#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/75/2017586.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017586_Fobs loop_ _publ_author_name 'Acosta, Lina M.' 'Palma, Alirio' 'Bahsas, Ali' 'Cobo, Justo' 'Glidewell, Christopher' _publ_section_title ; Hydrogen-bonded dimers, chains and rings in six differently substituted 2-vinyltetrahydro-1,4-epoxy-1-benzazepines ; _journal_coeditor_code SK3373 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o209 _journal_page_last o214 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.587 _cell_angle_gamma 90.000 _cell_length_a 11.0631 _cell_length_b 5.7212 _cell_length_c 21.2028 _exptl_crystal_F_000 560.00 _reflns_d_resolution_high 0.8394 _[local]_cod_data_source_file sk3373IIIsup4.hkl _[local]_cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' LIA4C12' _shelx_refln_list_code 4 _shelx_f_calc_maximum 163.92 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 87.05 59.25 4.40 o 4 0 0 3960.00 3492.30 89.58 o 6 0 0 2062.35 1900.68 56.38 o 8 0 0 2714.23 2733.40 96.40 o 10 0 0 1120.29 1084.29 52.23 o 12 0 0 163.35 179.30 24.17 o 1 1 0 4001.16 4584.80 101.00 o 2 1 0 1172.78 1237.41 23.95 o 3 1 0 1570.36 1694.38 34.67 o 4 1 0 3.34 -4.88 4.88 o 5 1 0 1008.98 1090.62 26.39 o 6 1 0 295.45 296.15 9.86 o 7 1 0 1151.94 1071.87 30.78 o 8 1 0 9.02 5.92 9.56 o 9 1 0 70.00 100.56 16.54 o 10 1 0 68.65 66.46 14.25 o 11 1 0 170.52 170.26 17.75 o 12 1 0 9.33 -15.82 15.82 o 0 2 0 5873.21 6957.82 226.75 o 1 2 0 0.31 2.07 3.52 o 2 2 0 1218.66 1388.12 29.36 o 3 2 0 2.69 -1.25 4.19 o 4 2 0 1041.50 1065.79 23.78 o 5 2 0 264.40 231.03 8.61 o 6 2 0 443.90 412.49 16.58 o 7 2 0 48.80 67.90 11.22 o 8 2 0 1506.60 1508.71 50.77 o 9 2 0 9.08 5.87 13.09 o 10 2 0 9.12 -11.02 18.80 o 11 2 0 138.08 172.34 25.13 o 12 2 0 381.48 340.39 24.58 o 1 3 0 2692.11 3094.93 84.48 o 2 3 0 153.54 150.40 5.85 o 3 3 0 2094.05 2077.24 44.16 o 4 3 0 262.48 292.59 10.18 o 5 3 0 453.60 447.76 16.15 o 6 3 0 2028.76 2099.69 66.30 o 7 3 0 1715.57 1821.17 59.21 o 8 3 0 11.63 -3.68 14.06 o 9 3 0 202.38 231.93 18.76 o 10 3 0 27.73 31.84 15.82 o 11 3 0 352.99 396.79 23.73 o 0 4 0 1071.34 1337.00 52.49 o 1 4 0 474.59 488.64 18.08 o 2 4 0 36.23 36.38 11.82 o 3 4 0 412.09 411.38 13.41 o 4 4 0 85.70 87.51 7.83 o 5 4 0 50.08 25.16 9.57 o 6 4 0 52.89 43.65 11.86 o 7 4 0 1220.36 1168.65 48.33 o 8 4 0 110.62 163.74 18.24 o 9 4 0 14.18 58.71 16.53 o 10 4 0 81.02 105.66 19.49 o 1 5 0 887.34 876.80 31.54 o 2 5 0 11.91 7.81 8.84 o 3 5 0 27.45 44.05 11.18 o 4 5 0 0.45 5.40 10.99 o 5 5 0 137.21 109.39 12.78 o 6 5 0 69.71 67.92 16.35 o 7 5 0 59.57 74.50 18.64 o 8 5 0 2.79 40.20 18.15 o 0 6 0 9.53 14.04 19.23 o 1 6 0 56.16 77.17 13.17 o 2 6 0 17.02 22.75 12.08 o 3 6 0 11.36 5.80 12.01 o 4 6 0 46.91 77.67 28.31 o 5 6 0 4.74 21.92 16.20 o 6 6 0 47.85 60.34 20.18 o -11 0 1 0.95 4.63 19.60 o -9 0 1 779.94 780.85 39.91 o -7 0 1 737.72 916.56 42.67 o -5 0 1 439.84 420.95 17.86 o -3 0 1 409.36 364.97 15.13 o 3 0 1 279.68 246.06 14.09 o 5 0 1 0.18 10.71 5.60 o 7 0 1 1294.47 1165.28 56.45 o 9 0 1 1087.30 1114.20 59.54 o 11 0 1 0.02 -15.69 21.41 o -12 1 1 126.58 161.43 22.72 o -11 1 1 315.27 330.42 19.61 o -10 1 1 25.99 24.22 14.38 o -9 1 1 8.87 36.90 9.38 o -8 1 1 986.96 986.81 51.81 o -7 1 1 642.92 661.67 24.11 o -6 1 1 214.26 185.20 8.06 o -5 1 1 4.31 5.98 5.04 o -4 1 1 0.89 -4.63 4.63 o -3 1 1 5895.80 6387.95 131.65 o -2 1 1 64.17 60.96 3.86 o -1 1 1 12.56 19.58 2.18 o 0 1 1 9143.55 9401.04 213.16 o 1 1 1 592.40 690.29 15.36 o 2 1 1 35.69 37.77 4.32 o 3 1 1 392.61 467.99 11.17 o 4 1 1 204.91 222.32 7.06 o 5 1 1 3937.05 3921.53 75.08 o 6 1 1 10.75 3.69 5.02 o 7 1 1 82.82 77.69 8.47 o 8 1 1 2.52 22.39 11.30 o 9 1 1 175.18 178.29 15.20 o 10 1 1 9.93 -1.90 13.49 o 11 1 1 1.88 18.14 14.50 o 12 1 1 108.05 118.28 20.89 o -12 2 1 151.80 157.28 22.06 o -11 2 1 25.42 44.32 18.47 o -10 2 1 0.83 5.28 14.02 o -9 2 1 86.08 102.25 16.98 o -8 2 1 6.36 27.74 13.73 o -7 2 1 54.93 55.19 9.49 o -6 2 1 167.22 166.93 9.76 o -5 2 1 67.53 67.83 5.76 o -4 2 1 234.62 243.31 9.00 o -3 2 1 1180.91 1347.97 30.21 o -2 2 1 548.08 518.47 12.05 o -1 2 1 23.40 30.01 3.53 o 0 2 1 1185.79 1292.45 32.51 o 1 2 1 1.72 0.63 4.16 o 2 2 1 527.72 512.98 12.07 o 3 2 1 37.92 28.93 3.64 o 4 2 1 0.43 2.89 4.16 o 5 2 1 3.07 -3.05 4.92 o 6 2 1 1138.81 1021.87 39.61 o 7 2 1 2.13 -0.20 7.75 o 8 2 1 438.05 444.97 21.24 o 9 2 1 138.44 130.04 14.98 o 10 2 1 82.25 65.65 23.61 o 11 2 1 13.61 15.28 17.00 o 12 2 1 96.06 136.16 22.40 o -11 3 1 5.59 10.85 17.96 o -10 3 1 105.93 145.93 17.26 o -9 3 1 27.37 18.74 14.74 o -8 3 1 522.98 557.92 24.55 o -7 3 1 1290.61 1325.36 44.67 o -6 3 1 36.84 90.34 13.98 o -5 3 1 243.12 275.23 11.53 o -4 3 1 91.09 110.70 6.49 o -3 3 1 741.66 778.72 18.56 o -2 3 1 357.26 379.14 10.87 o -1 3 1 171.13 213.89 9.99 o 0 3 1 3530.40 4119.07 96.21 o 1 3 1 42.10 38.50 6.44 o 2 3 1 1017.68 1091.20 23.94 o 3 3 1 25.06 25.84 6.16 o 4 3 1 406.06 411.69 12.58 o 5 3 1 16.72 5.56 9.17 o 6 3 1 32.49 49.38 8.83 o 7 3 1 36.42 27.94 12.89 o 8 3 1 20.30 18.81 12.55 o 9 3 1 87.86 104.44 30.16 o 10 3 1 0.94 3.93 14.11 o 11 3 1 90.69 73.66 17.42 o -10 4 1 68.85 52.01 23.75 o -9 4 1 135.15 132.42 20.72 o -8 4 1 257.68 329.63 21.98 o -7 4 1 3.07 15.56 13.69 o -6 4 1 1554.09 1637.37 57.54 o -5 4 1 153.60 162.39 11.16 o -4 4 1 55.35 69.67 7.63 o -3 4 1 2.33 3.79 6.42 o -2 4 1 287.52 310.23 15.76 o -1 4 1 304.05 350.50 14.54 o 0 4 1 458.52 486.36 17.27 o 1 4 1 97.85 102.40 9.11 o 2 4 1 72.85 88.26 9.91 o 3 4 1 4.34 7.85 6.56 o 4 4 1 443.22 442.00 16.78 o 5 4 1 609.31 563.59 18.27 o 6 4 1 0.27 -5.98 7.74 o 7 4 1 28.35 43.20 14.02 o 8 4 1 587.04 634.94 36.95 o 9 4 1 160.19 168.47 19.17 o 10 4 1 13.82 28.91 18.05 o -8 5 1 11.50 28.49 15.70 o -7 5 1 64.15 62.96 16.33 o -6 5 1 7.00 11.09 12.65 o -5 5 1 53.92 96.21 15.93 o -4 5 1 218.61 192.12 15.62 o -3 5 1 309.52 277.69 17.56 o -2 5 1 111.53 113.75 11.74 o -1 5 1 2.14 16.20 9.51 o 0 5 1 145.92 140.60 11.00 o 1 5 1 158.16 144.71 11.36 o 2 5 1 213.79 223.97 13.95 o 3 5 1 3.57 16.44 10.12 o 4 5 1 202.41 190.45 15.48 o 5 5 1 273.39 283.03 19.89 o 6 5 1 34.65 63.56 14.26 o 7 5 1 12.57 20.74 16.45 o 8 5 1 24.12 3.36 15.79 o -6 6 1 146.51 102.55 45.81 o -5 6 1 0.14 8.52 15.41 o -4 6 1 3.66 0.53 18.33 o -3 6 1 0.21 4.92 19.92 o -2 6 1 10.78 0.46 17.24 o -1 6 1 204.59 196.51 15.67 o 0 6 1 76.29 68.27 15.51 o 1 6 1 125.66 111.91 13.64 o 2 6 1 34.37 24.30 13.86 o 3 6 1 93.18 75.86 14.71 o 4 6 1 56.82 44.51 15.89 o 5 6 1 0.11 1.45 18.29 o -12 0 2 88.13 99.00 38.02 o -10 0 2 553.18 543.24 32.82 o -8 0 2 111.32 146.29 13.13 o -6 0 2 2072.74 1998.44 59.04 o -4 0 2 4319.20 4164.19 127.70 o -2 0 2 796.38 869.76 32.21 o 2 0 2 26868.83 23211.77 823.03 o 4 0 2 341.02 358.83 12.36 o 6 0 2 2357.46 2075.44 77.98 o 8 0 2 849.57 793.37 34.58 o 10 0 2 10.54 -15.77 17.68 o 12 0 2 22.20 67.76 25.16 o -12 1 2 12.19 22.13 16.06 o -11 1 2 5.26 18.20 15.51 o -10 1 2 34.47 36.14 13.24 o -9 1 2 531.47 497.27 25.79 o -8 1 2 101.07 114.45 10.19 o -7 1 2 21.44 33.47 10.73 o -6 1 2 0.01 3.30 4.84 o -5 1 2 780.95 806.62 20.22 o -4 1 2 593.07 642.71 15.22 o -3 1 2 9.40 26.07 6.20 o -2 1 2 220.59 291.80 7.84 o -1 1 2 955.90 1016.70 21.33 o 0 1 2 6342.06 7019.80 159.97 o 1 1 2 7898.68 8105.64 177.91 o 2 1 2 6331.05 6536.39 138.74 o 3 1 2 3826.20 3785.22 76.39 o 4 1 2 168.98 159.70 5.71 o 5 1 2 34.96 21.63 3.74 o 6 1 2 40.33 28.53 6.58 o 7 1 2 13.85 -6.05 6.51 o 8 1 2 0.01 -7.19 9.37 o 9 1 2 82.02 38.92 17.68 o 10 1 2 19.70 34.63 13.47 o 11 1 2 50.47 5.10 17.44 o 12 1 2 99.56 92.75 20.88 o -12 2 2 8.95 51.49 24.07 o -11 2 2 112.71 123.34 16.69 o -10 2 2 173.13 141.89 19.04 o -9 2 2 247.94 244.31 17.55 o -8 2 2 23.84 4.51 9.82 o -7 2 2 57.07 57.84 9.34 o -6 2 2 1975.91 1930.88 51.36 o -5 2 2 318.11 300.56 9.40 o -4 2 2 512.23 590.20 14.75 o -3 2 2 1519.83 1694.92 34.69 o -2 2 2 786.69 826.62 18.81 o -1 2 2 143.77 141.89 4.93 o 0 2 2 1.81 4.76 3.30 o 1 2 2 61.88 73.45 4.51 o 2 2 2 984.70 1021.19 23.06 o 3 2 2 1236.91 1408.98 30.26 o 4 2 2 193.45 200.74 7.41 o 5 2 2 40.21 52.33 6.52 o 6 2 2 4.56 6.93 8.06 o 7 2 2 5.12 10.09 10.02 o 8 2 2 335.53 319.59 21.51 o 9 2 2 128.92 119.49 14.71 o 10 2 2 245.14 253.69 20.22 o 11 2 2 13.28 35.66 17.27 o 12 2 2 12.43 6.30 19.79 o -11 3 2 76.36 107.36 18.85 o -10 3 2 22.80 21.08 15.77 o -9 3 2 359.80 377.40 22.53 o -8 3 2 458.41 464.55 24.81 o -7 3 2 973.18 1082.01 37.96 o -6 3 2 31.05 29.76 8.97 o -5 3 2 401.58 413.74 14.58 o -4 3 2 143.45 176.97 7.55 o -3 3 2 228.61 205.00 6.91 o -2 3 2 280.29 337.64 9.16 o -1 3 2 134.19 101.38 6.34 o 0 3 2 24.78 22.57 5.19 o 1 3 2 1624.15 1722.74 39.75 o 2 3 2 2.80 -0.14 3.29 o 3 3 2 1969.22 2255.35 50.85 o 4 3 2 278.11 277.40 14.18 o 5 3 2 320.73 323.71 14.21 o 6 3 2 12.35 2.13 8.89 o 7 3 2 45.93 67.35 12.12 o 8 3 2 585.50 614.83 26.50 o 9 3 2 758.72 787.72 31.81 o 10 3 2 23.03 10.01 15.31 o 11 3 2 106.41 114.74 19.83 o -10 4 2 1.10 28.09 19.20 o -9 4 2 18.32 46.80 16.11 o -8 4 2 18.39 21.58 16.59 o -7 4 2 474.04 437.02 21.54 o -6 4 2 76.52 107.50 15.66 o -5 4 2 825.14 815.36 26.72 o -4 4 2 600.02 597.95 18.75 o -3 4 2 158.82 132.94 9.04 o -2 4 2 84.15 85.38 11.10 o -1 4 2 94.36 101.77 9.38 o 0 4 2 0.12 4.80 7.24 o 1 4 2 520.03 550.47 21.18 o 2 4 2 7.89 12.99 9.36 o 3 4 2 141.17 140.06 7.93 o 4 4 2 17.61 20.73 9.58 o 5 4 2 23.37 34.18 7.81 o 6 4 2 204.33 235.17 15.88 o 7 4 2 5.16 26.86 13.90 o 8 4 2 17.26 1.78 17.73 o 9 4 2 424.62 415.67 26.64 o 10 4 2 0.03 -4.25 21.19 o -8 5 2 18.92 37.02 15.68 o -7 5 2 2.99 35.39 13.64 o -6 5 2 14.72 42.19 32.46 o -5 5 2 4.99 -6.61 11.52 o -4 5 2 338.01 310.65 26.46 o -3 5 2 516.46 473.27 23.86 o -2 5 2 2.62 6.86 9.42 o -1 5 2 2.42 0.97 8.71 o 0 5 2 13.49 20.38 8.65 o 1 5 2 67.92 90.53 15.76 o 2 5 2 29.47 39.97 11.00 o 3 5 2 17.70 19.04 12.31 o 4 5 2 20.01 21.66 11.97 o 5 5 2 311.46 314.91 19.13 o 6 5 2 4.37 11.56 17.63 o 7 5 2 109.02 82.22 15.30 o 8 5 2 30.60 36.79 16.20 o -6 6 2 296.32 324.39 30.15 o -5 6 2 16.61 37.70 19.78 o -4 6 2 1.30 4.28 13.87 o -3 6 2 2.32 -4.16 12.73 o -2 6 2 10.39 18.03 11.49 o -1 6 2 148.39 152.49 16.53 o 0 6 2 195.04 199.01 16.83 o 1 6 2 62.61 26.75 13.36 o 2 6 2 270.81 281.34 18.19 o 3 6 2 15.23 20.89 14.16 o 4 6 2 2.11 27.01 16.45 o 5 6 2 0.09 -13.92 16.21 o -13 0 3 37.28 105.65 33.85 o -11 0 3 538.82 665.05 45.19 o -9 0 3 44.17 97.84 25.70 o -7 0 3 9.40 5.60 8.94 o -5 0 3 1913.83 2057.13 84.96 o -3 0 3 28.05 66.83 16.55 o -1 0 3 2060.91 1748.40 82.11 o 1 0 3 9588.19 9119.44 336.43 o 3 0 3 4496.96 4408.58 141.46 o 5 0 3 1147.16 1164.25 38.10 o 7 0 3 262.62 244.78 28.46 o 9 0 3 729.50 704.68 37.27 o 11 0 3 35.49 10.40 19.15 o -12 1 3 31.36 66.77 18.66 o -11 1 3 94.97 116.00 20.52 o -10 1 3 94.97 75.29 14.37 o -9 1 3 2359.93 2371.44 83.45 o -8 1 3 165.13 114.45 13.01 o -7 1 3 6.39 19.52 11.20 o -6 1 3 214.95 178.99 8.09 o -5 1 3 5436.17 5723.09 117.36 o -4 1 3 1.60 -4.41 5.02 o -3 1 3 3614.09 3548.64 76.51 o -2 1 3 8337.74 8444.44 175.86 o -1 1 3 6595.81 6859.88 152.58 o 0 1 3 556.01 580.10 13.13 o 1 1 3 13797.37 13188.25 291.38 o 2 1 3 3267.83 3280.29 70.65 o 3 1 3 7866.10 8215.31 175.76 o 4 1 3 347.66 416.95 11.42 o 5 1 3 1124.59 1015.58 23.88 o 6 1 3 346.80 327.01 12.46 o 7 1 3 1859.82 1780.09 44.08 o 8 1 3 219.29 234.55 12.74 o 9 1 3 1206.92 1121.74 37.61 o 10 1 3 91.35 90.99 14.10 o 11 1 3 376.06 411.72 25.64 o 12 1 3 0.11 32.56 17.41 o -12 2 3 193.71 220.20 21.12 o -11 2 3 16.84 -11.55 18.93 o -10 2 3 327.22 336.95 20.46 o -9 2 3 33.03 53.07 14.47 o -8 2 3 27.37 23.62 10.56 o -7 2 3 135.66 152.17 10.79 o -6 2 3 794.86 856.09 25.25 o -5 2 3 111.11 174.24 7.04 o -4 2 3 352.77 408.48 10.44 o -3 2 3 668.54 748.49 16.95 o -2 2 3 4155.63 4586.61 91.66 o -1 2 3 2006.31 2294.67 49.33 o 0 2 3 2356.87 2598.53 57.85 o 1 2 3 238.63 264.59 7.63 o 2 2 3 6759.18 7274.54 150.27 o 3 2 3 117.70 114.54 5.40 o 4 2 3 454.87 404.59 11.46 o 5 2 3 145.57 137.23 8.73 o 6 2 3 491.91 482.57 18.01 o 7 2 3 199.85 207.14 14.02 o 8 2 3 3140.46 3144.78 107.05 o 9 2 3 182.01 203.38 17.61 o 10 2 3 239.55 241.47 19.84 o 11 2 3 8.17 26.28 16.95 o -11 3 3 468.81 521.82 26.77 o -10 3 3 1.00 8.81 15.22 o -9 3 3 10.55 13.91 14.44 o -8 3 3 269.21 265.51 19.13 o -7 3 3 8.38 40.56 13.09 o -6 3 3 103.26 94.44 10.65 o -5 3 3 1882.18 2052.34 49.31 o -4 3 3 8.45 10.30 5.07 o -3 3 3 191.61 198.44 6.67 o -2 3 3 509.57 529.37 13.64 o -1 3 3 1844.97 2039.00 48.42 o 0 3 3 11.97 21.51 6.27 o 1 3 3 129.52 170.41 6.05 o 2 3 3 226.66 222.95 7.23 o 3 3 3 64.88 71.84 6.45 o 4 3 3 225.36 210.20 10.43 o 5 3 3 74.20 84.24 8.61 o 6 3 3 1239.47 1293.52 38.04 o 7 3 3 10.10 38.60 13.90 o 8 3 3 206.84 220.62 17.32 o 9 3 3 4.17 19.63 22.04 o 10 3 3 0.01 14.76 16.41 o 11 3 3 18.33 63.94 19.21 o -10 4 3 220.52 202.08 22.11 o -9 4 3 98.86 81.63 19.52 o -8 4 3 219.22 261.28 24.64 o -7 4 3 7.51 27.13 12.18 o -6 4 3 1130.75 1196.79 43.55 o -5 4 3 1029.15 969.02 29.13 o -4 4 3 1858.90 1807.47 46.14 o -3 4 3 383.94 352.16 12.33 o -2 4 3 605.15 565.55 23.37 o -1 4 3 0.21 13.99 7.85 o 0 4 3 919.80 946.02 28.72 o 1 4 3 571.41 639.35 25.69 o 2 4 3 2427.95 2347.59 64.05 o 3 4 3 191.82 184.28 8.33 o 4 4 3 40.83 40.53 6.67 o 5 4 3 11.61 43.58 10.64 o 6 4 3 849.83 841.80 33.39 o 7 4 3 117.58 152.95 18.85 o 8 4 3 94.11 102.69 16.60 o 9 4 3 28.98 41.90 17.85 o -8 5 3 3.79 8.50 17.19 o -7 5 3 20.29 54.29 14.11 o -6 5 3 24.89 16.82 17.43 o -5 5 3 121.74 129.41 17.11 o -4 5 3 600.82 586.71 30.82 o -3 5 3 4.73 27.33 17.05 o -2 5 3 2.06 23.56 9.43 o -1 5 3 285.73 290.70 15.30 o 0 5 3 68.74 85.08 10.97 o 1 5 3 3.32 4.19 8.36 o 2 5 3 65.25 95.13 14.67 o 3 5 3 161.18 193.03 15.90 o 4 5 3 176.18 188.50 15.16 o 5 5 3 21.32 36.06 13.08 o 6 5 3 0.47 -14.53 14.53 o 7 5 3 48.07 48.84 15.58 o 8 5 3 131.59 144.77 22.34 o -6 6 3 259.26 262.70 28.51 o -5 6 3 159.72 174.24 32.09 o -4 6 3 227.49 279.58 29.61 o -3 6 3 110.49 118.50 20.71 o -2 6 3 42.07 58.63 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