#------------------------------------------------------------------------------ #$Date: 2010-12-22 21:36:50 +0200 (Wed, 22 Dec 2010) $ #$Revision: 5269 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2017796.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2017796_Fobs loop_ _publ_author_name 'Fielden, John' 'Ellern, Arkady' 'K\"ogerler, Paul' _publ_section_title ; [Cr~8~(PhCO~2~)~16~O~4~]·4CH~3~CN·2H~2~O: structural origin of magnetic anisotropy in a molecular spin cluster ; _journal_coeditor_code EG3055 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m253 _journal_page_last m256 _journal_volume 66 _journal_year 2010 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.730 _cell_angle_gamma 90.000 _cell_length_a 23.4063 _cell_length_b 18.9699 _cell_length_c 27.5923 _exptl_crystal_F_000 5344.00 _reflns_d_resolution_high 0.7999 _[local]_cod_data_source_file eg3055Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Koe18 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 952.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 800004.56 819124.69 24539.46 o 6 0 0 134778.34 174368.67 3717.59 o 8 0 0 18374.77 20087.39 419.50 o 10 0 0 114.85 114.04 74.52 o 12 0 0 75044.44 82209.35 1519.23 o 14 0 0 626.27 167.31 161.87 o 16 0 0 17165.31 17536.02 600.72 o 18 0 0 6.46 -166.34 198.56 o 20 0 0 5901.62 5578.50 470.37 o 22 0 0 8225.19 7331.21 555.12 o 24 0 0 12888.46 11243.10 1085.77 o 26 0 0 2543.75 1943.41 766.49 o 28 0 0 1871.23 1326.17 840.05 o 1 1 0 70374.07 94289.13 3140.59 o 3 1 0 33999.40 30060.34 433.24 o 5 1 0 13327.05 12458.70 271.08 o 7 1 0 21932.63 30247.36 460.47 o 9 1 0 12746.77 11913.25 232.55 o 11 1 0 61174.63 70970.02 1030.82 o 13 1 0 254.09 51.75 80.98 o 15 1 0 108.91 -225.08 233.58 o 17 1 0 125.55 -244.19 244.19 o 19 1 0 1511.38 1526.60 196.39 o 21 1 0 490.98 522.42 199.37 o 23 1 0 1447.44 1388.36 216.77 o 25 1 0 2162.38 1316.03 355.36 o 27 1 0 0.57 149.71 502.59 o 29 1 0 2158.92 2379.23 639.97 o 0 2 0 438991.16 385160.88 8574.38 o 10 2 0 2691.56 2325.63 179.05 o 12 2 0 16.43 82.05 82.26 o 14 2 0 682.82 435.50 94.93 o 16 2 0 2945.76 3136.68 281.33 o 18 2 0 119.18 -51.93 154.62 o 20 2 0 1921.13 2024.25 212.65 o 22 2 0 1716.29 1506.61 222.84 o 24 2 0 6102.17 5730.01 387.86 o 26 2 0 4518.63 4228.33 431.71 o 28 2 0 3698.44 3570.55 639.01 o 1 3 0 11673.70 14728.11 209.00 o 3 3 0 125.95 23.15 43.18 o 7 3 0 51350.91 53249.36 701.04 o 9 3 0 13820.25 13070.64 271.39 o 11 3 0 37297.11 41740.54 650.38 o 13 3 0 2406.09 2131.47 119.86 o 15 3 0 283.36 142.94 97.51 o 17 3 0 332.76 219.29 150.21 o 19 3 0 1281.40 1214.94 185.64 o 21 3 0 1746.50 1828.51 278.97 o 23 3 0 434.74 271.87 268.53 o 25 3 0 4997.92 5670.52 407.00 o 27 3 0 93.00 395.55 313.73 o 0 4 0 908166.56 1035061.31 18311.48 o 4 4 0 233688.41 285885.41 3590.04 o 6 4 0 57616.76 59587.48 777.28 o 8 4 0 1640.09 2154.40 103.04 o 10 4 0 968.76 1162.23 68.51 o 12 4 0 48551.37 50390.47 770.95 o 14 4 0 5612.55 5881.53 215.48 o 16 4 0 743.55 634.35 147.41 o 18 4 0 555.25 494.86 164.59 o 20 4 0 687.62 1071.30 256.26 o 22 4 0 3069.34 3086.40 317.58 o 24 4 0 64.95 -261.45 261.45 o 26 4 0 227.95 153.38 299.03 o 28 4 0 496.93 -19.55 502.13 o 1 5 0 65474.41 72883.59 938.36 o 3 5 0 26708.16 29976.56 418.65 o 5 5 0 26617.46 26679.17 429.26 o 7 5 0 28635.21 30631.41 431.64 o 9 5 0 1100.49 1523.91 76.44 o 11 5 0 13112.20 13824.51 250.93 o 13 5 0 9531.69 9340.65 248.60 o 15 5 0 11664.91 12250.78 296.83 o 17 5 0 6640.61 6746.81 297.85 o 19 5 0 5162.71 5176.77 342.68 o 21 5 0 3529.70 3729.34 407.38 o 23 5 0 1969.41 1828.87 395.61 o 25 5 0 1.02 -271.24 271.24 o 27 5 0 18.24 -231.02 310.03 o 0 6 0 75559.28 86905.66 1581.05 o 2 6 0 213.22 453.58 80.17 o 4 6 0 41829.61 40573.25 550.77 o 6 6 0 36455.69 35685.71 553.70 o 8 6 0 31493.35 37134.05 519.63 o 10 6 0 4414.38 4910.50 150.28 o 12 6 0 1062.42 1118.27 91.70 o 14 6 0 4431.12 4854.35 206.12 o 16 6 0 19342.64 19839.35 480.25 o 18 6 0 15806.13 16207.21 559.50 o 20 6 0 364.00 170.69 247.12 o 22 6 0 368.28 2.13 268.21 o 24 6 0 25.35 103.11 271.80 o 26 6 0 4.90 169.55 304.12 o 28 6 0 13.76 -360.73 360.73 o 1 7 0 81420.59 92129.22 1187.11 o 3 7 0 25780.59 23045.61 342.25 o 5 7 0 32782.48 34854.16 490.84 o 7 7 0 1248.29 1022.57 94.50 o 9 7 0 19113.58 19323.09 313.24 o 11 7 0 273.11 295.16 70.39 o 13 7 0 4333.17 4240.17 183.26 o 15 7 0 126.72 34.84 165.10 o 17 7 0 863.12 738.85 180.34 o 19 7 0 2518.31 2616.89 303.81 o 21 7 0 296.87 358.80 266.20 o 23 7 0 221.52 35.70 277.93 o 25 7 0 5779.19 5861.67 447.21 o 27 7 0 3161.24 2895.60 384.55 o 0 8 0 813.74 1625.68 214.07 o 2 8 0 576.36 990.20 106.00 o 4 8 0 14793.52 16003.28 275.88 o 6 8 0 74237.79 80703.98 1179.19 o 8 8 0 32159.03 31873.89 529.84 o 10 8 0 13925.36 13027.79 291.16 o 12 8 0 3294.88 3453.06 340.17 o 14 8 0 17483.26 16964.87 436.04 o 16 8 0 15927.57 16164.03 450.08 o 18 8 0 8780.54 8855.07 444.84 o 20 8 0 213.98 19.33 262.52 o 22 8 0 11.37 -181.99 268.15 o 24 8 0 1013.83 1587.80 334.58 o 26 8 0 1.96 992.71 331.44 o 1 9 0 81746.15 91294.26 1675.87 o 3 9 0 23694.16 24749.12 382.98 o 5 9 0 12417.88 13053.40 249.39 o 7 9 0 7282.79 7790.34 236.25 o 9 9 0 5839.06 5761.96 234.95 o 11 9 0 11435.63 12600.34 298.19 o 13 9 0 9791.88 9607.18 332.14 o 15 9 0 8002.26 7830.18 342.53 o 17 9 0 9123.36 8955.33 368.78 o 19 9 0 267.44 14.63 259.39 o 21 9 0 1888.72 1551.40 308.96 o 23 9 0 2883.88 3442.11 357.43 o 25 9 0 15828.02 16850.53 1003.70 o 0 10 0 199.84 326.75 122.23 o 2 10 0 3929.30 3860.07 172.79 o 4 10 0 60140.54 64171.47 867.11 o 6 10 0 47698.30 56125.02 890.34 o 8 10 0 360.16 600.44 105.45 o 10 10 0 857.36 849.17 116.51 o 12 10 0 7.16 -104.84 104.84 o 14 10 0 7072.38 6461.90 322.84 o 16 10 0 10883.35 10262.05 392.44 o 18 10 0 14247.48 14942.65 583.57 o 20 10 0 1073.15 915.39 298.90 o 22 10 0 302.79 -183.04 289.36 o 24 10 0 797.06 1920.90 347.50 o 26 10 0 128.90 1807.89 365.78 o 1 11 0 59467.52 58201.36 799.23 o 3 11 0 32400.28 34890.40 521.40 o 5 11 0 4213.11 3357.39 204.50 o 7 11 0 5.00 50.43 106.32 o 9 11 0 1846.98 1862.08 190.47 o 11 11 0 5627.07 5248.70 238.56 o 13 11 0 2364.73 1858.32 206.09 o 15 11 0 1970.45 2353.72 277.58 o 17 11 0 79.26 341.71 287.89 o 19 11 0 116.39 -91.00 273.39 o 21 11 0 409.48 81.92 424.11 o 23 11 0 3449.77 3561.03 387.00 o 25 11 0 4032.47 4245.31 420.02 o 0 12 0 13397.91 14433.85 1128.09 o 2 12 0 1843.69 1736.92 255.78 o 4 12 0 29124.22 30079.65 738.96 o 6 12 0 32532.96 35412.67 604.81 o 8 12 0 5.48 -94.57 113.02 o 10 12 0 497.51 501.97 153.74 o 12 12 0 2521.46 2631.80 237.27 o 14 12 0 3076.74 3113.07 248.08 o 16 12 0 7447.27 7607.17 374.62 o 18 12 0 10611.71 10426.69 420.95 o 20 12 0 0.06 -45.74 286.05 o 22 12 0 1097.32 1532.59 342.42 o 24 12 0 17.79 -171.43 361.88 o 1 13 0 63845.51 64895.60 896.54 o 3 13 0 21452.45 22008.26 435.69 o 5 13 0 2546.53 2365.75 221.08 o 7 13 0 1426.29 1114.62 143.93 o 9 13 0 4534.50 4202.07 230.02 o 11 13 0 186.95 33.44 135.70 o 13 13 0 5852.85 5412.59 331.82 o 15 13 0 4560.50 3958.49 276.13 o 17 13 0 2604.73 2966.14 268.63 o 19 13 0 1249.37 1388.83 316.91 o 21 13 0 3901.88 4687.02 460.98 o 23 13 0 5.46 -381.13 381.13 o 0 14 0 210.59 502.62 160.35 o 2 14 0 1095.17 1092.51 139.59 o 4 14 0 335.85 304.94 133.05 o 6 14 0 132.87 156.74 133.94 o 8 14 0 3041.32 3304.02 203.28 o 10 14 0 4317.65 4902.96 238.49 o 12 14 0 2918.25 2795.32 246.03 o 14 14 0 48.27 -194.41 194.41 o 16 14 0 46.51 -220.10 220.10 o 18 14 0 556.64 180.08 231.57 o 20 14 0 37.52 -54.11 300.08 o 22 14 0 695.52 197.56 329.28 o 1 15 0 11403.90 12848.34 380.61 o 3 15 0 15154.78 16651.82 422.16 o 5 15 0 2146.23 1949.83 171.71 o 7 15 0 2339.79 2606.56 187.48 o 9 15 0 2932.26 3181.95 204.67 o 11 15 0 1793.63 1830.58 184.88 o 13 15 0 2.34 -53.62 205.04 o 15 15 0 107.21 -215.66 215.66 o 17 15 0 71.42 -56.29 228.23 o 19 15 0 6.06 -228.19 228.19 o 21 15 0 1114.84 1107.85 337.04 o 0 16 0 21183.98 23614.43 826.72 o 2 16 0 387.56 382.86 158.04 o 4 16 0 1091.11 864.82 166.14 o 6 16 0 1666.16 1369.67 178.36 o 8 16 0 11444.53 10741.56 347.10 o 10 16 0 10143.09 9117.92 333.18 o 12 16 0 362.91 336.62 215.56 o 14 16 0 129.54 -223.25 223.25 o 16 16 0 1920.06 2112.58 283.50 o 18 16 0 11.60 -241.16 241.16 o 20 16 0 1331.62 1251.26 343.13 o 1 17 0 10090.73 12509.32 972.16 o 3 17 0 1696.54 1377.77 186.79 o 5 17 0 37.10 -159.33 159.33 o 7 17 0 2677.65 2399.84 207.42 o 9 17 0 1529.25 1454.90 193.64 o 11 17 0 1272.36 1167.16 241.56 o 13 17 0 2200.15 1979.39 299.66 o 15 17 0 34.26 -245.78 245.78 o 17 17 0 237.50 141.71 449.94 o 19 17 0 2.07 -168.70 262.94 o 0 18 0 91145.94 95396.65 4682.10 o 2 18 0 31031.40 31585.47 1463.16 o 4 18 0 4020.57 3851.83 274.26 o 6 18 0 71.36 -40.00 173.02 o 8 18 0 2301.90 2049.74 216.18 o 10 18 0 2514.87 2184.84 224.31 o 12 18 0 5664.59 5537.55 340.40 o 14 18 0 129.49 -48.18 249.09 o 16 18 0 1804.68 1612.05 414.99 o 18 18 0 5.79 -337.13 337.13 o 1 19 0 435.88 2566.61 474.25 o 3 19 0 5391.81 7088.78 581.79 o 5 19 0 15.12 96.80 218.39 o 7 19 0 3673.00 3746.76 251.63 o 9 19 0 6626.19 7530.29 431.72 o 11 19 0 1480.26 1375.52 278.43 o 13 19 0 522.92 152.20 286.51 o 15 19 0 185.12 -267.84 332.13 o 17 19 0 269.92 -17.75 292.66 o 0 20 0 7966.33 8088.89 639.63 o 2 20 0 9672.89 10367.26 479.31 o 4 20 0 4065.08 4249.09 313.05 o 6 20 0 799.72 934.39 249.89 o 8 20 0 692.94 666.39 249.34 o 10 20 0 58.78 206.54 309.44 o 12 20 0 1059.77 772.95 279.89 o 14 20 0 2220.31 2035.28 367.34 o 1 21 0 90.32 32.63 251.31 o 3 21 0 780.58 687.87 260.84 o 5 21 0 21.01 -200.57 245.30 o 7 21 0 2288.15 1817.43 286.74 o 9 21 0 2789.17 2497.30 403.43 o 11 21 0 804.39 595.88 353.89 o 13 21 0 54.55 328.78 422.66 o 0 22 0 4486.40 5157.58 602.32 o 2 22 0 368.50 628.53 278.15 o 4 22 0 754.98 564.40 273.26 o 6 22 0 639.69 637.24 276.07 o 8 22 0 12.07 -246.00 257.19 o 10 22 0 504.50 314.83 532.11 o 1 23 0 2036.52 3238.65 348.41 o 3 23 0 4440.41 5302.02 379.52 o 5 23 0 2831.81 3836.14 348.82 o 7 23 0 724.38 744.74 292.53 o -29 1 1 2074.62 2583.66 630.14 o -27 1 1 2559.95 2098.84 566.53 o -25 1 1 6273.19 5102.36 421.70 o -23 1 1 6827.33 6915.92 375.10 o -21 1 1 5376.11 5427.29 313.50 o -19 1 1 2795.95 2523.65 214.15 o -17 1 1 2625.03 2453.70 220.04 o -15 1 1 2405.38 2167.87 165.47 o -13 1 1 24661.50 24942.97 396.42 o -11 1 1 2759.10 1950.52 158.59 o -9 1 1 1556.33 1743.25 82.20 o -7 1 1 2858.44 3385.43 123.61 o -5 1 1 65633.54 78372.84 1102.42 o -3 1 1 27284.04 36138.81 515.92 o 1 1 1 670727.50 869975.88 19660.34 o 3 1 1 16417.74 11843.96 153.89 o 5 1 1 48824.39 65720.45 847.97 o 7 1 1 24314.87 27521.51 385.27 o 9 1 1 743.80 621.10 60.11 o 11 1 1 15165.31 14967.35 295.65 o 13 1 1 1537.06 1724.95 110.75 o 15 1 1 20260.34 17968.59 557.01 o 17 1 1 4728.83 4004.27 226.36 o 19 1 1 1119.07 660.77 183.30 o 21 1 1 6049.62 5995.78 326.69 o 23 1 1 9735.30 10232.15 402.13 o 25 1 1 2270.14 1775.44 363.09 o 27 1 1 3746.40 3077.53 601.98 o 29 1 1 1629.96 1514.43 598.94 o -28 2 1 2032.51 2453.40 410.60 o -26 2 1 2188.36 2154.34 387.72 o -24 2 1 54.04 387.73 351.10 o -22 2 1 759.69 754.78 208.41 o -20 2 1 2522.97 2667.07 227.08 o -18 2 1 394.91 457.39 201.42 o -16 2 1 722.76 473.84 142.60 o -14 2 1 3248.78 3491.33 166.14 o -12 2 1 1403.62 1576.55 103.21 o -10 2 1 57944.86 56740.90 1002.28 o -8 2 1 64181.34 62940.29 908.56 o -6 2 1 24998.06 29421.89 451.22 o -4 2 1 10151.16 12122.56 193.22 o -2 2 1 84.71 129.73 26.91 o 0 2 1 2373.70 1978.54 48.26 o 2 2 1 103214.15 119231.69 1662.77 o 4 2 1 605653.38 753474.81 9478.95 o 6 2 1 37384.26 45754.62 606.54 o 8 2 1 38472.91 37068.37 507.42 o 10 2 1 47135.42 46337.15 701.26 o 12 2 1 184.20 174.85 90.24 o 14 2 1 57.26 -90.05 109.97 o 16 2 1 10.58 111.33 183.07 o 18 2 1 617.56 379.18 165.85 o 20 2 1 4001.94 3949.79 248.33 o 22 2 1 2188.74 2162.31 292.44 o 24 2 1 6194.80 6139.29 431.78 o 26 2 1 6202.56 5430.08 515.45 o 28 2 1 1498.61 1908.00 731.84 o -27 3 1 6719.32 6981.86 470.23 o -25 3 1 9349.90 9119.35 498.31 o -23 3 1 1576.17 1575.17 297.33 o -21 3 1 32.63 70.89 236.16 o -19 3 1 97.66 -41.51 162.92 o -17 3 1 251.89 106.00 139.69 o -15 3 1 1493.39 1583.73 123.70 o -13 3 1 2383.25 1969.10 117.82 o -11 3 1 23255.79 24949.44 425.99 o -9 3 1 1248.31 1225.77 85.60 o -7 3 1 63658.82 65664.54 854.34 o -5 3 1 264893.38 315769.53 3948.37 o -3 3 1 24452.54 19149.31 289.23 o -1 3 1 45.55 2611.90 115.45 o 3 3 1 48044.65 35089.81 524.20 o 5 3 1 27605.92 33245.51 453.59 o 7 3 1 320.54 323.90 48.06 o 9 3 1 2577.63 3506.23 120.48 o 11 3 1 13132.96 12067.29 271.67 o 13 3 1 3669.83 3475.78 169.10 o 15 3 1 3146.22 3113.42 178.94 o 17 3 1 4040.81 4045.76 226.47 o 19 3 1 349.15 240.41 171.68 o 21 3 1 108.80 57.56 234.42 o 23 3 1 0.48 205.98 261.83 o 25 3 1 488.10 1102.52 349.72 o 27 3 1 866.90 921.97 323.36 o -28 4 1 1.27 -357.37 357.37 o -26 4 1 2311.53 1972.81 351.55 o -24 4 1 451.58 571.98 287.29 o -22 4 1 2982.95 2693.95 308.01 o -20 4 1 7072.19 6870.83 411.02 o -18 4 1 276.75 344.38 161.79 o -16 4 1 2648.45 2541.89 178.84 o -14 4 1 8028.03 7411.43 230.75 o -12 4 1 7659.85 8066.99 334.94 o -10 4 1 204.13 78.84 82.73 o -8 4 1 27646.13 26334.33 377.96 o -6 4 1 41899.70 42900.40 574.24 o -4 4 1 74073.66 92363.00 1181.33 o -2 4 1 3977.77 4258.38 146.81 o 0 4 1 207276.28 243861.55 3050.98 o 2 4 1 12790.03 13309.84 221.26 o 4 4 1 21864.38 25345.56 619.64 o 6 4 1 5945.87 5576.67 132.30 o 8 4 1 28888.00 25415.14 370.09 o 10 4 1 24490.95 24082.01 367.30 o 12 4 1 934.10 586.85 131.39 o 14 4 1 1717.82 1742.79 123.20 o 16 4 1 8687.17 8313.90 257.21 o 18 4 1 5.26 -137.28 154.40 o 20 4 1 11635.64 12641.93 607.23 o 22 4 1 1.47 -72.78 246.23 o 24 4 1 397.56 648.68 282.59 o 26 4 1 870.17 690.97 310.23 o 28 4 1 384.78 146.87 385.51 o -27 5 1 56.50 -308.02 308.02 o -25 5 1 66.23 189.45 289.29 o -23 5 1 899.96 972.32 283.20 o -21 5 1 1067.86 909.99 282.28 o -19 5 1 7967.53 7296.23 425.40 o -17 5 1 2148.08 2239.67 189.03 o -15 5 1 5724.96 6294.09 232.95 o -13 5 1 2973.18 2912.57 161.04 o -11 5 1 23667.89 22174.05 349.02 o -9 5 1 2030.96 2434.12 104.89 o -7 5 1 21376.30 20942.37 315.78 o -5 5 1 23101.54 22339.93 383.07 o -3 5 1 30224.80 33978.64 526.10 o -1 5 1 289849.97 362455.13 4521.13 o 3 5 1 129995.27 144638.44 2105.84 o 5 5 1 130074.32 138183.47 1940.78 o 7 5 1 17110.05 23031.95 386.69 o 9 5 1 10632.68 12385.51 357.15 o 11 5 1 34896.14 36514.59 520.52 o 13 5 1 3854.47 3242.89 164.46 o 15 5 1 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