 398.03 o -4 1 1 1976.42 1938.34 31.37 o -3 1 1 22849.74 24806.77 311.23 o -2 1 1 5937.46 6154.04 79.74 o -1 1 1 4814.92 5574.65 71.25 o 0 1 1 72.43 21.01 3.38 o 1 1 1 20803.41 20329.53 291.37 o 2 1 1 34016.00 33010.79 425.75 o 3 1 1 4930.02 6168.82 89.85 o 4 1 1 874.58 523.95 16.20 o 5 1 1 2310.13 2304.40 51.26 o 6 1 1 2.34 11.79 15.70 o 7 1 1 9051.98 9393.76 176.01 o 8 1 1 7002.42 7282.86 142.48 o 9 1 1 950.23 971.09 40.85 o 10 1 1 197.76 134.09 26.82 o 11 1 1 2347.44 2539.27 73.51 o 12 1 1 392.97 507.36 40.76 o 13 1 1 0.48 -30.49 30.49 o 14 1 1 216.75 194.02 36.31 o 15 1 1 9.94 -35.56 39.33 o 16 1 1 13.17 -50.70 50.70 o -16 2 1 10.76 -45.55 45.55 o -15 2 1 19.73 -39.47 39.47 o -14 2 1 62.55 -4.46 37.47 o -13 2 1 37.15 9.49 29.54 o -12 2 1 865.77 973.29 49.02 o -11 2 1 872.38 809.98 42.83 o -10 2 1 3.52 8.18 24.52 o -9 2 1 276.29 188.57 27.65 o -8 2 1 0.38 -14.06 18.01 o -7 2 1 480.70 418.57 23.24 o -6 2 1 308.64 356.31 19.04 o -5 2 1 37.44 41.45 14.66 o -4 2 1 3435.83 3553.08 49.45 o -3 2 1 8057.70 9315.02 119.67 o -2 2 1 14651.29 14992.86 201.35 o -1 2 1 19966.81 25587.39 385.19 o 0 2 1 972.98 712.74 10.85 o 1 2 1 4365.14 4685.80 70.19 o 2 2 1 23480.79 24967.31 366.78 o 3 2 1 12931.71 13730.99 194.43 o 4 2 1 6351.01 7110.55 103.68 o 5 2 1 30987.12 31535.14 505.49 o 6 2 1 3343.13 3789.21 71.18 o 7 2 1 11.06 26.58 17.26 o 8 2 1 148.86 136.02 20.63 o 9 2 1 837.34 798.40 36.66 o 10 2 1 5.65 16.94 25.95 o 11 2 1 2945.98 2916.07 79.92 o 12 2 1 43.57 51.80 31.66 o 13 2 1 47.04 21.84 31.96 o 14 2 1 0.39 -31.30 31.30 o 15 2 1 84.03 2.79 42.17 o 16 2 1 113.29 23.20 47.40 o -16 3 1 4.33 -55.50 55.50 o -15 3 1 69.42 35.30 43.57 o -14 3 1 44.94 -36.69 36.69 o -13 3 1 101.50 16.64 31.37 o -12 3 1 191.81 223.09 42.38 o -11 3 1 2658.57 2733.92 77.69 o -10 3 1 232.64 187.44 28.31 o -9 3 1 10.51 -22.38 27.64 o -8 3 1 1869.14 1994.63 48.24 o -7 3 1 3086.68 3098.23 57.50 o -6 3 1 5828.73 6171.32 113.20 o -5 3 1 5525.75 6269.92 94.35 o -4 3 1 4249.33 3690.51 76.31 o -3 3 1 32669.86 32407.28 427.33 o -2 3 1 1230.94 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