#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/77/2017787.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2017787_Fobs loop_ _publ_author_name 'Altaf, Muhammad' 'Stoeckli-Evans, Helen' _publ_section_title ; Green chemistry synthesis: 2-amino-3-[(E)-(2-pyridyl)methylideneamino]but-2-enedinitrile monohydrate and 5-cyano-2-(2-pyridyl)-1-(2-pyridylmethyl)-1H-imidazole-4-carboxamide ; _journal_coeditor_code BM3095 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o441 _journal_page_last o445 _journal_volume 66 _journal_year 2010 _space_group_IT_number 43 _symmetry_space_group_name_Hall 'F 2 -2d' _symmetry_space_group_name_H-M 'F d d 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 25.0720 _cell_length_b 46.9960 _cell_length_c 3.7592 _exptl_crystal_F_000 1792.00 _reflns_d_resolution_high 0.8372 _[local]_cod_data_source_file bm3095L1.H2Osup2.hkl _[local]_cod_data_source_block L1.H2O #BEGIN Tags that were not found in dictionaries: _shelx_title ' L1 IPDS2 -100DEGC FDD2 FDD2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 402.17 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x+1/4, y+1/4, z+1/4' 'x+3/4, -y+3/4, z+1/4' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' '-x+1/4, y+3/4, z+3/4' 'x+3/4, -y+5/4, z+3/4' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' '-x+3/4, y+1/4, z+3/4' 'x+5/4, -y+3/4, z+3/4' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' '-x+3/4, y+3/4, z+1/4' 'x+5/4, -y+5/4, z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 161740.42 269559.78 36871.59 o 8 0 0 88146.05 101193.44 1742.94 o 12 0 0 52479.88 62637.68 5779.96 o 16 0 0 2860.69 3447.07 260.92 o 20 0 0 201.20 273.80 167.55 o 24 0 0 75.02 137.87 120.11 o 28 0 0 2.08 77.49 171.04 o 2 2 0 4225.06 2167.81 224.61 o 4 2 0 19375.20 17719.42 1081.86 o 6 2 0 33606.16 37647.77 2313.01 o 8 2 0 3090.41 2925.91 245.80 o 10 2 0 3776.49 3963.58 101.93 o 12 2 0 1229.46 1472.25 146.18 o 14 2 0 5658.74 5896.60 247.75 o 16 2 0 9713.18 11501.04 1556.37 o 18 2 0 0.31 299.47 104.46 o 20 2 0 214.84 292.41 196.43 o 22 2 0 811.11 805.49 89.90 o 24 2 0 2772.05 2387.23 199.91 o 26 2 0 372.40 244.54 99.13 o 28 2 0 262.39 207.23 85.72 o 0 4 0 19939.25 18539.68 512.98 o 2 4 0 10894.69 12121.74 1373.17 o 4 4 0 23174.08 22955.70 604.41 o 6 4 0 1137.16 1214.34 111.53 o 8 4 0 5511.98 6165.47 164.84 o 10 4 0 5199.63 5356.04 656.23 o 12 4 0 2538.28 3074.89 173.10 o 14 4 0 180.09 101.36 84.75 o 16 4 0 4428.23 4090.51 346.58 o 18 4 0 467.48 512.38 71.67 o 20 4 0 420.52 654.66 108.94 o 22 4 0 219.92 110.95 82.60 o 24 4 0 432.98 450.61 100.64 o 26 4 0 52.42 232.38 97.24 o 28 4 0 107.09 15.18 84.58 o 2 6 0 2976.15 1667.82 166.34 o 4 6 0 28669.64 27992.19 5553.51 o 6 6 0 6633.92 6892.63 639.51 o 8 6 0 31337.87 36168.41 2292.26 o 10 6 0 7570.38 8756.02 1101.11 o 12 6 0 9586.70 9960.04 1554.43 o 14 6 0 501.05 332.96 79.23 o 16 6 0 905.70 764.10 101.70 o 18 6 0 168.18 149.20 69.84 o 20 6 0 1885.34 2135.01 314.64 o 22 6 0 36.93 11.89 70.80 o 24 6 0 1165.49 1511.00 427.44 o 26 6 0 5.18 78.49 95.01 o 28 6 0 315.31 323.16 123.46 o 0 8 0 118.41 1.12 139.95 o 2 8 0 47538.69 48992.67 674.72 o 4 8 0 3737.13 4438.84 866.75 o 6 8 0 24408.53 21937.96 5307.69 o 8 8 0 6714.64 6095.18 653.72 o 10 8 0 6256.98 5892.19 461.64 o 12 8 0 2554.09 2842.62 257.84 o 14 8 0 671.30 754.99 107.87 o 16 8 0 0.69 -19.75 102.17 o 18 8 0 294.52 312.08 82.00 o 20 8 0 1834.76 1831.89 180.61 o 22 8 0 36.83 131.35 77.49 o 24 8 0 54.82 191.30 94.74 o 26 8 0 117.43 -106.88 119.78 o 28 8 0 286.55 131.54 96.97 o 2 10 0 4962.87 4496.57 206.37 o 4 10 0 35746.39 37683.68 4569.17 o 6 10 0 1264.34 1063.15 223.52 o 8 10 0 6804.53 6401.04 443.89 o 10 10 0 825.83 731.64 109.56 o 12 10 0 899.01 925.08 158.56 o 14 10 0 5557.15 5472.12 273.28 o 16 10 0 144.26 152.28 74.55 o 18 10 0 166.88 28.75 117.82 o 20 10 0 21.58 13.94 76.13 o 22 10 0 1086.16 1034.88 108.99 o 24 10 0 80.80 49.74 100.94 o 26 10 0 467.31 441.29 95.49 o 28 10 0 440.38 421.87 89.22 o 0 12 0 47825.08 52720.41 884.22 o 2 12 0 9159.92 8390.41 501.39 o 4 12 0 4010.46 3859.29 454.09 o 6 12 0 19657.30 18937.71 2671.54 o 8 12 0 20296.41 20128.55 4048.87 o 10 12 0 6282.42 5789.41 516.05 o 12 12 0 460.25 409.70 77.72 o 14 12 0 53.34 125.44 69.39 o 16 12 0 242.68 280.88 68.87 o 18 12 0 2236.15 2009.32 134.95 o 20 12 0 1811.78 1772.24 352.46 o 22 12 0 5.80 132.73 104.40 o 24 12 0 82.28 155.79 87.75 o 26 12 0 94.24 45.99 95.08 o 28 12 0 822.66 646.43 95.50 o 2 14 0 1617.98 1385.37 100.65 o 4 14 0 47698.87 51645.98 3648.20 o 6 14 0 3295.03 2683.57 124.83 o 8 14 0 27.78 115.23 104.49 o 10 14 0 89.21 64.35 77.47 o 12 14 0 274.53 366.78 84.04 o 14 14 0 1605.10 1757.81 210.70 o 16 14 0 1613.71 1372.52 76.57 o 18 14 0 2869.09 2886.27 372.49 o 20 14 0 162.65 264.87 86.87 o 22 14 0 371.38 455.13 76.95 o 24 14 0 504.28 351.02 79.05 o 26 14 0 1.65 9.02 81.79 o 28 14 0 2.38 199.40 129.52 o 0 16 0 173.80 222.99 90.55 o 2 16 0 6757.95 6009.80 301.91 o 4 16 0 9314.42 7990.68 161.30 o 6 16 0 3119.56 3639.71 165.23 o 8 16 0 7340.34 6040.54 159.74 o 10 16 0 379.82 321.12 98.85 o 12 16 0 2341.78 1961.33 143.54 o 14 16 0 2567.20 2400.40 137.91 o 16 16 0 75.99 77.21 72.27 o 18 16 0 2647.57 2580.01 226.45 o 20 16 0 651.21 850.57 218.66 o 22 16 0 185.03 260.01 81.85 o 24 16 0 46.36 97.63 101.82 o 26 16 0 10.59 -69.34 74.31 o 28 16 0 12.57 180.48 184.78 o 2 18 0 40374.49 39367.29 630.66 o 4 18 0 16.43 299.24 114.48 o 6 18 0 16547.61 17639.22 661.99 o 8 18 0 11475.90 12380.28 1784.06 o 10 18 0 7842.73 8249.59 891.74 o 12 18 0 632.37 683.82 118.91 o 14 18 0 2149.94 1969.19 191.76 o 16 18 0 4748.17 4135.63 212.28 o 18 18 0 3715.07 3345.22 392.18 o 20 18 0 6459.66 6650.61 357.46 o 22 18 0 615.45 533.29 224.39 o 24 18 0 3.62 144.70 120.93 o 26 18 0 35.89 113.83 112.02 o 28 18 0 716.32 557.05 245.37 o 0 20 0 7668.35 6933.44 251.45 o 2 20 0 1369.03 1782.54 105.07 o 4 20 0 9409.77 7562.96 160.38 o 6 20 0 5832.82 6709.91 524.91 o 8 20 0 0.89 133.68 94.34 o 10 20 0 17530.81 21720.20 1511.10 o 12 20 0 307.63 340.11 76.26 o 14 20 0 223.93 295.74 74.18 o 16 20 0 1133.51 1161.95 83.42 o 18 20 0 16361.03 17566.11 2896.93 o 20 20 0 1535.52 1696.65 249.84 o 22 20 0 9484.67 10786.78 1907.00 o 24 20 0 714.56 810.18 100.56 o 26 20 0 494.40 473.83 90.97 o 2 22 0 8638.66 9923.98 562.56 o 4 22 0 17215.10 17470.62 271.62 o 6 22 0 23639.22 24321.39 1902.31 o 8 22 0 2015.31 2305.08 148.22 o 10 22 0 15.63 203.91 86.87 o 12 22 0 1609.21 1545.23 107.29 o 14 22 0 1863.89 2045.29 95.87 o 16 22 0 758.30 772.60 87.43 o 18 22 0 1136.21 1241.61 137.39 o 20 22 0 2546.83 2809.04 325.27 o 22 22 0 351.62 381.84 92.42 o 24 22 0 99.41 26.16 77.92 o 26 22 0 130.95 10.37 81.77 o 0 24 0 10433.66 11770.53 663.31 o 2 24 0 27.71 35.87 80.46 o 4 24 0 2050.91 2700.95 115.56 o 6 24 0 770.11 1171.93 110.92 o 8 24 0 1042.80 1253.49 112.85 o 10 24 0 43.22 38.26 81.04 o 12 24 0 1859.84 1769.25 222.60 o 14 24 0 6782.45 6722.11 826.06 o 16 24 0 49.79 76.77 78.18 o 18 24 0 6560.51 6284.24 490.88 o 20 24 0 2793.98 2742.64 360.93 o 22 24 0 2909.28 2898.44 416.74 o 24 24 0 465.80 422.84 82.17 o 26 24 0 133.33 -19.50 90.48 o 2 26 0 162.15 56.50 76.63 o 4 26 0 1444.90 1619.08 111.33 o 6 26 0 10.22 -54.97 100.22 o 8 26 0 1530.19 1761.44 164.38 o 10 26 0 205.26 273.77 98.53 o 12 26 0 3668.49 4013.45 428.09 o 14 26 0 55.51 131.52 75.43 o 16 26 0 965.25 976.67 123.86 o 18 26 0 4396.85 5166.13 829.61 o 20 26 0 4.04 25.59 76.36 o 22 26 0 81.12 131.75 87.27 o 24 26 0 756.78 962.24 105.87 o 26 26 0 83.50 240.18 107.72 o 0 28 0 3448.96 3137.77 123.16 o 2 28 0 676.78 673.16 92.07 o 4 28 0 1264.82 1391.09 101.16 o 6 28 0 1448.69 1913.78 132.49 o 8 28 0 5017.48 5699.89 390.36 o 10 28 0 241.90 314.86 88.73 o 12 28 0 649.56 726.02 93.77 o 14 28 0 89.45 124.12 70.11 o 16 28 0 1.24 2.12 130.65 o 18 28 0 156.27 133.36 81.37 o 20 28 0 108.54 301.92 112.43 o 22 28 0 51.96 116.90 87.15 o 24 28 0 21.91 29.59 83.32 o 2 30 0 1061.22 1293.10 84.18 o 4 30 0 0.82 -0.45 86.90 o 6 30 0 1061.68 1147.53 107.19 o 8 30 0 1630.24 1900.10 200.65 o 10 30 0 4556.03 4619.61 354.88 o 12 30 0 46.32 175.85 85.98 o 14 30 0 179.61 152.43 74.59 o 16 30 0 1819.30 1980.84 216.12 o 18 30 0 869.12 1139.58 113.28 o 20 30 0 94.42 102.83 95.25 o 22 30 0 1279.31 1048.04 101.24 o 24 30 0 552.51 412.21 106.09 o 0 32 0 2454.49 3042.73 281.94 o 2 32 0 5149.81 4756.24 158.82 o 4 32 0 4497.78 5440.99 331.13 o 6 32 0 1937.82 1938.15 124.30 o 8 32 0 89.78 143.20 79.50 o 10 32 0 106.94 134.79 80.27 o 12 32 0 14.40 -5.97 88.38 o 14 32 0 0.64 10.89 74.16 o 16 32 0 237.29 177.09 85.91 o 18 32 0 11.47 100.06 82.82 o 20 32 0 81.10 85.02 80.47 o 22 32 0 8.56 80.22 93.06 o 24 32 0 356.17 317.07 160.82 o 2 34 0 864.33 1030.33 86.15 o 4 34 0 67.82 180.86 73.93 o 6 34 0 26.30 105.01 83.77 o 8 34 0 112.36 154.85 74.56 o 10 34 0 261.90 304.48 93.22 o 12 34 0 11.32 84.61 91.07 o 14 34 0 143.57 120.10 76.08 o 16 34 0 92.27 99.75 65.63 o 18 34 0 626.96 750.14 96.83 o 20 34 0 31.60 55.68 77.25 o 22 34 0 1.62 58.65 93.69 o 0 36 0 2471.59 2625.73 161.45 o 2 36 0 0.21 94.47 82.73 o 4 36 0 7.39 57.64 92.33 o 6 36 0 55.20 164.47 96.33 o 8 36 0 42.47 50.52 107.25 o 10 36 0 761.52 878.01 114.56 o 12 36 0 1170.51 1221.17 110.10 o 14 36 0 80.57 116.50 69.20 o 16 36 0 84.65 172.38 79.17 o 18 36 0 142.80 215.79 91.08 o 20 36 0 909.63 827.82 143.69 o 22 36 0 299.18 318.66 89.46 o 2 38 0 1773.35 2094.75 104.62 o 4 38 0 3250.89 3585.14 275.00 o 6 38 0 0.21 -23.37 84.21 o 8 38 0 33.69 129.37 112.13 o 10 38 0 1508.61 1170.11 135.71 o 12 38 0 581.22 605.92 115.94 o 14 38 0 434.33 653.79 91.62 o 16 38 0 1237.23 1096.40 124.78 o 18 38 0 98.70 95.36 76.96 o 20 38 0 174.40 197.40 81.21 o 22 38 0 99.80 479.53 219.85 o 0 40 0 21147.29 22812.19 555.95 o 2 40 0 2659.40 2785.73 163.81 o 4 40 0 4066.59 4845.99 160.55 o 6 40 0 582.28 577.13 93.97 o 8 40 0 479.81 296.38 90.53 o 10 40 0 70.57 89.71 114.32 o 12 40 0 1846.65 1537.28 264.36 o 14 40 0 10.77 48.70 81.36 o 16 40 0 472.84 498.55 87.40 o 18 40 0 93.44 49.45 104.38 o 20 40 0 139.51 72.70 90.48 o 2 42 0 39.16 251.64 94.34 o 4 42 0 5074.95 6017.79 459.35 o 6 42 0 168.77 105.18 116.53 o 8 42 0 3.75 11.98 117.28 o 10 42 0 2.50 0.32 102.11 o 12 42 0 1048.74 900.03 161.23 o 14 42 0 306.96 323.94 94.37 o 16 42 0 1018.10 972.45 93.60 o 18 42 0 18.30 66.65 94.03 o 0 44 0 996.45 1021.60 118.10 o 2 44 0 12796.22 13603.03 880.18 o 4 44 0 4142.04 4476.08 585.68 o 6 44 0 1435.47 1468.23 212.36 o 8 44 0 705.10 786.79 116.61 o 10 44 0 1134.28 1056.39 171.11 o 12 44 0 218.64 153.39 122.03 o 14 44 0 309.94 240.59 92.69 o 16 44 0 43.21 10.32 104.57 o 18 44 0 24.97 69.82 96.70 o 2 46 0 54.01 119.25 120.74 o 4 46 0 421.66 458.98 95.54 o 6 46 0 179.06 327.38 120.35 o 8 46 0 25.64 -9.11 105.15 o 10 46 0 619.21 562.84 125.34 o 12 46 0 86.83 68.99 96.22 o 14 46 0 135.26 140.81 88.33 o 16 46 0 50.39 69.50 87.82 o 0 48 0 364.04 446.67 147.98 o 2 48 0 688.74 699.28 125.81 o 4 48 0 75.58 123.88 104.16 o 6 48 0 0.41 254.86 122.30 o 8 48 0 1.20 4.84 107.94 o 10 48 0 409.19 321.54 98.00 o 12 48 0 879.79 829.80 183.06 o 14 48 0 214.71 243.80 96.48 o 2 50 0 942.25 1035.04 158.09 o 4 50 0 6.02 109.40 107.25 o 6 50 0 0.98 -16.46 104.20 o 8 50 0 0.73 21.54 107.51 o 10 50 0 262.01 140.39 127.83 o 12 50 0 86.59 124.18 101.47 o 0 52 0 22.18 151.59 120.44 o 2 52 0 84.42 145.39 104.96 o 4 52 0 5.01 -22.65 124.59 o 6 52 0 0.35 24.39 106.74 o 8 52 0 3.65 62.72 109.82 o 10 52 0 0.05 129.54 126.05 o 2 54 0 51.62 -11.87 107.52 o 4 54 0 73.15 56.36 109.33 o 6 54 0 271.43 215.82 99.63 o 8 54 0 89.65 159.48 201.01 o 0 56 0 60.89 77.65 207.64 o 1 1 1 19379.79 12087.73 463.41 o 3 1 1 4856.53 4088.53 366.70 o 5 1 1 6334.87 7020.80 449.07 o 7 1 1 17161.29 17537.73 1367.19 o 9 1 1 6784.04 6072.57 483.49 o 11 1 1 676.72 449.45 67.14 o 13 1 1 3027.72 3424.76 294.22 o 15 1 1 473.56 453.98 66.52 o 17 1 1 1041.36 1066.62 83.43 o 19 1 1 1621.42 1694.02 215.49 o 21 1 1 1470.49 1618.21 174.00 o 23 1 1 98.78 84.23 55.24 o 25 1 1 410.60 308.57 56.81 o 27 1 1 144.54 147.63 67.79 o 29 1 1 165.60 220.19 81.97 o 1 3 1 50498.99 37044.11 2514.10 o 3 3 1 57147.07 46493.26 2609.20 o 5 3 1 48880.22 51032.27 3673.08 o 7 3 1 5685.29 5223.26 207.83 o 9 3 1 1109.00 868.05 90.64 o 11 3 1 2446.61 2692.65 175.92 o 13 3 1 938.75 1089.50 67.87 o 15 3 1 4154.18 5042.61 386.12 o 17 3 1 1083.09 1385.38 80.73 o 19 3 1 22.80 32.91 54.30 o 21 3 1 1012.76 1002.77 98.02 o 23 3 1 2.84 21.00 57.91 o 25 3 1 157.71 154.31 56.30 o 27 3 1 220.50 210.80 67.98 o 29 3 1 271.36 247.43 69.73 o 1 5 1 119310.13 134685.14 6125.78 o 3 5 1 119999.09 145088.86 4830.06 o 5 5 1 46489.45 49123.16 1018.08 o 7 5 1 8782.58 9359.01 689.69 o 9 5 1 15177.17 17041.54 657.67 o 11 5 1 7284.72 6806.65 683.99 o 13 5 1 8619.41 10703.55 741.12 o 15 5 1 299.18 367.69 59.15 o 17 5 1 2563.04 3017.31 175.96 o 19 5 1 988.66 979.70 56.91 o 21 5 1 1025.45 1173.18 170.03 o 23 5 1 466.64 447.85 62.82 o 25 5 1 360.35 353.78 57.41 o 27 5 1 162.02 80.15 73.35 o 29 5 1 144.91 89.41 118.49 o 1 7 1 417.45 221.49 60.38 o 3 7 1 15180.84 13458.19 1067.01 o 5 7 1 16603.60 15790.67 1704.04 o 7 7 1 10847.84 11036.12 438.13 o 9 7 1 6247.38 5507.08 390.39 o 11 7 1 1688.54 1803.76 176.02 o 13 7 1 2014.69 2972.48 251.20 o 15 7 1 190.25 208.77 59.47 o 17 7 1 674.85 834.23 74.00 o 19 7 1 729.20 739.60 59.55 o 21 7 1 52.31 -3.69 79.35 o 23 7 1 90.26 50.00 60.02 o 25 7 1 457.10 564.71 87.33 o 27 7 1 112.38 124.03 68.82 o 1 9 1 9517.80 8936.66 228.48 o 3 9 1 1264.79 1334.65 64.88 o 5 9 1 2960.95 3095.73 163.12 o 7 9 1 5981.64 4926.24 262.34 o 9 9 1 2184.36 2373.78 188.87 o 11 9 1 1191.21 1531.33 118.69 o 13 9 1 3143.78 3076.54 236.59 o 15 9 1 687.17 731.32 74.82 o 17 9 1 315.12 306.52 71.40 o 19 9 1 325.72 464.23 57.48 o 21 9 1 1548.35 1820.97 213.55 o 23 9 1 859.68 1012.48 112.66 o 25 9 1 325.98 381.88 64.44 o 27 9 1 167.01 110.40 61.61 o 1 11 1 13967.26 10950.76 400.76 o 3 11 1 528.48 348.15 62.74 o 5 11 1 369.30 409.63 69.08 o 7 11 1 2833.22 2686.52 232.33 o 9 11 1 6516.76 6433.98 353.72 o 11 11 1 5829.34 5868.93 448.59 o 13 11 1 291.78 176.20 62.69 o 15 11 1 963.91 919.13 86.05 o 17 11 1 1038.28 1075.70 66.53 o 19 11 1 275.27 268.80 54.69 o 21 11 1 407.54 483.58 69.91 o 23 11 1 119.60 136.38 64.23 o 25 11 1 240.35 232.85 115.69 o 27 11 1 54.76 174.89 79.81 o 1 13 1 3889.16 3029.20 92.58 o 3 13 1 2935.63 2815.15 133.37 o 5 13 1 6642.82 6381.45 340.84 o 7 13 1 10129.69 11646.58 335.77 o 9 13 1 2403.67 2265.75 93.50 o 11 13 1 4152.99 4470.30 275.52 o 13 13 1 2100.56 2412.46 187.57 o 15 13 1 1017.45 1081.36 118.90 o 17 13 1 1677.75 1841.98 162.71 o 19 13 1 1411.02 1557.80 202.25 o 21 13 1 456.14 544.04 97.64 o 23 13 1 852.30 872.82 170.44 o 25 13 1 265.88 347.55 70.60 o 27 13 1 199.76 81.97 97.82 o 1 15 1 25313.37 24962.01 452.31 o 3 15 1 4643.18 3913.62 88.68 o 5 15 1 291.98 318.76 89.99 o 7 15 1 1094.77 1166.23 76.29 o 9 15 1 4093.26 4226.22 121.76 o 11 15 1 2607.96 3351.88 307.27 o 13 15 1 1188.42 1318.27 74.00 o 15 15 1 193.53 199.31 77.44 o 17 15 1 4390.47 4462.02 406.13 o 19 15 1 2342.95 2860.09 343.99 o 21 15 1 3174.99 3082.22 275.91 o 23 15 1 2231.68 2069.25 103.89 o 25 15 1 334.40 327.19 61.42 o 27 15 1 31.58 53.55 65.80 o 1 17 1 20246.50 19297.01 525.31 o 3 17 1 17120.83 17070.26 914.68 o 5 17 1 3535.31 3400.19 187.77 o 7 17 1 3976.22 4332.73 105.32 o 9 17 1 2338.27 2383.39 144.52 o 11 17 1 2512.34 2535.13 233.96 o 13 17 1 1778.48 1608.28 216.93 o 15 17 1 165.72 139.12 78.94 o 17 17 1 3773.28 4310.61 474.41 o 19 17 1 1220.08 1216.32 95.51 o 21 17 1 127.89 189.92 64.73 o 23 17 1 380.52 442.66 64.77 o 25 17 1 341.65 302.81 85.55 o 27 17 1 76.36 164.51 68.85 o 1 19 1 3389.46 3222.82 125.65 o 3 19 1 2092.97 2322.17 76.99 o 5 19 1 4091.28 4044.52 241.02 o 7 19 1 3551.60 3283.37 211.94 o 9 19 1 3250.07 3529.09 189.93 o 11 19 1 2326.90 2470.04 86.03 o 13 19 1 477.34 468.58 67.17 o 15 19 1 3197.36 3783.56 102.90 o 17 19 1 4713.66 4877.43 213.44 o 19 19 1 2232.47 2257.72 231.86 o 21 19 1 1471.76 1445.45 110.41 o 23 19 1 675.44 852.17 83.24 o 25 19 1 157.55 182.63 78.80 o 27 19 1 276.33 213.25 84.48 o 1 21 1 1790.13 1826.82 122.62 o 3 21 1 5093.68 5238.36 275.02 o 5 21 1 994.55 926.39 72.51 o 7 21 1 3909.78 4168.57 273.02 o 9 21 1 961.61 1059.10 67.38 o 11 21 1 3996.27 4070.50 197.82 o 13 21 1 1160.73 1057.88 59.34 o 15 21 1 6517.85 6728.34 793.01 o 17 21 1 1396.78 1562.38 157.64 o 19 21 1 2204.86 2233.14 211.70 o 21 21 1 341.70 339.65 70.11 o 23 21 1 30.45 66.19 65.98 o 25 21 1 88.89 -11.04 81.64 o 1 23 1 78.36 128.53 73.87 o 3 23 1 931.72 781.06 61.22 o 5 23 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22 2 111.07 60.62 72.79 o 16 22 2 599.07 589.87 69.02 o 18 22 2 532.60 526.33 66.31 o 20 22 2 30.50 36.43 61.56 o 22 22 2 140.45 230.74 68.99 o 24 22 2 64.17 204.11 71.88 o 2 24 2 1119.17 1143.43 63.70 o 4 24 2 169.45 229.89 63.06 o 6 24 2 42.18 -33.90 69.32 o 8 24 2 340.32 446.40 78.45 o 10 24 2 362.68 327.37 61.33 o 12 24 2 468.65 649.88 85.88 o 14 24 2 262.51 439.06 78.28 o 16 24 2 276.90 212.13 64.94 o 18 24 2 157.06 170.26 68.54 o 20 24 2 121.69 164.18 69.55 o 22 24 2 51.90 141.05 78.51 o 0 26 2 1087.45 1164.58 94.15 o 2 26 2 3003.64 2872.91 99.69 o 4 26 2 268.40 273.33 59.21 o 6 26 2 1706.79 1643.96 79.45 o 8 26 2 849.64 799.96 68.69 o 10 26 2 843.76 1087.40 128.86 o 12 26 2 928.54 1004.26 65.63 o 14 26 2 1420.10 1470.45 72.60 o 16 26 2 1245.39 1288.99 80.35 o 18 26 2 24.90 60.12 64.10 o 20 26 2 33.85 36.79 70.12 o 22 26 2 54.33 99.46 73.36 o 2 28 2 748.74 849.29 71.23 o 4 28 2 1157.04 1113.25 78.02 o 6 28 2 631.51 775.66 81.44 o 8 28 2 497.82 485.21 69.73 o 10 28 2 2822.16 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82.30 o 8 42 2 8.22 132.10 99.20 o 10 42 2 40.26 9.83 89.18 o 12 42 2 66.04 125.24 79.24 o 14 42 2 2.78 42.05 83.74 o 2 44 2 5.79 49.89 78.47 o 4 44 2 201.12 124.06 105.93 o 6 44 2 112.96 118.05 90.21 o 8 44 2 6.24 -13.00 82.88 o 10 44 2 19.63 71.46 84.26 o 12 44 2 2.85 52.24 83.98 o 0 46 2 161.52 214.66 109.53 o 2 46 2 83.74 83.14 76.44 o 4 46 2 58.05 78.41 94.88 o 6 46 2 683.15 637.29 96.45 o 8 46 2 600.12 520.40 80.23 o 10 46 2 11.04 91.88 85.45 o 2 48 2 66.32 81.54 73.53 o 4 48 2 31.90 106.58 87.82 o 6 48 2 138.82 67.22 85.85 o 0 50 2 399.66 231.74 117.92 o 2 50 2 581.24 299.63 123.32 o 1 1 3 406.86 483.25 66.13 o 3 1 3 105.22 154.74 59.76 o 5 1 3 209.21 195.21 58.16 o 7 1 3 115.83 153.75 54.58 o 9 1 3 18.53 55.85 49.97 o 11 1 3 451.19 440.80 55.13 o 13 1 3 758.62 777.31 56.19 o 15 1 3 592.68 581.42 56.95 o 17 1 3 306.20 313.15 57.15 o 19 1 3 153.23 191.14 62.55 o 21 1 3 16.55 -49.23 68.74 o 1 3 3 171.90 346.34 74.76 o 3 3 3 329.62 399.13 59.79 o 5 3 3 334.54 474.56 58.56 o 7 3 3 339.95 332.02 54.45 o 9 3 3 172.67 179.18 63.52 o 11 3 3 193.27 135.05 47.19 o 13 3 3 161.91 211.38 53.23 o 15 3 3 235.53 145.18 54.61 o 17 3 3 23.87 40.72 72.74 o 19 3 3 356.58 365.23 68.81 o 21 3 3 197.48 168.01 70.61 o 1 5 3 316.45 322.37 69.36 o 3 5 3 1641.57 1593.58 115.11 o 5 5 3 642.54 611.26 56.62 o 7 5 3 44.07 149.87 50.72 o 9 5 3 751.59 798.32 108.67 o 11 5 3 811.08 739.61 59.87 o 13 5 3 104.39 67.36 55.70 o 15 5 3 316.74 255.61 53.69 o 17 5 3 175.56 222.68 62.79 o 19 5 3 92.88 111.59 64.14 o 21 5 3 128.83 247.80 68.48 o 1 7 3 816.60 878.86 59.07 o 3 7 3 169.94 269.29 63.09 o 5 7 3 951.85 900.80 55.68 o 7 7 3 146.60 152.89 61.37 o 9 7 3 236.96 237.02 51.91 o 11 7 3 618.76 623.66 64.52 o 13 7 3 494.70 528.44 61.26 o 15 7 3 465.82 392.53 73.15 o 17 7 3 252.99 184.00 63.47 o 19 7 3 10.52 84.56 67.31 o 21 7 3 117.79 149.65 73.86 o 1 9 3 2049.51 2161.78 177.10 o 3 9 3 419.12 472.49 64.94 o 5 9 3 1218.25 1243.36 114.80 o 7 9 3 1255.27 1269.35 110.24 o 9 9 3 1339.40 1325.98 76.13 o 11 9 3 825.29 817.05 72.25 o 13 9 3 2059.22 1960.08 140.88 o 15 9 3 1891.10 1886.63 79.40 o 17 9 3 181.58 199.22 69.10 o 19 9 3 208.47 126.63 65.57 o 21 9 3 111.53 90.56 67.21 o 1 11 3 235.96 310.70 60.97 o 3 11 3 2769.00 3245.17 153.84 o 5 11 3 1995.40 2298.11 142.77 o 7 11 3 1921.21 2035.34 118.64 o 9 11 3 4219.18 4456.98 267.03 o 11 11 3 4603.20 5023.87 288.61 o 13 11 3 550.38 485.43 56.95 o 15 11 3 1773.65 1785.89 99.81 o 17 11 3 4.99 91.98 69.44 o 19 11 3 312.97 283.82 84.31 o 21 11 3 102.35 119.93 84.50 o 1 13 3 31.13 -5.42 68.72 o 3 13 3 1107.46 1028.22 91.38 o 5 13 3 486.47 441.60 53.49 o 7 13 3 1392.99 1282.88 75.94 o 9 13 3 5102.25 4830.45 411.97 o 11 13 3 180.16 215.67 55.64 o 13 13 3 905.27 802.40 104.78 o 15 13 3 132.92 125.32 63.89 o 17 13 3 265.85 300.20 64.91 o 19 13 3 24.07 87.38 72.18 o 21 13 3 232.23 290.16 70.29 o 1 15 3 1168.06 1200.48 60.41 o 3 15 3 768.29 842.94 66.66 o 5 15 3 949.18 948.10 65.98 o 7 15 3 1506.37 1433.24 83.75 o 9 15 3 1061.20 1172.37 78.93 o 11 15 3 164.04 219.96 54.72 o 13 15 3 428.48 285.74 99.79 o 15 15 3 261.66 219.59 66.95 o 17 15 3 76.80 70.85 71.97 o 19 15 3 50.14 76.62 77.89 o 1 17 3 513.10 513.83 59.20 o 3 17 3 1190.26 1140.74 103.34 o 5 17 3 380.64 436.99 68.91 o 7 17 3 258.99 202.29 63.92 o 9 17 3 6.74 30.46 62.62 o 11 17 3 90.93 103.13 54.07 o 13 17 3 194.13 187.00 68.77 o 15 17 3 324.57 351.59 66.49 o 17 17 3 148.04 73.95 72.37 o 19 17 3 273.29 223.90 67.62 o 1 19 3 499.61 611.99 63.41 o 3 19 3 323.08 371.95 59.32 o 5 19 3 641.27 615.48 60.90 o 7 19 3 1120.36 1173.90 86.20 o 9 19 3 25.53 68.39 57.30 o 11 19 3 201.04 238.23 69.40 o 13 19 3 590.45 602.68 81.29 o 15 19 3 470.66 467.78 65.46 o 17 19 3 104.27 148.21 72.91 o 19 19 3 72.91 65.97 70.35 o 1 21 3 75.09 104.09 59.28 o 3 21 3 421.22 489.61 61.65 o 5 21 3 160.74 203.00 61.91 o 7 21 3 79.24 93.31 65.36 o 9 21 3 35.40 38.45 63.16 o 11 21 3 247.48 251.50 67.67 o 13 21 3 180.15 207.83 75.47 o 15 21 3 14.25 26.19 69.62 o 17 21 3 3.22 -6.81 79.78 o 19 21 3 33.05 186.73 69.09 o 1 23 3 31.90 -21.38 55.89 o 3 23 3 504.48 450.77 56.00 o 5 23 3 330.68 357.10 66.34 o 7 23 3 83.79 128.92 62.88 o 9 23 3 222.40 264.41 63.30 o 11 23 3 705.62 766.10 80.03 o 13 23 3 19.63 -51.73 73.73 o 15 23 3 51.93 130.57 70.15 o 17 23 3 44.72 95.86 71.22 o 1 25 3 115.16 152.88 59.19 o 3 25 3 11.26 2.40 58.22 o 5 25 3 158.39 215.82 66.47 o 7 25 3 90.79 94.82 67.19 o 9 25 3 132.54 147.76 68.18 o 11 25 3 398.57 286.27 71.79 o 13 25 3 263.50 207.50 78.72 o 15 25 3 69.70 137.23 83.09 o 17 25 3 90.71 9.24 70.66 o 1 27 3 214.99 153.75 55.50 o 3 27 3 125.12 81.48 55.81 o 5 27 3 253.63 216.32 83.20 o 7 27 3 741.88 827.31 73.38 o 9 27 3 302.24 244.60 86.63 o 11 27 3 116.28 169.10 84.96 o 13 27 3 38.76 178.28 100.96 o 15 27 3 25.50 -74.35 74.35 o 17 27 3 89.67 179.86 84.66 o 1 29 3 294.19 268.45 58.25 o 3 29 3 1603.32 1746.42 106.34 o 5 29 3 2771.24 2992.71 188.25 o 7 29 3 1464.71 1244.50 98.85 o 9 29 3 2394.54 2480.59 129.78 o 11 29 3 208.77 278.90 73.79 o 13 29 3 95.68 32.24 77.08 o 15 29 3 143.83 139.63 78.74 o 1 31 3 816.01 782.81 78.53 o 3 31 3 287.78 328.92 67.14 o 5 31 3 167.38 285.72 70.10 o 7 31 3 1660.37 1479.36 80.05 o 9 31 3 26.06 34.34 66.83 o 11 31 3 1569.85 1441.58 137.77 o 13 31 3 319.32 316.28 91.80 o 1 33 3 83.16 -34.71 80.51 o 3 33 3 3.32 -26.37 62.71 o 5 33 3 434.40 417.42 68.80 o 7 33 3 79.08 49.11 65.25 o 9 33 3 952.63 888.15 106.56 o 11 33 3 425.54 138.85 92.13 o 13 33 3 662.79 603.21 147.86 o 1 35 3 58.70 110.52 69.70 o 3 35 3 821.54 748.81 94.18 o 5 35 3 141.25 198.66 76.70 o 7 35 3 104.79 95.00 71.43 o 9 35 3 99.88 190.17 82.58 o 11 35 3 187.31 110.02 68.66 o 1 37 3 99.31 147.02 102.17 o 3 37 3 60.37 106.19 94.46 o 5 37 3 181.01 211.01 71.01 o 7 37 3 278.63 300.13 73.61 o 9 37 3 11.54 88.31 85.60 o 1 39 3 66.07 75.73 77.14 o 3 39 3 99.25 89.83 78.86 o 5 39 3 10.95 -98.60 98.60 o 7 39 3 40.49 64.20 73.90 o 1 41 3 13.82 80.37 77.56 o 3 41 3 50.97 155.04 98.54 o 0 0 4 1163.33 1177.14 171.32 o 4 0 4 16.40 -95.98 95.98 o 8 0 4 137.13 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o 4 12 4 154.79 247.60 67.48 o 6 12 4 43.69 115.05 81.32 o 8 12 4 164.51 191.27 70.99 o 10 12 4 104.22 99.44 67.51 o 12 12 4 152.57 1.08 231.75 o 2 14 4 98.64 131.11 75.48 o 4 14 4 61.72 4.67 75.04 o 6 14 4 33.65 64.54 70.34 o 8 14 4 109.46 47.81 71.03 o 10 14 4 145.87 86.00 74.36 o 0 16 4 477.97 314.41 240.35 o 2 16 4 272.99 177.31 76.40 o 4 16 4 751.15 734.97 88.24 o 6 16 4 193.12 231.17 83.01 o 8 16 4 336.20 280.35 75.11 o 10 16 4 667.37 469.18 78.23 o 2 18 4 46.82 143.95 73.13 o 4 18 4 33.38 -17.73 77.52 o 6 18 4 123.06 174.11 72.60 o 8 18 4 180.06 49.60 76.22 o 0 20 4 168.79 115.71 87.39 o 2 20 4 72.88 81.79 69.27 o 4 20 4 299.20 352.53 75.93 o 6 20 4 73.28 78.82 70.51 o 8 20 4 160.78 314.34 80.77 o 2 22 4 0.10 95.56 73.98 o 4 22 4 36.45 34.55 75.29 o 6 22 4 105.77 28.95 70.19 o 0 24 4 159.39 106.42 88.68 o 2 24 4 318.40 238.54 78.81 o 4 24 4 325.31 409.14 85.48 o