#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/77/2017715.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017715_Fobs loop_ _publ_author_name 'G\"orbitz, Carl Henrik' 'Backe, Paul Hoff' _publ_section_title ; L-Isoleucyl-L-asparagine 1.094-hydrate: a hybrid hydrogen-bonding pattern ; _journal_coeditor_code JZ3182 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o349 _journal_page_last o352 _journal_volume 66 _journal_year 2010 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 4.7855 _cell_length_b 18.2887 _cell_length_c 31.2475 _exptl_crystal_F_000 1143.60 _reflns_d_resolution_high 0.7501 _[local]_cod_data_source_file jz3182Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' unk in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 204.48 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 28868.76 29960.36 992.26 o 4 0 0 0.78 -25.28 28.71 o 6 0 0 65.91 94.68 53.55 o 1 1 0 4257.13 4306.74 84.12 o 2 1 0 1864.13 1856.43 39.22 o 3 1 0 0.01 -3.10 8.43 o 4 1 0 227.43 212.64 18.37 o 5 1 0 184.47 178.80 32.04 o 6 1 0 114.35 118.60 44.13 o 0 2 0 15534.05 15136.76 566.75 o 1 2 0 719.82 758.19 17.23 o 2 2 0 991.74 1024.87 23.82 o 3 2 0 438.51 447.94 28.08 o 4 2 0 102.04 101.36 16.31 o 5 2 0 367.17 365.70 37.91 o 6 2 0 29.32 97.21 38.04 o 1 3 0 2399.17 2516.54 51.00 o 2 3 0 896.30 949.63 19.69 o 3 3 0 834.48 819.26 23.92 o 4 3 0 2.83 -6.18 14.59 o 5 3 0 36.45 48.23 29.09 o 6 3 0 39.51 140.53 38.88 o 0 4 0 729.63 742.91 31.20 o 1 4 0 2021.80 1680.72 39.39 o 2 4 0 1415.10 1524.92 34.06 o 3 4 0 444.36 434.00 14.61 o 4 4 0 476.02 413.74 25.41 o 5 4 0 1120.40 1067.89 59.04 o 6 4 0 1148.54 1185.52 72.16 o 1 5 0 61.57 124.59 5.46 o 2 5 0 887.22 902.02 22.25 o 3 5 0 200.52 212.97 12.72 o 4 5 0 327.94 326.14 21.83 o 5 5 0 713.31 724.70 50.39 o 6 5 0 3.54 121.25 48.84 o 0 6 0 5096.57 5132.83 112.97 o 1 6 0 23094.96 23931.64 404.60 o 2 6 0 159.55 219.03 10.80 o 3 6 0 2147.14 1974.79 37.88 o 4 6 0 235.97 225.27 21.29 o 5 6 0 43.03 92.82 30.50 o 6 6 0 70.14 124.25 53.98 o 1 7 0 203.87 228.12 8.91 o 2 7 0 178.17 195.29 11.05 o 3 7 0 171.82 184.15 16.80 o 4 7 0 33.30 9.69 16.45 o 5 7 0 393.78 435.16 41.67 o 0 8 0 5289.91 5864.13 129.46 o 1 8 0 38.53 55.14 5.65 o 2 8 0 58.28 42.26 9.15 o 3 8 0 91.33 112.90 10.95 o 4 8 0 720.16 668.03 31.19 o 5 8 0 311.37 226.44 60.20 o 1 9 0 477.77 499.05 13.15 o 2 9 0 3.84 5.08 7.38 o 3 9 0 365.46 397.23 18.01 o 4 9 0 216.58 259.51 23.56 o 5 9 0 0.73 -41.56 41.56 o 0 10 0 49.71 40.01 7.92 o 1 10 0 0.31 -1.80 7.27 o 2 10 0 637.96 673.96 20.80 o 3 10 0 1973.96 1936.78 55.28 o 4 10 0 297.48 341.67 27.92 o 5 10 0 204.47 244.20 33.60 o 1 11 0 1147.42 1148.46 26.12 o 2 11 0 101.40 90.44 11.60 o 3 11 0 421.96 413.99 41.33 o 4 11 0 196.84 201.61 27.18 o 5 11 0 0.78 -5.90 28.21 o 0 12 0 4713.97 4843.40 109.71 o 1 12 0 27.61 15.16 6.84 o 2 12 0 0.03 0.52 9.81 o 3 12 0 132.76 121.67 21.24 o 4 12 0 5.26 8.60 23.38 o 5 12 0 61.43 33.57 31.33 o 1 13 0 1651.86 1757.66 36.01 o 2 13 0 110.80 117.67 14.51 o 3 13 0 125.76 127.87 22.03 o 4 13 0 5.74 7.14 43.06 o 5 13 0 31.79 18.10 32.15 o 0 14 0 28.66 9.98 11.10 o 1 14 0 227.28 264.17 14.66 o 2 14 0 131.36 149.15 16.12 o 3 14 0 507.88 529.70 34.16 o 4 14 0 0.01 -24.83 29.35 o 5 14 0 23.98 13.59 33.80 o 1 15 0 666.38 644.76 20.48 o 2 15 0 391.03 421.67 19.61 o 3 15 0 169.27 176.10 25.89 o 4 15 0 145.51 189.72 31.46 o 5 15 0 133.54 92.97 47.13 o 0 16 0 632.66 622.52 40.27 o 1 16 0 308.57 303.25 15.82 o 2 16 0 62.11 54.02 13.25 o 3 16 0 7.40 47.45 24.25 o 4 16 0 17.11 14.39 29.45 o 1 17 0 16.21 31.32 20.39 o 2 17 0 20.99 15.56 16.86 o 3 17 0 34.14 27.35 26.53 o 4 17 0 6.16 23.35 36.63 o 0 18 0 28.20 59.55 23.99 o 1 18 0 139.70 152.96 16.56 o 2 18 0 153.47 181.12 23.44 o 3 18 0 7.66 1.04 27.63 o 4 18 0 1.45 1.50 33.75 o 1 19 0 127.47 121.37 20.74 o 2 19 0 230.79 273.33 27.96 o 3 19 0 12.36 30.85 35.56 o 0 20 0 600.22 689.35 50.56 o 1 20 0 1.87 -17.78 19.45 o 2 20 0 60.06 2.57 31.28 o 3 20 0 285.64 291.34 45.41 o 1 21 0 37.72 52.08 22.14 o 2 21 0 46.36 0.86 35.99 o 0 22 0 164.21 259.20 38.13 o 1 22 0 4.70 -22.12 23.10 o 2 22 0 93.44 163.66 44.56 o 1 23 0 6.76 27.46 25.43 o 0 24 0 44.51 82.26 38.13 o 1 0 1 6515.27 6466.35 125.17 o 2 0 1 806.35 864.75 21.38 o 3 0 1 2900.14 2829.00 99.51 o 4 0 1 0.75 -13.64 13.64 o 5 0 1 140.36 166.75 32.41 o 6 0 1 60.66 109.25 38.78 o 1 1 1 193.66 179.39 6.06 o 2 1 1 6147.86 6421.52 88.57 o 3 1 1 370.53 345.22 18.28 o 4 1 1 2.80 7.10 11.61 o 5 1 1 243.87 246.02 24.55 o 6 1 1 8.35 87.71 26.18 o 0 2 1 3224.04 3096.99 61.24 o 1 2 1 3713.63 3370.64 47.66 o 2 2 1 914.29 817.80 14.40 o 3 2 1 290.40 315.12 10.57 o 4 2 1 55.76 50.24 11.20 o 5 2 1 521.75 485.07 30.29 o 6 2 1 106.26 159.45 27.46 o 0 3 1 629.86 669.11 11.88 o 1 3 1 846.34 840.59 13.47 o 2 3 1 373.85 356.83 7.89 o 3 3 1 325.96 341.75 9.13 o 4 3 1 435.03 397.14 17.57 o 5 3 1 180.74 189.33 21.68 o 6 3 1 21.33 69.72 25.95 o 0 4 1 142.62 160.88 5.21 o 1 4 1 912.69 968.50 18.20 o 2 4 1 616.99 625.63 12.34 o 3 4 1 362.26 373.60 9.59 o 4 4 1 596.64 515.06 19.17 o 5 4 1 778.28 697.53 34.97 o 6 4 1 31.90 73.66 25.79 o 0 5 1 4.59 3.12 3.03 o 1 5 1 590.56 641.80 10.31 o 2 5 1 397.40 415.73 9.95 o 3 5 1 685.92 693.82 12.83 o 4 5 1 73.63 69.61 11.41 o 5 5 1 99.31 97.81 20.54 o 6 5 1 183.12 242.92 40.14 o 0 6 1 5794.94 5498.85 85.61 o 1 6 1 1335.83 1362.64 18.16 o 2 6 1 1573.06 1632.61 25.56 o 3 6 1 2637.90 2497.58 35.23 o 4 6 1 542.93 540.10 19.17 o 5 6 1 309.19 336.94 25.75 o 6 6 1 47.88 122.79 36.79 o 0 7 1 1528.81 1644.43 42.98 o 1 7 1 1258.60 1281.18 17.58 o 2 7 1 627.23 670.40 13.36 o 3 7 1 416.59 441.67 12.99 o 4 7 1 901.51 791.63 23.81 o 5 7 1 18.59 58.78 22.13 o 6 7 1 145.70 139.24 55.27 o 0 8 1 224.77 218.12 8.91 o 1 8 1 3224.69 3347.78 41.72 o 2 8 1 196.00 222.97 9.59 o 3 8 1 234.04 235.68 10.61 o 4 8 1 184.32 189.11 14.08 o 5 8 1 27.93 19.96 23.44 o 0 9 1 360.33 364.23 12.93 o 1 9 1 1836.08 1892.71 24.86 o 2 9 1 365.22 376.91 10.45 o 3 9 1 469.40 457.68 14.66 o 4 9 1 4.02 0.91 12.41 o 5 9 1 85.77 69.34 25.65 o 0 10 1 2214.90 2380.11 39.78 o 1 10 1 1286.88 1273.71 18.98 o 2 10 1 1661.03 1710.12 27.83 o 3 10 1 789.30 763.51 18.76 o 4 10 1 134.10 119.95 15.17 o 5 10 1 70.95 85.92 25.11 o 0 11 1 2479.94 2464.60 56.97 o 1 11 1 365.36 388.59 8.79 o 2 11 1 230.61 272.98 10.50 o 3 11 1 1380.83 1298.50 32.21 o 4 11 1 204.05 222.37 29.93 o 5 11 1 10.93 2.97 21.01 o 0 12 1 63.04 57.44 6.85 o 1 12 1 214.37 219.28 7.21 o 2 12 1 133.90 155.78 9.18 o 3 12 1 138.29 139.79 15.40 o 4 12 1 88.00 73.40 17.53 o 5 12 1 14.06 -5.92 21.37 o 0 13 1 315.56 303.60 11.99 o 1 13 1 16.77 14.66 5.46 o 2 13 1 91.77 123.67 16.56 o 3 13 1 199.83 241.61 20.96 o 4 13 1 104.50 146.45 20.06 o 5 13 1 113.92 110.83 24.52 o 0 14 1 61.51 48.98 7.58 o 1 14 1 110.24 111.58 6.97 o 2 14 1 397.22 421.14 14.51 o 3 14 1 189.16 183.86 17.62 o 4 14 1 13.80 13.50 18.59 o 5 14 1 209.68 215.57 27.53 o 0 15 1 248.12 268.99 17.19 o 1 15 1 155.27 162.57 8.53 o 2 15 1 347.71 356.56 13.78 o 3 15 1 213.32 250.46 19.60 o 4 15 1 31.81 25.91 19.46 o 5 15 1 192.30 226.91 39.63 o 0 16 1 67.57 78.59 15.45 o 1 16 1 18.10 15.12 7.77 o 2 16 1 96.00 107.97 12.99 o 3 16 1 235.30 225.11 20.64 o 4 16 1 213.02 195.17 23.60 o 0 17 1 52.81 67.83 16.05 o 1 17 1 393.64 478.59 16.16 o 2 17 1 273.99 322.03 15.91 o 3 17 1 5.40 -14.77 17.80 o 4 17 1 118.96 98.32 23.76 o 0 18 1 0.20 -8.14 16.36 o 1 18 1 81.78 99.81 11.67 o 2 18 1 41.80 50.48 14.56 o 3 18 1 12.22 5.28 18.62 o 4 18 1 34.62 46.29 24.86 o 0 19 1 15.69 27.36 18.15 o 1 19 1 242.97 299.49 16.03 o 2 19 1 8.86 -17.59 17.59 o 3 19 1 42.53 37.09 27.63 o 0 20 1 133.64 92.36 21.50 o 1 20 1 77.20 77.63 14.99 o 2 20 1 147.26 113.58 20.83 o 3 20 1 45.98 37.67 27.71 o 0 21 1 704.10 883.84 40.74 o 1 21 1 8.74 0.35 15.01 o 2 21 1 118.44 85.59 33.85 o 0 22 1 256.07 424.06 72.19 o 1 22 1 13.56 16.20 16.35 o 2 22 1 6.74 -19.49 27.26 o 0 23 1 139.12 244.33 61.48 o 1 23 1 87.20 98.16 22.54 o 0 24 1 2.80 50.29 25.14 o 0 0 2 949.73 670.93 32.99 o 1 0 2 268.63 216.05 7.62 o 2 0 2 2645.67 2714.56 54.89 o 3 0 2 80.55 108.68 13.01 o 4 0 2 392.65 386.29 22.61 o 5 0 2 183.76 221.07 34.68 o 6 0 2 1.75 54.01 37.67 o 1 1 2 26409.07 24608.00 334.94 o 2 1 2 1778.69 1769.87 26.62 o 3 1 2 96.94 112.15 8.61 o 4 1 2 388.58 374.51 18.87 o 5 1 2 382.71 412.15 27.74 o 6 1 2 216.00 288.65 30.74 o 0 2 2 32.25 53.13 5.57 o 1 2 2 6146.00 5982.42 83.70 o 2 2 2 163.69 188.21 7.79 o 3 2 2 62.55 68.35 6.48 o 4 2 2 711.67 678.91 23.79 o 5 2 2 201.22 177.09 22.52 o 6 2 2 34.94 109.17 26.57 o 0 3 2 539.89 516.72 10.32 o 1 3 2 747.75 759.34 13.54 o 2 3 2 2784.16 2836.87 35.54 o 3 3 2 669.81 661.39 16.89 o 4 3 2 143.35 142.68 12.06 o 5 3 2 230.00 245.50 24.19 o 6 3 2 194.16 252.28 29.78 o 0 4 2 9813.24 9703.68 182.99 o 1 4 2 2615.07 2505.42 42.15 o 2 4 2 530.27 582.09 11.73 o 3 4 2 519.28 546.42 11.21 o 4 4 2 14.12 1.44 12.04 o 5 4 2 249.10 259.92 24.34 o 6 4 2 116.23 166.66 28.07 o 0 5 2 19850.63 19960.00 338.56 o 1 5 2 254.56 244.78 6.07 o 2 5 2 849.19 961.60 16.56 o 3 5 2 931.49 931.09 16.32 o 4 5 2 15.12 18.67 10.74 o 5 5 2 39.37 61.73 20.06 o 6 5 2 9.93 18.33 35.04 o 0 6 2 162.17 179.92 7.59 o 1 6 2 1493.42 1382.18 18.45 o 2 6 2 96.01 119.68 5.75 o 3 6 2 84.42 108.35 7.41 o 4 6 2 0.88 15.15 10.90 o 5 6 2 76.76 117.20 21.07 o 6 6 2 10.97 75.40 49.27 o 0 7 2 2.06 -3.96 3.96 o 1 7 2 4246.74 4454.52 54.62 o 2 7 2 2117.75 2195.10 33.39 o 3 7 2 326.52 304.03 12.17 o 4 7 2 1035.08 975.44 26.16 o 5 7 2 144.33 150.79 23.50 o 6 7 2 13.24 -6.85 49.70 o 0 8 2 363.82 389.87 11.15 o 1 8 2 2496.19 2665.98 34.26 o 2 8 2 509.32 533.45 12.86 o 3 8 2 30.06 33.89 7.88 o 4 8 2 397.08 413.21 17.73 o 5 8 2 359.92 339.22 32.99 o 0 9 2 2.05 3.58 4.65 o 1 9 2 933.68 960.87 14.31 o 2 9 2 460.48 468.60 10.97 o 3 9 2 909.77 900.70 20.15 o 4 9 2 586.48 573.93 21.57 o 5 9 2 44.84 57.52 21.06 o 0 10 2 3736.14 3773.03 67.16 o 1 10 2 123.14 160.12 10.49 o 2 10 2 170.63 191.57 8.48 o 3 10 2 401.26 389.07 14.28 o 4 10 2 241.76 236.51 17.06 o 5 10 2 339.11 337.39 31.60 o 0 11 2 894.89 900.32 20.85 o 1 11 2 524.78 503.69 10.08 o 2 11 2 290.30 307.81 10.44 o 3 11 2 71.74 73.96 10.33 o 4 11 2 202.07 202.11 19.08 o 5 11 2 31.37 57.53 26.12 o 0 12 2 950.29 965.65 21.59 o 1 12 2 552.75 583.22 11.37 o 2 12 2 923.70 979.19 21.00 o 3 12 2 251.60 266.78 15.83 o 4 12 2 254.27 283.00 21.07 o 5 12 2 176.73 185.31 30.30 o 0 13 2 676.64 758.60 18.82 o 1 13 2 2026.52 2080.40 30.87 o 2 13 2 205.32 225.76 9.02 o 3 13 2 425.10 421.87 21.69 o 4 13 2 210.62 211.91 20.51 o 5 13 2 58.91 23.04 26.34 o 0 14 2 972.36 977.84 25.00 o 1 14 2 239.29 239.20 8.66 o 2 14 2 27.28 18.57 7.81 o 3 14 2 22.43 21.63 15.07 o 4 14 2 64.14 40.17 19.28 o 5 14 2 103.33 56.81 25.11 o 0 15 2 767.04 760.43 44.51 o 1 15 2 69.58 75.14 7.48 o 2 15 2 766.54 854.84 20.67 o 3 15 2 120.79 120.56 17.67 o 4 15 2 19.42 2.61 19.29 o 5 15 2 124.94 78.64 34.47 o 0 16 2 212.37 229.66 16.03 o 1 16 2 1014.12 1004.61 34.03 o 2 16 2 44.45 43.82 10.66 o 3 16 2 275.16 286.05 21.18 o 4 16 2 295.17 319.87 26.02 o 0 17 2 108.84 119.19 18.02 o 1 17 2 1108.07 1107.51 23.85 o 2 17 2 220.36 229.27 15.67 o 3 17 2 344.62 408.75 24.44 o 4 17 2 67.00 38.35 22.71 o 0 18 2 118.05 162.34 47.77 o 1 18 2 422.88 461.78 17.58 o 2 18 2 9.41 25.53 15.18 o 3 18 2 8.57 -19.95 19.95 o 4 18 2 9.01 17.81 24.09 o 0 19 2 521.12 525.21 30.44 o 1 19 2 19.57 39.20 12.58 o 2 19 2 17.56 36.60 18.46 o 3 19 2 33.35 74.31 23.64 o 0 20 2 451.51 499.26 31.50 o 1 20 2 11.92 4.05 12.78 o 2 20 2 399.39 437.82 26.21 o 3 20 2 34.17 25.87 55.27 o 0 21 2 561.32 635.77 36.05 o 1 21 2 65.49 55.70 15.91 o 2 21 2 31.04 53.31 21.57 o 0 22 2 82.89 58.35 23.41 o 1 22 2 29.55 -15.65 18.92 o 2 22 2 93.99 88.45 40.27 o 0 23 2 27.01 61.14 24.79 o 1 23 2 17.03 10.94 25.70 o 0 24 2 2.93 40.57 25.60 o 1 24 2 0.68 -26.99 37.27 o 1 0 3 10986.30 10465.06 203.60 o 2 0 3 871.32 961.53 22.61 o 3 0 3 50.67 80.39 12.51 o 4 0 3 714.32 728.22 31.13 o 5 0 3 117.64 114.61 31.20 o 6 0 3 69.37 167.09 38.35 o 0 1 3 1088.04 1108.43 29.77 o 1 1 3 11203.96 10273.26 172.77 o 2 1 3 4013.25 3899.22 54.52 o 3 1 3 233.08 276.90 9.63 o 4 1 3 315.85 333.63 14.73 o 5 1 3 35.17 39.81 19.87 o 6 1 3 65.35 136.02 28.28 o 0 2 3 5.29 2.86 2.09 o 1 2 3 3594.47 3552.86 54.79 o 2 2 3 23.41 25.62 4.65 o 3 2 3 155.44 186.93 8.19 o 4 2 3 1233.13 1136.62 32.16 o 5 2 3 760.80 689.55 34.99 o 6 2 3 251.98 277.00 31.66 o 0 3 3 251.76 257.18 6.52 o 1 3 3 4431.28 4261.70 60.10 o 2 3 3 1392.29 1497.03 19.99 o 3 3 3 2002.60 2065.61 27.50 o 4 3 3 473.47 430.51 21.14 o 5 3 3 122.25 126.07 21.89 o 6 3 3 38.95 80.50 26.46 o 0 4 3 836.74 688.88 13.65 o 1 4 3 1556.18 1512.11 22.34 o 2 4 3 694.98 682.14 11.81 o 3 4 3 26.72 24.16 6.41 o 4 4 3 232.02 248.97 14.05 o 5 4 3 46.66 72.64 19.67 o 6 4 3 143.80 169.98 28.02 o 0 5 3 298.59 318.32 14.01 o 1 5 3 4863.35 4621.96 56.49 o 2 5 3 556.31 544.32 11.45 o 3 5 3 1048.79 1087.06 19.91 o 4 5 3 531.45 472.62 18.66 o 5 5 3 60.85 73.77 20.03 o 6 5 3 33.02 41.15 37.43 o 0 6 3 41811.87 41230.60 698.52 o 1 6 3 1700.43 1690.17 23.81 o 2 6 3 1177.69 1179.85 19.60 o 3 6 3 38.89 42.05 6.78 o 4 6 3 26.43 24.81 11.11 o 5 6 3 8.34 35.27 20.51 o 6 6 3 140.61 239.50 56.13 o 0 7 3 3449.25 3394.10 60.04 o 1 7 3 837.67 872.25 12.44 o 2 7 3 2760.24 2746.88 39.32 o 3 7 3 346.24 315.96 12.74 o 4 7 3 936.07 856.62 24.59 o 5 7 3 275.27 276.10 21.99 o 6 7 3 0.12 1.29 49.27 o 0 8 3 1699.54 1827.30 34.16 o 1 8 3 1425.47 1445.14 18.62 o 2 8 3 1140.12 1198.39 19.87 o 3 8 3 1645.27 1536.98 28.76 o 4 8 3 424.25 428.03 17.95 o 5 8 3 47.46 38.10 21.80 o 0 9 3 6.21 2.20 4.59 o 1 9 3 1923.20 1954.92 26.69 o 2 9 3 98.15 115.86 6.47 o 3 9 3 522.40 507.39 15.25 o 4 9 3 516.86 505.68 22.18 o 5 9 3 343.99 369.10 27.19 o 0 10 3 4.25 8.24 5.14 o 1 10 3 85.69 136.60 10.90 o 2 10 3 292.75 329.84 10.62 o 3 10 3 217.72 236.57 12.36 o 4 10 3 239.29 249.92 16.76 o 5 10 3 215.73 231.16 28.86 o 0 11 3 32.01 22.32 6.26 o 1 11 3 429.45 407.85 8.70 o 2 11 3 376.20 385.71 11.52 o 3 11 3 203.58 220.79 12.46 o 4 11 3 90.19 90.17 15.80 o 5 11 3 61.73 60.87 27.54 o 0 12 3 29.14 33.22 6.55 o 1 12 3 3187.55 3232.66 41.59 o 2 12 3 826.04 810.05 23.49 o 3 12 3 453.37 447.99 17.09 o 4 12 3 51.21 73.53 17.82 o 5 12 3 248.27 264.55 33.37 o 0 13 3 504.37 537.91 16.10 o 1 13 3 408.47 417.54 10.59 o 2 13 3 247.18 242.60 10.08 o 3 13 3 531.59 488.91 20.20 o 4 13 3 103.76 91.19 19.18 o 5 13 3 36.47 32.09 43.31 o 0 14 3 1486.21 1525.83 34.29 o 1 14 3 406.12 419.64 10.83 o 2 14 3 591.52 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1 39 7.23 -34.70 49.27 o 1 2 39 36.95 26.12 22.12 o 2 2 39 20.80 -62.14 80.55 o 1 3 39 64.66 52.20 22.38 o 2 3 39 83.29 29.86 97.47 o 0 4 39 184.31 197.21 30.38 o 1 4 39 74.11 28.31 28.00 o 0 5 39 10.91 6.76 38.34 o 1 5 39 82.96 34.00 20.98 o 0 6 39 421.00 408.30 53.55 o 1 6 39 48.51 7.07 28.20 o 0 7 39 0.92 -35.99 35.99 o 1 7 39 55.07 70.26 29.96 o 0 8 39 8.49 15.20 35.56 o 1 0 40 532.75 612.09 44.83 o 1 1 40 29.97 17.76 23.72 o 1 2 40 75.59 96.99 24.64 o 1 3 40 19.17 -31.23 31.23 o 1 4 40 7.14 -28.70 61.69 o 0 5 40 21.77 24.82 58.91 o 1 5 40 1.12 22.28 47.13 o 0 6 40 5.89 -28.20 28.20 o 1 0 41 0.05 -7.79 65.12 o 1 1 41 181.25 193.90 31.16 o 1 2 41 62.55 8.81 28.20 o