#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/76/2017697.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017697_Fobs loop_ _publ_author_name 'Schindler, Diana' 'Felsmann, Marika' 'Weber, Edwin' _publ_section_title ; Influence of 1,4-dioxane solvent inclusion on the crystal structure of 5,5'-diphenyl-2,2'-(p-phenylene)di-1,3-oxazole (POPOP) ; _journal_coeditor_code EG3047 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o361 _journal_page_last o363 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.977 _cell_angle_gamma 90.000 _cell_length_a 12.2424 _cell_length_b 5.9115 _cell_length_c 18.5046 _exptl_crystal_F_000 572.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file eg3047IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title 'compoundII in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 160.27 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 786.32 795.59 13.00 o 4 0 0 11928.60 11345.68 90.91 o 6 0 0 303.42 306.86 6.04 o 8 0 0 1430.89 1387.29 15.57 o 10 0 0 108.88 105.28 5.32 o 12 0 0 298.50 284.49 7.91 o 14 0 0 29.06 25.28 5.01 o 1 1 0 36.67 44.74 1.21 o 2 1 0 3984.81 3781.31 34.85 o 3 1 0 2916.18 2739.39 15.25 o 4 1 0 10.11 8.98 1.26 o 5 1 0 127.45 131.98 2.93 o 6 1 0 1032.32 1062.07 7.96 o 7 1 0 24.23 25.32 1.87 o 8 1 0 60.74 61.46 2.43 o 9 1 0 84.32 85.58 2.89 o 10 1 0 610.35 579.17 7.03 o 11 1 0 44.41 41.87 3.13 o 12 1 0 16.50 14.93 3.00 o 13 1 0 48.53 53.50 3.97 o 14 1 0 42.87 49.45 3.88 o 0 2 0 222.63 220.69 6.07 o 1 2 0 1129.61 1158.66 11.73 o 2 2 0 609.39 610.78 6.66 o 3 2 0 2540.92 2649.28 14.55 o 4 2 0 1793.23 1922.60 11.53 o 5 2 0 542.55 494.68 4.61 o 6 2 0 134.98 143.93 2.69 o 7 2 0 486.91 481.23 4.89 o 8 2 0 0.04 0.00 1.72 o 9 2 0 62.65 52.24 2.50 o 10 2 0 98.19 107.40 3.35 o 11 2 0 0.37 0.00 2.24 o 12 2 0 3.40 0.00 2.70 o 13 2 0 146.37 157.39 5.04 o 1 3 0 0.63 0.22 2.33 o 2 3 0 10.60 8.69 1.70 o 3 3 0 12.64 19.13 1.48 o 4 3 0 184.54 188.57 2.38 o 5 3 0 4.84 4.01 1.32 o 6 3 0 366.19 365.10 3.99 o 7 3 0 35.77 40.06 2.07 o 8 3 0 141.10 145.41 3.54 o 9 3 0 30.25 31.82 2.64 o 10 3 0 161.48 156.19 4.20 o 11 3 0 38.29 40.09 3.34 o 12 3 0 0.96 0.79 2.77 o 13 3 0 6.55 8.33 3.03 o 0 4 0 1109.76 1123.08 24.86 o 1 4 0 13.30 9.74 3.12 o 2 4 0 57.00 64.05 5.69 o 3 4 0 35.09 36.81 2.97 o 4 4 0 58.27 74.43 1.96 o 5 4 0 13.70 12.39 1.70 o 6 4 0 136.53 142.74 3.08 o 7 4 0 93.91 91.29 2.46 o 8 4 0 11.07 2.32 1.85 o 9 4 0 99.38 108.48 3.53 o 10 4 0 70.20 71.94 3.40 o 11 4 0 46.15 41.82 3.35 o 1 5 0 431.80 412.53 13.05 o 2 5 0 95.21 99.88 7.00 o 3 5 0 1784.86 1739.84 17.41 o 4 5 0 440.73 437.55 7.74 o 5 5 0 1027.78 996.55 12.08 o 6 5 0 267.90 241.57 7.18 o 7 5 0 22.52 33.33 4.18 o 8 5 0 173.04 166.64 5.22 o 9 5 0 12.77 14.26 3.09 o 10 5 0 12.53 13.33 2.68 o 0 6 0 401.52 426.57 17.45 o 1 6 0 633.63 622.91 14.88 o 2 6 0 18.39 28.30 5.47 o 3 6 0 24.04 24.51 3.00 o 4 6 0 29.49 26.98 3.37 o 5 6 0 27.08 30.04 3.84 o 6 6 0 0.18 2.46 3.36 o 7 6 0 73.28 82.77 6.37 o 1 7 0 44.86 40.41 6.65 o -13 0 1 8.25 14.37 4.47 o -11 0 1 949.37 963.23 13.77 o -9 0 1 490.89 495.35 8.65 o -7 0 1 696.80 713.08 9.45 o -5 0 1 66.08 66.61 2.95 o -3 0 1 24757.78 24382.95 234.23 o 3 0 1 1285.36 1182.65 11.35 o 5 0 1 119.61 97.15 4.49 o 7 0 1 282.16 245.42 6.85 o 9 0 1 4.98 2.88 3.67 o 11 0 1 667.32 679.37 11.36 o 13 0 1 130.60 146.37 6.81 o -14 1 1 190.25 213.67 5.68 o -13 1 1 52.29 55.59 3.69 o -12 1 1 139.33 147.76 4.74 o -11 1 1 24.28 22.92 2.88 o -10 1 1 57.63 50.36 3.12 o -9 1 1 434.93 452.53 5.48 o -8 1 1 281.43 306.50 4.27 o -7 1 1 51.10 44.18 2.11 o -6 1 1 197.21 204.08 3.17 o -5 1 1 21.32 18.51 1.52 o -4 1 1 196.20 198.03 2.70 o -3 1 1 460.18 470.83 3.85 o -2 1 1 13.26 10.54 1.97 o -1 1 1 569.25 533.93 5.07 o 0 1 1 75.21 68.09 1.92 o 1 1 1 32.35 37.83 1.08 o 2 1 1 4952.09 4735.94 29.92 o 3 1 1 941.70 862.23 5.71 o 4 1 1 30.75 25.64 1.41 o 5 1 1 291.87 304.81 3.51 o 6 1 1 748.82 732.88 6.19 o 7 1 1 63.82 65.89 2.26 o 8 1 1 9.93 4.64 1.80 o 9 1 1 0.65 0.00 2.20 o 10 1 1 45.42 44.45 3.03 o 11 1 1 486.47 494.23 6.80 o 12 1 1 0.73 0.00 2.64 o 13 1 1 33.11 37.55 3.53 o 14 1 1 0.00 0.00 3.10 o -13 2 1 18.43 20.08 3.28 o -12 2 1 251.30 260.82 5.69 o -11 2 1 15.03 9.25 2.52 o -10 2 1 21.05 19.27 2.23 o -9 2 1 53.99 49.35 2.50 o -8 2 1 1325.20 1297.92 9.58 o -7 2 1 3.94 7.36 1.64 o -6 2 1 256.12 244.54 3.40 o -5 2 1 0.33 0.00 1.03 o -4 2 1 2109.44 2220.72 16.69 o -3 2 1 863.25 925.11 6.15 o -2 2 1 33.80 36.67 2.17 o -1 2 1 877.01 866.55 9.35 o 0 2 1 56.34 64.15 2.66 o 1 2 1 7.76 8.14 1.89 o 2 2 1 147.18 149.94 2.10 o 3 2 1 8.39 4.36 0.98 o 4 2 1 95.70 113.22 2.10 o 5 2 1 1906.37 1985.62 12.72 o 6 2 1 106.82 112.77 2.46 o 7 2 1 321.46 320.69 4.01 o 8 2 1 434.91 429.20 5.09 o 9 2 1 174.62 164.17 3.68 o 10 2 1 148.47 162.34 4.02 o 11 2 1 4.96 3.46 2.38 o 12 2 1 165.69 173.11 5.30 o 13 2 1 68.30 70.48 4.80 o -13 3 1 46.19 37.50 3.68 o -12 3 1 56.28 63.66 4.26 o -11 3 1 66.64 54.85 3.78 o -10 3 1 30.98 36.37 3.52 o -9 3 1 276.88 278.76 4.90 o -8 3 1 103.73 103.67 3.19 o -7 3 1 119.21 129.90 2.85 o -6 3 1 104.11 120.87 2.54 o -5 3 1 42.18 42.82 1.70 o -4 3 1 67.63 65.38 1.85 o -3 3 1 17.68 19.55 1.60 o -2 3 1 288.25 314.21 4.26 o -1 3 1 228.43 226.57 4.93 o 0 3 1 1052.54 1034.64 13.36 o 1 3 1 520.03 556.79 8.96 o 2 3 1 15.79 23.71 1.98 o 3 3 1 223.98 213.45 2.80 o 4 3 1 27.31 24.15 1.44 o 5 3 1 20.07 25.21 1.49 o 6 3 1 175.66 183.62 2.91 o 7 3 1 83.52 89.31 3.26 o 8 3 1 15.08 10.66 2.14 o 9 3 1 130.53 138.40 3.64 o 10 3 1 244.74 227.92 4.92 o 11 3 1 2.10 0.00 2.43 o 12 3 1 0.69 0.00 2.68 o -11 4 1 39.60 48.94 3.41 o -10 4 1 0.46 0.00 2.28 o -9 4 1 1.49 0.00 2.46 o -8 4 1 259.53 255.60 4.23 o -7 4 1 0.00 0.00 1.49 o -6 4 1 25.99 29.83 2.04 o -5 4 1 0.04 0.00 1.45 o -4 4 1 265.99 277.77 5.08 o -3 4 1 764.02 771.77 7.07 o -2 4 1 0.12 0.00 2.27 o -1 4 1 312.68 319.41 7.67 o 0 4 1 64.86 73.05 4.32 o 1 4 1 475.38 448.76 8.99 o 2 4 1 85.57 87.41 4.22 o 3 4 1 2.67 2.33 1.52 o 4 4 1 77.81 88.92 2.18 o 5 4 1 833.79 823.17 6.97 o 6 4 1 61.80 55.03 2.02 o 7 4 1 133.85 130.61 2.91 o 8 4 1 4.52 0.00 1.96 o 9 4 1 135.81 158.48 3.92 o 10 4 1 0.39 1.72 2.41 o 11 4 1 31.21 29.01 3.02 o -10 5 1 231.04 231.45 5.04 o -9 5 1 56.48 58.39 3.88 o -8 5 1 65.55 71.13 4.06 o -7 5 1 18.80 20.24 3.40 o -6 5 1 647.88 619.38 9.38 o -5 5 1 0.05 0.00 2.52 o -4 5 1 41.00 42.40 2.97 o -3 5 1 297.07 304.31 5.79 o -2 5 1 77.85 81.86 5.29 o -1 5 1 10.01 9.70 4.34 o 0 5 1 946.83 925.81 17.01 o 1 5 1 137.67 151.98 6.56 o 2 5 1 177.89 178.25 5.08 o 3 5 1 920.72 905.60 12.46 o 4 5 1 27.97 28.10 3.09 o 5 5 1 32.60 29.40 3.26 o 6 5 1 158.17 171.94 5.69 o 7 5 1 103.87 113.12 4.83 o 8 5 1 163.45 174.99 5.35 o 9 5 1 134.12 128.04 4.55 o 10 5 1 22.30 30.30 3.90 o -7 6 1 0.00 2.34 3.32 o -6 6 1 43.00 50.78 5.99 o -5 6 1 3.63 1.81 4.29 o -4 6 1 1.32 4.73 2.85 o -3 6 1 30.24 24.58 3.18 o -2 6 1 178.34 184.20 8.81 o -1 6 1 84.79 98.40 7.26 o 0 6 1 79.78 95.40 7.09 o 1 6 1 465.58 469.54 12.91 o 2 6 1 8.48 3.80 2.98 o 3 6 1 48.76 45.37 3.41 o 4 6 1 1.73 1.06 2.98 o 5 6 1 63.68 69.59 4.89 o 6 6 1 37.75 43.60 4.30 o 7 6 1 3.34 0.00 4.99 o -1 7 1 15.16 20.41 6.20 o 0 7 1 8.68 1.22 5.41 o 1 7 1 9.62 15.42 5.85 o -14 0 2 30.41 38.33 5.28 o -12 0 2 37.95 32.49 4.55 o -10 0 2 16.89 12.50 4.84 o -8 0 2 106.57 94.25 4.30 o -6 0 2 1005.81 1007.59 11.37 o -4 0 2 13.22 2.72 3.01 o -2 0 2 4547.19 4401.54 87.69 o 2 0 2 25686.70 24148.98 231.36 o 4 0 2 386.79 374.59 5.59 o 6 0 2 7172.70 6891.93 62.94 o 8 0 2 56.39 51.85 3.73 o 10 0 2 1173.58 1157.99 15.05 o 12 0 2 444.89 448.49 9.71 o 14 0 2 26.50 24.64 4.60 o -14 1 2 60.15 74.17 4.18 o -13 1 2 134.57 147.81 4.79 o -12 1 2 31.88 31.00 3.17 o -11 1 2 871.15 869.24 11.87 o -10 1 2 210.02 205.95 4.18 o -9 1 2 195.38 200.52 3.90 o -8 1 2 4.54 2.99 1.85 o -7 1 2 2114.74 2134.89 14.73 o -6 1 2 395.10 407.92 4.64 o -5 1 2 207.43 207.45 3.20 o -4 1 2 559.66 557.97 5.58 o -3 1 2 2876.06 2873.39 18.89 o -2 1 2 396.27 378.36 4.72 o -1 1 2 2528.46 2467.10 21.15 o 0 1 2 1015.85 938.39 8.72 o 1 1 2 5791.58 5477.87 45.31 o 2 1 2 39.63 31.74 1.31 o 3 1 2 752.81 770.66 5.32 o 4 1 2 789.62 756.46 5.49 o 5 1 2 537.28 541.80 4.58 o 6 1 2 96.25 105.33 2.48 o 7 1 2 121.38 127.02 3.10 o 8 1 2 122.30 126.21 3.38 o 9 1 2 334.28 333.25 5.22 o 10 1 2 0.32 0.00 2.41 o 11 1 2 21.64 20.16 2.78 o 12 1 2 56.19 46.31 3.48 o 13 1 2 51.82 54.70 3.66 o 14 1 2 0.93 0.00 2.80 o -13 2 2 144.07 149.80 5.60 o -12 2 2 30.38 32.03 4.11 o -11 2 2 217.89 212.06 4.69 o -10 2 2 38.22 46.04 2.54 o -9 2 2 811.34 776.70 7.13 o -8 2 2 6.14 1.38 1.75 o -7 2 2 412.32 376.44 4.30 o -6 2 2 96.38 103.54 2.70 o -5 2 2 1198.21 1238.79 9.43 o -4 2 2 175.79 172.84 2.53 o -3 2 2 909.69 872.05 6.18 o -2 2 2 0.18 0.53 1.19 o -1 2 2 557.08 573.26 6.97 o 0 2 2 94.28 83.95 2.37 o 1 2 2 985.67 992.36 10.31 o 2 2 2 209.60 228.21 2.39 o 3 2 2 237.79 225.75 2.33 o 4 2 2 410.63 448.86 3.95 o 5 2 2 195.83 199.79 2.74 o 6 2 2 662.28 698.50 5.23 o 7 2 2 0.40 1.56 1.39 o 8 2 2 41.87 48.95 2.33 o 9 2 2 760.45 741.36 6.99 o 10 2 2 90.37 80.30 3.06 o 11 2 2 74.44 79.37 3.41 o 12 2 2 66.44 63.32 3.62 o 13 2 2 0.23 2.09 2.63 o -13 3 2 146.12 165.57 5.40 o -12 3 2 83.33 115.24 4.54 o -11 3 2 74.23 75.74 3.81 o -10 3 2 219.40 225.94 4.80 o -9 3 2 519.57 504.74 6.43 o -8 3 2 54.78 56.92 2.69 o -7 3 2 9.46 10.37 1.77 o -6 3 2 214.21 221.71 3.36 o -5 3 2 474.29 453.61 4.36 o -4 3 2 784.15 804.71 6.21 o -3 3 2 1292.86 1381.77 10.18 o -2 3 2 0.59 0.18 1.29 o -1 3 2 278.38 310.85 5.40 o 0 3 2 603.51 612.29 9.51 o 1 3 2 1253.87 1349.01 16.93 o 2 3 2 664.65 670.48 6.46 o 3 3 2 442.11 480.53 4.41 o 4 3 2 88.27 100.40 1.83 o 5 3 2 10.33 9.91 1.32 o 6 3 2 129.08 126.04 2.83 o 7 3 2 191.54 186.24 3.32 o 8 3 2 0.12 0.00 1.81 o 9 3 2 9.32 10.94 2.21 o 10 3 2 130.33 119.38 3.95 o 11 3 2 113.51 110.88 3.97 o 12 3 2 4.92 3.46 2.68 o -11 4 2 78.11 78.30 3.74 o -10 4 2 71.44 76.62 3.94 o -9 4 2 208.41 194.44 4.19 o -8 4 2 191.67 179.62 3.81 o -7 4 2 62.73 61.15 2.46 o -6 4 2 33.90 40.43 2.39 o -5 4 2 8.51 7.72 1.85 o -4 4 2 73.96 73.90 2.32 o -3 4 2 1282.78 1335.72 10.10 o -2 4 2 310.61 292.52 5.16 o -1 4 2 269.24 262.74 8.05 o 0 4 2 3.00 4.63 2.92 o 1 4 2 70.49 61.79 3.69 o 2 4 2 373.45 376.98 5.70 o 3 4 2 0.97 0.00 1.43 o 4 4 2 10.95 8.43 1.93 o 5 4 2 6.07 6.43 1.73 o 6 4 2 168.94 170.76 3.16 o 7 4 2 97.97 107.39 2.68 o 8 4 2 173.16 162.93 3.60 o 9 4 2 78.25 76.12 3.05 o 10 4 2 29.64 37.88 3.00 o 11 4 2 26.61 39.82 3.22 o -10 5 2 11.90 15.78 3.45 o -9 5 2 47.74 65.14 7.13 o -8 5 2 12.32 12.77 3.43 o -7 5 2 76.74 67.21 4.20 o -6 5 2 18.43 17.95 3.21 o -5 5 2 0.20 0.00 2.47 o -4 5 2 198.70 194.35 4.66 o -3 5 2 893.83 870.67 9.70 o -2 5 2 400.43 400.96 8.13 o -1 5 2 103.85 93.74 7.36 o 0 5 2 1471.25 1452.27 22.70 o 1 5 2 183.64 173.99 4.98 o 2 5 2 201.04 210.21 5.68 o 3 5 2 320.73 320.66 7.05 o 4 5 2 105.90 109.43 4.86 o 5 5 2 277.24 279.94 6.74 o 6 5 2 37.01 40.82 3.71 o 7 5 2 437.68 415.31 7.30 o 8 5 2 44.80 50.58 3.85 o 9 5 2 1.93 1.27 2.81 o -7 6 2 4.22 3.23 3.64 o -6 6 2 1.29 3.26 3.43 o -5 6 2 40.83 36.57 3.88 o -4 6 2 117.34 123.87 4.94 o -3 6 2 81.21 79.25 3.97 o -2 6 2 5.80 12.23 3.63 o -1 6 2 10.64 7.74 4.78 o 0 6 2 23.87 24.57 7.86 o 1 6 2 492.70 512.46 13.39 o 2 6 2 71.80 76.35 7.00 o 3 6 2 33.41 25.53 4.26 o 4 6 2 96.84 93.67 4.42 o 5 6 2 72.23 65.89 4.79 o 6 6 2 3.03 4.88 3.46 o 7 6 2 8.00 8.90 3.88 o 0 7 2 21.38 22.80 6.32 o -13 0 3 367.58 372.48 9.67 o -11 0 3 23.83 24.82 4.12 o -9 0 3 42.05 40.24 3.87 o -7 0 3 110.72 106.28 4.03 o -5 0 3 1366.20 1354.87 14.96 o -3 0 3 1484.28 1426.27 16.31 o -1 0 3 77.54 72.94 4.76 o 1 0 3 573.01 536.55 9.97 o 3 0 3 5444.71 5132.04 56.85 o 5 0 3 436.92 440.67 7.10 o 7 0 3 1037.23 976.54 11.93 o 9 0 3 102.00 97.52 4.87 o 11 0 3 207.05 197.81 7.04 o 13 0 3 60.98 72.83 5.32 o -14 1 3 171.26 180.30 5.37 o -13 1 3 22.84 25.60 3.36 o -12 1 3 62.20 68.56 4.35 o -11 1 3 36.88 30.91 3.02 o -10 1 3 202.66 206.36 4.22 o -9 1 3 71.54 77.82 3.10 o -8 1 3 339.88 312.79 4.67 o -7 1 3 4.16 3.25 1.86 o -6 1 3 999.24 1053.33 8.70 o -5 1 3 209.17 216.56 3.37 o -4 1 3 1092.27 1068.65 8.35 o -3 1 3 4563.21 4578.74 30.90 o -2 1 3 16754.83 16308.31 118.56 o -1 1 3 268.59 297.62 9.86 o 0 1 3 1347.44 1355.88 13.35 o 1 1 3 1986.04 1856.46 12.53 o 2 1 3 462.66 382.07 3.04 o 3 1 3 4.71 0.01 1.01 o 4 1 3 99.52 101.31 1.89 o 5 1 3 3.12 0.00 1.29 o 6 1 3 3.19 0.00 1.44 o 7 1 3 297.15 294.29 4.23 o 8 1 3 217.96 226.18 5.62 o 9 1 3 564.59 550.59 7.74 o 10 1 3 4.61 3.00 2.35 o 11 1 3 2.70 2.58 2.41 o 12 1 3 0.01 0.00 2.49 o 13 1 3 0.07 0.00 2.71 o -13 2 3 34.95 37.77 3.57 o -12 2 3 319.01 323.76 6.11 o -11 2 3 26.12 21.96 2.71 o -10 2 3 441.57 430.20 5.40 o -9 2 3 0.00 0.00 1.91 o -8 2 3 0.40 0.00 1.71 o -7 2 3 26.57 19.72 1.87 o -6 2 3 2518.35 2414.92 15.95 o -5 2 3 240.39 251.47 3.60 o -4 2 3 238.57 270.15 3.97 o -3 2 3 243.16 227.01 2.73 o -2 2 3 3987.03 3994.10 24.68 o -1 2 3 741.92 729.20 6.01 o 0 2 3 1504.51 1537.25 12.35 o 1 2 3 12.84 14.67 1.50 o 2 2 3 91.77 87.50 1.64 o 3 2 3 3.56 0.00 0.94 o 4 2 3 18.44 18.72 1.28 o 5 2 3 663.15 701.35 5.46 o 6 2 3 4.21 2.07 1.27 o 7 2 3 415.13 423.76 4.04 o 8 2 3 126.34 133.14 2.80 o 9 2 3 226.30 212.80 3.92 o 10 2 3 47.40 45.88 2.73 o 11 2 3 53.17 47.08 2.95 o 12 2 3 88.94 91.74 3.93 o 13 2 3 0.11 0.00 2.87 o -13 3 3 23.44 25.42 3.55 o -12 3 3 69.86 65.85 3.91 o -11 3 3 41.20 32.00 3.00 o -10 3 3 65.68 68.77 3.66 o -9 3 3 53.15 43.36 2.71 o -8 3 3 0.41 0.00 1.94 o -7 3 3 414.02 422.83 5.25 o -6 3 3 1056.28 1049.64 8.18 o -5 3 3 0.32 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