#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:17:49 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180845 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/76/2017661.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017661_Fobs loop_ _publ_author_name 'Ho, Douglas M.' _publ_section_title ; Bis(hinokitiolato)copper(II): modification (III) ; _journal_coeditor_code EG3045 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m145 _journal_page_last m148 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 72.847 _cell_angle_beta 79.812 _cell_angle_gamma 88.897 _cell_length_a 9.6263 _cell_length_b 12.8911 _cell_length_c 19.4499 _exptl_crystal_F_000 1015.00 _reflns_d_resolution_high 0.7709 _cod_data_source_file eg3045IIIsup2.hkl _cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' [cis-Cu(hino)2]2[trans-Cu(hino)2] . [cis-Cu(hino)2]2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 287.86 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 155.93 153.40 5.57 o 2 0 0 180.89 171.12 7.09 o 3 0 0 7420.45 6865.91 128.59 o 4 0 0 85.47 68.35 8.10 o 5 0 0 322.44 339.19 13.16 o 6 0 0 1417.93 1462.08 35.44 o 7 0 0 1194.97 1195.28 44.04 o 8 0 0 239.19 217.69 29.87 o 9 0 0 33.26 40.50 23.79 o 10 0 0 147.10 160.48 31.89 o 11 0 0 473.40 440.95 49.61 o 12 0 0 248.87 225.29 49.61 o -12 1 0 19.27 37.97 46.58 o -11 1 0 969.58 889.50 59.23 o -10 1 0 187.19 171.12 29.36 o -9 1 0 1766.51 2001.25 39.99 o -8 1 0 1028.27 1095.55 37.46 o -7 1 0 2935.98 3001.11 72.40 o -6 1 0 593.11 509.80 20.76 o -5 1 0 5749.31 6288.26 113.40 o -4 1 0 1733.29 1592.70 38.48 o -3 1 0 699.01 727.50 22.28 o -2 1 0 482.81 470.82 12.15 o -1 1 0 970.26 974.05 25.31 o 1 1 0 1444.12 1416.52 28.35 o 2 1 0 6155.39 6231.56 114.41 o 3 1 0 1778.49 1639.78 46.58 o 4 1 0 1170.82 922.91 31.89 o 5 1 0 229.01 291.61 19.74 o 6 1 0 189.75 144.28 18.73 o 7 1 0 629.75 568.53 27.84 o 8 1 0 206.71 191.87 24.30 o 9 1 0 1351.47 1514.23 59.74 o 10 1 0 12.40 -18.23 31.89 o 11 1 0 40.27 54.68 30.88 o 12 1 0 19.18 14.68 35.94 o -12 2 0 205.55 74.42 39.99 o -11 2 0 90.97 135.17 32.40 o -10 2 0 109.17 78.98 17.21 o -9 2 0 507.48 500.69 28.86 o -8 2 0 2.78 6.58 13.67 o -7 2 0 1137.41 1112.76 33.41 o -6 2 0 798.27 772.55 26.83 o -5 2 0 453.48 450.07 17.72 o -4 2 0 872.03 1064.16 30.38 o -3 2 0 97.53 181.24 10.13 o -2 2 0 6842.75 6462.92 156.43 o -1 2 0 119.07 131.12 12.66 o 0 2 0 2982.13 2908.97 122.52 o 1 2 0 190.75 171.12 8.61 o 2 2 0 23222.23 23140.16 479.43 o 3 2 0 19445.68 18897.70 341.73 o 4 2 0 285.03 211.11 11.64 o 5 2 0 20.28 21.26 10.63 o 6 2 0 1913.24 1981.50 57.21 o 7 2 0 4014.42 4377.13 111.38 o 8 2 0 1045.79 1113.27 57.21 o 9 2 0 269.78 227.82 24.30 o 10 2 0 21.80 48.60 28.86 o 11 2 0 22.96 2.53 36.45 o 12 2 0 9.31 29.87 68.35 o -12 3 0 8.04 45.06 57.71 o -11 3 0 267.31 300.72 64.30 o -10 3 0 49.20 57.71 23.29 o -9 3 0 46.01 76.45 17.21 o -8 3 0 1598.39 1734.45 56.70 o -7 3 0 3533.81 3984.78 93.66 o -6 3 0 639.58 607.51 24.30 o -5 3 0 718.03 735.09 34.43 o -4 3 0 4160.00 3900.23 92.65 o -3 3 0 1443.93 1496.00 45.06 o -2 3 0 4421.34 4451.55 139.22 o -1 3 0 3270.06 3232.98 136.18 o 0 3 0 9490.91 9252.92 388.30 o 1 3 0 4293.45 4047.05 175.67 o 2 3 0 13064.95 13157.21 322.49 o 3 3 0 1.07 5.06 5.06 o 4 3 0 1123.49 1054.03 26.83 o 5 3 0 859.10 817.61 30.38 o 6 3 0 590.93 619.16 28.86 o 7 3 0 1732.29 1847.85 60.25 o 8 3 0 504.78 503.73 36.96 o 9 3 0 361.03 321.98 39.49 o 10 3 0 15.78 31.89 38.48 o 11 3 0 839.23 854.06 74.42 o -11 4 0 220.44 189.34 53.16 o -10 4 0 67.52 89.10 29.36 o -9 4 0 55.59 40.50 28.35 o -8 4 0 1600.06 1630.16 54.17 o -7 4 0 162.23 141.25 19.74 o -6 4 0 42.35 21.26 16.20 o -5 4 0 78.51 74.42 17.72 o -4 4 0 516.44 464.75 24.81 o -3 4 0 3918.34 3864.29 133.65 o -2 4 0 4041.48 4152.35 221.74 o -1 4 0 917.53 949.24 58.22 o 0 4 0 4713.13 4432.31 221.74 o 1 4 0 42.01 79.99 18.23 o 2 4 0 6826.25 6449.76 148.84 o 3 4 0 170.42 99.23 9.62 o 4 4 0 9398.20 9694.38 184.28 o 5 4 0 2711.75 2692.80 58.73 o 6 4 0 1396.50 1422.09 57.71 o 7 4 0 1229.69 1195.28 49.61 o 8 4 0 187.99 214.15 29.36 o 9 4 0 299.34 204.53 39.49 o 10 4 0 273.39 176.18 52.14 o 11 4 0 40.18 79.99 40.50 o -11 5 0 525.04 559.92 54.68 o -10 5 0 65.92 17.21 33.92 o -9 5 0 418.70 417.66 36.96 o -8 5 0 7.44 -7.59 18.23 o -7 5 0 1656.73 1709.14 58.73 o -6 5 0 766.46 743.19 35.44 o -5 5 0 19.96 20.25 13.16 o -4 5 0 5770.71 5380.03 131.12 o -3 5 0 329.76 295.66 24.30 o -2 5 0 33.28 41.01 22.28 o -1 5 0 2860.02 2861.39 139.73 o 0 5 0 258.17 170.10 31.89 o 1 5 0 519.36 517.40 27.84 o 2 5 0 107.68 115.93 13.67 o 3 5 0 2497.80 2863.41 66.83 o 4 5 0 300.09 244.02 14.18 o 5 5 0 1033.36 1048.97 32.91 o 6 5 0 10.67 6.08 6.08 o 7 5 0 1751.48 2028.08 132.13 o 8 5 0 881.25 819.13 55.18 o 9 5 0 17.20 37.97 32.40 o 10 5 0 4.90 11.14 38.48 o 11 5 0 524.70 557.39 77.46 o -11 6 0 20.38 -41.01 41.01 o -10 6 0 217.73 197.95 43.03 o -9 6 0 132.57 60.25 26.83 o -8 6 0 386.20 345.27 29.36 o -7 6 0 443.87 390.33 26.33 o -6 6 0 675.13 701.68 30.88 o -5 6 0 229.43 198.45 21.77 o -4 6 0 1116.77 1111.24 37.97 o -3 6 0 1517.07 1607.38 74.93 o -2 6 0 1409.51 1445.88 71.38 o -1 6 0 180.04 168.58 25.82 o 0 6 0 3695.50 3425.87 158.46 o 1 6 0 16.59 12.66 18.73 o 2 6 0 20.78 29.87 11.64 o 3 6 0 2901.21 2983.39 81.51 o 4 6 0 3059.75 3133.25 69.36 o 5 6 0 1725.48 1735.97 50.12 o 6 6 0 180.17 164.53 16.71 o 7 6 0 3232.75 3559.52 176.18 o 8 6 0 108.48 141.75 31.39 o 9 6 0 84.22 42.53 32.40 o 10 6 0 345.72 325.02 62.27 o 11 6 0 97.37 82.52 46.58 o -11 7 0 92.06 79.48 41.51 o -10 7 0 142.81 74.93 32.40 o -9 7 0 219.44 169.09 34.93 o -8 7 0 626.49 573.09 38.48 o -7 7 0 271.82 304.26 27.84 o -6 7 0 174.77 171.12 20.25 o -5 7 0 4.83 -15.69 16.20 o -4 7 0 3242.11 3204.12 106.82 o -3 7 0 109.83 100.75 21.77 o -2 7 0 4338.41 4430.79 222.25 o -1 7 0 4296.62 4697.59 180.74 o 0 7 0 2409.34 2570.29 116.95 o 1 7 0 295.28 367.04 35.44 o 2 7 0 796.57 837.86 35.44 o 3 7 0 19.67 11.14 15.69 o 4 7 0 117.80 99.73 14.18 o 5 7 0 79.46 73.41 16.20 o 6 7 0 138.44 101.76 16.71 o 7 7 0 203.52 215.67 18.73 o 8 7 0 16.30 -22.78 33.92 o 9 7 0 272.79 305.28 39.99 o 10 7 0 18.12 14.18 38.98 o -10 8 0 258.58 252.62 48.60 o -9 8 0 0.93 -29.87 29.87 o -8 8 0 218.28 175.67 28.86 o -7 8 0 658.81 589.79 49.61 o -6 8 0 95.31 115.93 22.78 o -5 8 0 171.44 149.35 17.72 o -4 8 0 152.10 145.30 23.29 o -3 8 0 1329.73 1348.17 71.89 o -2 8 0 0.06 -5.06 22.28 o -1 8 0 13.89 50.63 35.44 o 0 8 0 8227.44 8627.19 358.43 o 1 8 0 8.91 8.10 17.21 o 2 8 0 37.31 32.40 19.24 o 3 8 0 621.13 561.44 31.89 o 4 8 0 417.33 421.72 26.33 o 5 8 0 523.83 482.47 27.34 o 6 8 0 96.05 66.32 17.72 o 7 8 0 1001.99 1047.96 51.64 o 8 8 0 6.97 -19.24 32.91 o 9 8 0 3.93 25.82 35.94 o 10 8 0 377.17 318.94 50.12 o -10 9 0 49.33 95.18 45.06 o -9 9 0 657.34 683.45 65.31 o -8 9 0 202.03 142.77 30.88 o -7 9 0 1785.84 1874.18 116.95 o -6 9 0 27.78 26.33 22.78 o -5 9 0 1054.18 971.01 47.59 o -4 9 0 1879.80 2140.47 86.06 o -3 9 0 988.66 1130.48 101.76 o -2 9 0 25.16 35.44 50.12 o -1 9 0 3457.69 3566.61 170.10 o 0 9 0 1117.97 1125.42 71.89 o 1 9 0 140.70 85.05 20.25 o 2 9 0 7.01 -8.10 16.20 o 3 9 0 738.21 722.94 39.49 o 4 9 0 75.63 51.64 20.25 o 5 9 0 308.32 287.05 28.35 o 6 9 0 4.34 76.95 25.82 o 7 9 0 60.94 39.49 24.30 o 8 9 0 67.91 -5.06 43.54 o 9 9 0 15.53 89.61 40.50 o -9 10 0 1.75 -29.36 29.36 o -8 10 0 781.10 768.00 56.70 o -7 10 0 26.13 -37.46 37.46 o -6 10 0 30.71 28.86 24.30 o -5 10 0 866.84 1011.51 63.79 o -4 10 0 13.94 -11.64 21.26 o -3 10 0 25.41 30.38 30.38 o -2 10 0 8.21 60.75 38.98 o -1 10 0 51.45 -12.15 37.97 o 0 10 0 145.04 95.68 37.46 o 1 10 0 68.83 30.88 30.88 o 2 10 0 348.37 305.28 34.93 o 3 10 0 382.59 399.44 37.97 o 4 10 0 389.61 342.23 36.96 o 5 10 0 97.73 119.98 25.82 o 6 10 0 5.58 44.55 30.88 o 7 10 0 592.65 637.89 52.14 o 8 10 0 18.43 -2.53 69.86 o 9 10 0 7.94 6.08 56.70 o -9 11 0 15.90 43.54 44.04 o -8 11 0 13.18 24.81 36.96 o -7 11 0 472.16 386.78 57.71 o -6 11 0 128.97 83.53 27.84 o -5 11 0 275.43 178.20 35.94 o -4 11 0 1099.03 1296.03 116.44 o -3 11 0 90.74 90.11 100.24 o -2 11 0 215.53 234.90 70.88 o -1 11 0 1955.46 2148.57 155.42 o 0 11 0 843.74 823.69 85.05 o 1 11 0 8.59 2.03 21.26 o 2 11 0 87.09 36.45 27.34 o 3 11 0 690.92 819.13 49.11 o 4 11 0 127.79 92.65 34.93 o 5 11 0 1.41 -10.13 23.29 o 6 11 0 22.01 9.11 31.89 o 7 11 0 0.53 -33.41 33.41 o 8 11 0 264.41 324.01 81.00 o -8 12 0 569.04 546.76 72.90 o -7 12 0 28.12 83.53 41.01 o -6 12 0 5.87 7.09 35.94 o -5 12 0 309.00 350.33 62.78 o -4 12 0 75.16 16.20 46.07 o -3 12 0 128.80 102.26 51.64 o -2 12 0 151.65 190.35 80.50 o 0 12 0 223.62 132.13 52.65 o 1 12 0 310.91 284.52 40.50 o 2 12 0 316.26 175.67 61.76 o 3 12 0 34.37 -5.57 31.89 o 4 12 0 426.47 382.23 45.06 o 5 12 0 588.61 563.97 54.68 o 6 12 0 28.62 18.73 33.41 o 7 12 0 274.07 299.71 49.11 o -7 13 0 188.47 367.04 122.01 o -6 13 0 17.62 -1.52 98.72 o -5 13 0 56.94 82.01 72.90 o -4 13 0 1008.49 1160.35 106.82 o -3 13 0 324.70 285.02 55.69 o -2 13 0 662.93 738.63 124.03 o -1 13 0 385.24 420.70 97.71 o 0 13 0 346.60 290.59 132.64 o 1 13 0 398.90 684.97 189.85 o 2 13 0 142.31 53.16 69.36 o 3 13 0 50.31 27.34 38.98 o 4 13 0 3.62 -14.18 30.88 o 5 13 0 51.96 15.19 30.88 o 6 13 0 180.45 159.98 54.17 o -6 14 0 1.43 188.33 98.21 o -5 14 0 324.31 552.33 139.73 o -4 14 0 133.19 123.53 100.24 o -3 14 0 80.65 96.70 89.61 o -2 14 0 45.35 62.27 68.85 o -1 14 0 90.40 67.84 67.84 o 0 14 0 44.88 3.54 79.48 o 1 14 0 448.54 596.37 145.30 o 2 14 0 37.71 -91.63 91.63 o 3 14 0 85.02 41.51 51.64 o 4 14 0 267.12 276.42 50.63 o 5 14 0 2.29 20.76 46.07 o -4 15 0 276.83 260.72 105.30 o -3 15 0 2.96 125.55 82.01 o -2 15 0 392.23 376.66 133.65 o -1 15 0 356.49 311.86 127.58 o 0 15 0 662.03 651.05 159.47 o 1 15 0 27.91 -62.78 239.46 o 2 15 0 10.36 -7.09 90.11 o 3 15 0 546.10 779.64 103.78 o -3 -15 1 12.81 82.52 71.89 o -2 -15 1 35.81 190.35 123.53 o -1 -15 1 0.77 269.84 121.50 o 0 -15 1 9.52 243.01 244.02 o 1 -15 1 36.94 -19.24 100.24 o 2 -15 1 51.39 -99.23 128.59 o 3 -15 1 24.94 -30.88 96.70 o 4 -15 1 0.10 10.63 121.50 o -5 -14 1 117.09 128.59 43.54 o -4 -14 1 236.74 184.28 40.50 o -3 -14 1 354.39 389.31 52.14 o -2 -14 1 4.36 0.00 84.55 o -1 -14 1 22.53 161.50 67.84 o 0 -14 1 132.75 -22.78 92.14 o 1 -14 1 334.61 400.45 105.30 o 2 -14 1 74.40 40.50 86.06 o 3 -14 1 15.94 7.09 68.85 o 4 -14 1 227.97 268.82 83.03 o 5 -14 1 6.92 11.14 77.46 o 6 -14 1 28.07 77.46 126.57 o -6 -13 1 85.83 62.78 49.11 o -5 -13 1 50.13 74.93 49.61 o -4 -13 1 60.23 41.01 35.44 o -3 -13 1 34.88 129.10 106.31 o -2 -13 1 23.06 25.31 53.66 o -1 -13 1 328.79 386.78 90.11 o 0 -13 1 647.66 616.12 100.75 o 1 -13 1 226.87 171.62 95.18 o 2 -13 1 239.15 267.31 109.35 o 3 -13 1 224.19 357.93 104.29 o 4 -13 1 26.68 63.28 112.39 o 5 -13 1 336.26 453.61 84.55 o 6 -13 1 60.59 23.29 66.83 o 7 -13 1 224.04 109.35 68.85 o -7 -12 1 5.29 25.82 61.76 o -6 -12 1 310.40 276.42 48.09 o -5 -12 1 269.95 250.60 55.18 o -4 -12 1 51.55 49.11 37.46 o -3 -12 1 654.29 561.95 76.45 o -2 -12 1 1019.75 1383.61 406.53 o -1 -12 1 895.49 854.06 89.61 o 0 -12 1 97.50 70.37 37.46 o 1 -12 1 262.83 146.82 38.48 o 2 -12 1 2.78 -2.53 123.53 o 3 -12 1 143.91 49.61 52.65 o 4 -12 1 545.32 613.08 76.45 o 5 -12 1 1.62 20.25 35.94 o 6 -12 1 17.49 29.36 21.77 o 7 -12 1 32.94 -11.64 30.88 o 8 -12 1 61.69 69.36 54.68 o -8 -11 1 37.48 67.33 60.75 o -7 -11 1 87.33 10.63 58.22 o -6 -11 1 37.78 37.97 35.44 o -5 -11 1 119.17 48.09 28.35 o -4 -11 1 125.88 85.05 24.81 o -3 -11 1 371.45 312.87 46.07 o -2 -11 1 266.49 196.43 29.36 o -1 -11 1 107.30 92.65 27.84 o 0 -11 1 2.01 -11.14 26.83 o 1 -11 1 11.53 -28.35 58.73 o 2 -11 1 903.07 2548.01 1383.10 o 3 -11 1 24.18 95.18 115.93 o 4 -11 1 63.49 121.50 39.49 o 5 -11 1 552.79 662.70 59.74 o 6 -11 1 30.72 42.53 28.86 o 7 -11 1 327.33 208.58 27.34 o 8 -11 1 568.70 581.69 60.25 o 9 -11 1 178.20 124.03 60.25 o -9 -10 1 148.21 97.71 67.33 o -8 -10 1 7.56 -53.16 53.16 o -7 -10 1 16.06 -7.09 39.99 o -6 -10 1 199.19 180.74 35.44 o -5 -10 1 1.69 21.26 25.82 o -4 -10 1 23.88 30.88 24.30 o -3 -10 1 423.40 354.89 35.44 o -2 -10 1 1021.87 937.59 63.79 o -1 -10 1 126.89 141.25 25.82 o 0 -10 1 10.20 -12.15 25.82 o 1 -10 1 6300.62 7579.73 441.97 o 2 -10 1 913.75 918.86 73.41 o 3 -10 1 346.13 307.81 57.21 o 4 -10 1 2377.05 2516.11 184.79 o 5 -10 1 3.56 -25.31 25.31 o 6 -10 1 38.12 30.38 25.82 o 7 -10 1 43.43 56.70 24.81 o 8 -10 1 81.42 52.65 32.40 o 9 -10 1 119.07 29.36 45.06 o -9 -9 1 49.15 66.32 60.25 o -8 -9 1 135.02 55.69 52.65 o -7 -9 1 569.33 560.94 47.59 o -6 -9 1 233.20 210.60 34.93 o -5 -9 1 456.00 478.92 33.41 o -4 -9 1 7.17 16.20 17.21 o -3 -9 1 1687.00 1779.00 90.11 o -2 -9 1 77.65 80.50 21.77 o -1 -9 1 17.93 29.87 19.74 o 0 -9 1 797.25 847.48 68.85 o 1 -9 1 644.30 689.02 54.68 o 2 -9 1 1227.55 1265.15 88.60 o 3 -9 1 361.60 408.55 59.74 o 4 -9 1 17.70 -15.69 24.30 o 5 -9 1 975.75 1029.23 51.13 o 6 -9 1 12.48 14.68 24.30 o 7 -9 1 329.81 300.21 26.33 o 8 -9 1 763.63 859.12 61.76 o 9 -9 1 115.27 127.58 45.56 o 10 -9 1 511.66 443.99 48.60 o -10 -8 1 104.65 163.02 50.63 o -9 -8 1 0.15 -6.58 31.39 o -8 -8 1 54.00 48.60 34.43 o -7 -8 1 92.69 50.63 21.26 o -6 -8 1 527.79 463.73 30.38 o -5 -8 1 137.21 174.15 23.79 o -4 -8 1 451.19 404.50 30.88 o -3 -8 1 784.80 757.37 40.50 o -2 -8 1 1207.57 1308.68 59.74 o -1 -8 1 1857.29 2160.21 102.77 o 0 -8 1 47.59 151.88 45.56 o 1 -8 1 5245.81 5550.13 236.42 o 2 -8 1 692.83 631.81 52.14 o 3 -8 1 198.88 204.02 31.89 o 4 -8 1 2042.44 2267.03 78.98 o 5 -8 1 19.46 22.78 17.72 o 6 -8 1 23.49 14.18 20.76 o 7 -8 1 943.02 940.63 47.59 o 8 -8 1 9.58 -13.16 26.83 o 9 -8 1 8.01 0.51 29.36 o 10 -8 1 3.82 -39.99 39.99 o -10 -7 1 494.38 449.05 58.73 o -9 -7 1 15.20 40.50 29.87 o -8 -7 1 256.22 234.90 38.48 o -7 -7 1 605.60 575.11 28.86 o -6 -7 1 1266.60 1390.70 48.60 o 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