#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:18:13 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180846 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/77/2017723.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017723_Fobs loop_ _publ_author_name 'Chapin, Brette M.' 'Hughs, Lauren D.' 'Golen, James A.' 'Rheingold, Arnold L.' 'Johnson, Adam R.' _publ_section_title ; Chlorido(\h^5^-cyclopentadienyl)bis(dimethylamido)titanium, [TiCl(\h^5^-C~5~H~5~)(NMe~2~)~2~] ; _journal_coeditor_code SF3132 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m191 _journal_page_last m193 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.259 _cell_angle_gamma 90.000 _cell_length_a 9.3621 _cell_length_b 11.0618 _cell_length_c 11.5907 _exptl_crystal_F_000 496.00 _reflns_d_resolution_high 0.8289 _cod_data_source_file sf31321asup2.hkl _cod_data_source_block 1a #BEGIN Tags that were not found in dictionaries: _shelx_title ' hmc02 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 129.90 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5510.29 5718.70 121.83 o 4 0 0 165.36 156.79 6.60 o 6 0 0 513.55 463.76 13.31 o 8 0 0 616.06 654.76 31.19 o 10 0 0 175.01 152.31 11.11 o 1 1 0 963.97 954.73 8.19 o 2 1 0 222.43 239.84 3.98 o 3 1 0 165.61 180.09 3.55 o 5 1 0 193.32 195.91 5.97 o 6 1 0 3805.02 3872.32 43.48 o 7 1 0 271.62 274.35 10.37 o 8 1 0 1659.65 1645.47 27.91 o 9 1 0 479.31 449.79 13.82 o 10 1 0 430.30 428.39 11.97 o 0 2 0 2597.79 2565.91 31.15 o 1 2 0 8827.12 9319.02 66.08 o 2 2 0 2561.98 2698.00 21.78 o 3 2 0 2499.32 2396.17 20.64 o 4 2 0 558.86 466.23 7.03 o 5 2 0 1198.88 1305.01 14.33 o 6 2 0 1389.75 1387.75 19.06 o 7 2 0 94.46 77.82 4.36 o 8 2 0 48.39 48.11 3.64 o 9 2 0 297.26 290.51 8.84 o 10 2 0 320.70 287.36 11.38 o 1 3 0 736.18 741.62 8.60 o 2 3 0 2062.45 2117.01 21.72 o 3 3 0 4297.98 4234.68 33.89 o 4 3 0 714.55 639.40 9.18 o 5 3 0 5601.94 5562.71 41.42 o 6 3 0 209.92 210.45 5.40 o 7 3 0 1451.47 1451.09 20.62 o 8 3 0 83.62 83.18 5.67 o 9 3 0 163.28 146.97 7.66 o 10 3 0 379.07 385.32 13.50 o 0 4 0 2482.63 2739.39 32.47 o 1 4 0 728.56 679.75 8.77 o 2 4 0 1467.96 1400.78 13.65 o 3 4 0 999.76 909.82 10.73 o 4 4 0 655.14 672.49 9.23 o 5 4 0 1290.04 1257.30 15.80 o 6 4 0 433.80 439.20 9.70 o 7 4 0 320.80 313.27 9.37 o 8 4 0 12.81 6.78 2.82 o 9 4 0 538.70 496.81 14.72 o 10 4 0 149.19 128.46 9.17 o 1 5 0 55.37 63.81 2.74 o 2 5 0 5437.69 5653.47 46.99 o 3 5 0 167.57 195.33 4.50 o 4 5 0 7028.86 7034.31 62.04 o 5 5 0 554.73 527.86 17.15 o 6 5 0 992.93 1017.05 16.03 o 7 5 0 28.08 33.45 3.17 o 8 5 0 482.62 477.11 13.80 o 9 5 0 48.65 37.72 6.34 o 10 5 0 3.45 6.50 3.66 o 0 6 0 1484.28 1398.70 20.70 o 1 6 0 347.50 300.38 6.23 o 2 6 0 3538.13 3487.29 32.26 o 3 6 0 89.11 90.83 3.52 o 4 6 0 201.67 168.52 4.74 o 5 6 0 6.55 7.32 2.24 o 6 6 0 411.86 387.77 11.94 o 7 6 0 331.17 345.19 13.82 o 8 6 0 24.52 29.84 4.61 o 9 6 0 62.80 52.57 7.67 o 1 7 0 42.06 46.05 2.79 o 2 7 0 93.42 101.19 4.15 o 3 7 0 941.63 949.94 15.38 o 4 7 0 4.01 4.93 1.51 o 5 7 0 9.66 6.22 2.52 o 6 7 0 454.09 474.44 15.15 o 7 7 0 758.19 761.49 22.23 o 8 7 0 1401.46 1487.24 34.36 o 9 7 0 111.06 119.75 9.89 o 0 8 0 2615.76 2593.98 44.76 o 1 8 0 4574.82 4755.51 52.39 o 2 8 0 1061.64 1048.72 18.48 o 3 8 0 904.08 888.00 20.88 o 4 8 0 0.11 0.49 1.73 o 5 8 0 14.30 7.82 3.52 o 6 8 0 138.56 138.23 7.96 o 7 8 0 255.39 237.91 12.02 o 8 8 0 175.28 153.26 9.81 o 1 9 0 33.20 47.69 4.28 o 2 9 0 25.54 17.57 3.23 o 3 9 0 3.21 2.89 2.08 o 4 9 0 144.82 159.59 9.59 o 5 9 0 97.79 113.84 8.20 o 6 9 0 6.74 9.86 3.22 o 7 9 0 1637.52 1695.94 35.33 o 8 9 0 0.05 -2.26 3.21 o 0 10 0 1330.36 1399.85 40.48 o 1 10 0 382.17 392.62 12.70 o 2 10 0 388.19 421.77 13.02 o 3 10 0 130.85 124.39 6.76 o 4 10 0 410.33 378.58 15.68 o 5 10 0 168.80 164.94 10.30 o 6 10 0 60.20 65.02 7.01 o 7 10 0 1.43 -1.64 4.68 o 1 11 0 139.54 146.93 9.15 o 2 11 0 528.44 513.22 14.85 o 3 11 0 1291.00 1351.62 60.35 o 4 11 0 119.97 116.81 10.42 o 5 11 0 351.78 346.59 18.50 o 6 11 0 515.61 527.00 23.95 o 0 12 0 73.60 45.33 9.67 o 1 12 0 53.65 38.68 8.21 o 2 12 0 67.43 78.44 6.03 o 3 12 0 25.04 14.37 4.88 o 4 12 0 470.41 510.49 23.21 o 1 13 0 242.59 232.34 11.43 o 2 13 0 380.01 380.78 18.48 o -11 0 1 949.61 989.40 32.42 o -9 0 1 785.96 769.61 25.01 o -7 0 1 3048.47 3018.54 58.67 o -5 0 1 1723.62 1983.77 27.01 o -3 0 1 1069.73 1158.88 16.06 o -1 0 1 49.75 45.13 1.63 o 1 0 1 2953.74 2993.84 47.12 o 3 0 1 541.91 485.90 9.39 o 5 0 1 1316.41 1295.50 19.76 o 7 0 1 5488.33 5660.06 95.12 o 9 0 1 1947.99 1935.45 48.56 o -11 1 1 78.52 64.08 4.56 o -10 1 1 170.77 159.68 7.83 o -9 1 1 73.37 78.35 5.53 o -8 1 1 672.68 664.30 16.09 o -7 1 1 57.02 47.47 3.53 o -6 1 1 6.82 2.23 1.69 o -5 1 1 756.67 721.44 10.00 o -4 1 1 1888.02 1931.83 17.88 o -3 1 1 1961.61 1906.60 16.18 o -2 1 1 14185.41 14462.08 116.56 o -1 1 1 16873.84 17254.35 145.27 o 0 1 1 4796.54 5174.60 42.30 o 1 1 1 8805.88 9026.01 93.59 o 2 1 1 361.26 418.87 6.61 o 3 1 1 383.57 340.80 6.71 o 4 1 1 29.43 20.51 2.02 o 5 1 1 1.99 4.57 1.05 o 6 1 1 498.20 501.88 9.59 o 7 1 1 1071.10 1027.36 18.14 o 8 1 1 11.86 10.38 2.69 o 9 1 1 42.36 53.52 4.46 o 10 1 1 55.16 44.21 4.42 o -10 2 1 612.30 614.75 15.41 o -9 2 1 83.50 69.23 5.17 o -8 2 1 513.32 486.65 13.54 o -7 2 1 3476.02 3485.12 40.58 o -6 2 1 84.37 64.16 3.34 o -5 2 1 907.05 833.50 10.70 o -4 2 1 43.12 29.86 1.95 o -3 2 1 1905.82 1798.52 16.58 o -2 2 1 1234.20 1247.30 10.44 o -1 2 1 733.79 748.48 7.16 o 0 2 1 2359.18 2467.66 18.31 o 1 2 1 1622.53 1668.38 14.44 o 2 2 1 925.63 956.08 10.15 o 3 2 1 4808.96 4744.88 40.15 o 4 2 1 3281.13 3321.30 32.93 o 5 2 1 18.77 6.77 1.64 o 6 2 1 3599.66 3567.94 37.87 o 7 2 1 471.47 436.86 11.50 o 8 2 1 833.32 811.49 18.35 o 9 2 1 148.54 145.99 9.28 o 10 2 1 170.06 166.21 8.46 o -10 3 1 58.66 54.17 4.22 o -9 3 1 288.32 264.89 9.14 o -8 3 1 424.91 424.39 11.47 o -7 3 1 214.28 224.19 7.20 o -6 3 1 1167.47 1184.08 16.85 o -5 3 1 7.71 2.14 1.39 o -4 3 1 1325.40 1329.46 13.48 o -3 3 1 761.93 786.52 8.80 o -2 3 1 3794.19 3667.02 26.80 o -1 3 1 4083.01 4113.40 29.85 o 0 3 1 174.67 207.90 3.34 o 1 3 1 1.13 6.44 0.96 o 2 3 1 1748.66 1697.21 15.84 o 3 3 1 103.55 151.33 3.66 o 4 3 1 4539.04 4820.28 39.71 o 5 3 1 929.89 896.02 16.31 o 6 3 1 54.71 52.18 3.44 o 7 3 1 6.42 7.92 1.92 o 8 3 1 1463.74 1418.02 25.93 o 9 3 1 2.55 4.50 2.12 o 10 3 1 873.81 887.82 21.91 o -10 4 1 90.10 88.53 8.65 o -9 4 1 547.09 550.79 14.12 o -8 4 1 1140.39 1140.89 19.02 o -7 4 1 92.80 99.67 4.74 o -6 4 1 1745.62 1770.87 26.68 o -5 4 1 1091.13 1071.90 13.02 o -4 4 1 5923.75 5931.32 43.65 o -3 4 1 475.87 487.59 6.92 o -2 4 1 549.57 574.39 7.65 o -1 4 1 353.43 324.78 5.00 o 0 4 1 2657.66 2628.25 22.75 o 1 4 1 452.82 431.94 5.72 o 2 4 1 7116.15 7565.18 57.84 o 3 4 1 548.30 569.34 8.31 o 4 4 1 1410.50 1326.91 16.14 o 5 4 1 1502.01 1559.63 22.41 o 6 4 1 411.07 378.11 10.05 o 7 4 1 0.31 -1.00 1.45 o 8 4 1 2.13 4.01 1.92 o 9 4 1 32.92 37.24 4.39 o 10 4 1 19.29 21.21 4.07 o -10 5 1 60.10 57.92 7.54 o -9 5 1 82.83 85.01 8.17 o -8 5 1 112.66 103.52 6.39 o -7 5 1 2039.26 1991.92 31.46 o -6 5 1 13.57 21.74 2.45 o -5 5 1 210.45 192.17 4.95 o -4 5 1 527.72 530.90 8.16 o -3 5 1 859.80 954.40 10.93 o -2 5 1 4365.02 4482.97 37.76 o -1 5 1 2.22 2.32 0.74 o 0 5 1 76.76 59.81 3.27 o 2 5 1 395.14 366.52 6.20 o 3 5 1 1570.62 1480.18 16.30 o 4 5 1 330.11 336.89 7.25 o 5 5 1 411.51 415.98 10.24 o 6 5 1 0.40 -0.65 1.78 o 7 5 1 1.92 1.90 1.71 o 8 5 1 303.02 308.28 11.16 o 9 5 1 837.66 819.84 21.91 o -9 6 1 828.45 845.49 28.96 o -8 6 1 51.60 38.04 5.58 o -7 6 1 494.61 527.21 13.64 o -6 6 1 719.08 735.40 16.55 o -5 6 1 1648.34 1706.34 23.38 o -4 6 1 789.04 788.05 13.87 o -3 6 1 1477.44 1546.09 17.93 o -2 6 1 141.43 146.83 4.65 o -1 6 1 408.82 429.45 7.92 o 0 6 1 244.17 257.23 5.76 o 1 6 1 1312.71 1320.05 15.28 o 2 6 1 415.46 395.20 7.41 o 3 6 1 2111.33 2113.71 26.56 o 4 6 1 2.37 -0.44 2.00 o 5 6 1 1963.51 1958.33 29.95 o 6 6 1 284.67 270.31 10.41 o 7 6 1 515.79 523.49 14.31 o 8 6 1 165.93 161.34 11.04 o 9 6 1 280.40 270.81 15.39 o -9 7 1 539.71 571.64 20.52 o -8 7 1 164.75 163.12 10.00 o -7 7 1 9.61 5.92 2.89 o -6 7 1 34.85 44.05 4.58 o -5 7 1 52.47 54.28 4.35 o -4 7 1 9.56 12.28 2.05 o -3 7 1 2563.62 2532.41 30.14 o -2 7 1 107.82 112.86 5.62 o -1 7 1 5734.33 5572.62 53.89 o 0 7 1 2587.53 2634.58 29.82 o 1 7 1 1821.04 1799.10 19.87 o 2 7 1 463.07 422.89 8.36 o 3 7 1 441.00 442.20 9.98 o 4 7 1 7.10 8.35 2.08 o 5 7 1 391.98 407.69 13.34 o 6 7 1 3.23 2.98 2.20 o 7 7 1 164.57 152.80 9.39 o 8 7 1 54.83 44.90 5.48 o 9 7 1 2.90 0.76 3.67 o -8 8 1 618.91 638.15 28.75 o -7 8 1 222.26 221.45 10.81 o -6 8 1 21.57 22.16 2.78 o -5 8 1 76.84 68.35 4.77 o -4 8 1 132.37 115.95 5.40 o -3 8 1 113.79 103.09 5.40 o -2 8 1 132.52 126.70 6.11 o -1 8 1 0.23 -1.57 1.57 o 0 8 1 9.24 9.48 2.16 o 1 8 1 275.78 261.59 7.52 o 2 8 1 67.07 57.40 3.75 o 3 8 1 51.14 44.07 3.67 o 4 8 1 406.98 395.87 13.04 o 5 8 1 559.66 544.54 16.21 o 6 8 1 1835.34 1848.35 37.39 o 7 8 1 319.28 341.77 19.44 o 8 8 1 985.46 1036.72 28.52 o -8 9 1 116.34 95.12 7.55 o -7 9 1 1.41 2.03 3.29 o -6 9 1 73.82 78.22 7.13 o -5 9 1 160.23 150.02 7.76 o -4 9 1 729.22 702.49 15.84 o -3 9 1 68.38 60.26 4.54 o -2 9 1 1824.46 1755.18 27.12 o -1 9 1 7.14 2.94 2.05 o 0 9 1 3739.03 3805.59 51.88 o 1 9 1 30.49 22.30 3.30 o 2 9 1 181.49 168.22 9.17 o 3 9 1 146.29 138.98 7.56 o 4 9 1 15.48 13.87 3.30 o 5 9 1 80.38 78.43 6.77 o 6 9 1 335.72 357.44 13.70 o 7 9 1 13.32 16.33 3.91 o -7 10 1 3.56 2.57 3.51 o -6 10 1 964.01 963.53 28.47 o -5 10 1 172.74 157.14 7.80 o -4 10 1 997.97 1021.49 27.84 o -3 10 1 46.60 43.80 4.18 o -2 10 1 337.86 328.33 11.66 o -1 10 1 14.65 10.99 3.04 o 0 10 1 287.68 277.22 10.78 o 1 10 1 6.45 1.68 2.05 o 2 10 1 339.15 337.37 10.55 o 3 10 1 27.50 32.61 5.66 o 4 10 1 774.49 816.00 27.81 o 5 10 1 656.20 614.57 24.33 o 6 10 1 398.15 398.05 17.08 o 7 10 1 535.90 557.08 25.04 o -6 11 1 59.62 81.83 7.76 o -5 11 1 304.06 316.31 17.61 o -4 11 1 15.90 15.67 3.52 o -3 11 1 286.22 314.75 11.72 o -2 11 1 34.35 37.90 5.03 o -1 11 1 1203.59 1207.25 26.12 o 0 11 1 26.70 30.68 3.63 o 1 11 1 189.74 185.23 9.65 o 2 11 1 57.61 52.61 8.61 o 3 11 1 46.34 43.86 6.94 o 4 11 1 399.86 379.02 20.87 o 5 11 1 84.41 69.02 8.63 o -4 12 1 38.14 33.25 4.41 o -3 12 1 696.57 691.35 23.43 o -2 12 1 9.61 4.66 2.72 o -1 12 1 10.79 8.69 2.86 o 0 12 1 3.59 2.71 2.82 o 1 12 1 855.31 917.91 23.51 o 2 12 1 1.16 -3.49 3.49 o 3 12 1 422.69 447.97 21.03 o 4 12 1 0.02 5.20 4.20 o -2 13 1 3.03 2.36 3.24 o -1 13 1 73.81 75.22 6.10 o 0 13 1 2.37 4.41 2.99 o 1 13 1 204.11 205.64 13.02 o 2 13 1 47.62 38.37 13.39 o -10 0 2 675.94 733.10 25.59 o -8 0 2 917.96 883.84 25.51 o -6 0 2 191.44 170.49 7.19 o -4 0 2 4964.38 4453.28 50.09 o -2 0 2 4181.34 4280.54 79.14 o 0 0 2 12254.85 12303.27 140.47 o 2 0 2 6.98 14.88 2.60 o 4 0 2 2530.29 2869.35 45.10 o 6 0 2 1295.86 1330.74 57.12 o 8 0 2 78.50 76.48 9.37 o 10 0 2 44.31 48.59 12.49 o -11 1 2 297.36 296.68 13.15 o -10 1 2 477.26 493.85 14.56 o -9 1 2 1.70 1.81 1.79 o -8 1 2 347.16 360.79 11.36 o -7 1 2 256.80 263.94 7.51 o -6 1 2 1751.30 1741.76 20.17 o -5 1 2 35.12 44.04 2.30 o -3 1 2 2592.51 2603.76 21.12 o -2 1 2 694.53 728.34 7.70 o -1 1 2 34.53 35.97 1.81 o 0 1 2 723.31 818.45 10.50 o 1 1 2 12.10 12.67 1.66 o 2 1 2 96.19 109.14 3.28 o 3 1 2 1444.54 1437.54 17.14 o 4 1 2 2352.54 2292.44 25.82 o 5 1 2 3566.25 3566.59 39.08 o 6 1 2 2005.94 1947.15 30.61 o 7 1 2 1241.26 1221.01 21.93 o 8 1 2 588.16 622.41 16.69 o 9 1 2 221.38 198.01 10.93 o 10 1 2 38.50 32.04 3.91 o -11 2 2 507.08 549.71 16.73 o -10 2 2 166.89 160.53 11.47 o -9 2 2 264.19 266.62 10.31 o -8 2 2 681.19 661.52 15.62 o -7 2 2 194.34 208.12 7.07 o -6 2 2 92.18 82.71 3.77 o -5 2 2 1643.21 1626.74 16.71 o -4 2 2 29.89 23.21 1.77 o -3 2 2 3590.04 3447.14 26.91 o -2 2 2 5382.04 5552.41 43.27 o -1 2 2 2233.49 2236.27 17.81 o 0 2 2 9884.57 10326.00 89.42 o 1 2 2 1071.47 1251.65 11.90 o 2 2 2 3549.09 3684.28 48.84 o 3 2 2 0.17 0.66 0.94 o 4 2 2 584.89 607.92 9.79 o 5 2 2 212.13 224.65 7.62 o 6 2 2 197.75 200.91 8.14 o 7 2 2 0.88 -0.27 1.69 o 8 2 2 503.57 480.58 13.87 o 9 2 2 116.41 97.29 6.12 o 10 2 2 393.45 393.52 14.14 o -10 3 2 11.65 6.83 2.50 o -9 3 2 1437.86 1414.10 26.76 o -8 3 2 25.05 27.47 3.84 o -7 3 2 589.73 603.92 12.70 o -6 3 2 2136.21 2186.67 26.17 o -5 3 2 2464.45 2367.78 23.23 o -4 3 2 165.53 134.86 3.72 o -3 3 2 826.25 797.71 9.44 o -2 3 2 244.12 255.27 4.09 o -1 3 2 1642.57 1577.96 15.61 o 0 3 2 491.87 494.76 6.10 o 1 3 2 2662.73 2673.23 22.90 o 2 3 2 319.39 339.42 6.51 o 3 3 2 1396.30 1349.66 13.79 o 4 3 2 840.02 876.41 12.88 o 5 3 2 1390.81 1421.39 21.91 o 6 3 2 79.53 92.30 4.91 o 7 3 2 11.93 9.93 2.23 o 8 3 2 181.46 165.25 8.89 o 9 3 2 2.08 7.49 2.44 o 10 3 2 0.09 -0.38 2.52 o -10 4 2 18.47 16.30 3.35 o -9 4 2 174.30 167.40 8.78 o -8 4 2 248.09 236.65 8.41 o -7 4 2 216.69 224.82 7.25 o -6 4 2 49.99 50.65 3.24 o -5 4 2 81.95 87.33 3.48 o -4 4 2 11.35 14.88 1.53 o -3 4 2 889.93 933.70 10.68 o -2 4 2 1550.49 1493.84 15.78 o -1 4 2 2170.38 2113.86 19.53 o 1 4 2 3785.94 3743.15 31.25 o 2 4 2 2132.54 2194.96 21.75 o 3 4 2 1891.35 1832.47 18.26 o 4 4 2 327.71 345.60 7.64 o 5 4 2 400.82 415.52 10.63 o 6 4 2 103.50 111.06 5.77 o 7 4 2 570.41 548.02 15.24 o 8 4 2 412.52 426.11 12.38 o 9 4 2 1615.75 1595.58 32.68 o -10 5 2 181.79 153.52 11.28 o -9 5 2 365.70 371.45 15.17 o -8 5 2 1251.32 1271.82 25.02 o -7 5 2 31.06 25.56 3.19 o -6 5 2 1435.20 1455.81 28.61 o -5 5 2 557.80 552.48 9.40 o -4 5 2 2676.72 2747.05 25.03 o -3 5 2 314.98 323.22 5.68 o -2 5 2 734.30 749.19 10.47 o -1 5 2 197.02 214.65 4.31 o 0 5 2 1952.04 1913.90 16.32 o 1 5 2 907.83 993.71 12.46 o 2 5 2 2159.27 2156.04 20.90 o 3 5 2 118.20 101.11 3.42 o 4 5 2 526.84 480.42 10.55 o 5 5 2 789.66 763.88 17.31 o 6 5 2 29.12 27.98 3.59 o 7 5 2 212.95 224.11 8.97 o 8 5 2 49.21 48.66 4.61 o 9 5 2 53.65 55.62 5.00 o -10 6 2 99.45 102.18 9.45 o -9 6 2 651.29 642.88 17.82 o -8 6 2 111.18 122.06 6.67 o -7 6 2 2.38 0.52 2.12 o -6 6 2 140.37 138.81 7.06 o -5 6 2 551.87 551.60 12.04 o -4 6 2 1141.99 1119.94 17.56 o -3 6 2 446.09 410.52 9.45 o -2 6 2 2949.27 2918.03 27.89 o -1 6 2 292.78 251.96 5.54 o 0 6 2 112.94 83.53 2.94 o 1 6 2 1212.67 1262.52 16.88 o 2 6 2 826.37 775.18 13.26 o 3 6 2 604.13 573.87 11.60 o 4 6 2 54.76 45.67 3.94 o 5 6 2 73.03 78.30 5.31 o 6 6 2 99.80 92.67 7.24 o 7 6 2 346.06 316.69 11.11 o 8 6 2 115.71 108.12 7.22 o 9 6 2 51.50 56.82 7.06 o -9 7 2 141.11 141.77 9.56 o -8 7 2 265.31 276.38 10.41 o -7 7 2 705.82 729.49 17.97 o -6 7 2 24.39 19.27 3.11 o -5 7 2 204.21 191.30 7.16 o -4 7 2 194.98 194.00 6.93 o -3 7 2 346.61 391.47 9.41 o -2 7 2 36.50 35.65 2.97 o -1 7 2 774.26 803.05 15.64 o 0 7 2 74.69 59.43 2.83 o 1 7 2 195.08 180.47 5.78 o 2 7 2 25.09 26.56 2.54 o 3 7 2 47.89 44.61 3.49 o 4 7 2 3873.63 3924.54 49.06 o 5 7 2 103.80 95.97 6.13 o 6 7 2 1891.66 1958.00 37.63 o 7 7 2 14.72 13.22 3.33 o 8 7 2 685.03 704.34 25.24 o -9 8 2 84.15 80.80 9.89 o -8 8 2 82.85 89.45 5.94 o -7 8 2 1.30 1.09 2.11 o -6 8 2 123.63 130.29 6.93 o -5 8 2 137.74 155.13 6.55 o -4 8 2 197.09 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