#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:17:23 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180844 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/75/2017551.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017551_Fobs loop_ _publ_author_name 'Czapik, Agnieszka' 'Konowalska, Hanna' 'Gdaniec, Maria' _publ_section_title ; p-Phenylenediamine and its dihydrate: two-dimensional isomorphism and mechanism of the dehydration process, and N---H···N and N---H···\p interactions ; _journal_coeditor_code FG3154 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o128 _journal_page_last o132 _journal_volume 66 _journal_year 2010 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.8599 _cell_length_b 15.0248 _cell_length_c 5.8952 _exptl_crystal_F_000 312.00 _reflns_d_resolution_high 0.8004 _cod_data_source_file fg3154Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' h1 in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 94.57 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x, y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z-1/2' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 21.89 18.03 1.49 o 4 0 0 318.44 340.70 5.48 o 6 0 0 69.00 79.23 2.28 o 8 0 0 200.70 207.47 4.63 o 10 0 0 29.98 29.64 8.84 o 2 1 0 1170.31 1110.36 3.44 o 4 1 0 6.06 7.31 1.07 o 6 1 0 7.54 8.17 1.66 o 8 1 0 26.38 19.12 3.35 o 10 1 0 147.32 153.28 5.88 o 2 2 0 3444.89 3345.52 8.97 o 4 2 0 301.59 275.68 2.49 o 6 2 0 1530.88 1604.17 11.06 o 8 2 0 43.03 36.46 3.41 o 10 2 0 26.69 24.75 5.28 o 2 3 0 1836.06 1862.13 40.33 o 4 3 0 60.39 59.72 1.99 o 6 3 0 539.42 534.00 7.14 o 8 3 0 79.50 79.93 3.41 o 10 3 0 70.87 74.06 6.38 o 0 4 0 819.96 860.67 8.32 o 2 4 0 390.05 397.90 2.98 o 4 4 0 2236.09 2315.69 15.21 o 6 4 0 195.17 189.72 3.96 o 8 4 0 0.44 -0.22 1.38 o 10 4 0 91.40 92.48 6.36 o 2 5 0 73.86 83.23 3.04 o 4 5 0 64.93 74.73 2.61 o 6 5 0 479.04 518.87 8.95 o 8 5 0 1.67 -0.55 4.14 o 10 5 0 172.27 174.92 8.54 o 0 6 0 8942.80 8531.96 20.98 o 2 6 0 373.55 366.63 3.43 o 4 6 0 56.57 54.87 2.35 o 6 6 0 192.50 203.94 5.19 o 8 6 0 3.42 7.14 4.32 o 10 6 0 14.04 23.94 9.25 o 2 7 0 290.24 322.96 4.36 o 4 7 0 36.88 32.41 1.86 o 6 7 0 768.90 783.24 8.12 o 8 7 0 0.92 1.25 3.35 o 10 7 0 16.42 19.45 8.62 o 0 8 0 353.72 309.52 5.16 o 2 8 0 1164.91 1190.14 6.05 o 4 8 0 0.19 0.49 1.60 o 6 8 0 298.02 290.11 4.30 o 8 8 0 31.93 28.43 5.62 o 10 8 0 19.39 21.09 9.13 o 2 9 0 340.78 334.31 4.41 o 4 9 0 216.83 228.63 3.63 o 6 9 0 770.09 799.42 11.25 o 8 9 0 38.27 31.76 5.64 o 0 10 0 583.77 641.85 7.19 o 2 10 0 70.96 78.21 2.03 o 4 10 0 1072.37 1097.27 8.04 o 6 10 0 12.35 10.02 2.54 o 8 10 0 46.03 43.06 11.13 o 2 11 0 117.39 121.10 2.56 o 4 11 0 941.78 980.19 8.63 o 6 11 0 34.62 37.00 3.59 o 8 11 0 68.13 76.25 8.69 o 0 12 0 123.70 130.05 3.77 o 2 12 0 8.13 7.20 2.40 o 4 12 0 3.78 2.01 2.67 o 6 12 0 265.64 274.08 6.22 o 8 12 0 9.82 11.05 9.22 o 2 13 0 57.26 63.11 2.83 o 4 13 0 117.65 112.49 3.70 o 6 13 0 69.64 70.70 5.52 o 0 14 0 743.11 741.73 9.47 o 2 14 0 183.61 174.97 4.06 o 4 14 0 25.97 23.74 3.96 o 6 14 0 3.05 3.28 4.71 o 2 15 0 77.54 75.08 3.83 o 4 15 0 19.67 18.01 4.50 o 6 15 0 111.76 113.63 6.72 o 0 16 0 0.77 0.33 1.98 o 2 16 0 65.66 67.63 4.02 o 4 16 0 165.55 178.38 5.84 o 2 17 0 19.60 16.89 4.21 o 4 17 0 100.61 98.93 5.39 o 0 18 0 85.50 89.59 9.34 o 2 18 0 143.36 153.07 6.65 o 1 0 1 1116.10 1067.29 11.95 o 2 0 1 3801.62 3387.97 19.84 o 3 0 1 2716.87 2644.56 7.30 o 4 0 1 103.59 107.40 1.64 o 5 0 1 240.43 275.25 3.63 o 6 0 1 144.65 139.74 2.27 o 7 0 1 442.27 442.59 3.97 o 8 0 1 363.74 365.24 7.03 o 9 0 1 47.40 49.00 5.46 o 10 0 1 0.08 -2.10 2.90 o 1 1 1 181.63 185.72 2.25 o 2 1 1 1100.64 1052.65 7.55 o 3 1 1 30.50 29.15 0.74 o 4 1 1 169.77 179.08 1.47 o 5 1 1 146.24 141.36 1.48 o 6 1 1 57.10 55.53 1.26 o 7 1 1 37.82 35.07 1.47 o 8 1 1 20.43 22.76 2.42 o 9 1 1 12.43 11.53 4.49 o 10 1 1 91.02 88.96 4.68 o 1 2 1 5417.53 4939.92 13.29 o 2 2 1 1073.97 1067.45 5.54 o 3 2 1 1395.69 1395.60 7.17 o 4 2 1 455.12 472.90 2.36 o 5 2 1 10.88 11.91 0.64 o 6 2 1 0.04 0.05 0.54 o 7 2 1 42.76 40.33 1.88 o 8 2 1 105.78 102.89 2.41 o 9 2 1 51.74 55.50 3.86 o 10 2 1 0.03 -0.79 1.07 o 0 3 1 1948.24 1875.26 17.81 o 1 3 1 645.84 635.11 4.93 o 2 3 1 4536.18 4245.90 12.79 o 3 3 1 1147.39 1183.25 6.65 o 4 3 1 6.07 6.30 0.92 o 5 3 1 40.92 43.63 0.93 o 6 3 1 18.77 17.63 1.49 o 7 3 1 29.76 26.18 1.85 o 8 3 1 61.93 58.71 2.44 o 9 3 1 66.48 70.79 3.96 o 10 3 1 187.37 190.03 5.17 o 1 4 1 1013.69 992.19 4.15 o 2 4 1 299.55 288.38 1.89 o 3 4 1 872.84 834.44 4.58 o 4 4 1 1115.13 1197.45 5.58 o 5 4 1 105.62 112.99 3.31 o 6 4 1 12.76 11.15 2.04 o 7 4 1 99.06 90.76 2.27 o 8 4 1 104.00 108.05 2.98 o 9 4 1 83.57 89.72 3.87 o 10 4 1 85.87 94.07 5.30 o 0 5 1 1309.57 1347.00 8.97 o 1 5 1 118.31 129.71 1.89 o 2 5 1 11.23 12.57 0.78 o 3 5 1 201.98 209.72 1.96 o 4 5 1 113.14 111.00 1.23 o 5 5 1 2.04 2.28 2.03 o 6 5 1 10.81 10.99 3.17 o 7 5 1 0.05 0.15 2.19 o 8 5 1 201.50 215.78 3.73 o 9 5 1 9.15 8.17 4.31 o 10 5 1 127.72 125.63 7.18 o 1 6 1 1.51 2.32 0.73 o 2 6 1 38.84 35.43 0.84 o 3 6 1 1114.38 1196.46 15.16 o 4 6 1 659.99 680.41 5.58 o 5 6 1 8.18 6.45 1.45 o 6 6 1 1.80 2.82 1.67 o 7 6 1 149.68 156.12 3.08 o 8 6 1 127.13 120.93 4.14 o 9 6 1 25.75 23.02 3.80 o 10 6 1 12.28 8.74 5.69 o 0 7 1 413.37 455.36 3.61 o 1 7 1 0.39 0.03 0.47 o 2 7 1 104.10 102.90 1.29 o 3 7 1 38.68 44.31 1.28 o 4 7 1 454.96 472.41 5.37 o 5 7 1 158.78 175.92 2.49 o 6 7 1 114.66 109.84 2.10 o 7 7 1 237.14 251.47 4.40 o 8 7 1 139.58 132.18 4.22 o 9 7 1 5.07 7.41 4.07 o 10 7 1 0.00 1.18 6.25 o 1 8 1 996.12 1102.08 5.76 o 2 8 1 0.07 0.07 0.59 o 3 8 1 413.82 409.29 3.03 o 4 8 1 128.65 130.05 2.03 o 5 8 1 9.06 8.47 1.76 o 6 8 1 336.51 353.54 6.68 o 7 8 1 55.99 53.62 3.13 o 8 8 1 2.61 -2.29 2.91 o 9 8 1 13.81 16.32 4.49 o 0 9 1 543.16 571.86 5.36 o 1 9 1 1.20 2.03 1.02 o 2 9 1 28.26 25.63 1.37 o 3 9 1 205.51 210.57 2.07 o 4 9 1 8.59 7.84 1.48 o 5 9 1 117.98 114.57 2.26 o 6 9 1 4.00 4.07 1.99 o 7 9 1 35.92 35.57 4.16 o 8 9 1 56.69 54.07 6.68 o 9 9 1 50.04 51.32 5.87 o 1 10 1 48.02 39.72 1.33 o 2 10 1 60.17 62.78 2.02 o 3 10 1 125.23 127.82 1.85 o 4 10 1 309.87 320.48 3.67 o 5 10 1 154.82 153.31 2.68 o 6 10 1 115.38 113.07 3.01 o 7 10 1 33.68 30.01 3.67 o 8 10 1 32.13 26.34 4.63 o 9 10 1 117.19 129.20 4.28 o 0 11 1 115.34 105.79 2.83 o 1 11 1 30.89 34.30 1.50 o 2 11 1 320.95 313.42 3.18 o 3 11 1 85.92 89.71 1.99 o 4 11 1 54.96 54.99 2.40 o 5 11 1 51.27 49.94 2.16 o 6 11 1 75.04 74.48 3.56 o 7 11 1 26.04 28.28 3.90 o 8 11 1 0.00 -0.09 4.37 o 1 12 1 34.84 29.87 1.80 o 2 12 1 176.40 169.98 2.57 o 3 12 1 426.68 431.00 3.97 o 4 12 1 172.07 179.44 3.03 o 5 12 1 24.66 24.23 2.76 o 6 12 1 26.98 26.23 3.31 o 7 12 1 47.24 51.74 3.78 o 8 12 1 0.85 4.68 4.25 o 0 13 1 111.11 112.77 3.59 o 1 13 1 17.42 16.36 1.94 o 2 13 1 139.78 129.30 2.43 o 3 13 1 78.50 74.38 2.16 o 4 13 1 118.05 123.99 3.00 o 5 13 1 17.23 18.51 3.02 o 6 13 1 5.19 5.56 3.84 o 7 13 1 99.07 109.01 5.02 o 1 14 1 83.12 91.61 2.37 o 2 14 1 214.47 200.45 4.05 o 3 14 1 51.22 51.09 2.52 o 4 14 1 1.92 -0.27 1.16 o 5 14 1 9.92 9.71 2.93 o 6 14 1 256.51 278.54 5.55 o 7 14 1 39.33 38.34 5.29 o 0 15 1 210.49 184.84 4.30 o 1 15 1 6.25 7.26 2.35 o 2 15 1 19.26 14.93 2.89 o 3 15 1 1.65 2.76 2.49 o 4 15 1 1.33 0.96 1.15 o 5 15 1 38.75 36.69 3.38 o 6 15 1 57.18 57.42 5.65 o 1 16 1 56.44 51.62 3.37 o 2 16 1 6.46 3.01 2.75 o 3 16 1 19.94 13.54 3.16 o 4 16 1 13.42 15.04 3.18 o 5 16 1 15.16 18.60 3.47 o 0 17 1 293.06 274.60 5.37 o 1 17 1 4.69 6.57 2.71 o 2 17 1 25.10 30.35 3.60 o 3 17 1 0.77 -0.08 3.33 o 4 17 1 0.53 -0.15 3.58 o 1 18 1 0.02 1.48 3.30 o 2 18 1 22.05 17.99 3.70 o 0 0 2 222.52 219.43 2.21 o 1 0 2 93.65 101.32 1.38 o 2 0 2 261.05 246.02 3.76 o 3 0 2 65.44 74.96 1.57 o 4 0 2 966.35 923.12 9.26 o 5 0 2 18.98 15.53 1.82 o 6 0 2 497.76 492.60 8.00 o 7 0 2 545.22 561.12 7.15 o 8 0 2 85.61 84.58 4.36 o 9 0 2 29.62 18.17 7.27 o 10 0 2 65.35 67.48 8.41 o 1 1 2 37.60 35.08 0.51 o 2 1 2 50.68 40.84 1.13 o 3 1 2 1101.81 1104.06 9.78 o 4 1 2 280.67 306.57 2.78 o 5 1 2 1.36 0.14 1.13 o 6 1 2 132.97 127.00 3.52 o 7 1 2 57.32 58.43 2.50 o 8 1 2 81.35 89.31 2.59 o 9 1 2 6.88 3.96 4.33 o 10 1 2 0.00 -7.16 7.16 o 0 2 2 3650.27 3496.69 26.15 o 1 2 2 542.36 565.31 6.22 o 2 2 2 85.77 88.81 0.83 o 3 2 2 242.42 260.11 3.19 o 4 2 2 195.56 175.29 1.85 o 5 2 2 27.75 29.13 1.04 o 6 2 2 38.99 36.15 1.79 o 7 2 2 33.69 31.97 2.53 o 8 2 2 44.05 45.82 3.49 o 9 2 2 57.70 61.36 4.04 o 10 2 2 43.15 45.56 6.00 o 1 3 2 621.79 652.54 8.68 o 2 3 2 10.95 9.86 0.57 o 3 3 2 68.29 63.64 1.46 o 4 3 2 983.83 997.55 4.49 o 5 3 2 211.20 227.81 2.03 o 6 3 2 1.51 1.43 1.03 o 7 3 2 1.05 -1.53 2.57 o 8 3 2 102.99 97.48 3.48 o 9 3 2 496.62 525.16 6.06 o 10 3 2 77.92 83.91 5.98 o 0 4 2 1644.04 1601.43 9.43 o 1 4 2 15.22 8.95 0.73 o 2 4 2 2008.44 2153.02 9.57 o 3 4 2 701.20 731.59 5.48 o 4 4 2 29.98 37.11 0.95 o 5 4 2 124.67 121.78 2.19 o 6 4 2 200.37 196.96 5.40 o 7 4 2 1.25 1.43 2.59 o 8 4 2 18.26 21.72 3.55 o 9 4 2 4.78 4.91 4.09 o 10 4 2 23.16 19.79 5.54 o 1 5 2 219.92 235.70 3.14 o 2 5 2 570.21 649.93 4.42 o 3 5 2 1281.21 1326.23 10.24 o 4 5 2 154.97 147.10 1.73 o 5 5 2 105.32 109.16 3.32 o 6 5 2 25.69 21.58 2.41 o 7 5 2 110.36 108.55 2.54 o 8 5 2 0.01 -0.85 1.63 o 9 5 2 104.75 95.94 4.70 o 10 5 2 3.08 3.27 8.49 o 0 6 2 554.84 600.03 7.88 o 1 6 2 56.04 51.54 1.09 o 2 6 2 398.33 430.95 4.75 o 3 6 2 43.08 45.84 1.02 o 4 6 2 319.29 311.47 3.51 o 5 6 2 174.34 182.59 4.14 o 6 6 2 55.44 47.01 4.37 o 7 6 2 275.42 265.41 4.13 o 8 6 2 10.36 9.48 3.85 o 9 6 2 4.80 1.96 4.49 o 10 6 2 133.41 153.59 5.38 o 1 7 2 3.39 2.82 1.06 o 2 7 2 221.19 224.91 2.37 o 3 7 2 144.97 132.24 1.86 o 4 7 2 25.45 23.74 1.68 o 5 7 2 159.91 174.92 3.40 o 6 7 2 398.82 395.79 6.77 o 7 7 2 0.33 0.19 1.72 o 8 7 2 128.58 141.11 4.29 o 9 7 2 114.05 108.12 4.53 o 0 8 2 0.45 0.31 1.47 o 1 8 2 32.47 33.83 1.20 o 2 8 2 0.43 0.91 0.82 o 3 8 2 41.75 44.98 1.33 o 4 8 2 226.66 225.10 3.03 o 5 8 2 116.88 120.08 4.08 o 6 8 2 124.72 129.71 3.33 o 7 8 2 72.02 61.25 5.23 o 8 8 2 11.09 12.01 3.92 o 9 8 2 24.05 22.73 4.74 o 1 9 2 191.36 189.02 2.33 o 2 9 2 83.48 81.18 1.65 o 3 9 2 49.31 46.25 1.60 o 4 9 2 4.32 3.78 1.77 o 5 9 2 14.51 10.71 3.12 o 6 9 2 0.16 -0.85 1.09 o 7 9 2 48.67 43.25 7.23 o 8 9 2 15.47 8.83 4.20 o 9 9 2 18.38 18.85 4.44 o 0 10 2 582.39 589.97 7.64 o 1 10 2 21.52 20.03 1.79 o 2 10 2 459.81 465.01 3.75 o 3 10 2 289.68 293.79 3.03 o 4 10 2 10.33 11.32 1.99 o 5 10 2 8.55 9.82 2.65 o 6 10 2 43.67 41.68 3.23 o 7 10 2 62.11 65.81 6.59 o 8 10 2 1.39 1.67 5.41 o 1 11 2 77.98 79.68 1.89 o 2 11 2 22.36 24.69 1.94 o 3 11 2 175.06 192.60 2.48 o 4 11 2 156.58 152.41 2.78 o 5 11 2 36.76 32.75 3.11 o 6 11 2 4.86 4.98 3.37 o 7 11 2 11.55 12.33 3.98 o 8 11 2 21.18 25.75 4.83 o 0 12 2 539.15 557.12 6.36 o 1 12 2 131.66 126.80 2.63 o 2 12 2 10.94 16.07 2.08 o 3 12 2 209.20 196.10 2.78 o 4 12 2 12.01 6.92 2.70 o 5 12 2 80.18 79.89 3.13 o 6 12 2 10.61 7.09 3.82 o 7 12 2 20.80 17.12 4.39 o 1 13 2 66.15 57.58 2.45 o 2 13 2 5.31 3.92 1.96 o 3 13 2 50.82 47.64 3.08 o 4 13 2 140.10 137.67 4.66 o 5 13 2 127.22 127.30 3.90 o 6 13 2 11.92 10.33 3.40 o 7 13 2 18.79 21.89 4.24 o 0 14 2 104.77 111.49 3.43 o 1 14 2 18.55 14.10 2.62 o 2 14 2 0.61 -0.06 1.49 o 3 14 2 82.44 74.05 3.06 o 4 14 2 134.42 143.28 3.94 o 5 14 2 100.67 94.97 4.73 o 6 14 2 92.11 104.59 4.66 o 1 15 2 379.88 387.30 4.73 o 2 15 2 9.79 8.35 3.40 o 3 15 2 19.87 22.37 3.25 o 4 15 2 1.00 1.24 3.86 o 5 15 2 23.19 18.87 4.21 o 0 16 2 239.70 250.07 6.05 o 1 16 2 0.41 1.18 2.69 o 2 16 2 3.48 -0.30 3.91 o 3 16 2 5.05 7.34 3.64 o 4 16 2 13.83 11.12 3.74 o 1 17 2 35.84 26.12 3.41 o 2 17 2 31.93 26.42 3.71 o 3 17 2 19.96 18.77 4.70 o 0 18 2 80.04 79.70 7.16 o 1 0 3 1479.89 1489.21 6.59 o 2 0 3 65.62 59.47 1.27 o 3 0 3 216.96 191.86 2.60 o 4 0 3 74.51 72.92 2.72 o 5 0 3 35.84 32.90 2.67 o 6 0 3 1131.07 1165.03 10.55 o 7 0 3 21.86 20.62 3.88 o 8 0 3 5.57 3.61 5.18 o 9 0 3 3.19 1.24 6.36 o 10 0 3 33.47 34.10 8.17 o 0 1 3 1885.40 1942.25 14.38 o 1 1 3 272.32 289.52 2.54 o 2 1 3 219.43 219.92 3.16 o 3 1 3 9.03 7.37 1.19 o 4 1 3 1.59 -0.02 1.00 o 5 1 3 29.97 30.60 1.79 o 6 1 3 146.66 141.06 4.20 o 7 1 3 12.38 8.84 3.00 o 8 1 3 47.01 44.76 3.39 o 9 1 3 8.82 9.51 4.03 o 10 1 3 24.33 17.61 6.17 o 1 2 3 108.38 131.38 1.33 o 2 2 3 55.25 48.62 0.91 o 3 2 3 190.73 201.64 2.01 o 4 2 3 3.77 2.26 1.07 o 5 2 3 42.89 41.24 1.99 o 6 2 3 513.58 519.00 4.65 o 7 2 3 172.94 181.15 3.15 o 8 2 3 70.50 64.75 3.25 o 9 2 3 1.90 0.05 2.90 o 10 2 3 37.17 40.76 6.40 o 0 3 3 2.89 2.13 0.92 o 1 3 3 3.87 4.80 0.78 o 2 3 3 1.68 0.46 0.51 o 3 3 3 10.95 11.22 1.38 o 4 3 3 1206.94 1214.32 6.13 o 5 3 3 2.73 1.12 1.59 o 6 3 3 43.97 37.27 2.60 o 7 3 3 38.09 37.04 2.99 o 8 3 3 54.48 51.80 3.65 o 9 3 3 7.07 7.85 4.45 o 1 4 3 274.16 299.42 2.31 o 2 4 3 214.74 235.41 1.71 o 3 4 3 45.22 38.76 1.49 o 4 4 3 242.05 247.34 2.41 o 5 4 3 46.41 44.42 1.99 o 6 4 3 183.57 185.69 3.38 o 7 4 3 12.48 12.69 3.10 o 8 4 3 22.54 18.68 4.21 o 9 4 3 45.42 42.30 4.84 o 0 5 3 36.60 34.96 1.51 o 1 5 3 24.17 29.58 1.00 o 2 5 3 43.75 41.74 1.43 o 3 5 3 27.67 29.97 1.24 o 4 5 3 2.03 2.05 0.97 o 5 5 3 224.99 245.13 5.03 o 6 5 3 347.18 349.64 4.55 o 7 5 3 67.31 54.83 3.28 o 8 5 3 15.18 14.73 3.62 o 9 5 3 17.43 15.66 4.23 o 1 6 3 35.22 26.90 1.14 o 2 6 3 6.51 4.78 1.13 o 3 6 3 206.95 216.72 2.85 o 4 6 3 4.55 2.71 1.96 o 5 6 3 9.60 9.32 2.67 o 6 6 3 219.04 197.42 3.68 o 7 6 3 35.37 36.04 3.92 o 8 6 3 3.28 1.92 3.94 o 9 6 3 8.34 4.33 4.63 o 0 7 3 3674.71 3774.77 22.15 o 1 7 3 83.04 88.91 1.59 o 2 7 3 71.59 69.46 1.45 o 3 7 3 5.61 4.41 1.45 o 4 7 3 24.86 24.63 2.48 o 5 7 3 45.96 38.51 3.97 o 6 7 3 0.21 -0.15 1.04 o 7 7 3 40.77 34.48 4.16 o 8 7 3 55.39 53.94 4.33 o 9 7 3 0.79 -0.40 0.42 o 1 8 3 3.89 4.62 1.33 o 2 8 3 78.87 80.12 1.53 o 3 8 3 46.21 42.25 1.74 o 4 8 3 17.36 13.83 2.58 o 5 8 3 19.72 15.41 3.69 o 6 8 3 55.87 44.16 4.06 o 7 8 3 5.09 6.05 4.01 o 8 8 3 182.58 176.37 4.34 o 0 9 3 121.50 129.54 2.98 o 1 9 3 3.57 4.26 1.44 o 2 9 3 293.03 294.84 3.03 o 3 9 3 16.64 15.46 1.86 o 4 9 3 188.03 188.75 5.58 o 5 9 3 114.62 91.10 4.00 o 6 9 3 200.24 207.65 4.63 o 7 9 3 26.01 22.84 3.85 o 8 9 3 55.68 53.18 4.96 o 1 10 3 145.23 142.78 2.77 o 2 10 3 274.20 276.32 3.02 o 3 10 3 31.83 25.65 2.18 o 4 10 3 28.97 22.97 3.00 o 5 10 3 68.57 64.20 3.49 o 6 10 3 50.26 52.47 5.18 o 7 10 3 18.82 23.48 4.64 o 8 10 3 67.81 61.40 5.21 o 0 11 3 107.36 111.90 4.19 o 1 11 3 23.42 19.07 2.34 o 2 11 3 171.15 179.28 2.97 o 3 11 3 174.31 170.14 3.42 o 4 11 3 28.21 30.83 3.36 o 5 11 3 1.90 1.80 3.87 o 6 11 3 38.28 39.34 4.02 o 7 11 3 0.14 2.37 2.55 o 1 12 3 13.80 13.35 2.37 o 2 12 3 43.57 41.65 2.86 o 3 12 3 28.91 31.43 2.97 o 4 12 3 110.04 98.43 3.49 o 5 12 3 26.70 22.94 5.43 o 6 12 3 1.12 2.51 3.87 o 7 12 3 43.35 44.32 4.49 o 0 13 3 537.38 593.15 8.61 o 1 13 3 0.71 -0.33 3.65 o 2 13 3 68.36 70.61 2.86 o 3 13 3 74.71 62.22 3.89 o 4 13 3 31.46 35.73 3.69 o 5 13 3 19.03 17.71 3.55 o 6 13 3 11.36 12.87 4.46 o 1 14 3 74.11 75.27 3.24 o 2 14 3 6.64 6.89 2.71 o 3 14 3 20.65 12.78 3.60 o 4 14 3 33.65 30.84 4.18 o 5 14 3 0.70 -0.14 4.37 o 0 15 3 0.78 0.36 3.81 o 1 15 3 46.46 46.54 3.90 o 2 15 3 188.17 193.12 3.96 o 3 15 3 33.45 27.19 4.15 o 4 15 3 0.02 0.71 3.30 o 1 16 3 1.12 -2.66 3.87 o 2 16 3 83.52 89.52 4.18 o 3 16 3 35.77 37.21 4.08 o 0 17 3 55.86 62.77 5.89 o 1 17 3 2.74 -0.54 4.32 o 0 0 4 0.07 0.51 2.37 o 1 0 4 207.96 221.03 3.12 o 2 0 4 458.83 464.52 5.83 o 3 0 4 71.41 65.91 2.17 o 4 0 4 136.69 128.93 2.60 o 5 0 4 384.08 375.28 6.95 o 6 0 4 27.04 24.22 3.74 o 7 0 4 255.60 270.80 6.16 o 8 0 4 38.88 31.45 7.25 o 9 0 4 3.48 2.55 5.83 o 1 1 4 64.45 58.36 1.05 o 2 1 4 35.60 35.58 1.28 o 3 1 4 260.31 246.36 3.45 o 4 1 4 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