#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:17:49 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180845 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/76/2017613.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017613_Fobs loop_ _publ_author_name 'Guzei, Ilia A.' 'Spencer, Lara C.' 'Ainooson, Michael K.' 'Darkwa, James' _publ_section_title ; Constructor graph description of the hydrogen-bonding supramolecular assembly in two ionic compounds: 2-(pyrazol-1-yl)ethylammonium chloride and diaquadichloridobis(2-hydroxyethylammonium)cobalt(II) dichloride ; _journal_coeditor_code KU3022 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m89 _journal_page_last m96 _journal_volume 66 _journal_year 2010 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.9634 _cell_length_b 9.3732 _cell_length_c 10.9416 _exptl_crystal_F_000 312.00 _reflns_d_resolution_high 0.7104 _cod_data_source_file ku3022Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' DARKWA106 IN P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 110.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1807.02 1987.49 60.00 o 4 0 0 4970.72 5234.71 69.84 o 6 0 0 1978.70 1981.51 71.85 o 8 0 0 74.95 60.49 3.89 o 1 1 0 407.67 493.04 5.26 o 2 1 0 5288.50 5304.53 47.97 o 3 1 0 329.46 363.86 3.63 o 4 1 0 242.66 243.16 2.48 o 5 1 0 0.21 -0.12 0.19 o 6 1 0 59.41 65.26 1.25 o 7 1 0 67.36 56.74 2.13 o 8 1 0 124.85 131.38 5.35 o 9 1 0 6.90 10.59 1.50 o 0 2 0 132.87 139.16 1.88 o 1 2 0 26.41 25.87 0.44 o 2 2 0 0.61 0.22 0.24 o 3 2 0 109.32 124.77 1.46 o 4 2 0 347.69 328.83 3.24 o 5 2 0 0.88 0.85 0.36 o 6 2 0 39.94 36.92 1.04 o 7 2 0 28.77 28.57 1.15 o 8 2 0 42.09 38.53 1.78 o 9 2 0 2.06 1.59 0.94 o 1 3 0 91.23 106.06 1.10 o 2 3 0 1834.74 1842.57 21.18 o 3 3 0 73.43 71.89 1.08 o 4 3 0 302.66 319.73 3.78 o 5 3 0 89.47 88.84 1.62 o 6 3 0 713.95 680.39 8.55 o 7 3 0 22.87 21.39 1.06 o 8 3 0 216.28 217.89 5.73 o 9 3 0 14.97 17.01 1.50 o 0 4 0 426.37 416.47 5.46 o 1 4 0 1593.69 1713.54 24.07 o 2 4 0 6.77 8.68 0.30 o 3 4 0 129.97 122.70 1.88 o 4 4 0 345.65 333.06 4.66 o 5 4 0 79.07 89.33 1.67 o 6 4 0 18.76 18.98 0.82 o 7 4 0 17.16 15.13 0.84 o 8 4 0 48.73 43.37 1.61 o 9 4 0 55.10 59.04 2.46 o 1 5 0 1235.41 1350.57 12.15 o 2 5 0 2321.50 2383.30 22.63 o 3 5 0 384.04 380.97 4.87 o 4 5 0 167.44 163.15 2.54 o 5 5 0 281.12 270.13 5.20 o 6 5 0 9.24 11.32 0.71 o 7 5 0 30.50 28.70 1.11 o 8 5 0 209.49 209.55 4.19 o 0 6 0 3452.74 3497.86 56.78 o 1 6 0 3.63 3.29 0.22 o 2 6 0 152.03 146.47 1.94 o 3 6 0 22.04 22.25 0.73 o 4 6 0 517.39 476.77 6.12 o 5 6 0 0.44 0.22 0.38 o 6 6 0 428.74 396.15 5.47 o 7 6 0 13.42 15.54 0.92 o 8 6 0 30.34 26.47 1.42 o 1 7 0 491.12 484.71 5.55 o 2 7 0 419.79 393.83 5.08 o 3 7 0 2.15 2.30 0.37 o 4 7 0 229.33 207.38 3.12 o 5 7 0 367.88 339.48 5.37 o 6 7 0 52.60 49.89 1.39 o 7 7 0 13.19 14.16 0.90 o 8 7 0 120.18 116.67 4.39 o 0 8 0 106.80 109.71 2.56 o 1 8 0 347.08 354.48 4.26 o 2 8 0 157.98 142.98 2.26 o 3 8 0 571.48 548.19 6.99 o 4 8 0 154.26 150.49 2.52 o 5 8 0 0.27 0.46 0.49 o 6 8 0 251.55 252.74 3.96 o 7 8 0 108.34 106.73 2.33 o 1 9 0 47.81 46.78 1.24 o 2 9 0 33.51 32.01 0.96 o 3 9 0 90.76 90.26 1.78 o 4 9 0 93.84 92.75 1.89 o 5 9 0 1.18 1.63 0.51 o 6 9 0 49.03 50.61 1.51 o 7 9 0 0.02 0.96 1.55 o 0 10 0 291.54 289.52 5.79 o 1 10 0 101.39 104.99 2.40 o 2 10 0 26.89 25.59 1.02 o 3 10 0 6.17 6.44 0.61 o 4 10 0 104.85 99.62 2.05 o 5 10 0 38.80 39.93 1.33 o 6 10 0 137.00 133.24 3.92 o 1 11 0 68.07 72.74 1.81 o 2 11 0 158.04 151.89 2.93 o 3 11 0 33.67 35.38 1.32 o 4 11 0 41.18 39.48 1.34 o 5 11 0 61.68 74.30 4.39 o 0 12 0 1.11 0.61 1.02 o 1 12 0 15.02 17.54 1.17 o 2 12 0 0.88 1.95 0.66 o 3 12 0 179.54 184.80 3.53 o 1 0 1 207.46 177.21 1.76 o 2 0 1 3356.04 3558.14 33.49 o 3 0 1 192.13 175.75 1.81 o 4 0 1 733.33 858.77 7.92 o 5 0 1 8.99 9.50 0.37 o 6 0 1 367.51 354.93 4.94 o 7 0 1 351.62 339.24 5.52 o 8 0 1 143.15 156.97 4.88 o 9 0 1 40.99 43.43 2.62 o -9 1 1 177.48 175.50 5.59 o -8 1 1 8.43 5.69 1.19 o -7 1 1 42.39 41.23 1.61 o -6 1 1 6.94 6.63 0.47 o -5 1 1 351.74 333.30 3.52 o -4 1 1 139.02 144.70 1.61 o -3 1 1 276.17 307.38 2.97 o -2 1 1 160.75 159.12 1.65 o -1 1 1 1426.05 1506.75 16.39 o 0 1 1 13.20 12.38 0.32 o 1 1 1 1488.14 1555.08 15.20 o 2 1 1 167.10 161.78 1.70 o 3 1 1 269.01 290.86 2.84 o 4 1 1 131.18 136.38 1.53 o 5 1 1 348.46 333.58 3.53 o 6 1 1 9.79 8.02 0.52 o 7 1 1 40.58 37.39 1.59 o 8 1 1 8.11 6.75 0.92 o 9 1 1 173.47 175.59 6.65 o -9 2 1 171.78 179.99 5.30 o -8 2 1 42.93 37.72 1.74 o -7 2 1 441.99 428.30 6.83 o -6 2 1 76.36 75.18 1.58 o -5 2 1 294.97 303.55 3.72 o -4 2 1 51.59 53.59 0.83 o -3 2 1 1643.97 1700.69 15.96 o -2 2 1 1583.36 1655.74 16.48 o -1 2 1 3898.98 4324.14 52.24 o 0 2 1 339.59 408.46 4.35 o 1 2 1 3839.15 4074.67 49.39 o 2 2 1 1584.29 1623.13 15.18 o 3 2 1 1673.90 1773.80 17.71 o 4 2 1 45.63 45.71 0.77 o 5 2 1 296.06 299.84 3.67 o 6 2 1 79.60 81.24 1.61 o 7 2 1 428.18 415.66 7.79 o 8 2 1 42.65 43.60 1.88 o 9 2 1 171.07 170.42 4.29 o -9 3 1 38.47 39.23 2.00 o -8 3 1 51.13 49.41 2.05 o -7 3 1 362.84 357.29 5.42 o -6 3 1 381.14 366.10 4.99 o -5 3 1 617.01 621.97 7.75 o -4 3 1 1447.46 1446.48 15.48 o -3 3 1 84.64 91.55 1.17 o -2 3 1 134.68 150.92 1.62 o -1 3 1 2264.01 2491.14 23.14 o 0 3 1 12317.05 11984.60 261.33 o 1 3 1 2238.12 2457.82 24.02 o 2 3 1 132.69 145.28 1.99 o 3 3 1 87.81 94.87 1.25 o 4 3 1 1449.84 1472.03 16.90 o 5 3 1 621.38 623.70 7.76 o 6 3 1 382.17 359.16 4.88 o 7 3 1 356.07 343.60 5.24 o 8 3 1 51.98 52.04 2.05 o 9 3 1 42.18 42.38 2.09 o -9 4 1 124.99 123.24 6.15 o -8 4 1 25.38 23.10 1.26 o -7 4 1 223.14 209.77 3.81 o -6 4 1 199.71 189.22 3.46 o -5 4 1 136.11 125.53 2.11 o -4 4 1 35.87 31.32 0.85 o -3 4 1 869.82 851.46 12.36 o -2 4 1 660.01 677.37 6.99 o -1 4 1 279.00 295.03 2.95 o 0 4 1 99.06 104.15 1.12 o 1 4 1 292.68 319.28 3.17 o 2 4 1 675.73 680.79 7.57 o 3 4 1 865.56 840.87 11.78 o 4 4 1 35.70 32.52 0.86 o 5 4 1 133.56 123.62 2.07 o 6 4 1 203.82 189.02 2.96 o 7 4 1 235.02 226.29 3.84 o 8 4 1 27.58 28.82 1.69 o 9 4 1 125.61 122.32 3.62 o -8 5 1 34.59 32.15 1.50 o -7 5 1 151.55 153.15 2.73 o -6 5 1 94.08 92.72 1.87 o -5 5 1 758.15 749.96 9.31 o -4 5 1 178.11 169.10 2.56 o -3 5 1 207.01 227.36 3.14 o -2 5 1 148.19 161.75 1.79 o -1 5 1 821.16 845.64 7.72 o 0 5 1 76.52 78.18 0.92 o 1 5 1 830.41 868.23 7.90 o 2 5 1 156.16 172.41 2.05 o 3 5 1 203.79 221.70 3.05 o 4 5 1 183.47 174.83 2.61 o 5 5 1 766.73 744.06 10.80 o 6 5 1 95.69 95.93 1.91 o 7 5 1 154.35 153.20 2.72 o 8 5 1 34.64 35.11 1.54 o -8 6 1 61.11 57.06 2.02 o -7 6 1 145.51 145.86 2.69 o -6 6 1 81.30 76.70 1.71 o -5 6 1 51.09 45.37 1.20 o -4 6 1 229.91 221.22 3.24 o -3 6 1 195.23 191.62 2.77 o -2 6 1 212.07 199.83 2.54 o -1 6 1 11.06 12.34 0.44 o 0 6 1 72.48 85.60 1.10 o 1 6 1 11.11 11.16 0.35 o 2 6 1 206.73 194.39 2.87 o 3 6 1 203.95 199.12 2.87 o 4 6 1 237.60 224.21 3.24 o 5 6 1 50.44 46.32 1.22 o 6 6 1 77.52 73.31 1.65 o 7 6 1 149.04 148.97 2.73 o 8 6 1 59.04 60.61 1.86 o -8 7 1 67.08 60.23 2.48 o -7 7 1 1.41 0.71 0.59 o -6 7 1 53.90 51.99 1.42 o -5 7 1 37.22 34.08 1.08 o -4 7 1 95.63 94.63 1.79 o -3 7 1 137.84 131.64 2.16 o -2 7 1 17.57 17.38 0.77 o -1 7 1 425.13 429.05 5.81 o 0 7 1 247.71 236.81 2.71 o 1 7 1 445.94 459.91 5.28 o 2 7 1 18.87 17.69 0.65 o 3 7 1 136.68 129.56 2.11 o 4 7 1 92.11 92.97 1.99 o 5 7 1 39.55 36.93 1.11 o 6 7 1 53.64 51.52 1.42 o 7 7 1 1.61 1.94 0.62 o 8 7 1 66.79 67.00 2.64 o -7 8 1 55.35 51.34 1.59 o -6 8 1 52.87 55.77 1.53 o -5 8 1 96.32 88.70 1.86 o -4 8 1 10.31 10.04 0.77 o -3 8 1 271.65 261.65 3.73 o -2 8 1 227.37 235.31 4.04 o -1 8 1 479.06 469.55 5.48 o 0 8 1 4.20 4.60 0.36 o 1 8 1 474.38 465.28 5.41 o 2 8 1 225.60 233.08 3.43 o 3 8 1 278.25 263.15 3.85 o 4 8 1 10.22 10.43 0.73 o 5 8 1 97.27 90.92 2.15 o 6 8 1 54.16 56.73 1.91 o 7 8 1 54.81 45.03 1.49 o -7 9 1 11.54 15.56 2.05 o -6 9 1 7.34 8.11 0.81 o -5 9 1 66.83 64.99 1.62 o -4 9 1 264.08 258.47 3.88 o -3 9 1 23.49 22.12 0.87 o -2 9 1 182.55 172.81 3.27 o -1 9 1 200.60 195.29 2.92 o 0 9 1 7.65 8.67 0.56 o 1 9 1 193.48 186.12 3.12 o 2 9 1 177.24 177.72 2.75 o 3 9 1 26.18 24.84 1.22 o 4 9 1 271.95 264.07 3.94 o 5 9 1 68.38 64.43 1.61 o 6 9 1 6.18 6.94 0.83 o 7 9 1 10.21 12.73 2.04 o -6 10 1 275.85 285.49 12.16 o -5 10 1 77.02 77.86 2.20 o -4 10 1 119.03 115.85 2.25 o -3 10 1 166.74 165.56 2.77 o -2 10 1 145.50 139.19 2.38 o -1 10 1 106.29 105.36 2.15 o 0 10 1 311.39 298.36 4.63 o 1 10 1 108.40 110.13 2.23 o 2 10 1 151.99 147.66 3.56 o 3 10 1 165.27 157.06 2.67 o 4 10 1 119.07 116.41 2.25 o 5 10 1 77.23 73.40 1.79 o 6 10 1 277.62 264.66 5.30 o -5 11 1 79.75 82.82 3.50 o -4 11 1 54.10 56.82 1.58 o -3 11 1 180.47 174.38 3.29 o -2 11 1 89.33 87.28 2.04 o -1 11 1 166.83 171.12 3.14 o 0 11 1 20.85 20.48 1.10 o 1 11 1 170.40 170.45 3.13 o 2 11 1 95.53 94.59 2.15 o 3 11 1 180.13 177.45 3.33 o 4 11 1 53.50 54.54 1.54 o 5 11 1 80.74 75.87 3.32 o -3 12 1 58.91 60.86 1.81 o -2 12 1 10.78 9.99 1.14 o -1 12 1 108.05 114.67 2.81 o 0 12 1 49.82 49.36 1.82 o 1 12 1 107.68 111.01 2.76 o 2 12 1 10.16 9.27 0.87 o 3 12 1 60.97 58.48 1.77 o 0 0 2 1013.58 1058.51 21.26 o 2 0 2 80.57 71.41 0.87 o 3 0 2 6.96 7.06 0.27 o 4 0 2 17.47 16.27 0.43 o 5 0 2 460.97 444.31 5.16 o 6 0 2 1.69 1.63 0.37 o 7 0 2 290.67 274.96 4.69 o 8 0 2 0.00 -0.25 0.89 o 9 0 2 146.43 147.13 4.92 o -9 1 2 189.37 197.43 6.03 o -8 1 2 105.92 117.13 3.15 o -7 1 2 405.87 380.02 7.14 o -6 1 2 79.52 81.54 1.52 o -5 1 2 146.44 145.71 1.67 o -4 1 2 369.58 409.09 4.06 o -3 1 2 1288.44 1322.28 11.90 o -2 1 2 851.05 953.05 9.00 o -1 1 2 991.81 1129.75 10.67 o 0 1 2 3916.16 3817.37 41.33 o 1 1 2 1030.73 1162.51 10.37 o 2 1 2 858.93 928.72 8.78 o 3 1 2 1265.73 1299.50 11.74 o 4 1 2 363.96 405.00 3.94 o 5 1 2 146.01 149.75 1.97 o 6 1 2 82.02 85.24 1.56 o 7 1 2 416.78 404.91 7.55 o 8 1 2 108.87 109.41 4.09 o 9 1 2 190.47 194.59 5.99 o -9 2 2 191.91 202.89 8.28 o -8 2 2 37.35 35.91 1.75 o -7 2 2 301.62 295.20 5.03 o -6 2 2 170.99 154.63 2.70 o -5 2 2 1595.05 1605.71 17.29 o -4 2 2 289.19 301.58 3.15 o -3 2 2 57.48 69.01 1.03 o -2 2 2 40.32 42.27 0.61 o -1 2 2 2765.29 2972.08 31.01 o 0 2 2 2645.96 2825.36 27.62 o 1 2 2 2752.55 2918.83 25.89 o 2 2 2 38.15 39.20 0.59 o 3 2 2 55.70 63.82 0.89 o 4 2 2 289.40 294.99 3.13 o 5 2 2 1593.28 1597.98 17.16 o 6 2 2 174.81 157.44 2.72 o 7 2 2 306.55 298.87 5.27 o 8 2 2 37.15 38.50 2.08 o 9 2 2 192.06 203.68 4.87 o -9 3 2 90.52 93.68 3.04 o -8 3 2 2.90 0.69 0.90 o -7 3 2 352.21 344.85 5.27 o -6 3 2 8.04 8.19 0.60 o -5 3 2 186.05 194.60 2.89 o -4 3 2 115.92 122.86 2.04 o -3 3 2 1092.28 1134.97 11.50 o -2 3 2 1.61 0.77 0.13 o -1 3 2 15.20 15.16 0.34 o 0 3 2 395.19 441.49 4.76 o 1 3 2 17.87 18.08 0.36 o 2 3 2 1.99 1.86 0.23 o 3 3 2 1094.30 1124.72 10.77 o 4 3 2 117.64 125.38 1.66 o 5 3 2 186.78 190.27 2.83 o 6 3 2 6.83 6.97 0.63 o 7 3 2 349.02 347.39 5.30 o 8 3 2 3.69 3.84 1.05 o 9 3 2 88.63 95.86 3.09 o -9 4 2 57.99 58.87 3.06 o -8 4 2 48.47 44.15 1.65 o -7 4 2 35.42 35.10 1.24 o -6 4 2 96.84 92.79 1.84 o -5 4 2 121.80 111.76 2.28 o -4 4 2 107.96 104.57 1.76 o -3 4 2 40.83 40.44 0.98 o -2 4 2 41.31 40.14 0.69 o -1 4 2 188.88 197.76 2.17 o 0 4 2 144.60 146.51 1.81 o 1 4 2 212.30 226.13 2.35 o 2 4 2 42.80 39.88 0.67 o 3 4 2 40.24 38.36 0.82 o 4 4 2 107.92 104.56 1.78 o 5 4 2 118.90 106.65 2.50 o 6 4 2 91.86 89.24 1.79 o 7 4 2 34.29 34.36 1.36 o 8 4 2 48.84 45.20 2.03 o 9 4 2 54.11 52.75 2.88 o -8 5 2 43.67 48.95 3.93 o -7 5 2 307.67 300.13 4.83 o -6 5 2 328.61 323.05 4.61 o -5 5 2 4.06 4.43 0.47 o -4 5 2 107.57 100.92 1.78 o -3 5 2 403.90 377.85 4.85 o -2 5 2 297.51 303.42 3.14 o -1 5 2 523.91 539.13 5.24 o 0 5 2 463.92 471.10 4.88 o 1 5 2 508.62 537.24 5.53 o 2 5 2 289.20 292.61 3.45 o 3 5 2 411.04 398.51 5.08 o 4 5 2 105.28 95.82 1.70 o 5 5 2 3.99 4.25 0.47 o 6 5 2 328.03 311.23 4.45 o 7 5 2 302.04 289.91 4.69 o 8 5 2 41.18 42.88 1.53 o -8 6 2 182.59 181.08 3.52 o -7 6 2 66.86 67.20 1.85 o -6 6 2 51.25 51.34 1.37 o -5 6 2 131.21 126.71 2.24 o -4 6 2 383.35 357.09 4.80 o -3 6 2 412.87 417.25 5.37 o -2 6 2 182.35 182.69 2.75 o -1 6 2 518.99 538.97 5.32 o 0 6 2 0.07 0.54 0.17 o 1 6 2 493.93 518.60 5.50 o 2 6 2 178.07 172.18 2.47 o 3 6 2 418.24 422.60 5.41 o 4 6 2 376.57 352.59 4.73 o 5 6 2 134.49 135.77 2.35 o 6 6 2 52.05 52.56 1.39 o 7 6 2 63.37 63.52 1.77 o 8 6 2 182.28 185.33 3.59 o -8 7 2 67.20 72.19 2.71 o -7 7 2 141.36 139.86 2.89 o -6 7 2 326.39 332.53 5.61 o -5 7 2 38.98 34.78 1.28 o -4 7 2 146.33 145.43 2.42 o -3 7 2 501.43 490.73 6.28 o -2 7 2 360.81 365.29 5.74 o -1 7 2 404.56 395.73 4.64 o 0 7 2 27.45 27.62 0.62 o 1 7 2 414.32 416.38 4.48 o 2 7 2 359.49 367.84 4.42 o 3 7 2 494.95 480.99 6.13 o 4 7 2 143.97 139.56 2.39 o 5 7 2 39.71 34.68 1.09 o 6 7 2 323.99 319.47 4.68 o 7 7 2 147.21 135.63 2.85 o 8 7 2 68.50 69.76 3.14 o -7 8 2 128.36 126.78 2.59 o -6 8 2 16.84 16.27 0.93 o -5 8 2 838.50 801.18 10.13 o -4 8 2 49.43 45.58 1.29 o -3 8 2 32.20 29.43 0.95 o -2 8 2 49.74 43.26 1.16 o -1 8 2 949.57 958.36 10.57 o 0 8 2 194.51 189.84 2.52 o 1 8 2 958.18 934.06 11.21 o 2 8 2 49.23 46.85 1.03 o 3 8 2 29.72 27.81 0.91 o 4 8 2 52.19 51.14 1.30 o 5 8 2 836.91 792.75 10.01 o 6 8 2 15.82 15.40 0.91 o 7 8 2 132.50 134.32 2.68 o -7 9 2 57.32 59.24 4.89 o -6 9 2 42.44 43.50 1.41 o -5 9 2 27.22 24.96 1.14 o -4 9 2 11.21 11.05 0.73 o -3 9 2 281.16 259.15 4.15 o -2 9 2 19.98 20.59 1.79 o -1 9 2 94.81 88.25 1.66 o 0 9 2 55.82 51.27 1.18 o 1 9 2 92.09 89.01 1.83 o 2 9 2 20.84 23.12 1.02 o 3 9 2 282.62 269.22 5.16 o 4 9 2 12.86 12.22 0.74 o 5 9 2 27.30 24.51 1.07 o 6 9 2 42.29 43.43 1.41 o 7 9 2 54.40 56.73 4.77 o -6 10 2 3.55 3.76 2.13 o -5 10 2 22.85 23.95 1.09 o -4 10 2 95.80 95.06 1.99 o -3 10 2 55.68 52.65 1.49 o -2 10 2 201.54 198.57 3.09 o -1 10 2 85.41 78.93 1.79 o 0 10 2 2.71 2.65 0.52 o 1 10 2 88.37 83.58 1.88 o 2 10 2 202.04 199.56 3.61 o 3 10 2 54.38 54.89 1.78 o 4 10 2 93.80 91.37 1.95 o 5 10 2 21.52 21.92 1.34 o 6 10 2 3.46 4.98 1.20 o -5 11 2 53.95 56.12 3.95 o -4 11 2 16.91 18.10 1.00 o -3 11 2 1.04 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155.10 145.89 3.04 o -2 4 14 72.38 75.03 4.71 o -1 4 14 113.51 121.15 3.12 o 0 4 14 203.16 200.41 3.73 o 1 4 14 116.86 114.39 2.58 o 2 4 14 70.57 80.19 4.64 o -1 5 14 74.83 69.40 4.64 o 0 5 14 26.81 23.66 2.95 o 1 5 14 73.16 77.81 4.52 o 1 0 15 20.28 15.76 2.00 o 2 0 15 4.24 12.64 2.07 o -1 1 15 149.58 144.61 4.07 o 0 1 15 7.47 5.98 1.43 o 1 1 15 154.12 161.07 6.40 o -1 2 15 112.05 120.10 5.77 o 0 2 15 17.94 17.70 2.38 o