#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:18:13 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180846 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/77/2017706.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017706_Fobs loop_ _publ_author_name 'Quiroz-Guzman, Mauricio' 'Brown, Seth N.' _publ_section_title ; Tris(4-bromophenyl)aminium hexachloridoantimonate (`Magic Blue'): a strong oxidant with low inner-sphere reorganization ; _journal_coeditor_code FN3059 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m171 _journal_page_last m173 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.534 _cell_angle_gamma 90.000 _cell_length_a 9.3970 _cell_length_b 16.0352 _cell_length_c 11.3688 _exptl_crystal_F_000 928.00 _reflns_d_resolution_high 0.7969 _cod_data_source_file fn3059IIsup3.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' mqg011 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 442.94 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 186.97 155.91 12.93 o 2 0 0 30938.80 32064.02 314.83 o 3 0 0 322.63 329.84 20.41 o 4 0 0 809.15 824.08 40.59 o 5 0 0 2853.89 2839.52 72.51 o 6 0 0 1024.41 1138.44 37.55 o 7 0 0 28243.98 27036.69 1381.56 o 8 0 0 286.18 392.62 82.20 o 9 0 0 21775.66 21390.76 621.56 o 10 0 0 976.67 1088.79 134.00 o 11 0 0 379.16 444.27 125.62 o 1 1 0 257.43 235.36 7.22 o 2 1 0 8572.11 9180.31 76.36 o 3 1 0 2299.83 2111.79 35.35 o 4 1 0 2241.97 2251.52 40.45 o 5 1 0 763.01 618.20 26.16 o 6 1 0 6095.41 6217.94 107.24 o 7 1 0 26.34 59.00 29.32 o 8 1 0 446.34 351.69 77.10 o 9 1 0 1438.37 1226.94 90.57 o 10 1 0 2.60 -11.26 59.96 o 11 1 0 1504.84 1516.77 134.99 o 0 2 0 59.75 62.84 19.44 o 1 2 0 112.46 102.22 13.46 o 2 2 0 1541.30 1475.92 28.31 o 3 2 0 32066.65 32140.99 244.26 o 4 2 0 34713.38 34167.96 279.79 o 5 2 0 27918.19 27873.09 236.29 o 6 2 0 16614.90 16395.15 188.21 o 7 2 0 824.61 864.89 49.89 o 8 2 0 19.81 79.03 49.00 o 9 2 0 155.56 76.50 66.47 o 10 2 0 301.47 381.70 86.77 o 11 2 0 1146.55 1164.81 120.76 o 1 3 0 18364.21 19474.63 313.22 o 2 3 0 819.14 795.61 42.39 o 3 3 0 3807.29 3863.90 60.31 o 4 3 0 1878.78 1757.26 33.38 o 5 3 0 5324.56 5298.38 77.68 o 6 3 0 22.94 48.57 19.57 o 7 3 0 4720.42 4705.49 112.41 o 8 3 0 476.80 415.00 50.27 o 9 3 0 2.95 -6.75 61.08 o 10 3 0 1377.72 1520.45 121.84 o 11 3 0 45.11 185.58 89.78 o 0 4 0 231.21 265.12 62.84 o 1 4 0 196194.81 196384.06 4184.94 o 2 4 0 262.61 226.97 24.63 o 3 4 0 2068.33 2102.70 49.42 o 4 4 0 156.90 171.28 20.01 o 5 4 0 1243.88 1304.12 34.74 o 6 4 0 11924.19 11596.26 138.86 o 7 4 0 640.86 645.81 56.63 o 8 4 0 24325.69 24340.14 347.84 o 9 4 0 2827.03 2629.25 141.20 o 10 4 0 6931.99 6701.50 219.20 o 11 4 0 346.34 239.17 89.78 o 1 5 0 6734.51 7090.59 332.87 o 2 5 0 2710.39 2722.01 62.34 o 3 5 0 5580.70 5543.47 97.32 o 4 5 0 955.49 955.66 40.18 o 5 5 0 385.89 367.68 26.41 o 6 5 0 828.37 818.90 44.42 o 7 5 0 2061.11 2088.72 63.04 o 8 5 0 357.94 336.84 55.01 o 9 5 0 2.00 116.52 69.76 o 10 5 0 2566.66 2591.59 190.23 o 0 6 0 444.42 408.48 76.59 o 1 6 0 360.15 312.09 50.56 o 2 6 0 12062.39 11363.28 159.08 o 3 6 0 7888.34 7563.04 148.53 o 4 6 0 21386.26 21484.01 307.38 o 5 6 0 24331.40 23730.44 268.19 o 6 6 0 6199.12 6231.09 136.34 o 7 6 0 1886.36 1835.39 71.42 o 8 6 0 877.02 789.67 78.18 o 9 6 0 12.36 11.54 107.03 o 10 6 0 18.60 147.61 102.73 o 1 7 0 718.91 590.22 95.25 o 2 7 0 2049.70 1993.80 59.35 o 3 7 0 6017.27 6076.90 110.09 o 4 7 0 6742.93 6426.25 145.29 o 5 7 0 362.70 435.57 40.99 o 6 7 0 9022.37 8680.85 158.29 o 7 7 0 160.12 108.73 40.86 o 8 7 0 26.43 50.59 57.54 o 9 7 0 231.12 269.47 70.85 o 10 7 0 114.66 108.61 96.66 o 0 8 0 90482.00 91925.41 2071.85 o 1 8 0 857.08 700.53 125.69 o 2 8 0 17973.24 17449.29 234.64 o 3 8 0 208.62 203.14 31.61 o 4 8 0 588.72 604.77 44.29 o 5 8 0 1089.86 1183.82 59.86 o 6 8 0 920.51 840.07 60.79 o 7 8 0 13901.81 14348.53 256.41 o 8 8 0 1467.96 1701.01 186.62 o 9 8 0 9216.02 9264.61 322.90 o 10 8 0 1557.48 1657.00 237.62 o 1 9 0 91.92 122.80 54.84 o 2 9 0 5065.93 4660.84 122.91 o 3 9 0 575.74 628.63 59.87 o 4 9 0 1321.55 1355.96 62.25 o 5 9 0 1489.33 1601.62 79.40 o 6 9 0 133.23 100.41 79.68 o 7 9 0 92.05 107.57 45.34 o 8 9 0 14.24 -42.91 61.56 o 9 9 0 1311.22 1319.45 109.52 o 10 9 0 53.04 54.43 100.10 o 0 10 0 1760.30 1816.55 170.85 o 1 10 0 1123.64 1355.53 105.54 o 2 10 0 5.55 -2.23 37.18 o 3 10 0 12954.51 12640.98 194.27 o 4 10 0 14814.65 14402.24 218.14 o 5 10 0 7411.00 7551.81 152.46 o 6 10 0 3040.19 3234.25 122.53 o 7 10 0 251.58 152.20 50.64 o 8 10 0 154.96 91.06 66.19 o 9 10 0 669.27 475.78 89.55 o 1 11 0 395.43 332.65 74.83 o 2 11 0 3224.82 3331.99 113.95 o 3 11 0 1532.14 1449.63 66.37 o 4 11 0 5150.76 5213.10 120.75 o 5 11 0 8278.91 7896.11 153.92 o 6 11 0 48.15 15.88 55.47 o 7 11 0 336.88 378.22 68.60 o 8 11 0 319.35 224.24 78.84 o 9 11 0 208.11 327.49 86.09 o 0 12 0 945.63 742.33 133.54 o 1 12 0 15658.07 15443.66 360.76 o 2 12 0 27.12 21.04 45.12 o 3 12 0 415.05 419.06 44.99 o 4 12 0 85.89 132.31 39.59 o 5 12 0 1524.52 1209.08 121.35 o 6 12 0 2212.06 2234.16 159.99 o 7 12 0 135.61 123.72 97.21 o 8 12 0 5262.17 5546.41 233.63 o 9 12 0 2263.89 2560.06 190.52 o 1 13 0 271.87 188.41 53.05 o 2 13 0 49.90 -46.29 46.29 o 3 13 0 1650.62 1696.78 102.69 o 4 13 0 750.64 607.91 74.30 o 5 13 0 937.02 896.65 168.89 o 6 13 0 437.97 369.62 97.30 o 7 13 0 657.84 673.00 85.86 o 8 13 0 113.81 -20.14 74.60 o 0 14 0 160.55 200.31 109.98 o 1 14 0 713.98 598.74 71.12 o 2 14 0 1674.20 1674.01 116.84 o 3 14 0 627.67 776.14 122.30 o 4 14 0 4722.44 4775.96 157.46 o 5 14 0 4700.46 5014.62 260.21 o 6 14 0 194.72 250.53 101.72 o 7 14 0 302.24 372.51 81.95 o 8 14 0 561.09 575.85 102.01 o 1 15 0 2028.23 2172.33 121.81 o 2 15 0 104.67 116.93 62.28 o 3 15 0 3891.46 3796.63 149.14 o 4 15 0 2205.91 2107.41 122.95 o 5 15 0 1153.27 1114.90 127.66 o 6 15 0 1995.40 1890.14 234.68 o 7 15 0 24.91 -27.94 70.62 o 0 16 0 3105.59 3091.09 272.97 o 1 16 0 337.62 460.58 72.62 o 2 16 0 2248.92 2346.71 148.10 o 3 16 0 241.36 280.86 81.92 o 4 16 0 268.18 234.34 99.17 o 5 16 0 82.41 19.64 157.11 o 6 16 0 731.91 665.81 124.95 o 1 17 0 257.94 349.90 100.92 o 2 17 0 1012.79 743.25 165.94 o 3 17 0 11.95 113.66 119.79 o 4 17 0 228.81 165.58 92.26 o 5 17 0 693.27 436.18 111.26 o 0 18 0 1615.21 1492.52 219.95 o 1 18 0 52.60 -49.78 91.40 o 2 18 0 53.13 208.55 104.08 o 3 18 0 621.23 747.37 265.12 o 4 18 0 1360.99 1461.10 233.70 o 1 19 0 36.70 78.10 101.34 o 2 19 0 1786.76 1878.94 173.16 o 3 19 0 182.39 182.99 108.29 o 0 20 0 343.67 508.63 180.67 o -11 1 1 1562.71 1476.36 131.34 o -10 1 1 120.84 66.64 76.57 o -9 1 1 966.47 947.16 80.83 o -8 1 1 1518.65 1551.17 67.34 o -7 1 1 12364.59 12324.11 169.21 o -6 1 1 36.92 36.87 13.85 o -5 1 1 899.90 941.29 24.48 o -4 1 1 10399.91 10235.55 87.58 o -3 1 1 8141.83 7846.95 68.31 o -2 1 1 2223.97 2548.45 31.23 o -1 1 1 41.42 19.70 6.83 o 0 1 1 9269.10 9251.71 68.62 o 1 1 1 2040.93 2062.88 21.56 o 2 1 1 18488.12 18258.73 193.04 o 3 1 1 2684.23 2986.70 52.75 o 4 1 1 4941.81 5299.54 74.80 o 5 1 1 4339.90 4479.24 67.26 o 6 1 1 7784.55 7411.95 150.55 o 7 1 1 384.05 485.30 56.78 o 8 1 1 85.20 38.28 50.75 o 9 1 1 4009.53 4027.53 177.44 o 10 1 1 813.42 833.91 90.02 o -11 2 1 1064.98 1023.45 117.09 o -10 2 1 321.83 365.45 83.94 o -9 2 1 54.62 22.78 60.38 o -8 2 1 186.15 145.22 45.07 o -7 2 1 199.66 214.40 30.71 o -6 2 1 17.55 24.35 14.11 o -5 2 1 3492.86 3329.13 45.24 o -4 2 1 8208.92 8289.82 79.09 o -3 2 1 15712.37 16046.36 131.46 o -2 2 1 1224.86 1128.64 24.99 o -1 2 1 44.44 34.29 9.41 o 0 2 1 561.69 496.37 15.10 o 1 2 1 9255.12 9929.38 93.32 o 2 2 1 17852.21 18653.31 165.19 o 3 2 1 5841.47 5925.20 69.84 o 4 2 1 11571.60 11325.77 131.88 o 5 2 1 1504.27 1313.77 53.13 o 6 2 1 1044.26 987.69 66.76 o 7 2 1 100.54 59.60 29.12 o 8 2 1 2015.82 1903.63 98.68 o 9 2 1 3535.56 3141.52 133.61 o 10 2 1 267.89 161.90 80.94 o -11 3 1 1069.51 970.79 114.93 o -10 3 1 373.16 444.64 87.00 o -9 3 1 1.33 88.17 62.21 o -8 3 1 1763.47 1752.07 82.69 o -7 3 1 794.73 831.77 64.73 o -6 3 1 3876.46 3919.06 72.93 o -5 3 1 3777.54 3774.77 53.71 o -4 3 1 5114.73 5294.37 64.28 o -3 3 1 7082.57 7207.80 75.63 o -2 3 1 16109.03 16949.24 144.24 o -1 3 1 2998.09 3006.47 59.81 o 0 3 1 4671.80 4768.00 62.44 o 1 3 1 3060.15 2687.25 49.49 o 2 3 1 1206.74 1226.83 36.80 o 3 3 1 433.13 446.44 23.22 o 4 3 1 5046.11 5235.42 59.59 o 5 3 1 12581.51 12401.16 161.79 o 6 3 1 1103.41 1242.83 55.94 o 7 3 1 1983.70 1849.74 111.57 o 8 3 1 1994.74 2040.94 121.23 o 9 3 1 1205.93 1180.30 109.08 o 10 3 1 1555.44 1435.98 123.76 o -11 4 1 154.81 63.73 164.58 o -10 4 1 33.74 -67.65 67.65 o -9 4 1 24.44 7.61 48.30 o -8 4 1 23.56 -28.04 45.35 o -7 4 1 368.41 386.08 37.25 o -6 4 1 399.45 399.76 28.91 o -5 4 1 1553.80 1590.19 39.02 o -4 4 1 3.76 7.09 16.00 o -3 4 1 97.18 104.52 19.50 o -2 4 1 252.05 240.94 24.68 o -1 4 1 10783.65 11482.83 179.85 o 0 4 1 3586.70 3789.59 67.71 o 1 4 1 18.19 -22.75 22.75 o 2 4 1 0.03 3.89 26.90 o 3 4 1 2257.13 2277.13 51.05 o 4 4 1 39.38 68.78 19.04 o 5 4 1 115.05 146.92 20.55 o 6 4 1 594.19 621.64 50.58 o 7 4 1 265.55 280.26 67.46 o 8 4 1 238.62 217.24 67.41 o 9 4 1 433.52 369.04 99.52 o 10 4 1 8.07 -36.89 90.95 o -11 5 1 15.68 -38.18 81.11 o -10 5 1 66.09 90.15 77.54 o -9 5 1 455.39 396.05 62.14 o -8 5 1 8147.49 8289.57 172.97 o -7 5 1 557.88 446.68 40.74 o -6 5 1 11906.13 11852.97 147.22 o -5 5 1 1666.41 1689.56 45.89 o -4 5 1 95.09 72.72 21.45 o -3 5 1 945.87 810.23 43.73 o -2 5 1 2757.45 2394.37 47.06 o -1 5 1 2862.20 2549.04 161.08 o 0 5 1 156.04 137.61 23.82 o 1 5 1 47864.20 46845.05 620.17 o 2 5 1 1545.91 1500.40 51.03 o 3 5 1 3110.47 3107.21 63.39 o 4 5 1 2181.58 2204.34 54.77 o 5 5 1 9857.58 9992.95 117.62 o 6 5 1 1303.61 1419.68 96.61 o 7 5 1 1831.54 1883.13 111.97 o 8 5 1 5028.70 5090.88 167.10 o 9 5 1 106.55 26.19 88.11 o 10 5 1 2953.00 2884.98 198.83 o -10 6 1 1237.82 1243.11 206.20 o -9 6 1 9.21 32.15 53.36 o -8 6 1 150.08 113.23 61.79 o -7 6 1 2422.08 2527.25 160.07 o -6 6 1 967.34 1021.25 58.99 o -5 6 1 823.40 856.57 43.97 o -4 6 1 8935.81 8575.46 126.17 o -3 6 1 2189.35 2133.40 54.16 o -2 6 1 648.18 571.28 30.65 o -1 6 1 2143.32 2035.20 76.95 o 0 6 1 117.21 89.15 26.69 o 1 6 1 2420.57 2629.15 76.46 o 2 6 1 1406.10 1544.41 53.84 o 3 6 1 17845.31 17155.62 248.59 o 4 6 1 1116.74 1124.98 58.76 o 5 6 1 6682.00 6423.84 105.86 o 6 6 1 10.26 38.16 33.98 o 7 6 1 68.14 135.12 53.71 o 8 6 1 2017.90 1786.52 128.08 o 9 6 1 262.61 250.21 113.90 o 10 6 1 2453.87 2050.66 179.63 o -10 7 1 864.24 599.27 122.11 o -9 7 1 24.70 42.96 65.13 o -8 7 1 188.03 244.92 46.87 o -7 7 1 556.12 667.89 56.34 o -6 7 1 12.63 65.07 30.40 o -5 7 1 1016.86 939.75 53.09 o -4 7 1 12894.43 13280.81 230.50 o -3 7 1 14171.74 14187.17 196.77 o -2 7 1 1960.37 1827.54 58.19 o -1 7 1 3809.40 3783.01 128.31 o 0 7 1 3330.43 3362.06 121.50 o 1 7 1 6179.35 6432.31 133.54 o 2 7 1 45.42 19.12 26.50 o 3 7 1 25.39 26.31 27.51 o 4 7 1 4283.86 3981.98 91.83 o 5 7 1 2362.10 2447.63 106.86 o 6 7 1 3678.63 3709.27 106.01 o 7 7 1 0.75 65.77 53.36 o 8 7 1 10.73 -1.52 56.57 o 9 7 1 1829.46 1766.29 209.15 o 10 7 1 2880.35 2865.55 358.40 o -10 8 1 78.04 84.26 101.34 o -9 8 1 90.19 201.99 73.24 o -8 8 1 10.82 6.65 43.09 o -7 8 1 135.48 106.51 44.13 o -6 8 1 3187.28 3282.32 100.08 o -5 8 1 17.28 72.62 35.72 o -4 8 1 210.25 276.88 45.92 o -3 8 1 932.29 847.77 54.14 o -2 8 1 3422.98 3545.75 84.62 o -1 8 1 6152.34 6035.58 201.29 o 0 8 1 2679.41 2714.62 116.62 o 1 8 1 9.04 18.85 32.64 o 2 8 1 1026.64 1026.36 75.16 o 3 8 1 78.90 103.18 30.64 o 4 8 1 2702.66 2794.53 80.36 o 5 8 1 628.09 651.44 54.99 o 6 8 1 146.07 50.03 44.46 o 7 8 1 473.83 415.17 51.31 o 8 8 1 2514.39 2253.73 122.82 o 9 8 1 365.99 493.78 113.17 o 10 8 1 5.64 -50.30 149.25 o -10 9 1 202.21 190.70 104.78 o -9 9 1 3159.94 3154.11 157.14 o -8 9 1 1887.75 1752.88 129.78 o -7 9 1 14245.35 14180.79 327.96 o -6 9 1 722.86 652.68 59.44 o -5 9 1 1856.84 1783.57 78.26 o -4 9 1 371.59 399.98 58.17 o -3 9 1 3427.78 3435.40 123.30 o -2 9 1 260.33 311.12 73.64 o -1 9 1 141.09 172.67 55.34 o 0 9 1 18627.21 17476.67 363.11 o 1 9 1 55.37 35.01 34.66 o 2 9 1 18807.87 18361.49 300.36 o 3 9 1 7.13 32.37 30.71 o 4 9 1 656.59 644.18 49.13 o 5 9 1 245.51 259.38 47.62 o 6 9 1 4445.79 4393.92 138.16 o 7 9 1 640.68 739.86 97.08 o 8 9 1 93.85 30.11 96.43 o 9 9 1 3155.23 3251.13 208.30 o -9 10 1 1130.74 1104.65 110.85 o -8 10 1 219.32 289.48 60.62 o -7 10 1 81.35 76.54 49.64 o -6 10 1 873.55 966.33 81.91 o -5 10 1 1722.51 1797.72 123.59 o -4 10 1 18.35 35.93 31.64 o -3 10 1 3216.22 3384.48 112.53 o -2 10 1 1672.40 1604.65 113.50 o -1 10 1 844.96 769.21 83.80 o 0 10 1 656.65 758.66 56.38 o 1 10 1 2.96 14.77 42.83 o 2 10 1 11669.57 11289.52 225.57 o 3 10 1 2.04 -9.63 30.80 o 4 10 1 8805.09 8626.02 161.81 o 5 10 1 353.33 318.53 132.76 o 6 10 1 577.20 671.34 72.78 o 7 10 1 0.60 -43.78 43.78 o 8 10 1 46.37 82.21 70.38 o 9 10 1 2067.86 2170.79 136.68 o -9 11 1 0.51 36.69 74.93 o -8 11 1 140.40 162.09 57.30 o -7 11 1 74.56 114.67 54.30 o -6 11 1 195.18 254.34 62.41 o -5 11 1 2715.54 2472.68 112.51 o -4 11 1 7230.54 7042.32 224.50 o -3 11 1 6394.66 6161.00 119.10 o -2 11 1 7483.68 7261.58 218.55 o -1 11 1 125.16 -26.98 55.08 o 0 11 1 916.80 1109.21 69.62 o 1 11 1 683.02 557.86 57.34 o 2 11 1 741.90 784.13 69.03 o 3 11 1 1759.01 1882.47 78.01 o 4 11 1 39.86 46.11 44.79 o 5 11 1 2821.05 2871.11 117.44 o 6 11 1 406.13 494.29 69.83 o 7 11 1 924.95 1004.18 84.32 o 8 11 1 161.75 293.13 81.30 o 9 11 1 1230.60 1325.62 116.35 o -9 12 1 266.69 298.32 135.58 o -8 12 1 21.46 24.69 57.08 o -7 12 1 200.72 195.52 57.44 o -6 12 1 396.39 339.93 69.10 o -5 12 1 1911.88 1802.25 103.93 o -4 12 1 123.92 225.43 60.07 o -3 12 1 1.14 50.79 50.98 o -2 12 1 2772.82 2559.98 147.89 o -1 12 1 3703.02 3849.28 238.61 o 0 12 1 2973.11 3008.05 144.75 o 1 12 1 505.93 474.07 60.02 o 2 12 1 88.35 21.23 47.31 o 3 12 1 965.03 838.98 58.51 o 4 12 1 793.50 785.09 104.03 o 5 12 1 1279.11 1154.86 85.07 o 6 12 1 1309.62 1276.24 138.45 o 7 12 1 2169.65 2273.12 181.21 o 8 12 1 1018.56 947.65 124.77 o -8 13 1 5766.84 6021.96 165.61 o -7 13 1 143.31 213.34 63.41 o -6 13 1 4893.29 4685.50 159.22 o -5 13 1 112.03 152.73 63.83 o -4 13 1 83.59 198.48 62.15 o -3 13 1 5.48 18.26 50.33 o -2 13 1 681.96 740.89 79.49 o -1 13 1 2697.39 2723.38 617.63 o 0 13 1 43.68 124.77 47.92 o 1 13 1 16940.69 16555.76 299.49 o 2 13 1 520.13 641.03 68.72 o 3 13 1 642.73 612.40 55.81 o 4 13 1 84.61 44.76 56.39 o 5 13 1 1691.90 1753.17 143.32 o 6 13 1 15.02 113.31 91.32 o 7 13 1 1171.97 1061.66 97.37 o 8 13 1 1870.59 1707.79 168.77 o -8 14 1 629.07 587.15 79.97 o -7 14 1 309.62 355.19 128.16 o 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