#------------------------------------------------------------------------------ #$Date: 2010-11-03 10:57:48 +0200 (Wed, 03 Nov 2010) $ #$Revision: 1704 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2017742.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017742_Fobs loop_ _publ_author_name 'Wiklund, Tove' 'McKenzie, Christine J.' 'Lennartson, Anders' _publ_section_title ; Graphene-like nets of hydrogen-bonded water molecules in the dihydrate of 2-[(2-ammonioethyl)amino]acetate and the structure of its anhydrous hydroiodide salt ; _journal_coeditor_code DN3147 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o410 _journal_page_last o413 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.154 _cell_angle_gamma 90.000 _cell_length_a 4.7106 _cell_length_b 22.8634 _cell_length_c 7.2804 _exptl_crystal_F_000 336.00 _reflns_d_resolution_high 0.8108 _[local]_cod_data_source_file dn3147Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CM1004 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 106.26 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4609.02 4537.26 38.92 o 4 0 0 77.67 77.74 2.07 o 1 1 0 46.66 57.36 0.48 o 2 1 0 493.41 468.12 2.97 o 3 1 0 61.92 65.21 1.04 o 4 1 0 679.06 669.27 5.86 o 5 1 0 18.73 18.73 2.60 o 1 2 0 238.85 257.20 1.83 o 2 2 0 103.74 112.73 0.96 o 3 2 0 689.32 644.36 5.33 o 4 2 0 59.54 60.91 1.31 o 5 2 0 3.10 3.41 2.01 o 1 3 0 279.70 260.42 2.33 o 2 3 0 534.32 502.47 3.50 o 3 3 0 0.22 0.28 0.54 o 4 3 0 243.81 237.83 3.11 o 5 3 0 1.13 2.34 2.20 o 0 4 0 1725.30 1593.97 20.62 o 1 4 0 581.08 590.76 4.98 o 2 4 0 760.70 815.95 5.79 o 3 4 0 115.31 102.86 1.33 o 4 4 0 246.72 243.30 3.46 o 5 4 0 17.96 18.12 2.01 o 1 5 0 85.09 92.82 0.97 o 2 5 0 146.07 149.55 1.46 o 3 5 0 65.94 71.77 1.35 o 4 5 0 75.99 77.22 2.01 o 5 5 0 10.91 12.72 2.06 o 0 6 0 11292.11 9670.99 117.28 o 1 6 0 8399.71 7963.85 64.36 o 2 6 0 283.20 282.76 2.47 o 3 6 0 0.64 0.51 0.60 o 4 6 0 21.21 19.11 1.35 o 5 6 0 12.40 10.34 2.13 o 1 7 0 444.04 464.95 4.10 o 2 7 0 56.20 61.14 1.12 o 3 7 0 899.06 866.62 8.04 o 4 7 0 168.56 162.73 3.02 o 5 7 0 185.87 190.04 4.67 o 0 8 0 94.13 115.49 1.99 o 1 8 0 98.66 90.58 1.19 o 2 8 0 39.86 46.76 0.87 o 3 8 0 461.66 451.31 4.54 o 4 8 0 136.35 130.41 2.69 o 5 8 0 6.56 6.83 2.41 o 1 9 0 428.09 471.41 4.24 o 2 9 0 46.32 48.11 0.94 o 3 9 0 30.10 34.09 1.02 o 4 9 0 155.61 160.94 3.59 o 5 9 0 1.04 -2.29 2.29 o 0 10 0 247.80 309.94 4.36 o 1 10 0 159.43 161.47 1.76 o 2 10 0 0.85 1.15 0.58 o 3 10 0 182.03 182.00 2.36 o 4 10 0 48.94 47.87 1.85 o 5 10 0 14.08 11.81 2.58 o 1 11 0 708.32 772.22 6.29 o 2 11 0 93.20 103.19 1.65 o 3 11 0 171.41 171.26 2.32 o 4 11 0 0.75 1.28 1.36 o 5 11 0 1.75 1.97 2.53 o 0 12 0 36.48 35.77 1.29 o 1 12 0 54.73 54.29 1.04 o 2 12 0 34.63 30.59 0.89 o 3 12 0 839.88 820.46 8.18 o 4 12 0 1.94 2.21 1.51 o 5 12 0 6.09 6.64 2.73 o 1 13 0 21.24 21.64 0.80 o 2 13 0 117.17 116.20 2.06 o 3 13 0 263.60 267.48 5.25 o 4 13 0 46.97 45.02 2.16 o 5 13 0 1.26 1.48 2.97 o 0 14 0 39.70 39.17 1.95 o 1 14 0 319.16 319.03 3.35 o 2 14 0 13.37 14.66 0.85 o 3 14 0 504.11 508.29 11.57 o 4 14 0 60.82 65.07 2.92 o 1 15 0 149.56 166.22 2.24 o 2 15 0 1.79 0.28 0.73 o 3 15 0 33.43 30.12 2.19 o 4 15 0 4.61 0.39 2.12 o 0 16 0 1.47 3.59 1.16 o 1 16 0 529.07 546.83 6.36 o 2 16 0 27.56 22.10 1.15 o 3 16 0 4.76 3.97 1.74 o 4 16 0 23.87 25.86 2.63 o 1 17 0 250.40 252.12 3.39 o 2 17 0 133.78 141.02 2.49 o 3 17 0 171.71 177.13 5.15 o 4 17 0 87.49 77.37 3.54 o 0 18 0 438.99 444.84 6.47 o 1 18 0 2.24 1.55 1.06 o 2 18 0 828.55 775.36 9.71 o 3 18 0 180.99 182.72 7.88 o 4 18 0 172.46 178.43 5.17 o 1 19 0 8.24 11.20 1.21 o 2 19 0 6.75 4.29 1.55 o 3 19 0 0.29 -1.27 2.37 o 4 19 0 0.60 0.55 2.71 o 0 20 0 0.04 0.76 1.81 o 1 20 0 0.10 0.47 1.48 o 2 20 0 11.83 13.22 2.14 o 3 20 0 62.14 73.02 4.35 o 4 20 0 0.48 0.71 3.44 o 1 21 0 18.18 16.92 1.83 o 2 21 0 0.17 4.81 2.33 o 3 21 0 0.02 -1.42 2.97 o 0 22 0 383.68 361.85 9.23 o 1 22 0 11.89 17.18 2.09 o 2 22 0 11.00 14.78 3.69 o 3 22 0 3.67 3.09 3.51 o 1 23 0 17.41 15.86 2.17 o 2 23 0 174.65 173.42 6.74 o 3 23 0 0.15 2.49 4.62 o 0 24 0 23.86 22.54 3.48 o 1 24 0 181.83 167.86 4.84 o 2 24 0 178.87 183.28 10.30 o 3 24 0 36.81 46.61 6.45 o 1 25 0 17.25 18.84 2.68 o 2 25 0 0.00 -0.35 3.05 o 0 26 0 114.34 117.64 6.78 o 1 26 0 1.77 0.80 2.75 o 2 26 0 90.72 88.75 4.88 o 1 27 0 0.55 -2.13 3.67 o 0 28 0 12.44 12.15 6.22 o -5 0 1 40.47 40.36 4.27 o -3 0 1 1132.45 1141.61 10.71 o -1 0 1 484.66 528.89 5.46 o 1 0 1 2647.10 2713.51 25.81 o 3 0 1 0.01 -0.26 0.74 o 5 0 1 864.97 867.12 71.77 o -5 1 1 1.31 -0.56 1.76 o -4 1 1 1.62 1.67 0.72 o -3 1 1 26.99 31.72 0.76 o -2 1 1 8.86 7.36 0.38 o -1 1 1 55.71 54.68 0.61 o 1 1 1 5277.27 4944.72 37.27 o 2 1 1 297.02 311.12 2.42 o 3 1 1 12.10 13.45 0.63 o 4 1 1 28.02 29.00 1.27 o 5 1 1 8.51 9.76 2.05 o -5 2 1 19.49 21.58 2.10 o -4 2 1 98.92 100.04 1.48 o -3 2 1 448.98 458.62 3.39 o -2 2 1 1363.21 1367.23 8.54 o -1 2 1 1002.15 1070.74 7.28 o 1 2 1 3823.05 3842.58 31.99 o 2 2 1 170.67 151.91 1.41 o 3 2 1 1035.83 1000.07 7.50 o 4 2 1 177.19 160.45 2.56 o 5 2 1 0.44 -1.32 1.91 o -5 3 1 52.40 53.25 2.51 o -4 3 1 0.10 1.09 0.93 o -3 3 1 322.30 354.56 2.80 o -2 3 1 1253.73 1306.31 8.71 o -1 3 1 516.43 461.86 3.28 o 0 3 1 270.17 275.60 2.03 o 1 3 1 7812.50 7343.16 69.13 o 2 3 1 1.66 2.20 0.35 o 3 3 1 141.09 154.45 1.71 o 4 3 1 31.78 36.21 1.15 o 5 3 1 43.86 42.47 2.60 o -5 4 1 14.59 18.11 2.13 o -4 4 1 19.70 20.17 1.30 o -3 4 1 109.18 114.78 1.57 o -2 4 1 1190.75 1198.75 8.44 o -1 4 1 328.59 296.06 2.25 o 0 4 1 244.66 281.92 2.15 o 1 4 1 2345.86 2295.33 20.78 o 2 4 1 559.88 541.19 4.47 o 3 4 1 5.23 5.88 0.65 o 4 4 1 198.77 198.94 3.73 o 5 4 1 183.65 167.75 4.43 o -5 5 1 2.47 1.31 2.04 o -4 5 1 16.52 16.55 1.67 o -3 5 1 183.41 182.59 1.84 o -2 5 1 220.80 239.50 2.19 o -1 5 1 610.61 583.68 4.21 o 0 5 1 1042.67 912.64 6.37 o 1 5 1 141.26 149.84 1.53 o 2 5 1 93.02 94.88 1.71 o 3 5 1 156.46 154.61 1.95 o 4 5 1 234.42 238.45 3.50 o 5 5 1 89.68 93.76 3.65 o -5 6 1 62.24 54.24 4.23 o -4 6 1 222.00 223.04 3.71 o -3 6 1 67.22 59.17 0.99 o -2 6 1 1211.97 1216.19 9.27 o -1 6 1 1494.08 1495.84 10.90 o 0 6 1 238.86 263.01 2.03 o 1 6 1 24.94 29.19 0.82 o 2 6 1 222.32 253.42 2.78 o 3 6 1 1.19 0.95 0.66 o 4 6 1 289.89 283.15 3.96 o 5 6 1 316.89 291.38 6.65 o -5 7 1 26.93 26.94 2.74 o -4 7 1 66.58 62.97 1.87 o -3 7 1 55.19 57.29 1.61 o -2 7 1 35.17 34.46 0.80 o -1 7 1 0.59 -0.35 0.35 o 0 7 1 1848.15 1871.07 12.87 o 1 7 1 447.22 511.48 4.46 o 2 7 1 2914.74 2945.26 26.78 o 3 7 1 2.04 1.66 0.67 o 4 7 1 173.65 171.78 3.10 o 5 7 1 11.15 13.43 2.10 o -5 8 1 18.55 21.21 2.69 o -4 8 1 13.61 10.15 1.39 o -3 8 1 315.34 325.29 3.35 o -2 8 1 356.80 369.81 3.32 o -1 8 1 164.83 155.13 1.52 o 0 8 1 4.81 4.30 0.51 o 1 8 1 23.07 18.40 0.57 o 2 8 1 1024.08 1026.41 12.02 o 3 8 1 173.87 169.57 2.20 o 4 8 1 4.33 4.91 1.30 o 5 8 1 0.09 -1.67 1.96 o -5 9 1 8.38 4.68 2.82 o -4 9 1 18.83 17.59 1.52 o -3 9 1 0.04 -0.77 0.77 o -2 9 1 1640.24 1750.31 14.12 o -1 9 1 1672.88 1721.70 12.96 o 0 9 1 4.60 5.03 0.42 o 1 9 1 3068.97 3048.06 23.32 o 2 9 1 239.30 263.77 4.26 o 3 9 1 344.10 346.71 5.55 o 4 9 1 63.96 65.99 3.43 o 5 9 1 72.51 79.29 3.33 o -5 10 1 152.10 159.04 5.68 o -4 10 1 4.21 1.84 1.37 o -3 10 1 168.18 168.14 2.44 o -2 10 1 203.14 214.66 3.27 o -1 10 1 472.13 448.11 3.73 o 0 10 1 0.53 0.61 0.44 o 1 10 1 829.42 906.43 7.74 o 2 10 1 14.11 14.03 1.00 o 3 10 1 17.33 20.53 1.09 o 4 10 1 109.02 103.04 2.76 o 5 10 1 68.37 69.11 3.27 o -5 11 1 0.13 1.47 2.95 o -4 11 1 7.78 8.68 1.76 o -3 11 1 22.04 19.75 1.14 o -2 11 1 295.97 302.30 3.07 o -1 11 1 143.06 141.25 1.81 o 0 11 1 132.40 130.09 1.66 o 1 11 1 167.27 175.36 2.55 o 2 11 1 666.43 679.13 9.04 o 3 11 1 0.03 -0.95 1.05 o 4 11 1 461.60 472.03 6.82 o 5 11 1 4.49 6.22 2.45 o -5 12 1 38.64 36.95 3.66 o -4 12 1 158.34 153.23 3.94 o -3 12 1 420.62 426.55 4.60 o -2 12 1 433.44 422.85 4.50 o -1 12 1 716.86 718.07 6.12 o 0 12 1 750.61 769.43 6.28 o 1 12 1 3.71 4.12 0.64 o 2 12 1 60.31 76.70 1.60 o 3 12 1 27.40 27.41 1.42 o 4 12 1 113.12 106.68 2.74 o 5 12 1 1.19 1.78 2.48 o -5 13 1 0.94 3.10 3.47 o -4 13 1 53.21 51.77 3.26 o -3 13 1 40.55 37.14 1.70 o -2 13 1 446.39 453.08 5.02 o -1 13 1 28.53 29.42 0.92 o 0 13 1 17.92 17.05 0.76 o 1 13 1 746.47 727.32 7.95 o 2 13 1 558.02 585.64 6.32 o 3 13 1 480.84 471.98 6.72 o 4 13 1 28.89 31.49 1.77 o -5 14 1 29.08 26.16 5.90 o -4 14 1 0.26 0.06 2.03 o -3 14 1 181.67 168.54 3.59 o -2 14 1 316.02 315.64 3.81 o -1 14 1 248.61 251.01 2.72 o 0 14 1 524.62 561.11 5.30 o 1 14 1 21.14 27.72 1.20 o 2 14 1 0.81 1.18 0.94 o 3 14 1 0.31 0.91 1.26 o 4 14 1 0.34 0.13 1.58 o -4 15 1 4.39 3.56 2.24 o -3 15 1 0.65 0.46 1.43 o -2 15 1 166.33 166.91 2.55 o -1 15 1 691.55 668.71 6.07 o 0 15 1 221.07 243.92 2.68 o 1 15 1 126.78 118.61 3.12 o 2 15 1 238.53 236.99 4.34 o 3 15 1 63.44 62.87 3.27 o 4 15 1 31.09 27.03 2.05 o -4 16 1 5.92 7.42 2.41 o -3 16 1 62.34 67.05 3.31 o -2 16 1 297.81 295.62 3.77 o -1 16 1 272.85 268.63 2.98 o 0 16 1 190.76 206.38 2.62 o 1 16 1 513.72 510.88 6.30 o 2 16 1 102.24 112.99 2.88 o 3 16 1 24.12 29.80 2.59 o 4 16 1 84.65 81.99 3.63 o -4 17 1 43.31 43.67 5.38 o -3 17 1 37.51 36.09 2.88 o -2 17 1 77.63 80.28 2.59 o -1 17 1 19.23 28.05 1.11 o 0 17 1 57.28 52.19 1.40 o 1 17 1 1.31 1.36 1.02 o 2 17 1 189.35 194.88 3.73 o 3 17 1 68.92 76.77 2.79 o 4 17 1 93.81 105.02 4.20 o -4 18 1 112.69 113.12 4.74 o -3 18 1 15.37 15.89 2.69 o -2 18 1 284.06 274.60 4.46 o -1 18 1 192.39 188.96 2.80 o 0 18 1 125.10 123.81 2.17 o 1 18 1 49.96 52.54 2.16 o 2 18 1 141.91 138.36 5.24 o 3 18 1 9.87 12.44 2.45 o 4 18 1 8.81 11.72 2.82 o -4 19 1 1.54 1.42 3.57 o -3 19 1 21.53 31.82 4.11 o -2 19 1 293.44 295.01 9.54 o -1 19 1 547.65 502.76 7.75 o 0 19 1 275.66 248.42 3.68 o 1 19 1 34.03 35.20 1.85 o 2 19 1 79.02 78.80 3.41 o 3 19 1 60.20 62.82 3.50 o 4 19 1 30.01 33.21 3.67 o -4 20 1 74.00 75.35 5.93 o -3 20 1 48.94 56.52 4.14 o -2 20 1 0.15 1.47 1.84 o -1 20 1 427.36 431.22 7.40 o 0 20 1 24.44 26.69 1.68 o 1 20 1 175.69 170.63 3.95 o 2 20 1 0.36 1.65 2.29 o 3 20 1 38.75 28.94 3.02 o -3 21 1 0.01 0.75 3.17 o -2 21 1 20.20 24.54 2.44 o -1 21 1 249.13 229.31 4.44 o 0 21 1 19.18 21.01 1.99 o 1 21 1 22.23 18.25 1.95 o 2 21 1 0.13 2.57 2.69 o 3 21 1 28.16 27.00 3.52 o -3 22 1 6.60 4.61 3.54 o -2 22 1 38.43 48.53 3.30 o -1 22 1 0.04 2.15 1.73 o 0 22 1 106.97 110.92 3.67 o 1 22 1 8.27 6.37 1.93 o 2 22 1 28.59 37.72 2.68 o 3 22 1 4.11 5.26 3.36 o -3 23 1 5.74 6.16 3.79 o -2 23 1 21.97 30.12 4.33 o -1 23 1 41.06 34.41 2.80 o 0 23 1 0.00 3.02 2.04 o 1 23 1 0.19 -0.40 1.96 o 2 23 1 7.89 4.05 3.15 o 3 23 1 7.72 6.88 4.02 o -3 24 1 8.41 11.20 4.20 o -2 24 1 2.47 2.61 2.83 o -1 24 1 18.58 22.93 2.76 o 0 24 1 37.85 36.56 2.63 o 1 24 1 6.72 5.94 2.41 o 2 24 1 5.41 4.17 3.28 o -2 25 1 60.25 66.65 4.09 o -1 25 1 664.40 655.12 12.97 o 0 25 1 30.76 32.32 3.04 o 1 25 1 35.97 39.82 3.49 o 2 25 1 0.92 0.60 3.50 o -2 26 1 0.53 1.03 3.68 o -1 26 1 8.54 17.44 3.24 o 0 26 1 32.88 37.57 3.23 o 1 26 1 20.14 21.48 3.41 o 2 26 1 85.75 85.35 5.44 o -1 27 1 58.87 63.88 9.04 o 0 27 1 1.46 1.25 3.10 o 1 27 1 0.02 -1.85 3.58 o 0 28 1 10.78 11.57 4.70 o -4 0 2 85.68 87.03 2.52 o -2 0 2 182.79 158.43 2.44 o 0 0 2 596.00 525.70 6.18 o 2 0 2 879.83 849.58 9.95 o 4 0 2 167.20 160.46 3.42 o -5 1 2 77.48 80.80 2.87 o -4 1 2 254.50 240.52 3.15 o -3 1 2 0.27 -0.42 0.55 o -2 1 2 1615.06 1674.28 11.68 o -1 1 2 463.64 450.44 3.88 o 0 1 2 1548.16 1600.89 14.14 o 1 1 2 992.89 1001.66 7.40 o 2 1 2 1064.13 1102.54 8.21 o 3 1 2 68.76 64.20 1.21 o 4 1 2 30.93 30.43 1.19 o 5 1 2 142.36 143.84 3.98 o -5 2 2 24.90 26.89 2.15 o -4 2 2 24.78 28.80 1.29 o -3 2 2 7.15 6.53 0.59 o -2 2 2 15.18 15.95 0.62 o -1 2 2 18.00 14.44 0.49 o 0 2 2 1701.51 1637.27 11.63 o 1 2 2 45.09 36.09 0.70 o 2 2 2 38.10 34.35 0.84 o 3 2 2 245.79 230.88 2.40 o 4 2 2 0.03 0.26 0.90 o 5 2 2 0.30 -0.77 2.00 o -5 3 2 56.88 62.97 2.66 o -4 3 2 154.98 147.98 2.56 o -3 3 2 256.36 256.41 2.47 o -2 3 2 279.31 283.40 2.35 o -1 3 2 460.90 454.39 3.69 o 0 3 2 940.65 859.75 6.22 o 1 3 2 299.72 298.30 2.49 o 2 3 2 516.09 490.43 4.50 o 3 3 2 64.24 62.28 1.24 o 4 3 2 39.72 39.76 1.47 o 5 3 2 14.41 16.21 2.25 o -5 4 2 9.10 11.36 2.38 o -4 4 2 67.89 70.02 1.62 o -3 4 2 15.37 18.52 0.71 o -2 4 2 129.98 120.77 1.37 o -1 4 2 2526.63 2524.16 17.78 o 0 4 2 29.11 28.49 0.70 o 1 4 2 1371.75 1319.65 10.52 o 2 4 2 127.96 136.46 1.81 o 3 4 2 194.34 187.11 2.14 o 4 4 2 42.75 41.85 1.46 o 5 4 2 17.33 18.85 2.31 o -5 5 2 44.48 43.10 3.13 o -4 5 2 29.87 38.71 1.39 o -3 5 2 14.38 15.10 0.77 o -2 5 2 8.20 9.52 0.58 o -1 5 2 966.48 1050.31 7.81 o 0 5 2 86.34 89.14 0.95 o 1 5 2 259.21 251.36 2.32 o 2 5 2 10.78 10.65 0.69 o 3 5 2 91.34 84.16 1.40 o 4 5 2 125.73 119.81 2.31 o 5 5 2 460.29 446.25 8.85 o -5 6 2 108.24 108.53 6.68 o -4 6 2 0.15 0.72 1.06 o -3 6 2 38.15 38.57 1.10 o -2 6 2 147.21 137.99 1.44 o -1 6 2 503.80 477.99 3.79 o 0 6 2 422.98 380.14 2.89 o 1 6 2 57.99 59.81 0.97 o 2 6 2 16.92 24.68 0.86 o 3 6 2 224.80 222.29 2.88 o 4 6 2 14.97 14.57 1.56 o 5 6 2 21.79 25.47 3.14 o -5 7 2 15.47 12.94 3.09 o -4 7 2 243.78 231.87 3.63 o -3 7 2 744.40 725.23 6.31 o -2 7 2 357.02 349.00 3.01 o -1 7 2 3043.19 3195.84 23.05 o 0 7 2 1611.13 1693.78 11.74 o 1 7 2 77.06 87.81 1.39 o 2 7 2 2888.20 2970.04 27.16 o 3 7 2 219.15 218.31 2.87 o 4 7 2 158.98 158.34 3.24 o 5 7 2 20.12 17.12 2.39 o -5 8 2 3.11 3.54 2.70 o -4 8 2 71.57 69.10 1.96 o -3 8 2 33.40 30.45 1.08 o -2 8 2 308.60 315.32 3.12 o -1 8 2 285.36 301.74 2.60 o 0 8 2 99.03 110.41 1.20 o 1 8 2 356.98 369.41 3.69 o 2 8 2 54.21 52.39 1.37 o 3 8 2 410.22 386.01 4.37 o 4 8 2 3.20 4.72 2.00 o 5 8 2 43.02 39.44 3.31 o -5 9 2 48.12 52.07 4.06 o -4 9 2 40.97 47.93 1.78 o -3 9 2 108.60 107.76 1.68 o -2 9 2 24.30 20.07 0.80 o -1 9 2 299.24 312.89 2.86 o 0 9 2 207.25 220.52 2.08 o 1 9 2 173.39 170.58 1.74 o 2 9 2 109.35 112.23 2.03 o 3 9 2 261.05 261.83 4.48 o 4 9 2 1.90 -0.78 2.03 o 5 9 2 10.75 12.93 2.17 o -5 10 2 6.59 8.36 3.24 o -4 10 2 11.74 13.81 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