#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/75/2017537.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017537_Fobs loop_ _publ_author_name 'Becker, Clifford A. L.' 'Black, Robert S.' 'Forbes, Roy P.' _publ_section_title ; Tris(tert-butyl isocyanide)bis[tris(4-methoxyphenyl)phosphine]cobalt(I) perchlorate dichloromethane disolvate and tris(tert-butyl isocyanide)bis[tris(4-methoxyphenyl)phosphine]cobalt(II) bis(perchlorate) dichloromethane disolvate: modification of a trigonal--bipyramidal structure with change of metal oxidation state ; _journal_coeditor_code TR3058 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m40 _journal_page_last m43 _journal_volume 66 _journal_year 2010 _space_group_IT_number 176 _symmetry_space_group_name_Hall '-P 6c' _symmetry_space_group_name_H-M 'P 63/m' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 21.7568 _cell_length_b 21.7568 _cell_length_c 23.3983 _exptl_crystal_F_000 4020.00 _reflns_d_resolution_high 0.8109 _[local]_cod_data_source_file tr3058Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 8p_Co_I_yellow_s in P6(3)/m' _shelx_refln_list_code 4 _shelx_f_calc_maximum 1069.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' '-x, -y, z+1/2' 'y, -x+y, z+1/2' 'x-y, x, z+1/2' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' 'x, y, -z-1/2' '-y, x-y, -z-1/2' '-x+y, -x, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 1 0 1253.52 59.10 29.21 o -1 2 0 112514.08 140688.27 1330.83 o 0 2 0 130.20 104.71 17.87 o -2 3 0 12204.61 10860.84 140.41 o -1 3 0 647.23 944.32 41.63 o 0 3 0 227868.06 243616.80 2190.43 o -3 4 0 717.31 653.73 26.97 o -2 4 0 30767.64 32812.14 380.44 o -1 4 0 3529.48 3162.86 52.68 o 0 4 0 31899.88 33574.16 344.60 o -4 5 0 14972.90 17178.53 174.36 o -3 5 0 79.03 223.44 45.89 o -2 5 0 3980.06 3834.04 74.24 o -1 5 0 108863.37 112415.63 1031.85 o 0 5 0 23701.11 22662.09 299.18 o -5 6 0 10700.89 11130.98 178.40 o -4 6 0 99.46 66.08 41.23 o -3 6 0 136249.03 138444.00 1535.13 o -2 6 0 8684.66 7729.85 114.64 o -1 6 0 5317.85 5389.49 119.85 o 0 6 0 44654.83 43225.46 478.87 o -6 7 0 23637.61 24119.07 285.19 o -5 7 0 4610.04 5053.62 77.06 o -4 7 0 782.66 818.23 54.16 o -3 7 0 13133.37 12214.33 161.11 o -2 7 0 32213.54 32532.78 391.76 o -1 7 0 3909.45 3558.55 75.29 o 0 7 0 25312.22 25197.08 310.47 o -7 8 0 40183.21 39282.49 446.30 o -6 8 0 3857.02 4520.49 93.24 o -5 8 0 14276.58 14056.74 258.38 o -4 8 0 43055.30 43337.01 566.49 o -3 8 0 32559.77 30360.00 371.81 o -2 8 0 47153.45 46928.30 549.78 o -1 8 0 64646.75 65081.94 716.69 o 0 8 0 26049.13 25445.16 302.68 o -8 9 0 11812.47 12390.49 203.38 o -7 9 0 1408.04 1490.03 73.10 o -6 9 0 38947.91 37291.51 375.47 o -5 9 0 6863.99 6609.91 179.87 o -4 9 0 2131.30 2103.20 105.98 o -3 9 0 41424.38 37010.56 449.76 o -2 9 0 4263.58 3818.83 119.19 o -1 9 0 2548.61 3060.15 195.40 o 0 9 0 106372.66 103200.85 1118.01 o -9 10 0 5804.73 5641.07 125.97 o -8 10 0 61680.01 62672.27 763.20 o -7 10 0 9062.14 8972.32 173.37 o -6 10 0 1621.89 1412.69 174.06 o -5 10 0 61453.05 60548.38 1120.11 o -4 10 0 1022.83 797.31 68.78 o -3 10 0 5474.40 4962.40 136.08 o -2 10 0 27366.02 27319.70 350.87 o -1 10 0 11639.27 11045.78 155.02 o 0 10 0 10613.33 12029.47 190.89 o -10 11 0 3142.03 3301.94 115.94 o -9 11 0 467.30 534.14 59.54 o -8 11 0 2194.63 2304.47 88.31 o -7 11 0 2941.46 2513.08 64.12 o -5 11 0 4494.51 4352.48 145.85 o -4 11 0 47014.28 48340.61 579.80 o -3 11 0 10206.80 10184.58 171.63 o -2 11 0 3447.73 3626.94 150.87 o -1 11 0 32086.71 30729.29 374.16 o 0 11 0 9359.00 9978.74 166.36 o -11 12 0 13799.98 14288.03 214.89 o -10 12 0 723.35 887.66 107.15 o -9 12 0 79932.64 77251.19 938.74 o -8 12 0 2106.37 2083.90 81.35 o -7 12 0 1410.67 1774.72 140.47 o -6 12 0 23674.85 21612.79 384.12 o -5 12 0 4238.44 3913.29 148.33 o -4 12 0 155.55 319.64 151.24 o -3 12 0 163652.86 161029.78 1988.07 o -2 12 0 1689.64 1916.59 87.15 o -1 12 0 5.73 136.48 63.85 o 0 12 0 17723.01 16313.83 237.86 o -12 13 0 15240.53 15180.20 230.05 o -11 13 0 99053.17 96041.42 1161.46 o -10 13 0 4193.11 4031.64 125.31 o -9 13 0 11884.93 12439.58 332.63 o -8 13 0 60464.32 57991.49 722.69 o -7 13 0 99.31 160.09 141.41 o -6 13 0 536.10 922.76 99.95 o -5 13 0 40265.29 39037.77 627.24 o -4 13 0 46.09 -22.35 61.45 o -3 13 0 1719.50 1859.55 91.90 o -2 13 0 46355.75 44405.23 606.53 o -1 13 0 580.72 376.17 67.34 o 0 13 0 4118.97 4393.25 135.45 o -13 14 0 41846.34 41236.29 504.92 o -12 14 0 3976.02 4179.66 255.47 o -11 14 0 98.09 111.12 69.34 o -10 14 0 30514.15 28252.19 398.35 o -9 14 0 149.23 324.38 61.13 o -8 14 0 103.60 -59.79 75.43 o -7 14 0 47899.22 47186.36 742.52 o -6 14 0 290.73 203.45 90.66 o -5 14 0 0.68 229.25 88.91 o -4 14 0 18388.71 17908.38 301.47 o -3 14 0 6064.91 6006.70 184.14 o -2 14 0 22.22 176.62 107.35 o -1 14 0 38990.16 34880.62 379.47 o 0 14 0 3177.50 3595.02 124.98 o -14 15 0 1415.41 1733.73 143.51 o -13 15 0 27.57 19.32 67.38 o -12 15 0 22176.80 21964.86 308.63 o -11 15 0 4251.61 4566.88 144.59 o -10 15 0 1839.83 1927.80 95.36 o -9 15 0 36770.39 36455.03 491.71 o -8 15 0 5906.45 5630.25 232.46 o -7 15 0 1173.35 1455.44 169.03 o -6 15 0 22365.74 20518.90 395.58 o -5 15 0 2766.70 2652.58 139.14 o -4 15 0 6532.30 7452.54 183.96 o -3 15 0 28132.84 28395.03 427.81 o -2 15 0 3.17 58.03 75.03 o -1 15 0 2606.69 2557.34 131.25 o 0 15 0 8352.71 8219.21 178.00 o -15 16 0 1099.56 1125.10 90.26 o -14 16 0 15792.11 13964.18 270.35 o -13 16 0 574.94 635.80 81.98 o -12 16 0 5847.91 5021.98 154.36 o -11 16 0 105067.81 101304.59 1236.85 o -10 16 0 1293.47 1362.74 87.87 o -9 16 0 1756.60 1882.63 89.70 o -8 16 0 33391.86 31381.13 551.58 o -7 16 0 5770.77 5741.54 211.59 o -6 16 0 4675.50 5090.17 199.84 o -5 16 0 29713.00 28968.64 516.06 o -4 16 0 5975.33 5933.44 169.66 o -3 16 0 440.33 682.58 86.01 o -2 16 0 20216.72 19398.35 272.22 o -1 16 0 17.49 179.58 104.41 o 0 16 0 807.45 870.24 89.10 o -16 17 0 1910.83 2150.11 107.90 o -15 17 0 1962.29 2268.84 110.37 o -14 17 0 1681.07 1624.79 98.90 o -13 17 0 1699.81 1466.32 95.90 o -12 17 0 66.42 94.08 90.18 o -11 17 0 178.64 216.29 88.49 o -10 17 0 19873.19 18415.63 297.90 o -9 17 0 919.17 1016.60 148.72 o -8 17 0 4255.01 4590.52 207.48 o -7 17 0 28908.09 26264.51 500.34 o -6 17 0 4421.03 4256.60 195.20 o -5 17 0 610.80 761.15 122.05 o -4 17 0 62663.84 62362.64 844.76 o -3 17 0 781.90 885.30 88.09 o -2 17 0 265.48 234.19 92.05 o -1 17 0 655.29 703.33 113.51 o 0 17 0 28.92 -38.77 88.43 o -17 18 0 38.89 266.55 81.71 o -16 18 0 81.61 236.06 79.05 o -15 18 0 1710.14 1484.50 99.29 o -14 18 0 1871.55 1891.99 104.28 o -13 18 0 283.45 184.99 77.41 o -12 18 0 3621.65 3908.62 147.09 o -11 18 0 2624.97 2720.97 123.59 o -10 18 0 5813.36 5981.99 233.90 o -9 18 0 18283.26 17679.39 384.12 o -8 18 0 199.83 381.40 125.14 o -7 18 0 0.46 65.29 114.73 o -6 18 0 40100.95 38632.81 658.66 o -5 18 0 100.61 177.03 107.75 o -4 18 0 227.93 345.95 85.11 o -3 18 0 2442.00 2444.49 128.90 o -2 18 0 2325.64 2481.67 129.98 o -1 18 0 1004.27 1042.98 109.21 o 0 18 0 19321.29 18832.39 349.27 o -18 19 0 219.93 332.00 86.74 o -17 19 0 17649.05 17638.41 288.24 o -16 19 0 180.71 303.24 88.41 o -15 19 0 9.56 -10.96 75.88 o -14 19 0 7877.00 8136.46 184.61 o -13 19 0 2.73 -1.00 82.91 o -12 19 0 1.35 -79.38 79.38 o -11 19 0 1800.79 1298.35 96.02 o -10 19 0 1179.54 1083.75 93.26 o -9 19 0 2460.98 2612.30 167.60 o -8 19 0 24783.96 24486.83 481.35 o -7 19 0 687.82 822.58 127.67 o -6 19 0 1676.10 1808.64 183.82 o -5 19 0 15286.01 15971.11 352.12 o -4 19 0 475.26 579.56 104.61 o -3 19 0 1375.96 1544.03 114.34 o -2 19 0 17016.44 16348.53 313.85 o -1 19 0 126.22 116.09 118.87 o 0 19 0 303.48 457.51 126.79 o -19 20 0 15848.24 14974.46 369.57 o -18 20 0 368.27 814.08 95.59 o -17 20 0 968.97 898.21 94.81 o -16 20 0 10423.46 9669.96 205.59 o -15 20 0 2371.44 2247.89 114.55 o -14 20 0 609.70 423.29 82.10 o -13 20 0 5771.67 5907.78 178.19 o -12 20 0 1747.34 1438.29 105.56 o -11 20 0 4718.83 4290.30 143.78 o -10 20 0 9161.81 9086.12 321.84 o -9 20 0 216.55 201.87 124.37 o -8 20 0 13.83 -0.22 116.34 o -7 20 0 21457.50 20654.02 431.95 o -6 20 0 61.57 52.14 111.12 o -5 20 0 3364.71 3381.98 289.15 o -4 20 0 2232.28 2174.73 148.71 o -3 20 0 603.02 657.33 126.38 o -2 20 0 780.53 1249.88 214.63 o -1 20 0 9144.27 9175.29 284.21 o 0 20 0 51.19 27.65 124.09 o -20 21 0 11.38 474.71 134.40 o -19 21 0 474.50 569.82 111.18 o -18 21 0 13945.30 13803.65 475.14 o -17 21 0 619.00 907.71 106.38 o -16 21 0 134.57 112.90 83.15 o -15 21 0 22592.56 21350.36 330.07 o -14 21 0 26.04 -71.43 78.06 o -13 21 0 261.89 225.06 89.94 o -12 21 0 10723.72 10547.89 241.40 o -11 21 0 1499.62 1690.01 108.49 o -10 21 0 114.33 21.67 123.89 o -9 21 0 15056.10 15717.28 385.88 o -8 21 0 1510.75 1710.26 155.85 o -7 21 0 18.05 74.52 116.70 o -6 21 0 12330.01 13547.38 525.24 o -5 21 0 1271.04 1432.05 221.24 o -4 21 0 37.92 73.32 120.48 o -3 21 0 7460.45 7563.48 260.51 o -2 21 0 674.96 778.90 141.08 o -1 21 0 45.98 52.88 129.27 o 0 21 0 13402.74 13460.49 363.43 o -21 22 0 335.75 416.08 151.13 o -20 22 0 15862.54 16123.10 398.30 o -19 22 0 7.78 364.54 108.27 o -18 22 0 398.79 490.75 107.32 o -17 22 0 16246.98 16597.17 289.46 o -16 22 0 1.04 51.02 87.22 o -15 22 0 516.29 592.76 104.88 o -14 22 0 18210.23 17467.49 291.16 o -13 22 0 1117.05 1394.70 113.78 o -12 22 0 103.49 72.42 87.40 o -11 22 0 15313.29 15612.07 445.40 o -10 22 0 1157.82 1265.25 170.59 o -9 22 0 1269.61 1450.08 158.48 o -8 22 0 6024.84 6192.00 250.37 o -7 22 0 203.27 202.14 125.63 o -6 22 0 135.88 -39.45 200.13 o -5 22 0 6139.96 5897.02 234.83 o -4 22 0 341.15 231.16 222.43 o -3 22 0 582.49 822.06 146.06 o -2 22 0 5977.63 5663.64 250.17 o -1 22 0 283.56 383.16 141.35 o 0 22 0 241.86 530.43 146.06 o -22 23 0 6745.97 6920.06 279.64 o -21 23 0 182.63 584.48 156.64 o -20 23 0 328.44 432.75 116.91 o -19 23 0 12963.13 13308.58 294.21 o -18 23 0 439.99 537.00 111.01 o -17 23 0 63.19 79.64 98.88 o -16 23 0 11841.30 11675.86 238.62 o -15 23 0 266.96 221.17 89.94 o -14 23 0 527.13 481.96 106.27 o -13 23 0 6571.50 6434.04 193.36 o -12 23 0 38.46 -45.89 93.56 o -11 23 0 2260.52 2131.54 213.55 o -10 23 0 8104.10 8844.80 294.08 o -9 23 0 0.17 100.17 146.25 o -8 23 0 44.97 -125.85 125.85 o -7 23 0 2916.61 2788.35 281.98 o -6 23 0 44.51 131.30 122.82 o -5 23 0 557.48 585.55 136.56 o -4 23 0 4502.43 4694.93 264.97 o -3 23 0 146.67 253.81 137.43 o -2 23 0 25.96 170.26 140.87 o -1 23 0 10822.36 11623.08 346.04 o 0 23 0 18.90 33.48 138.70 o -22 24 0 61.19 92.20 146.00 o -21 24 0 11754.94 11570.01 346.55 o -20 24 0 339.03 398.18 117.70 o -19 24 0 360.17 253.57 122.24 o -18 24 0 8281.51 8189.70 256.84 o -17 24 0 532.81 430.94 122.34 o -16 24 0 114.35 248.42 107.52 o -15 24 0 5582.83 5651.85 197.51 o -14 24 0 362.26 438.64 115.77 o -13 24 0 532.49 434.22 103.67 o -12 24 0 12927.71 13071.35 421.23 o -11 24 0 44.82 188.77 143.73 o -10 24 0 836.39 857.60 218.77 o -9 24 0 4304.68 5026.81 484.90 o -8 24 0 278.95 107.04 312.15 o -7 24 0 329.97 322.41 217.96 o -6 24 0 9852.97 10609.69 316.69 o -5 24 0 841.08 725.38 160.11 o -4 24 0 1005.53 1216.64 166.27 o -3 24 0 6769.70 6519.80 277.55 o -2 24 0 4.79 -21.34 143.08 o -20 25 0 9923.09 9987.11 301.11 o -19 25 0 544.50 657.89 138.17 o -18 25 0 8.89 18.31 117.44 o -17 25 0 3164.30 3234.85 182.21 o -16 25 0 0.52 21.23 114.57 o -15 25 0 600.95 879.91 156.84 o -14 25 0 9890.96 10340.14 296.67 o -13 25 0 19.27 8.14 142.37 o -12 25 0 13.82 -156.42 159.57 o -11 25 0 5328.27 5841.83 266.90 o -10 25 0 373.66 347.10 150.50 o -9 25 0 204.72 -84.17 295.19 o -8 25 0 6732.18 6924.21 442.76 o -7 25 0 14.16 126.03 228.59 o -6 25 0 48.71 -111.92 136.85 o -5 25 0 5671.06 5984.18 269.18 o -18 26 0 129.30 160.70 213.82 o -17 26 0 0.78 103.98 124.03 o -16 26 0 8929.96 9971.24 284.86 o -15 26 0 469.17 482.15 114.76 o -14 26 0 150.64 192.60 106.20 o -13 26 0 2570.47 2667.78 210.93 o -12 26 0 98.15 -81.35 320.83 o -11 26 0 128.38 -8.70 145.95 o -10 26 0 4660.59 4687.16 377.06 o -9 26 0 1.73 -227.79 227.79 o -8 26 0 20.41 -149.47 248.80 o 0 1 1 21.60 5.86 3.29 o -1 2 1 2485.34 5226.19 92.13 o 0 2 1 225.23 256.81 8.69 o -2 3 1 9.09 38.24 23.24 o -1 3 1 2025.97 2063.39 32.66 o 0 3 1 2971.31 4963.11 249.26 o -3 4 1 561.41 581.60 17.66 o -2 4 1 12032.38 12427.73 114.41 o -1 4 1 9183.30 9873.01 150.36 o 0 4 1 1356.41 1532.91 50.92 o -4 5 1 35029.91 36770.98 288.80 o -3 5 1 7497.56 8411.70 156.92 o -2 5 1 14574.04 15487.49 155.34 o -1 5 1 2745.31 3607.96 135.18 o 0 5 1 3545.00 3588.36 66.51 o -5 6 1 852.40 1070.97 66.21 o -4 6 1 1815.46 1835.77 51.43 o -3 6 1 36889.69 37606.31 299.29 o -2 6 1 17177.58 17594.56 135.70 o -1 6 1 891.13 941.80 30.47 o 0 6 1 5579.73 5915.15 65.08 o -6 7 1 192.20 218.59 33.26 o -5 7 1 54577.20 55195.91 379.63 o -4 7 1 635.75 638.76 33.49 o -3 7 1 11247.38 11258.48 117.18 o -2 7 1 10479.37 10422.73 103.47 o -1 7 1 4579.82 4121.58 141.92 o 0 7 1 15.30 -17.45 20.79 o -7 8 1 1.52 75.49 38.95 o -6 8 1 18.11 28.76 24.76 o -5 8 1 240.61 99.87 30.41 o -4 8 1 618.07 562.47 37.19 o -3 8 1 21166.18 22786.18 270.25 o -2 8 1 9251.82 9500.30 99.21 o -1 8 1 93.04 290.51 35.78 o 0 8 1 121.00 91.55 32.44 o -8 9 1 36.93 62.33 30.00 o -7 9 1 21.20 149.57 49.87 o -6 9 1 513.72 1102.61 83.42 o -5 9 1 1213.25 1123.44 46.44 o -4 9 1 860.92 1153.18 82.73 o -3 9 1 2579.42 3494.33 99.12 o -2 9 1 8541.53 9075.14 142.03 o -1 9 1 11.81 -39.32 39.32 o 0 9 1 4185.29 8507.54 157.91 o -9 10 1 36.70 217.48 40.78 o -8 10 1 1294.91 1699.15 54.64 o -7 10 1 264.66 422.85 34.23 o -6 10 1 6122.37 5471.79 132.15 o -5 10 1 130.36 409.02 49.46 o -4 10 1 337.66 501.15 49.88 o -3 10 1 4102.14 3817.39 83.58 o -2 10 1 914.33 1110.20 43.45 o -1 10 1 190.39 485.87 66.09 o 0 10 1 1425.24 1540.11 39.36 o -10 11 1 171.85 634.30 55.65 o -9 11 1 5.77 41.34 34.97 o -8 11 1 44.23 265.99 52.07 o -7 11 1 2798.18 3446.50 68.43 o -6 11 1 0.05 -41.85 41.85 o -5 11 1 1085.87 1088.67 61.46 o -4 11 1 2169.56 2292.77 73.17 o -3 11 1 49.03 225.77 39.65 o -2 11 1 446.71 358.40 37.75 o -1 11 1 1215.03 1607.89 53.48 o 0 11 1 0.27 48.46 30.34 o -11 12 1 911.64 873.59 50.10 o -10 12 1 1884.99 2017.66 60.83 o -9 12 1 3055.49 3398.04 97.21 o -8 12 1 2.57 127.32 52.84 o -7 12 1 285.58 238.43 57.71 o -6 12 1 11549.58 10578.98 180.39 o -5 12 1 1074.24 1096.92 62.35 o -4 12 1 1280.83 1187.56 58.16 o -3 12 1 233.11 556.27 48.88 o -2 12 1 340.08 661.37 41.63 o -1 12 1 1615.56 1312.25 46.54 o 0 12 1 1065.03 1096.80 54.55 o -12 13 1 34.39 2.63 44.42 o -11 13 1 266.69 597.53 50.12 o -10 13 1 1.32 85.82 41.28 o -9 13 1 974.33 1379.99 54.63 o -8 13 1 7504.41 8173.76 114.15 o -7 13 1 47.58 107.17 59.28 o -6 13 1 1024.04 963.45 94.40 o -5 13 1 2133.92 2129.68 84.45 o -4 13 1 95.65 93.92 47.02 o -3 13 1 172.61 216.83 44.17 o -2 13 1 306.29 746.40 65.21 o -1 13 1 43.74 130.42 34.27 o 0 13 1 1413.50 1323.35 57.74 o -13 14 1 6161.93 6819.41 110.47 o -12 14 1 17.75 218.92 48.92 o -11 14 1 1084.82 945.63 54.78 o -10 14 1 12525.98 12851.06 160.27 o -9 14 1 880.97 951.73 50.62 o -8 14 1 477.91 786.42 51.28 o -7 14 1 6612.69 6733.91 207.83 o -6 14 1 5.29 276.09 65.53 o -5 14 1 718.38 1021.44 76.12 o -4 14 1 375.19 486.75 60.57 o -3 14 1 587.79 601.75 53.62 o -2 14 1 1116.38 1134.30 79.45 o -1 14 1 71.35 247.92 43.75 o 0 14 1 1764.60 1756.82 64.26 o -14 15 1 220.96 148.82 52.03 o -13 15 1 904.37 840.91 58.99 o -12 15 1 39.32 88.74 49.57 o -11 15 1 65.14 117.62 49.08 o -10 15 1 455.13 622.24 67.26 o -9 15 1 101.94 532.31 97.36 o -8 15 1 5393.57 5585.68 144.44 o -7 15 1 1902.64 2618.97 149.01 o -6 15 1 8.72 263.51 69.81 o -5 15 1 475.25 636.13 73.76 o -4 15 1 4152.95 4196.55 113.53 o -3 15 1 241.60 346.07 55.51 o -2 15 1 518.07 695.09 49.50 o -1 15 1 527.29 411.11 58.08 o 0 15 1 2155.12 1961.56 71.03 o -15 16 1 1030.09 1011.05 63.50 o -14 16 1 4384.14 4412.46 101.54 o -13 16 1 0.06 45.90 53.96 o -12 16 1 826.64 830.70 59.58 o -11 16 1 478.68 313.66 67.46 o -10 16 1 215.12 255.20 50.03 o -9 16 1 1027.59 1245.33 69.53 o -8 16 1 436.89 465.97 84.15 o -7 16 1 132.78 284.32 74.97 o -6 16 1 1252.77 1108.67 85.81 o 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1671.92 105.77 o -6 18 1 181.80 98.94 81.21 o -5 18 1 9.96 102.94 75.31 o -4 18 1 1.06 -61.65 61.65 o -3 18 1 311.94 334.00 70.19 o -2 18 1 6.69 97.41 60.39 o -1 18 1 213.33 272.49 65.90 o 0 18 1 294.14 421.15 68.87 o -18 19 1 1705.76 1816.31 110.74 o -17 19 1 117.10 110.29 57.49 o -16 19 1 345.52 256.72 57.74 o -15 19 1 183.23 167.41 56.29 o -14 19 1 1049.68 1075.10 68.80 o -13 19 1 143.67 161.96 57.66 o -12 19 1 175.29 176.20 56.11 o -11 19 1 1886.11 1968.18 78.34 o -10 19 1 681.70 578.86 54.51 o -9 19 1 208.44 48.97 96.61 o -8 19 1 2632.12 2487.82 117.46 o -7 19 1 447.31 537.68 86.39 o -6 19 1 1217.39 1534.91 98.87 o -5 19 1 28.97 41.17 71.21 o -4 19 1 28.69 -40.73 60.74 o -3 19 1 648.23 572.71 77.62 o -2 19 1 882.39 933.22 84.46 o -1 19 1 64.25 83.08 73.75 o 0 19 1 1254.30 1183.50 92.39 o -19 20 1 1.96 -75.01 75.01 o -18 20 1 144.84 155.04 64.84 o -17 20 1 60.35 97.87 61.44 o -16 20 1 0.69 -55.61 55.61 o -15 20 1 34.15 91.69 54.99 o -14 20 1 151.88 185.19 58.90 o -13 20 1 962.92 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77.34 o -8 9 2 1.05 -20.13 30.29 o -7 9 2 0.64 3.19 30.23 o -6 9 2 42715.77 41590.08 324.72 o -5 9 2 10557.45 10914.51 134.09 o -4 9 2 3547.39 4186.99 113.90 o -3 9 2 99051.84 102193.53 901.33 o -2 9 2 1602.60 2174.51 75.16 o -1 9 2 3085.87 3098.76 72.52 o 0 9 2 29525.04 30777.62 240.47 o -9 10 2 589.88 715.47 41.47 o -8 10 2 1824.45 2862.81 71.37 o -7 10 2 1456.91 1577.30 44.49 o -6 10 2 2720.65 2878.01 61.66 o -5 10 2 26119.13 25617.64 277.46 o -4 10 2 6435.65 6472.66 162.73 o -3 10 2 1577.71 1662.05 57.28 o -2 10 2 42959.72 43229.79 374.76 o -1 10 2 106.70 18.96 29.86 o 0 10 2 1678.14 1479.16 45.29 o -10 11 2 3457.39 2796.07 65.11 o -9 11 2 449.05 625.05 39.05 o -8 11 2 934.91 1185.87 46.42 o -7 11 2 13119.19 12969.84 135.05 o -6 11 2 1804.82 1560.29 63.24 o -5 11 2 7661.51 7365.96 119.50 o -4 11 2 45370.68 44523.46 424.12 o -3 11 2 3523.84 3468.67 87.88 o -2 11 2 1440.17 1387.19 46.72 o -1 11 2 4645.29 4251.74 70.64 o 0 11 2 72.31 73.98 37.05 o -11 12 2 3.20 222.32 42.57 o -10 12 2 1452.97 1662.63 56.22 o -9 12 2 19900.15 18268.47 192.33 o -8 12 2 59.14 120.28 40.85 o -7 12 2 1142.19 1258.62 47.74 o -6 12 2 16589.12 15630.95 199.88 o -5 12 2 4306.00 4072.40 149.54 o -4 12 2 71.77 62.06 43.42 o -3 12 2 11485.73 10993.52 136.94 o -2 12 2 4.52 95.14 35.74 o -1 12 2 337.79 415.05 45.40 o 0 12 2 28166.96 27458.22 264.61 o -12 13 2 3195.89 3079.66 80.27 o -11 13 2 7690.94 8223.94 116.90 o -10 13 2 6.33 94.76 41.62 o -9 13 2 77.85 -4.78 37.89 o -8 13 2 1244.27 1151.90 42.43 o -7 13 2 1195.71 1403.26 76.44 o -6 13 2 1895.25 1657.71 86.30 o -5 13 2 15114.09 14051.60 178.42 o -4 13 2 135.31 111.36 47.55 o -3 13 2 2947.90 2798.82 108.35 o -2 13 2 6011.95 5271.46 81.70 o -1 13 2 879.00 896.25 43.92 o 0 13 2 3675.22 3814.40 96.26 o -13 14 2 7172.11 7057.94 115.54 o -12 14 2 51.33 171.39 48.97 o -11 14 2 1465.93 1523.92 60.19 o -10 14 2 29365.41 28292.47 267.47 o -9 14 2 1.14 29.36 37.85 o -8 14 2 49.76 86.84 46.25 o -7 14 2 11649.10 11083.04 203.70 o -6 14 2 1.63 13.96 52.91 o -5 14 2 2353.27 2350.27 80.67 o -4 14 2 23924.64 24443.17 267.89 o -3 14 2 981.75 1125.10 55.81 o -2 14 2 643.90 886.80 46.17 o -1 14 2 13069.81 11546.49 145.02 o 0 14 2 30.25 73.81 50.56 o -14 15 2 0.45 342.19 56.60 o -13 15 2 45.29 166.17 52.33 o -12 15 2 20610.23 19862.87 211.82 o -11 15 2 423.64 397.74 52.18 o -10 15 2 9.54 -44.81 44.81 o -9 15 2 37234.84 37916.30 358.86 o -8 15 2 226.62 95.37 72.00 o -7 15 2 965.58 799.40 86.03 o -6 15 2 33841.14 32421.55 393.03 o -5 15 2 399.96 432.61 59.39 o -4 15 2 687.66 651.68 64.35 o -3 15 2 23499.64 23039.51 242.11 o -2 15 2 341.46 366.82 43.22 o -1 15 2 95.46 280.29 60.03 o 0 15 2 14549.85 14504.07 182.29 o -15 16 2 58.69 26.87 52.36 o -14 16 2 3611.46 3403.18 91.79 o -13 16 2 308.50 446.70 58.42 o -12 16 2 191.93 210.12 54.49 o -11 16 2 1963.66 2192.25 72.70 o -10 16 2 134.86 62.64 45.40 o -9 16 2 664.13 776.42 55.67 o -8 16 2 11360.13 11481.59 201.91 o -7 16 2 888.73 1060.57 93.78 o -6 16 2 1717.94 1749.86 95.57 o -5 16 2 18635.95 18613.13 246.68 o -4 16 2 3.12 -58.47 58.47 o -3 16 2 7896.29 8004.59 135.31 o -2 16 2 10116.92 9433.22 128.03 o -1 16 2 308.87 246.54 58.07 o 0 16 2 9.65 292.85 60.48 o -16 17 2 9523.13 9209.09 136.56 o -15 17 2 1800.80 2181.21 77.60 o -14 17 2 0.38 -55.79 55.79 o -13 17 2 21470.54 19949.99 220.22 o -12 17 2 1570.94 1251.31 66.71 o -11 17 2 215.00 172.81 59.82 o -10 17 2 15206.67 13676.68 164.26 o -9 17 2 47.35 87.14 54.97 o -8 17 2 421.22 610.43 78.42 o -7 17 2 11537.80 10749.24 201.41 o -6 17 2 1027.70 1033.68 89.52 o -5 17 2 174.98 179.52 69.07 o -4 17 2 11809.27 11569.98 184.62 o -3 17 2 1898.51 2214.48 84.70 o -2 17 2 5.81 160.14 67.75 o -1 17 2 7289.08 7179.36 129.45 o 0 17 2 517.99 564.96 64.09 o -17 18 2 366.36 443.48 64.17 o -16 18 2 71.16 40.12 53.22 o -15 18 2 12630.51 12602.66 169.87 o -14 18 2 6.62 55.21 57.18 o -13 18 2 251.10 294.27 59.51 o -12 18 2 20455.65 20794.91 227.33 o -11 18 2 143.37 80.89 54.40 o -10 18 2 1945.45 1911.52 73.15 o -9 18 2 8021.64 8063.39 181.31 o 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