#------------------------------------------------------------------------------ #$Date: 2010-04-11 15:29:29 +0300 (Sun, 11 Apr 2010) $ #$Revision: 1088 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2017560.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017560_Fobs loop_ _publ_author_name 'Balamurugan, P.' 'Jagan, R.' 'Sivakumar, K.' _publ_section_title ; Dihydrogen phosphate mediated supramolecular frameworks in 2- and 4-chloroanilinium dihydrogen phosphate salts ; _journal_coeditor_code GD3320 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o109 _journal_page_last o113 _journal_volume 66 _journal_year 2010 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.7371 _cell_length_b 7.8756 _cell_length_c 25.1409 _exptl_crystal_F_000 928.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file gd33204CADHPsup3.hkl _[local]_cod_data_source_block 4CADHP #BEGIN Tags that were not found in dictionaries: _shelx_title ' phos2 in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 243.12 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 18982.48 18733.43 76.56 o 6 0 0 756.46 704.88 17.18 o 8 0 0 16819.77 15832.44 93.29 o 10 0 0 464.54 396.70 18.88 o 4 1 0 544.10 550.28 10.24 o 6 1 0 12942.28 12724.27 76.52 o 8 1 0 307.68 344.53 5.49 o 10 1 0 2316.69 2357.61 63.65 o 0 2 0 1754.36 1893.95 17.75 o 2 2 0 8580.11 8525.05 144.87 o 4 2 0 1418.35 1162.34 16.49 o 6 2 0 4.55 5.68 1.67 o 8 2 0 108.22 158.44 12.10 o 10 2 0 105.23 139.24 10.81 o 2 3 0 12199.63 12732.04 184.99 o 4 3 0 7.37 5.03 2.38 o 6 3 0 843.42 802.08 13.05 o 8 3 0 20.77 13.76 4.07 o 10 3 0 113.89 101.10 6.84 o 0 4 0 14410.75 14973.64 70.53 o 2 4 0 3763.24 3908.63 86.12 o 4 4 0 671.48 625.15 9.23 o 6 4 0 68.32 62.68 5.63 o 8 4 0 499.94 442.05 11.40 o 10 4 0 88.62 86.58 7.10 o 2 5 0 1241.64 1166.91 37.26 o 4 5 0 104.52 107.14 4.88 o 6 5 0 126.90 133.35 8.59 o 8 5 0 13.19 25.33 4.95 o 0 6 0 3817.46 3881.29 43.23 o 2 6 0 30.68 31.11 4.89 o 4 6 0 8.65 16.20 9.78 o 6 6 0 27.26 30.08 4.85 o 8 6 0 305.23 322.19 11.42 o 2 7 0 372.22 379.33 15.98 o 4 7 0 7.03 5.46 6.26 o 6 7 0 439.46 384.98 18.32 o 0 8 0 19.17 15.81 6.83 o 2 8 0 35.50 46.76 9.10 o 4 8 0 712.25 660.51 23.89 o 6 8 0 0.93 4.21 7.28 o 2 9 0 73.65 127.76 13.54 o 1 1 1 21.42 12.40 0.44 o 2 1 1 22792.32 21390.48 427.24 o 3 1 1 616.42 593.25 7.33 o 4 1 1 23.09 25.91 1.21 o 5 1 1 160.50 146.23 3.00 o 6 1 1 437.10 405.50 8.17 o 7 1 1 62.12 58.17 2.29 o 8 1 1 188.99 190.88 3.55 o 9 1 1 33.29 73.02 3.11 o 10 1 1 715.87 767.22 12.53 o 11 1 1 0.90 7.59 4.52 o 0 2 1 59109.24 57540.79 721.21 o 1 2 1 6901.85 6899.44 50.41 o 2 2 1 4011.65 4095.33 32.89 o 3 2 1 572.32 684.22 13.20 o 4 2 1 627.67 569.31 6.21 o 5 2 1 694.54 676.84 8.82 o 6 2 1 0.37 2.14 0.78 o 7 2 1 874.40 870.62 10.38 o 8 2 1 1421.23 1373.32 10.49 o 9 2 1 96.42 82.97 3.88 o 10 2 1 108.30 108.47 4.24 o 11 2 1 1.53 10.15 2.74 o 1 3 1 9089.47 8748.07 70.60 o 2 3 1 1000.09 930.76 7.13 o 3 3 1 7103.49 6925.07 96.89 o 4 3 1 1207.93 1202.01 89.48 o 5 3 1 2300.09 2078.56 22.08 o 6 3 1 370.89 391.80 5.71 o 7 3 1 971.50 945.21 10.80 o 8 3 1 24.63 28.17 3.25 o 9 3 1 680.45 631.32 9.05 o 10 3 1 0.32 4.53 2.78 o 0 4 1 496.53 439.84 9.21 o 1 4 1 6111.26 6037.68 36.05 o 2 4 1 575.22 571.27 7.01 o 3 4 1 4509.61 4201.54 77.19 o 4 4 1 305.66 332.73 6.10 o 5 4 1 2531.04 2473.92 47.07 o 6 4 1 2.37 2.67 2.24 o 7 4 1 2895.69 2921.31 18.41 o 8 4 1 0.11 2.68 2.73 o 9 4 1 419.21 408.45 8.10 o 10 4 1 43.80 45.77 5.32 o 1 5 1 710.60 685.13 8.57 o 2 5 1 2.49 4.05 3.67 o 3 5 1 860.58 836.02 13.23 o 4 5 1 28.92 34.25 2.30 o 5 5 1 3491.51 3131.13 22.02 o 6 5 1 35.10 38.65 3.79 o 7 5 1 161.80 172.26 5.77 o 8 5 1 24.71 22.28 3.44 o 9 5 1 348.20 374.28 8.49 o 0 6 1 38.76 64.09 6.15 o 1 6 1 35.32 43.71 3.53 o 2 6 1 50.45 58.36 2.88 o 3 6 1 1068.37 1056.30 21.96 o 4 6 1 287.53 263.81 8.56 o 5 6 1 0.03 -1.75 2.33 o 6 6 1 1.95 2.74 2.59 o 7 6 1 133.33 115.17 5.50 o 8 6 1 24.86 26.70 4.01 o 1 7 1 119.62 105.57 5.29 o 2 7 1 0.50 3.18 3.21 o 3 7 1 36.92 53.05 6.22 o 4 7 1 0.95 -3.90 3.90 o 5 7 1 84.23 88.76 7.64 o 6 7 1 169.98 136.75 8.93 o 7 7 1 0.24 -4.14 4.14 o 0 8 1 90.42 107.97 8.00 o 1 8 1 24.61 8.39 3.29 o 2 8 1 17.69 21.68 5.41 o 3 8 1 146.74 153.72 9.61 o 4 8 1 26.04 47.33 6.78 o 5 8 1 23.79 20.52 8.02 o 6 8 1 1.01 1.00 4.77 o 1 9 1 7.15 -4.54 4.54 o 2 9 1 2.04 -1.38 4.87 o 3 9 1 2.72 -4.90 4.90 o 1 0 2 14.44 15.16 4.84 o 2 0 2 1.88 11.47 0.72 o 3 0 2 1152.33 1206.04 13.88 o 4 0 2 7987.61 8528.30 161.53 o 5 0 2 124.76 122.18 4.24 o 6 0 2 6.57 6.96 1.25 o 7 0 2 1586.45 1535.70 19.35 o 8 0 2 1782.39 1597.68 37.66 o 9 0 2 425.94 419.98 25.71 o 10 0 2 7.99 16.91 5.80 o 11 0 2 0.04 -0.46 7.39 o 1 1 2 1241.25 1261.15 13.27 o 2 1 2 4507.33 4679.17 58.89 o 3 1 2 2117.19 2092.02 28.47 o 4 1 2 422.63 449.90 10.74 o 5 1 2 2310.35 2234.06 32.79 o 6 1 2 4024.05 4110.68 55.66 o 7 1 2 28.59 30.16 1.84 o 8 1 2 96.75 103.83 3.39 o 9 1 2 199.19 183.62 4.23 o 10 1 2 410.90 393.07 7.97 o 11 1 2 1.92 8.04 4.59 o 0 2 2 4358.08 4163.54 37.81 o 1 2 2 13097.50 12777.80 80.22 o 2 2 2 4008.80 4106.43 37.88 o 3 2 2 365.72 274.13 17.69 o 4 2 2 715.48 579.42 7.65 o 5 2 2 237.75 237.76 2.56 o 6 2 2 385.69 352.01 18.59 o 7 2 2 1283.77 1354.63 8.03 o 8 2 2 521.91 580.93 7.20 o 9 2 2 179.90 199.96 5.00 o 10 2 2 6.62 8.91 2.49 o 11 2 2 72.11 75.62 4.38 o 1 3 2 5.75 17.32 3.60 o 2 3 2 1061.68 862.54 8.26 o 3 3 2 459.28 460.53 6.35 o 4 3 2 189.06 167.90 10.89 o 5 3 2 309.76 255.49 5.91 o 6 3 2 196.69 190.20 3.53 o 7 3 2 282.81 286.25 4.77 o 8 3 2 8.43 11.49 2.06 o 9 3 2 13.11 30.98 3.13 o 10 3 2 90.93 110.08 4.98 o 0 4 2 700.18 843.72 11.94 o 1 4 2 4650.78 4695.56 31.46 o 2 4 2 1121.27 1115.96 18.61 o 3 4 2 73.34 75.65 3.15 o 4 4 2 1283.29 1296.40 22.62 o 5 4 2 0.64 0.13 2.46 o 6 4 2 8.30 7.37 2.42 o 7 4 2 967.96 956.38 10.99 o 8 4 2 0.95 1.24 2.67 o 9 4 2 1.09 5.97 2.30 o 10 4 2 40.05 55.35 4.24 o 1 5 2 544.31 520.15 9.84 o 2 5 2 4.85 7.29 3.61 o 3 5 2 976.84 923.32 20.72 o 4 5 2 359.81 351.87 8.45 o 5 5 2 1064.43 1024.70 11.37 o 6 5 2 180.36 199.96 6.24 o 7 5 2 19.92 23.77 3.30 o 8 5 2 4.31 3.93 2.89 o 9 5 2 50.01 55.51 4.60 o 0 6 2 136.16 161.52 21.16 o 1 6 2 17.44 19.34 3.01 o 2 6 2 23.16 25.03 3.07 o 3 6 2 90.92 104.73 4.10 o 4 6 2 1210.38 1156.91 22.77 o 5 6 2 106.23 104.13 4.75 o 6 6 2 0.46 0.58 2.56 o 7 6 2 106.03 108.70 5.50 o 8 6 2 110.34 111.66 5.84 o 1 7 2 204.17 179.29 6.22 o 2 7 2 532.20 604.78 10.15 o 3 7 2 6.14 9.46 4.66 o 4 7 2 2.30 1.85 4.17 o 5 7 2 11.25 19.08 5.29 o 6 7 2 630.99 572.42 15.16 o 7 7 2 47.72 40.90 9.33 o 0 8 2 248.61 285.66 11.26 o 1 8 2 8.05 5.42 3.22 o 2 8 2 17.17 18.77 5.39 o 3 8 2 0.33 -1.75 4.60 o 4 8 2 296.57 311.19 16.95 o 5 8 2 7.35 6.07 6.20 o 1 9 2 138.23 129.31 9.49 o 2 9 2 159.91 196.69 10.98 o 3 9 2 61.20 75.30 8.45 o 1 1 3 2412.31 2551.24 24.34 o 2 1 3 239.17 390.83 3.51 o 3 1 3 272.26 228.35 4.28 o 4 1 3 520.63 499.20 4.53 o 5 1 3 2026.60 2101.74 27.51 o 6 1 3 77.01 104.42 3.26 o 7 1 3 215.14 187.44 3.49 o 8 1 3 57.66 63.71 3.14 o 9 1 3 230.17 211.19 6.20 o 10 1 3 26.09 14.17 6.57 o 11 1 3 163.76 154.75 10.05 o 0 2 3 139.89 77.33 9.20 o 1 2 3 127.47 178.32 7.95 o 2 2 3 347.53 385.22 3.35 o 3 2 3 461.92 491.37 6.86 o 4 2 3 4769.99 5078.84 55.98 o 5 2 3 235.71 229.12 2.63 o 6 2 3 85.78 76.33 2.91 o 7 2 3 12.09 21.42 1.45 o 8 2 3 53.74 47.80 4.39 o 9 2 3 711.06 635.27 7.77 o 10 2 3 31.26 47.00 3.36 o 11 2 3 84.27 89.70 6.49 o 1 3 3 2864.92 2807.82 22.79 o 2 3 3 3516.63 3835.49 27.57 o 3 3 3 564.05 620.53 7.19 o 4 3 3 439.32 491.65 10.19 o 5 3 3 16.11 23.98 2.45 o 6 3 3 121.23 116.11 3.59 o 7 3 3 1946.38 1885.49 23.61 o 8 3 3 101.06 111.59 3.52 o 9 3 3 48.59 45.44 3.46 o 10 3 3 2.46 7.42 2.74 o 0 4 3 169.30 89.64 20.08 o 1 4 3 1201.20 1157.97 10.10 o 2 4 3 242.24 237.78 5.95 o 3 4 3 598.73 590.89 12.08 o 4 4 3 160.15 106.00 3.58 o 5 4 3 465.40 435.01 6.56 o 6 4 3 316.92 289.54 7.50 o 7 4 3 297.42 308.29 8.52 o 8 4 3 50.34 81.41 4.60 o 9 4 3 187.63 182.86 4.85 o 10 4 3 7.11 5.47 2.39 o 1 5 3 1848.39 1807.30 18.24 o 2 5 3 4215.83 4245.29 42.11 o 3 5 3 1358.85 1359.17 18.60 o 4 5 3 264.41 261.71 5.31 o 5 5 3 990.04 948.19 12.19 o 6 5 3 2612.96 2479.39 25.29 o 7 5 3 23.50 36.41 3.62 o 8 5 3 10.67 11.23 3.14 o 9 5 3 619.07 661.83 10.84 o 0 6 3 2348.58 2272.73 23.85 o 1 6 3 873.05 871.62 15.37 o 2 6 3 34.10 33.47 3.28 o 3 6 3 1569.36 1656.28 35.25 o 4 6 3 5893.69 5694.20 144.20 o 5 6 3 290.92 256.53 7.32 o 6 6 3 66.31 71.81 4.41 o 7 6 3 781.65 771.47 14.67 o 8 6 3 623.12 629.54 16.66 o 1 7 3 92.54 84.69 5.25 o 2 7 3 1117.12 1089.97 29.61 o 3 7 3 299.80 304.52 11.09 o 4 7 3 49.42 44.29 6.88 o 5 7 3 1000.30 892.19 18.10 o 6 7 3 213.24 173.61 9.57 o 7 7 3 11.10 -3.28 4.61 o 0 8 3 0.71 12.13 4.70 o 1 8 3 0.81 -2.74 2.74 o 2 8 3 5.50 0.92 5.23 o 3 8 3 22.05 17.31 5.97 o 4 8 3 22.82 15.30 5.47 o 5 8 3 0.86 -0.59 4.73 o 1 9 3 47.66 67.10 7.80 o 2 9 3 77.64 108.06 9.08 o 0 0 4 18309.88 19032.70 214.52 o 1 0 4 6060.24 6529.51 102.23 o 2 0 4 110.08 89.65 7.73 o 3 0 4 11148.41 10360.16 683.18 o 4 0 4 10319.83 10947.89 258.65 o 5 0 4 2404.67 2600.43 54.23 o 6 0 4 179.26 202.43 3.59 o 7 0 4 1067.59 1016.87 27.62 o 8 0 4 818.74 801.26 36.90 o 9 0 4 44.50 40.50 8.65 o 10 0 4 65.64 85.89 11.04 o 11 0 4 374.63 324.46 18.77 o 1 1 4 8060.03 8187.01 57.83 o 2 1 4 12807.91 12856.04 326.99 o 3 1 4 3032.04 3187.43 65.35 o 4 1 4 40.95 40.03 2.51 o 5 1 4 361.84 412.05 8.52 o 6 1 4 3462.15 3629.95 53.40 o 7 1 4 370.28 372.21 7.36 o 8 1 4 110.96 108.06 3.68 o 9 1 4 748.65 671.92 18.30 o 10 1 4 324.01 313.39 5.59 o 11 1 4 2.34 2.16 2.85 o 0 2 4 6468.64 6596.71 89.19 o 1 2 4 3.03 7.17 0.82 o 2 2 4 11.39 14.94 1.00 o 3 2 4 4021.42 3888.24 44.38 o 4 2 4 2718.27 2811.96 51.31 o 5 2 4 1827.89 1791.86 20.52 o 6 2 4 18.79 18.06 1.09 o 7 2 4 222.36 280.67 2.99 o 8 2 4 805.77 787.43 8.97 o 9 2 4 224.09 225.20 5.24 o 10 2 4 2.53 3.03 2.47 o 11 2 4 188.10 203.48 9.61 o 1 3 4 9.64 2.94 1.24 o 2 3 4 0.09 2.09 1.27 o 3 3 4 2582.74 2611.06 30.70 o 4 3 4 1.75 0.91 1.03 o 5 3 4 1947.09 1716.17 107.37 o 6 3 4 10.53 12.29 1.44 o 7 3 4 236.64 262.82 4.62 o 8 3 4 7.40 10.66 2.07 o 9 3 4 7.66 25.94 2.33 o 10 3 4 69.55 72.57 4.19 o 0 4 4 1675.57 1927.24 17.70 o 1 4 4 278.02 246.45 6.23 o 2 4 4 3.48 -0.33 2.81 o 3 4 4 137.14 148.52 3.92 o 4 4 4 1828.95 1889.71 20.73 o 5 4 4 61.71 56.72 3.33 o 6 4 4 13.64 13.77 2.62 o 7 4 4 8.81 14.35 3.41 o 8 4 4 143.36 126.21 4.09 o 9 4 4 2.37 11.89 2.56 o 10 4 4 17.24 20.04 2.92 o 1 5 4 233.26 250.80 5.81 o 2 5 4 1888.55 1964.24 27.73 o 3 5 4 598.18 587.03 9.28 o 4 5 4 0.20 0.96 1.82 o 5 5 4 243.33 258.32 8.01 o 6 5 4 1035.54 1040.56 26.29 o 7 5 4 79.32 87.92 5.06 o 8 5 4 2.24 2.25 2.83 o 9 5 4 45.40 47.64 3.67 o 0 6 4 320.33 337.95 10.65 o 1 6 4 69.68 99.25 4.84 o 2 6 4 0.22 -2.20 2.20 o 3 6 4 465.15 492.31 13.71 o 4 6 4 245.57 323.01 11.60 o 5 6 4 104.40 110.03 5.64 o 6 6 4 5.39 10.57 2.89 o 7 6 4 24.51 53.51 4.40 o 8 6 4 40.96 49.83 5.36 o 1 7 4 0.53 -2.57 2.57 o 2 7 4 0.59 9.67 4.27 o 3 7 4 2.79 -1.75 4.08 o 4 7 4 5.13 6.37 5.35 o 5 7 4 47.53 48.91 6.51 o 6 7 4 24.12 19.35 7.62 o 7 7 4 24.10 20.83 8.25 o 0 8 4 9.57 9.67 4.87 o 1 8 4 49.13 60.71 4.82 o 2 8 4 1.28 -2.51 4.14 o 3 8 4 567.14 597.42 15.89 o 4 8 4 16.38 14.23 5.37 o 5 8 4 284.31 230.53 11.22 o 1 9 4 318.59 334.05 18.15 o 2 9 4 111.73 139.84 9.73 o 1 1 5 3945.38 3965.78 25.06 o 2 1 5 103.14 199.45 1.64 o 3 1 5 5395.47 5542.52 44.14 o 4 1 5 285.31 282.93 3.32 o 5 1 5 5517.89 5992.71 69.93 o 6 1 5 95.32 121.60 2.46 o 7 1 5 933.80 1004.61 19.93 o 8 1 5 8.55 6.52 1.39 o 9 1 5 4.79 10.16 3.48 o 10 1 5 11.58 17.01 3.17 o 11 1 5 65.40 77.01 5.15 o 0 2 5 2029.41 1749.47 36.12 o 1 2 5 4405.48 4491.51 50.74 o 2 2 5 619.43 646.80 6.63 o 3 2 5 9425.65 9728.88 94.08 o 4 2 5 1251.07 1278.57 17.39 o 5 2 5 3627.60 3899.70 47.19 o 6 2 5 68.65 69.99 1.77 o 7 2 5 918.85 955.29 11.63 o 8 2 5 88.64 70.06 3.71 o 9 2 5 113.80 122.80 4.67 o 10 2 5 0.03 -1.84 2.37 o 11 2 5 43.43 60.38 4.00 o 1 3 5 1065.74 1070.82 13.33 o 2 3 5 14.11 25.59 1.53 o 3 3 5 3777.47 3853.66 48.94 o 4 3 5 106.13 125.83 2.43 o 5 3 5 1695.24 1682.43 22.88 o 6 3 5 464.01 510.67 7.77 o 7 3 5 17.65 20.60 2.23 o 8 3 5 360.94 377.75 5.50 o 9 3 5 123.96 121.91 3.91 o 10 3 5 50.89 42.81 3.94 o 0 4 5 1585.36 1402.62 56.71 o 1 4 5 523.08 511.73 6.16 o 2 4 5 0.01 -1.20 1.55 o 3 4 5 475.23 462.19 8.28 o 4 4 5 1953.56 1736.86 22.74 o 5 4 5 76.43 76.49 3.67 o 6 4 5 314.17 309.68 6.34 o 7 4 5 241.73 221.53 6.34 o 8 4 5 484.50 568.82 9.94 o 9 4 5 3.81 4.45 2.37 o 10 4 5 32.23 33.36 3.29 o 1 5 5 258.36 238.78 5.68 o 2 5 5 4136.11 3993.32 67.90 o 3 5 5 82.43 78.74 4.11 o 4 5 5 315.55 300.57 10.30 o 5 5 5 314.70 318.96 10.08 o 6 5 5 2195.33 2040.07 62.74 o 7 5 5 43.66 48.47 4.57 o 8 5 5 6.93 15.95 3.89 o 9 5 5 61.45 65.76 4.43 o 0 6 5 2678.68 2468.85 35.84 o 1 6 5 91.41 91.49 4.72 o 2 6 5 8.76 9.51 2.71 o 3 6 5 32.35 29.65 3.50 o 4 6 5 2696.19 2477.82 33.96 o 5 6 5 19.18 27.38 5.15 o 6 6 5 33.95 37.12 5.51 o 7 6 5 146.46 161.26 8.06 o 8 6 5 541.02 565.53 12.06 o 1 7 5 0.00 -2.59 2.59 o 2 7 5 1168.36 1163.36 22.04 o 3 7 5 11.02 5.08 4.36 o 4 7 5 55.19 65.87 6.63 o 5 7 5 15.26 17.62 5.33 o 6 7 5 151.59 120.88 8.69 o 7 7 5 10.24 1.65 4.95 o 0 8 5 107.77 48.41 6.43 o 1 8 5 32.41 31.14 4.09 o 2 8 5 73.54 70.07 7.15 o 3 8 5 74.78 90.47 8.04 o 4 8 5 126.21 151.71 9.56 o 5 8 5 79.16 84.49 8.04 o 1 9 5 13.65 18.49 15.98 o 2 9 5 14.96 5.80 5.26 o 0 0 6 42.85 84.93 3.87 o 1 0 6 13597.31 13395.98 157.78 o 2 0 6 541.84 527.16 6.35 o 3 0 6 12934.56 13418.85 397.94 o 4 0 6 1335.87 1064.81 154.28 o 5 0 6 2144.54 2345.03 40.15 o 6 0 6 11.86 14.38 1.47 o 7 0 6 6786.46 6867.86 206.60 o 8 0 6 107.36 112.84 3.88 o 9 0 6 15.79 16.29 2.27 o 10 0 6 2.00 -0.74 2.41 o 11 0 6 680.77 694.53 25.82 o 1 1 6 16576.75 16733.34 118.38 o 2 1 6 3032.33 3078.05 20.69 o 3 1 6 2339.24 2249.84 38.16 o 4 1 6 260.79 262.68 17.70 o 5 1 6 6110.86 6175.29 58.45 o 6 1 6 282.07 256.37 10.45 o 7 1 6 188.35 207.02 4.90 o 8 1 6 69.59 71.77 2.43 o 9 1 6 1239.02 1173.02 25.09 o 10 1 6 110.21 121.64 4.25 o 11 1 6 10.47 12.93 2.78 o 0 2 6 3014.05 3068.18 37.67 o 1 2 6 3569.34 3409.07 28.39 o 2 2 6 696.86 738.09 6.79 o 3 2 6 540.78 465.02 12.95 o 4 2 6 1869.16 2035.53 41.96 o 5 2 6 123.12 101.77 4.51 o 6 2 6 149.48 163.97 3.06 o 7 2 6 891.98 1017.16 12.18 o 8 2 6 172.50 150.96 3.27 o 9 2 6 17.48 19.67 2.09 o 10 2 6 14.37 10.72 2.83 o 11 2 6 147.26 148.98 5.25 o 1 3 6 1323.51 1499.58 15.45 o 2 3 6 174.21 241.04 3.35 o 3 3 6 323.08 307.02 4.50 o 4 3 6 58.68 52.42 1.88 o 5 3 6 40.25 30.62 2.59 o 6 3 6 7.25 16.35 1.74 o 7 3 6 3.42 8.41 1.93 o 8 3 6 113.11 99.55 3.33 o 9 3 6 1.02 -1.18 1.96 o 10 3 6 27.77 24.01 3.83 o 0 4 6 44.14 62.85 4.19 o 1 4 6 1136.93 1165.04 17.24 o 2 4 6 519.22 564.79 8.14 o 3 4 6 8.23 6.70 1.50 o 4 4 6 1794.24 1723.07 26.62 o 5 4 6 66.54 73.70 3.65 o 6 4 6 298.83 287.26 5.95 o 7 4 6 306.36 293.64 6.63 o 8 4 6 5.60 14.22 2.69 o 9 4 6 68.91 77.18 3.96 o 10 4 6 3.35 2.58 2.38 o 1 5 6 396.16 366.97 13.14 o 2 5 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154.63 150.93 4.05 o 4 1 21 34.59 43.02 3.88 o 5 1 21 6.69 22.98 3.45 o 6 1 21 127.36 113.53 5.30 o 7 1 21 22.31 18.83 3.38 o 8 1 21 0.90 -0.13 2.82 o 0 2 21 114.13 98.19 5.12 o 1 2 21 25.98 27.74 2.45 o 2 2 21 491.03 481.51 6.73 o 3 2 21 139.77 149.86 4.10 o 4 2 21 1033.70 920.72 23.92 o 5 2 21 31.67 33.44 3.79 o 6 2 21 52.03 63.38 4.57 o 7 2 21 0.82 2.30 3.06 o 1 3 21 1.44 0.38 2.00 o 2 3 21 163.26 151.85 4.26 o 3 3 21 218.67 212.84 5.56 o 4 3 21 20.21 9.60 3.22 o 5 3 21 53.54 58.23 4.53 o 6 3 21 138.77 135.79 6.00 o 7 3 21 14.06 15.64 3.62 o 0 4 21 67.32 93.67 5.40 o 1 4 21 23.45 8.91 2.26 o 2 4 21 2.19 -1.93 1.93 o 3 4 21 7.89 10.68 2.80 o 4 4 21 632.83 633.25 17.09 o 5 4 21 14.50 12.10 3.63 o 6 4 21 39.12 43.10 4.56 o 1 5 21 132.94 149.83 4.64 o 2 5 21 763.46 806.50 11.35 o 3 5 21 55.56 67.69 4.23 o 4 5 21 11.61 10.91 3.65 o 5 5 21 1.08 2.37 3.33 o 0 6 21 1635.26 1662.61 38.51 o 1 6 21 167.17 180.26 6.11 o 2 6 21 72.53 73.72 4.67 o 3 6 21 9.16 11.71 3.84 o 0 0 22 1171.33 1051.03 32.37 o 1 0 22 19.44 30.36 3.33 o 2 0 22 35.70 34.47 3.60 o 3 0 22 110.37 92.79 4.98 o 4 0 22 710.86 663.46 21.62 o 5 0 22 12.58 9.78 4.35 o 6 0 22 71.99 85.56 9.78 o 7 0 22 0.00 -2.34 5.01 o 1 1 22 24.10 31.04 2.44 o 2 1 22 3.66 6.75 2.00 o 3 1 22 186.38 173.37 4.33 o 4 1 22 0.40 -0.26 2.62 o 5 1 22 43.88 46.30 4.15 o 6 1 22 42.29 57.72 4.42 o 7 1 22 71.53 73.38 4.94 o 0 2 22 43.11 60.27 4.30 o 1 2 22 735.78 730.16 8.34 o 2 2 22 68.13 73.86 3.30 o 3 2 22 214.69 222.34 5.31 o 4 2 22 0.01 3.06 2.78 o 5 2 22 167.70 150.64 5.98 o 6 2 22 31.74 23.00 3.68 o 7 2 22 272.38 292.60 7.96 o 1 3 22 565.30 541.87 7.28 o 2 3 22 0.43 -0.65 1.92 o 3 3 22 184.12 175.83 5.32 o 4 3 22 7.86 5.29 3.15 o 5 3 22 293.93 321.62 8.24 o 6 3 22 0.52 -0.64 3.05 o 0 4 22 31.76 25.61 3.84 o 1 4 22 0.20 -1.90 1.90 o 2 4 22 24.75 16.73 2.76 o 3 4 22 219.57 256.36 7.17 o 4 4 22 57.31 65.34 4.98 o 5 4 22 85.29 92.44 5.65 o 6 4 22 110.81 120.75 6.17 o 1 5 22 11.42 13.04 2.66 o 2 5 22 36.14 44.70 3.91 o 3 5 22 12.35 13.98 3.49 o 4 5 22 2.47 0.75 3.36 o 0 6 22 249.69 271.71 9.77 o 1 6 22 14.37 22.38 3.75 o 2 6 22 17.93 12.71 3.40 o 1 1 23 405.47 428.76 6.20 o 2 1 23 235.46 218.77 4.77 o 3 1 23 240.74 263.13 5.93 o 4 1 23 9.97 14.34 3.35 o 5 1 23 98.04 87.07 5.12 o 6 1 23 0.08 -2.69 2.69 o 7 1 23 3.14 -1.97 2.90 o 0 2 23 265.07 263.25 8.85 o 1 2 23 921.53 917.34 14.38 o 2 2 23 18.74 25.02 2.54 o 3 2 23 229.83 256.95 6.83 o 4 2 23 58.12 53.63 4.45 o 5 2 23 50.95 51.90 4.54 o 6 2 23 0.56 3.39 3.09 o 1 3 23 104.86 110.33 3.86 o 2 3 23 239.56 202.43 4.80 o 3 3 23 89.80 88.51 4.37 o 4 3 23 50.94 50.30 4.54 o 5 3 23 177.69 175.00 6.79 o 6 3 23 53.65 47.22 6.60 o 0 4 23 605.34 574.33 10.85 o 1 4 23 11.73 20.98 2.71 o 2 4 23 18.64 23.73 3.32 o 3 4 23 23.22 33.43 3.85 o 4 4 23 275.35 253.93 12.17 o 5 4 23 17.64 11.11 3.69 o 1 5 23 343.69 371.02 7.23 o 2 5 23 862.07 892.16 12.15 o 3 5 23 72.35 79.38 5.71 o 4 5 23 9.64 12.76 3.94 o 0 0 24 1.89 10.89 4.21 o 1 0 24 1108.00 1143.07 21.38 o 2 0 24 31.76 36.82 3.82 o 3 0 24 628.80 590.66 20.19 o 4 0 24 38.63 36.04 5.68 o 5 0 24 33.76 41.23 11.77 o 6 0 24 90.36 110.83 11.60 o 1 1 24 439.83 498.59 6.78 o 2 1 24 25.32 32.75 2.64 o 3 1 24 745.67 722.37 17.06 o 4 1 24 5.96 4.10 3.03 o 5 1 24 647.05 591.71 15.35 o 6 1 24 17.17 24.25 3.84 o 0 2 24 22.23 56.88 4.35 o 1 2 24 368.40 333.63 5.80 o 2 2 24 113.96 108.91 3.89 o 3 2 24 387.72 414.30 9.83 o 4 2 24 151.18 143.63 6.91 o 5 2 24 102.27 98.29 5.63 o 6 2 24 11.96 11.24 3.79 o 1 3 24 76.58 72.48 3.55 o 2 3 24 216.66 238.98 5.69 o 3 3 24 5.34 0.88 2.83 o 4 3 24 0.02 -2.81 2.81 o 5 3 24 96.91 127.53 6.23 o 0 4 24 861.28 871.23 15.39 o 1 4 24 92.10 85.02 3.91 o 2 4 24 2.88 -2.52 2.52 o 3 4 24 0.42 2.15 3.25 o 4 4 24 10.97 17.29 3.82 o 1 5 24 0.04 3.01 2.87 o 2 5 24 90.42 113.55 5.34 o 3 5 24 91.84 93.85 6.09 o 1 1 25 15.46 21.42 2.44 o 2 1 25 651.16 687.44 8.06 o 3 1 25 47.88 58.76 4.19 o 4 1 25 63.70 61.73 4.89 o 5 1 25 19.19 12.53 3.52 o 6 1 25 118.31 113.33 5.94 o 0 2 25 1709.61 1717.20 36.78 o 1 2 25 61.17 77.97 3.61 o 2 2 25 0.39 -2.03 2.06 o 3 2 25 81.72 68.99 4.52 o 4 2 25 326.33 305.67 12.25 o 5 2 25 1.24 -0.57 3.11 o 1 3 25 101.00 111.56 4.18 o 2 3 25 720.17 670.58 10.45 o 3 3 25 308.31 264.54 10.49 o 4 3 25 56.24 43.62 4.61 o 5 3 25 371.33 382.25 11.43 o 0 4 25 172.20 149.12 6.86 o 1 4 25 203.13 212.40 5.42 o 2 4 25 4.45 1.73 2.80 o 3 4 25 604.59 632.06 12.01 o 1 5 25 444.28 463.50 8.93 o 0 0 26 2690.00 2737.70 112.40 o 1 0 26 55.78 51.31 4.56 o 2 0 26 24.71 3.94 3.40 o 3 0 26 27.74 26.57 5.68 o 4 0 26 1780.15 1738.84 56.09 o 5 0 26 34.94 26.37 5.82 o 1 1 26 8.21 12.74 2.49 o 2 1 26 1782.00 1812.84 21.88 o 3 1 26 2.80 -2.86 2.92 o 4 1 26 126.20 108.87 6.00 o 5 1 26 0.62 -0.33 3.08 o 0 2 26 322.36 360.35 9.01 o 1 2 26 5.17 1.98 2.18 o 2 2 26 2.88 -2.62 2.62 o 3 2 26 13.14 12.14 3.57 o 4 2 26 189.38 194.09 9.11 o 5 2 26 13.71 14.50 3.84 o 1 3 26 5.09 5.10 2.33 o 2 3 26 7.96 10.92 2.94 o 3 3 26 26.21 23.86 4.12 o 4 3 26 8.12 -2.56 3.21 o 0 4 26 106.58 120.68 6.57 o 1 4 26 7.44 2.66 2.75 o 2 4 26 1.28 -2.09 2.78 o 1 1 27 18.20 19.45 2.66 o 2 1 27 225.55 230.21 5.87 o 3 1 27 45.35 49.17 4.72 o 4 1 27 3.07 1.78 3.21 o 0 2 27 377.00 359.83 11.71 o 1 2 27 164.55 173.38 4.94 o 2 2 27 23.27 9.06 2.93 o 3 2 27 116.42 100.13 5.98 o 4 2 27 468.33 485.07 12.79 o 1 3 27 88.78 100.62 4.62 o 2 3 27 316.16 340.06 8.25 o 3 3 27 131.01 137.91 6.85 o 0 4 27 34.80 66.22 5.60 o 0 0 28 28.76 29.17 5.87 o 1 0 28 341.86 358.82 9.27 o 2 0 28 50.62 32.11 5.24 o 3 0 28 485.79 446.49 14.67 o 4 0 28 11.88 18.97 5.87 o 1 1 28 147.20 150.00 4.87 o 2 1 28 0.57 8.43 3.28 o 3 1 28 170.23 173.26 7.26 o 0 2 28 93.83 107.34 6.26 o 1 2 28 15.67 11.07 2.66 o 2 2 28 1.84 -2.99 2.99 o 3 2 28 5.98 5.77 3.82 o 1 3 28 93.45 97.82 4.79 o 1 1 29 126.82 119.27 4.72 o 2 1 29 109.52 118.35 6.68 o 0 2 29 249.47 199.73 8.35 o 1 2 29 16.44 11.86 3.09 o