#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/76/2017671.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017671_Fobs loop_ _publ_author_name 'Freire, Eleonora' 'Vega, Daniel R.' 'Baggio, Ricardo' _publ_section_title ; Zoledronate complexes. III. Two zoledronate complexes with alkaline earth metals: [Mg(C~5~H~9~N~2~O~7~P~2~)~2~(H~2~O)~2~] and [Ca(C~5~H~8~N~2~O~7~P~2~)(H~2~O)]~n~ ; _journal_coeditor_code GD3341 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m166 _journal_page_last m170 _journal_volume 66 _journal_year 2010 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 105.108 _cell_angle_beta 111.980 _cell_angle_gamma 97.038 _cell_length_a 7.4680 _cell_length_b 8.4390 _cell_length_c 9.8190 _exptl_crystal_F_000 310.00 _reflns_d_resolution_high 0.8108 _[local]_cod_data_source_file gd3341Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' pp in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 98.17 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h 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3.60 0.30 o 0 2 0 3096.04 2522.14 15.80 o 1 2 0 4052.61 3273.80 20.43 o 2 2 0 2813.21 2849.00 19.37 o 3 2 0 4.37 5.20 0.43 o 4 2 0 1324.49 1363.56 12.32 o 5 2 0 34.91 39.13 1.55 o 6 2 0 152.97 159.49 4.77 o 7 2 0 105.95 120.42 5.10 o -8 3 0 51.20 47.40 1.98 o -7 3 0 8.88 9.24 0.94 o -6 3 0 11.56 12.83 0.83 o -5 3 0 940.48 1039.24 11.19 o -4 3 0 98.56 93.50 2.78 o -3 3 0 329.80 380.00 4.79 o -2 3 0 9637.31 9257.95 58.36 o -1 3 0 535.40 456.65 4.20 o 0 3 0 37.54 35.10 1.15 o 1 3 0 306.13 331.95 3.50 o 2 3 0 127.52 117.89 2.15 o 3 3 0 821.28 795.28 7.53 o 4 3 0 355.32 349.05 5.11 o 5 3 0 1005.27 974.78 10.66 o 6 3 0 396.62 425.89 7.43 o 7 3 0 3.22 6.77 0.94 o -8 4 0 0.23 -0.70 2.61 o -7 4 0 53.43 52.50 2.03 o -6 4 0 1049.43 1045.72 12.11 o -5 4 0 943.09 952.22 10.36 o -4 4 0 129.09 142.97 3.35 o -3 4 0 3337.22 3262.66 23.13 o -2 4 0 127.68 138.85 2.56 o -1 4 0 4.90 9.55 0.43 o 0 4 0 1134.49 950.08 7.55 o 1 4 0 814.29 695.39 6.14 o 2 4 0 2342.06 2221.37 16.12 o 3 4 0 187.97 141.62 2.88 o 4 4 0 281.64 259.89 4.49 o 5 4 0 181.66 204.68 4.63 o 6 4 0 0.90 -0.39 2.06 o -8 5 0 0.08 -1.62 2.64 o -7 5 0 123.23 117.02 4.37 o -6 5 0 1.18 1.41 1.88 o -5 5 0 28.12 26.78 1.11 o -4 5 0 385.79 382.01 5.55 o -3 5 0 41.50 49.16 1.99 o -2 5 0 809.76 803.32 7.61 o -1 5 0 2213.27 1950.17 14.35 o 0 5 0 989.52 878.41 7.70 o 1 5 0 292.24 286.86 3.87 o 2 5 0 483.24 407.21 4.98 o 3 5 0 55.03 39.31 1.38 o 4 5 0 68.20 72.19 2.72 o 5 5 0 32.43 29.89 1.17 o 6 5 0 326.90 325.14 6.69 o -7 6 0 106.30 109.33 4.22 o -6 6 0 69.81 61.86 2.28 o -5 6 0 175.13 146.83 4.01 o -4 6 0 104.30 115.70 3.30 o -3 6 0 6.27 7.31 0.52 o -2 6 0 445.07 432.39 5.45 o -1 6 0 446.11 400.61 5.04 o 0 6 0 473.71 451.55 5.48 o 1 6 0 790.06 712.81 7.33 o 2 6 0 15.81 14.07 0.59 o 3 6 0 2.50 1.15 1.38 o 4 6 0 82.00 72.34 2.80 o 5 6 0 72.61 81.25 3.34 o -7 7 0 219.34 209.04 5.67 o -6 7 0 8.39 8.12 0.74 o -5 7 0 169.59 179.38 4.47 o -4 7 0 5.67 4.22 0.59 o -3 7 0 406.23 390.29 5.82 o -2 7 0 76.95 75.15 2.71 o -1 7 0 1520.56 1434.00 12.68 o 0 7 0 1564.84 1432.07 12.64 o 1 7 0 3.83 4.58 0.52 o 2 7 0 139.62 113.04 3.20 o 3 7 0 96.64 102.15 3.34 o 4 7 0 0.09 -1.23 1.62 o -6 8 0 86.45 80.83 2.58 o -5 8 0 26.75 26.53 1.10 o -4 8 0 9.47 9.02 0.67 o -3 8 0 239.99 261.25 5.12 o -2 8 0 111.67 117.82 3.38 o -1 8 0 382.81 373.29 5.99 o 0 8 0 7.49 7.18 0.60 o 1 8 0 13.17 13.32 0.67 o 2 8 0 198.23 199.81 4.64 o 3 8 0 10.64 12.07 0.71 o -5 9 0 8.46 8.12 0.78 o -4 9 0 73.42 81.82 2.50 o -3 9 0 15.63 15.43 0.77 o -2 9 0 2.04 1.44 1.84 o -1 9 0 158.58 163.90 4.34 o 0 9 0 62.73 70.89 3.05 o 1 9 0 374.98 430.42 7.13 o -2 10 0 289.00 337.12 6.83 o 0 -10 1 0.01 1.33 1.34 o 1 -10 1 4.46 2.78 2.17 o 2 -10 1 4.56 4.62 0.74 o 3 -10 1 188.01 216.23 5.53 o -2 -9 1 23.32 24.41 1.05 o -1 -9 1 9.36 10.46 0.72 o 0 -9 1 28.82 29.69 1.16 o 1 -9 1 247.75 260.88 5.33 o 2 -9 1 264.42 279.20 5.69 o 3 -9 1 73.49 72.22 2.34 o 4 -9 1 54.61 51.83 2.13 o 5 -9 1 86.98 89.02 2.79 o -3 -8 1 39.55 39.01 1.45 o -2 -8 1 3.25 1.33 1.67 o -1 -8 1 73.32 73.31 2.91 o 0 -8 1 475.47 459.91 6.57 o 1 -8 1 8.80 8.54 0.62 o 2 -8 1 0.11 0.34 0.94 o 3 -8 1 75.93 86.18 3.17 o 4 -8 1 2.04 1.90 1.69 o 5 -8 1 140.92 126.25 4.22 o 6 -8 1 99.97 84.73 2.81 o -4 -7 1 9.79 8.50 0.64 o -3 -7 1 139.67 135.46 3.54 o -2 -7 1 0.53 0.94 1.38 o -1 -7 1 40.90 36.20 1.45 o 0 -7 1 119.12 111.91 2.97 o 1 -7 1 275.93 255.55 4.39 o 2 -7 1 162.42 173.29 3.78 o 3 -7 1 27.44 21.35 0.82 o 4 -7 1 63.73 75.32 3.13 o 5 -7 1 179.47 167.49 4.51 o 6 -7 1 13.08 14.06 0.86 o 7 -7 1 8.41 9.49 0.94 o -5 -6 1 2.47 3.11 0.60 o -4 -6 1 76.42 76.41 2.84 o -3 -6 1 2.13 1.11 1.32 o -2 -6 1 565.53 498.35 5.93 o -1 -6 1 342.46 299.06 4.36 o 0 -6 1 848.96 727.45 7.27 o 1 -6 1 907.38 883.44 8.55 o 2 -6 1 29.76 29.41 1.06 o 3 -6 1 161.27 159.74 3.59 o 4 -6 1 79.31 79.38 3.09 o 5 -6 1 26.83 24.79 0.99 o 6 -6 1 71.19 64.95 2.49 o 7 -6 1 596.79 525.72 9.25 o -6 -5 1 0.84 0.66 1.79 o -5 -5 1 2.52 -0.42 1.76 o -4 -5 1 154.03 130.54 3.20 o -3 -5 1 18.70 13.14 0.50 o -2 -5 1 264.26 223.25 3.48 o -1 -5 1 118.40 107.45 2.29 o 0 -5 1 293.69 247.19 3.47 o 1 -5 1 446.53 418.07 4.87 o 2 -5 1 366.56 375.46 4.94 o 3 -5 1 691.48 727.82 7.96 o 4 -5 1 48.86 46.71 1.68 o 5 -5 1 1165.08 1167.06 12.65 o 6 -5 1 245.35 229.13 5.55 o 7 -5 1 32.35 27.59 1.09 o -7 -4 1 54.65 51.22 2.00 o -6 -4 1 19.40 18.45 0.81 o -5 -4 1 44.54 45.87 1.66 o -4 -4 1 0.02 0.79 0.46 o -3 -4 1 7.62 6.62 0.43 o -2 -4 1 33.61 31.64 0.99 o -1 -4 1 37.07 38.36 1.41 o 0 -4 1 13.43 11.50 0.45 o 1 -4 1 39.44 49.37 1.71 o 2 -4 1 3847.64 4277.29 29.66 o 3 -4 1 63.57 55.15 2.20 o 4 -4 1 336.29 360.16 5.67 o 5 -4 1 9.90 8.43 0.77 o 6 -4 1 211.68 208.04 5.41 o 7 -4 1 79.60 78.73 2.93 o 8 -4 1 450.66 399.11 8.90 o -7 -3 1 13.86 16.82 0.99 o -6 -3 1 380.71 381.21 6.84 o -5 -3 1 11.65 11.29 0.65 o -4 -3 1 873.52 830.83 8.18 o -3 -3 1 478.93 489.80 5.17 o -2 -3 1 931.57 853.03 6.93 o -1 -3 1 0.38 0.72 0.84 o 0 -3 1 39.33 44.47 1.37 o 1 -3 1 606.15 697.64 6.30 o 2 -3 1 1413.30 1526.86 12.10 o 3 -3 1 127.60 148.66 3.30 o 4 -3 1 130.72 175.27 4.03 o 5 -3 1 1081.88 1167.81 12.66 o 6 -3 1 948.75 984.32 12.43 o 7 -3 1 298.85 306.49 7.36 o 8 -3 1 110.22 92.67 3.66 o -8 -2 1 2.35 3.20 1.09 o -7 -2 1 3.67 2.16 1.94 o -6 -2 1 18.86 20.21 0.94 o -5 -2 1 278.35 298.39 5.37 o -4 -2 1 646.97 723.70 7.70 o -3 -2 1 21.08 28.42 1.03 o -2 -2 1 923.00 825.77 6.40 o -1 -2 1 0.75 0.56 0.54 o 0 -2 1 442.63 430.82 3.86 o 1 -2 1 3264.50 3679.08 24.78 o 2 -2 1 65.74 79.77 2.25 o 3 -2 1 43.06 56.65 2.24 o 4 -2 1 746.33 843.59 9.52 o 5 -2 1 5.45 4.76 0.78 o 6 -2 1 28.34 28.95 1.18 o 7 -2 1 583.03 582.73 10.20 o 8 -2 1 544.71 524.10 10.72 o -8 -1 1 21.32 24.93 1.32 o -7 -1 1 0.06 -0.99 1.38 o -6 -1 1 32.33 40.37 1.97 o -5 -1 1 29.66 42.50 1.26 o -4 -1 1 138.47 215.30 3.01 o -3 -1 1 1475.14 1882.74 26.57 o -2 -1 1 60.32 56.72 1.00 o -1 -1 1 2920.46 2427.39 113.31 o 0 -1 1 3302.20 3801.11 142.33 o 1 -1 1 56.50 86.71 2.41 o 2 -1 1 350.86 474.38 3.87 o 3 -1 1 47.80 92.04 2.05 o 4 -1 1 3.45 7.02 0.51 o 5 -1 1 396.87 457.76 8.59 o 6 -1 1 1402.69 1585.95 12.25 o 7 -1 1 1344.68 1433.14 22.24 o 8 -1 1 123.59 125.99 5.81 o -8 0 1 98.99 106.70 2.74 o -7 0 1 9.61 12.10 0.94 o -6 0 1 37.50 51.19 2.40 o -5 0 1 28.92 31.01 1.61 o -4 0 1 82.88 115.19 4.50 o -3 0 1 72.75 107.70 7.13 o -2 0 1 377.11 430.61 16.50 o -1 0 1 127.85 110.62 1.73 o 0 0 1 125.80 125.45 1.40 o 1 0 1 796.71 970.28 5.45 o 2 0 1 69.27 107.85 2.85 o 3 0 1 4.62 4.80 2.38 o 4 0 1 5.48 6.77 0.49 o 5 0 1 488.15 608.76 6.32 o 6 0 1 14.77 18.14 1.82 o 7 0 1 48.57 48.81 4.90 o -8 1 1 27.29 27.64 0.94 o -7 1 1 15.80 17.66 0.76 o -6 1 1 400.04 462.89 11.26 o -5 1 1 1.56 0.85 1.35 o -4 1 1 319.25 355.69 6.04 o -3 1 1 183.37 249.55 2.52 o -2 1 1 2484.44 2323.12 33.86 o -1 1 1 4094.38 2876.99 12.03 o 0 1 1 2848.67 1977.74 8.47 o 1 1 1 754.55 643.14 13.56 o 2 1 1 959.83 1008.90 7.72 o 3 1 1 200.10 203.45 2.56 o 4 1 1 88.18 99.26 2.22 o 5 1 1 579.17 652.46 6.40 o 6 1 1 403.62 414.93 10.29 o 7 1 1 177.04 190.46 4.32 o -8 2 1 29.72 30.86 1.31 o -7 2 1 9.79 11.66 0.91 o -6 2 1 9.77 13.47 0.78 o -5 2 1 573.86 614.93 7.70 o -4 2 1 15.72 16.56 0.67 o -3 2 1 14.88 14.70 0.61 o -2 2 1 3099.95 2483.04 16.06 o -1 2 1 772.20 617.71 4.71 o 0 2 1 0.03 0.40 0.49 o 1 2 1 241.20 170.81 2.25 o 2 2 1 501.70 505.36 5.17 o 3 2 1 1093.72 1193.45 10.62 o 4 2 1 2107.70 2157.76 17.89 o 5 2 1 629.01 671.67 9.04 o 6 2 1 148.39 175.47 5.27 o 7 2 1 14.51 15.01 1.05 o -8 3 1 1.74 1.26 1.50 o -7 3 1 12.34 13.64 0.86 o -6 3 1 7.56 8.10 0.71 o -5 3 1 4.76 8.32 0.60 o -4 3 1 8.19 8.37 0.47 o -3 3 1 78.27 78.56 1.95 o -2 3 1 92.15 99.28 1.89 o -1 3 1 991.04 813.43 6.31 o 0 3 1 63.74 61.32 1.40 o 1 3 1 1882.16 1667.81 11.96 o 2 3 1 596.97 576.92 5.79 o 3 3 1 649.93 615.84 6.77 o 4 3 1 166.62 161.44 3.71 o 5 3 1 67.95 69.58 2.20 o 6 3 1 340.33 338.14 6.89 o -8 4 1 273.15 269.15 6.52 o -7 4 1 54.25 53.57 2.24 o -6 4 1 41.65 38.12 1.44 o -5 4 1 46.99 49.97 1.67 o -4 4 1 36.40 33.25 1.21 o -3 4 1 109.12 114.21 2.41 o -2 4 1 6.65 10.08 0.43 o -1 4 1 128.63 93.60 1.89 o 0 4 1 194.18 158.68 2.44 o 1 4 1 48.12 41.22 1.44 o 2 4 1 37.33 29.35 1.11 o 3 4 1 60.37 57.08 2.08 o 4 4 1 80.38 66.75 1.90 o 5 4 1 327.26 323.03 6.16 o 6 4 1 247.43 254.13 6.02 o -8 5 1 71.09 70.17 2.60 o -7 5 1 92.45 84.42 2.64 o -6 5 1 0.81 -1.18 1.87 o -5 5 1 3.85 0.75 1.62 o -4 5 1 111.07 106.07 2.73 o -3 5 1 38.24 39.94 1.26 o -2 5 1 89.45 80.41 2.07 o -1 5 1 319.43 291.14 3.86 o 0 5 1 3.60 4.35 0.39 o 1 5 1 492.11 433.58 5.11 o 2 5 1 220.05 175.41 3.31 o 3 5 1 66.26 51.23 1.63 o 4 5 1 12.08 13.59 0.69 o 5 5 1 95.21 98.01 3.69 o -8 6 1 1.48 2.10 2.23 o -7 6 1 84.51 77.13 2.55 o -6 6 1 2.39 2.29 1.99 o -5 6 1 151.47 156.72 3.82 o -4 6 1 23.01 21.76 0.84 o -3 6 1 163.63 159.04 3.39 o -2 6 1 13.37 12.83 0.52 o -1 6 1 396.40 357.75 4.80 o 0 6 1 336.62 301.30 4.39 o 1 6 1 699.95 622.76 6.96 o 2 6 1 0.44 0.46 0.56 o 3 6 1 148.06 143.60 3.65 o 4 6 1 0.56 0.77 1.29 o -7 7 1 29.96 27.49 1.10 o -6 7 1 4.90 1.75 2.06 o -5 7 1 63.27 74.77 2.89 o -4 7 1 93.84 89.30 3.01 o -3 7 1 1.82 2.08 0.51 o -2 7 1 15.52 14.34 0.60 o -1 7 1 2.80 2.41 0.53 o 0 7 1 30.55 30.73 1.14 o 1 7 1 15.86 16.50 0.70 o 2 7 1 56.18 57.32 1.90 o 3 7 1 73.43 64.91 2.04 o -6 8 1 22.01 19.32 0.85 o -5 8 1 2.31 2.57 0.63 o -4 8 1 68.05 74.51 3.11 o -3 8 1 0.23 -0.33 1.65 o -2 8 1 2.05 2.60 0.55 o -1 8 1 84.87 91.78 3.10 o 0 8 1 24.97 24.64 0.94 o 1 8 1 0.99 0.53 0.95 o 2 8 1 40.44 44.15 1.58 o -5 9 1 16.50 15.71 0.82 o -4 9 1 20.48 19.77 0.83 o -3 9 1 13.75 15.86 0.78 o -2 9 1 14.68 13.84 0.73 o -1 9 1 76.60 81.38 3.23 o 0 9 1 7.52 9.87 0.72 o 1 9 1 51.29 61.34 2.24 o 0 -10 2 47.39 47.54 1.72 o 1 -10 2 2.87 2.48 0.72 o 2 -10 2 46.46 46.11 1.78 o 3 -10 2 0.05 -2.05 2.06 o -2 -9 2 2.42 1.91 1.94 o -1 -9 2 40.53 40.35 1.50 o 0 -9 2 13.82 13.07 0.75 o 1 -9 2 56.62 60.18 2.05 o 2 -9 2 62.21 58.72 2.17 o 3 -9 2 3.04 3.23 0.72 o 4 -9 2 3.33 4.27 0.73 o 5 -9 2 4.46 4.38 0.82 o -4 -8 2 2.13 2.58 0.64 o -3 -8 2 13.77 14.79 0.71 o -2 -8 2 117.30 118.62 3.52 o -1 -8 2 0.69 -0.57 1.59 o 0 -8 2 31.15 34.54 1.32 o 1 -8 2 61.03 60.07 1.96 o 2 -8 2 16.42 15.49 0.70 o 3 -8 2 138.73 127.34 3.86 o 4 -8 2 35.51 31.48 1.29 o 5 -8 2 10.59 7.32 0.82 o 6 -8 2 2.00 1.56 0.85 o -5 -7 2 126.19 121.56 3.83 o -4 -7 2 3.27 2.93 0.57 o -3 -7 2 1.30 0.90 0.54 o -2 -7 2 115.74 115.95 3.07 o -1 -7 2 75.64 74.55 2.63 o 0 -7 2 16.75 14.91 0.62 o 1 -7 2 1.04 1.15 1.49 o 2 -7 2 53.07 61.33 1.92 o 3 -7 2 42.88 37.07 1.41 o 4 -7 2 133.74 144.28 4.10 o 5 -7 2 0.35 -0.63 2.08 o 6 -7 2 2.69 3.81 0.84 o -6 -6 2 160.20 160.79 4.33 o -5 -6 2 0.01 -0.28 1.55 o -4 -6 2 112.04 98.26 2.89 o -3 -6 2 47.21 41.27 1.44 o -2 -6 2 57.29 51.29 2.10 o -1 -6 2 586.40 551.09 6.30 o 0 -6 2 75.70 71.61 2.30 o 1 -6 2 326.35 329.41 4.88 o 2 -6 2 59.62 68.50 2.56 o 3 -6 2 28.86 33.62 1.32 o 4 -6 2 214.04 202.14 4.71 o 5 -6 2 42.94 42.28 1.75 o 6 -6 2 119.60 123.88 4.53 o 7 -6 2 25.99 23.54 1.13 o -6 -5 2 8.51 6.85 0.65 o -5 -5 2 0.07 0.33 1.47 o -4 -5 2 214.15 191.02 3.65 o -3 -5 2 2.01 1.51 1.28 o -2 -5 2 82.82 77.71 2.18 o -1 -5 2 1324.14 1229.12 10.21 o 0 -5 2 8.50 7.46 0.46 o 1 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232.23 245.11 6.38 o -1 0 9 4.57 4.63 1.12 o 0 0 9 111.85 112.31 2.90 o 1 0 9 77.87 78.26 1.90 o 2 0 9 14.25 12.88 0.68 o -8 1 9 94.67 98.93 2.56 o -7 1 9 106.91 112.50 6.79 o -6 1 9 130.75 124.56 3.48 o -5 1 9 55.79 52.69 3.72 o -4 1 9 153.18 152.49 2.79 o -3 1 9 3.61 2.53 1.35 o -2 1 9 25.73 24.25 1.14 o -1 1 9 154.51 162.05 8.24 o 0 1 9 55.60 52.99 1.44 o 1 1 9 0.60 1.01 1.62 o -7 2 9 216.16 217.92 4.82 o -6 2 9 194.96 178.06 4.26 o -5 2 9 24.44 24.74 1.04 o -4 2 9 238.70 253.24 5.02 o -3 2 9 50.82 47.58 1.90 o -2 2 9 289.16 301.93 6.03 o -1 2 9 0.20 0.45 1.88 o 0 2 9 13.69 13.61 0.85 o 1 2 9 115.98 123.99 4.66 o -7 3 9 158.26 184.22 4.71 o -6 3 9 1.51 0.15 1.59 o -5 3 9 167.23 155.53 4.20 o -4 3 9 94.65 100.95 3.46 o -3 3 9 115.70 137.04 4.06 o -2 3 9 15.30 16.69 0.79 o -1 3 9 50.25 59.49 2.24 o 0 3 9 66.69 61.71 2.46 o -6 4 9 94.50 116.50 3.94 o -5 4 9 149.04 189.09 4.85 o -4 4 9 23.74 26.30 1.09 o -3 4 9 169.61 201.69 5.10 o -2 4 9 123.08 150.06 4.58 o -4 -7 10 277.76 238.03 7.19 o -3 -7 10 8.24 8.33 1.26 o -2 -7 10 124.44 133.96 5.73 o -1 -7 10 215.82 229.50 7.22 o 0 -7 10 46.23 43.95 1.83 o -5 -6 10 124.55 99.72 3.83 o -4 -6 10 117.95 119.13 3.99 o -3 -6 10 23.51 26.76 1.39 o -2 -6 10 287.15 311.95 7.95 o -1 -6 10 66.55 66.59 2.63 o 0 -6 10 234.36 236.93 7.19 o 1 -6 10 817.19 820.42 13.13 o -6 -5 10 3.21 -0.43 3.52 o -5 -5 10 140.40 172.40 6.50 o -4 -5 10 22.06 23.83 1.30 o -3 -5 10 157.26 171.69 6.21 o -2 -5 10 3.02 4.85 0.99 o -1 -5 10 241.38 275.06 7.24 o 0 -5 10 489.62 487.87 9.54 o 1 -5 10 49.46 45.95 1.78 o -6 -4 10 392.42 402.88 9.07 o -5 -4 10 31.28 27.52 1.30 o -4 -4 10 0.15 -1.65 2.99 o -3 -4 10 229.75 242.05 6.43 o -2 -4 10 66.11 71.64 2.95 o -1 -4 10 50.87 46.07 1.91 o 0 -4 10 106.35 95.74 3.33 o 1 -4 10 54.66 57.17 2.46 o -7 -3 10 190.96 149.25 5.55 o -6 -3 10 0.76 1.46 2.82 o -5 -3 10 28.76 26.88 1.18 o -4 -3 10 167.25 177.90 5.59 o -3 -3 10 24.17 25.46 1.10 o -2 -3 10 69.24 71.45 2.97 o -1 -3 10 416.54 444.48 8.53 o 0 -3 10 79.14 86.82 3.01 o 1 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5.53 o -1 -2 11 43.21 42.46 1.79 o 0 -2 11 67.37 73.18 2.92 o -6 -1 11 1.63 -0.92 1.46 o -5 -1 11 16.29 17.49 1.97 o -4 -1 11 35.30 31.37 1.84 o -3 -1 11 42.14 42.19 2.86 o -2 -1 11 1.59 1.72 0.76 o -1 -1 11 1.60 0.60 1.46 o -6 0 11 11.96 13.37 1.05 o -5 0 11 6.36 7.55 0.85 o -4 0 11 0.14 0.23 1.22 o -3 0 11 56.84 65.71 1.83 o -2 0 11 1.36 1.62 0.68 o -1 0 11 119.93 119.30 3.21 o -5 1 11 30.37 31.30 0.92 o -4 1 11 30.91 36.84 1.15 o -3 1 11 65.29 82.51 1.91 o -2 1 11 28.50 34.99 1.08 o -3 -4 12 144.20 146.64 5.59 o -4 -3 12 41.35 36.84 1.53 o -3 -3 12 21.20 19.34 1.16 o -4 -2 12 89.94 79.65 3.08 o -3 -2 12 49.72 42.02 1.63 o