#------------------------------------------------------------------------------ #$Date: 2010-12-22 21:36:50 +0200 (Wed, 22 Dec 2010) $ #$Revision: 5269 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2017798.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2017798_Fobs loop_ _publ_author_name 'Ho, Douglas M.' _publ_section_title ; A urea adduct of bis(hinokitiolato)copper(II) ; _journal_coeditor_code EG3059 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m294 _journal_page_last m299 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 110.385 _cell_angle_gamma 90.000 _cell_length_a 17.0125 _cell_length_b 11.0470 _cell_length_c 17.2731 _exptl_crystal_F_000 1324.00 _reflns_d_resolution_high 0.7698 _[local]_cod_data_source_file eg3059IVsup2.hkl _[local]_cod_data_source_block IV #BEGIN Tags that were not found in dictionaries: _shelx_title ' [cis-Cu(C10H11O2)2]2 . 6CH4N2O . 2C3H6O, P2(1)/c (No. 14), Z=2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 219.45 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 17773.71 17386.64 394.48 o 3 0 0 23504.26 22461.62 448.13 o 4 0 0 9517.98 9358.86 197.02 o 5 0 0 8845.74 7879.68 157.10 o 6 0 0 7345.04 7853.93 181.57 o 7 0 0 365.36 290.60 9.87 o 8 0 0 1240.00 1196.31 27.90 o 9 0 0 785.29 736.59 22.75 o 10 0 0 211.17 276.01 11.59 o 11 0 0 4240.95 4520.40 112.46 o 12 0 0 1801.37 1793.39 42.92 o 13 0 0 467.56 433.54 17.17 o 14 0 0 371.66 375.16 14.17 o 15 0 0 82.09 71.25 24.47 o 16 0 0 42.64 35.63 38.63 o 17 0 0 766.77 937.05 94.43 o 18 0 0 583.26 658.46 51.94 o 19 0 0 607.68 605.24 83.70 o 20 0 0 97.48 97.87 68.25 o 1 1 0 0.11 5.15 1.29 o 2 1 0 278.67 248.10 4.29 o 3 1 0 42.86 44.21 3.00 o 4 1 0 1111.81 977.82 16.31 o 5 1 0 8562.67 8569.05 118.04 o 6 1 0 9.17 9.44 4.29 o 7 1 0 3.59 3.00 3.86 o 8 1 0 11.23 15.02 4.72 o 9 1 0 454.93 416.37 10.73 o 10 1 0 13.41 14.59 5.58 o 11 1 0 78.60 77.26 6.01 o 12 1 0 1.82 8.16 5.58 o 13 1 0 106.99 107.74 9.87 o 14 1 0 82.91 66.10 12.02 o 15 1 0 3.91 -4.29 10.30 o 16 1 0 13.46 2.58 12.45 o 17 1 0 158.75 112.46 28.76 o 18 1 0 28.27 -1.29 30.05 o 19 1 0 4.42 66.96 43.78 o 20 1 0 0.46 18.46 52.37 o 0 2 0 2345.59 2251.40 155.82 o 1 2 0 4071.05 3759.77 71.68 o 2 2 0 663.90 612.54 10.30 o 3 2 0 789.40 759.34 12.45 o 4 2 0 9070.34 8071.98 121.05 o 5 2 0 8317.89 8077.99 127.49 o 6 2 0 7820.64 7403.65 120.62 o 7 2 0 860.75 752.90 15.88 o 8 2 0 114.77 76.84 6.44 o 9 2 0 214.23 205.18 7.73 o 10 2 0 516.45 503.94 12.02 o 11 2 0 3225.43 3341.26 54.09 o 12 2 0 1088.53 1080.41 26.61 o 13 2 0 3102.22 3477.76 69.54 o 14 2 0 482.16 476.46 18.46 o 15 2 0 0.32 -10.30 10.30 o 16 2 0 1204.36 1351.70 52.80 o 17 2 0 461.60 454.14 29.19 o 18 2 0 388.38 385.46 44.64 o 19 2 0 107.59 57.52 33.05 o 20 2 0 15.27 94.43 75.98 o 1 3 0 470.53 417.66 12.02 o 2 3 0 5637.35 5842.91 100.44 o 3 3 0 1314.64 1322.94 25.33 o 4 3 0 10070.22 10362.44 183.29 o 5 3 0 13277.49 13980.99 224.07 o 6 3 0 121.62 114.61 7.30 o 7 3 0 363.86 380.74 12.45 o 8 3 0 153.29 148.95 8.58 o 9 3 0 13.73 22.32 6.44 o 10 3 0 567.19 587.21 15.45 o 11 3 0 2.58 5.15 6.01 o 12 3 0 20.34 12.88 6.01 o 13 3 0 623.14 633.57 20.17 o 14 3 0 220.74 173.84 15.02 o 15 3 0 0.30 -9.44 14.17 o 16 3 0 166.69 107.74 19.75 o 17 3 0 0.10 -18.89 18.89 o 18 3 0 0.79 -16.31 28.33 o 19 3 0 7.52 1.29 47.65 o 20 3 0 25.29 4.72 51.08 o 0 4 0 1060.64 958.51 54.09 o 1 4 0 2183.04 1856.49 52.37 o 2 4 0 497.89 430.53 12.45 o 3 4 0 13.38 14.17 4.29 o 4 4 0 4523.32 4342.26 81.99 o 5 4 0 3568.99 3261.42 53.23 o 6 4 0 3135.44 2766.92 50.65 o 7 4 0 4547.30 4674.07 84.56 o 8 4 0 5068.37 5477.19 97.01 o 9 4 0 196.36 193.59 11.16 o 10 4 0 3230.33 3553.73 66.53 o 11 4 0 5641.75 6414.66 125.34 o 12 4 0 1674.63 1889.97 36.49 o 13 4 0 336.04 291.46 12.45 o 14 4 0 1.03 -12.02 19.32 o 15 4 0 142.94 106.88 21.89 o 16 4 0 694.54 682.07 37.34 o 17 4 0 438.52 433.54 33.48 o 18 4 0 574.72 521.11 52.37 o 19 4 0 515.24 462.73 65.67 o 1 5 0 173.12 223.21 18.46 o 2 5 0 7.44 16.74 5.58 o 3 5 0 123.95 109.89 8.16 o 4 5 0 148.90 141.22 11.16 o 5 5 0 3986.80 4106.17 79.84 o 6 5 0 1423.87 1498.07 27.90 o 7 5 0 14.88 26.18 7.73 o 8 5 0 57.13 76.41 9.87 o 9 5 0 271.29 290.17 13.74 o 10 5 0 27.00 15.45 9.01 o 11 5 0 1427.34 1487.34 41.21 o 12 5 0 115.21 102.59 16.31 o 13 5 0 14.11 9.87 10.73 o 14 5 0 29.29 7.30 10.30 o 15 5 0 0.87 -8.58 28.33 o 16 5 0 25.67 70.83 28.33 o 17 5 0 54.84 31.76 25.33 o 18 5 0 10.08 -9.44 26.61 o 19 5 0 4.76 -29.62 55.80 o 0 6 0 5876.03 6382.47 280.73 o 1 6 0 10620.59 10643.17 265.70 o 2 6 0 284.48 271.28 26.61 o 3 6 0 138.33 127.49 8.58 o 4 6 0 202.71 154.96 12.45 o 5 6 0 6452.56 7032.35 182.43 o 6 6 0 252.64 213.76 16.31 o 7 6 0 3234.87 3652.03 88.85 o 8 6 0 993.50 1035.34 37.77 o 9 6 0 1.97 6.01 14.59 o 10 6 0 1954.70 2193.02 59.67 o 11 6 0 270.61 245.53 19.32 o 12 6 0 3806.53 4488.63 128.34 o 13 6 0 105.53 109.03 15.45 o 14 6 0 377.66 374.73 22.75 o 15 6 0 48.17 21.46 17.17 o 16 6 0 274.97 249.82 34.34 o 17 6 0 599.15 626.27 46.79 o 18 6 0 533.32 612.54 51.08 o 1 7 0 1412.85 1515.24 59.24 o 2 7 0 753.57 814.28 35.63 o 3 7 0 122.64 103.88 17.60 o 4 7 0 1223.66 1206.18 34.77 o 5 7 0 83.64 81.99 16.31 o 6 7 0 345.87 365.72 19.75 o 7 7 0 390.45 415.94 11.16 o 8 7 0 3.78 -12.02 16.74 o 9 7 0 32.51 31.34 19.75 o 10 7 0 389.48 361.85 26.61 o 11 7 0 224.51 234.80 23.61 o 12 7 0 5.99 0.86 23.18 o 13 7 0 23.69 -7.30 19.75 o 14 7 0 15.66 11.16 21.03 o 15 7 0 11.01 29.19 26.18 o 16 7 0 56.56 71.68 34.34 o 17 7 0 7.39 19.32 36.06 o 18 7 0 22.93 12.02 40.35 o 0 8 0 3746.75 3891.98 203.46 o 1 8 0 2584.78 2712.41 90.14 o 2 8 0 2897.94 3138.22 86.28 o 3 8 0 32.12 21.89 11.59 o 4 8 0 124.18 123.19 27.90 o 5 8 0 1690.86 1813.57 48.93 o 6 8 0 2898.94 3114.18 74.69 o 7 8 0 301.53 358.42 15.45 o 8 8 0 91.50 93.15 18.03 o 9 8 0 225.62 198.74 20.60 o 10 8 0 5.23 2.58 17.60 o 11 8 0 648.23 618.97 42.07 o 12 8 0 666.95 694.09 45.07 o 13 8 0 518.53 486.34 42.50 o 14 8 0 101.68 69.54 33.48 o 15 8 0 0.72 -42.07 42.07 o 16 8 0 244.22 230.51 59.24 o 17 8 0 138.37 150.24 64.39 o 1 9 0 124.37 66.53 30.48 o 2 9 0 869.47 913.01 32.19 o 3 9 0 1452.67 1462.87 83.70 o 4 9 0 972.69 865.36 50.65 o 5 9 0 27.27 14.59 27.90 o 6 9 0 1444.00 1735.87 49.36 o 7 9 0 271.19 298.33 16.31 o 8 9 0 963.24 1037.92 42.50 o 9 9 0 171.60 133.07 23.18 o 10 9 0 1.26 -18.03 24.47 o 11 9 0 9.01 11.59 24.47 o 12 9 0 19.32 34.77 28.33 o 13 9 0 12.94 138.65 40.78 o 14 9 0 24.07 -22.75 32.62 o 15 9 0 1.28 -36.06 55.80 o 16 9 0 1.21 107.31 121.91 o 0 10 0 1467.56 1331.52 140.79 o 1 10 0 1723.99 1794.25 115.47 o 2 10 0 326.15 357.99 20.60 o 3 10 0 24.18 -9.01 35.63 o 4 10 0 245.86 213.76 45.07 o 5 10 0 657.58 660.18 40.78 o 6 10 0 2116.82 2492.64 105.17 o 7 10 0 2174.60 2635.15 104.74 o 8 10 0 1027.90 958.08 52.37 o 9 10 0 29.95 48.93 28.76 o 10 10 0 321.18 202.18 43.78 o 11 10 0 469.80 394.05 52.80 o 12 10 0 296.21 308.63 47.65 o 13 10 0 9.20 40.35 46.36 o 14 10 0 8.60 39.92 65.25 o 1 11 0 67.55 72.97 13.74 o 2 11 0 0.44 36.06 49.79 o 3 11 0 1.41 -10.30 36.49 o 4 11 0 58.81 31.34 34.77 o 5 11 0 102.84 201.75 44.64 o 6 11 0 222.44 212.91 43.35 o 7 11 0 0.05 -1.72 20.17 o 8 11 0 72.76 157.53 72.97 o 9 11 0 0.67 49.79 66.96 o 10 11 0 2.58 21.89 44.21 o 11 11 0 41.11 -3.86 39.06 o 12 11 0 10.73 44.21 54.09 o 13 11 0 9.05 55.37 49.79 o 0 12 0 324.04 103.45 99.16 o 1 12 0 313.45 387.18 75.98 o 2 12 0 535.04 653.31 61.81 o 3 12 0 124.58 200.03 43.35 o 4 12 0 132.91 91.43 42.07 o 5 12 0 815.36 841.32 72.97 o 6 12 0 978.87 1134.07 81.99 o 7 12 0 343.01 407.78 77.26 o 8 12 0 114.64 81.56 42.07 o 9 12 0 256.10 186.72 51.08 o 10 12 0 29.78 121.05 62.67 o 11 12 0 365.35 309.49 49.79 o 1 13 0 0.08 -35.63 35.63 o 2 13 0 20.54 -3.43 27.90 o 3 13 0 3.94 -44.64 44.64 o 4 13 0 0.32 21.46 31.34 o 5 13 0 0.82 64.39 47.22 o 6 13 0 25.44 53.66 51.94 o 7 13 0 99.11 75.12 49.36 o 8 13 0 29.51 36.06 49.36 o 0 14 0 204.96 145.09 61.81 o 1 14 0 175.12 194.45 45.07 o 2 14 0 158.42 164.83 43.35 o 3 14 0 24.20 -3.43 33.05 o 4 14 0 69.74 191.01 75.55 o -20 1 1 28.70 18.46 36.49 o -19 1 1 226.12 136.50 39.92 o -18 1 1 268.14 200.46 38.63 o -17 1 1 2302.68 2657.90 78.98 o -16 1 1 1593.02 1784.38 66.53 o -15 1 1 471.31 494.06 15.88 o -14 1 1 149.34 122.76 10.30 o -13 1 1 2617.58 2705.54 46.36 o -12 1 1 5263.30 5677.22 100.01 o -11 1 1 645.70 613.39 18.03 o -10 1 1 98.77 51.94 7.30 o -9 1 1 180.94 147.66 9.87 o -8 1 1 53.70 65.67 6.87 o -7 1 1 10956.60 10666.78 231.36 o -6 1 1 164.17 110.75 10.30 o -5 1 1 23595.86 21577.80 318.50 o -4 1 1 11184.99 10638.02 177.28 o -3 1 1 108.04 138.65 5.15 o -2 1 1 780.33 681.64 12.45 o -1 1 1 12222.06 11951.94 233.94 o 0 1 1 21877.47 20078.44 430.96 o 1 1 1 16086.44 15353.72 393.19 o 2 1 1 13856.56 12239.11 230.51 o 3 1 1 13202.09 11995.73 195.74 o 4 1 1 6335.47 5535.99 80.70 o 5 1 1 23.06 37.77 3.86 o 6 1 1 45.30 27.90 4.72 o 7 1 1 1385.86 1172.27 19.75 o 8 1 1 152.56 109.89 6.01 o 9 1 1 23.20 15.88 5.58 o 10 1 1 719.68 674.78 15.02 o 11 1 1 3608.65 4096.30 68.68 o 12 1 1 5287.99 5852.35 111.17 o 13 1 1 3673.18 4140.08 84.13 o 14 1 1 427.83 468.31 15.88 o 15 1 1 25.61 47.22 18.46 o 16 1 1 904.23 915.58 45.93 o 17 1 1 476.01 527.11 31.76 o 18 1 1 147.01 120.19 28.33 o 19 1 1 233.77 266.56 39.49 o 20 1 1 0.80 21.89 37.77 o -20 2 1 25.54 85.85 48.93 o -19 2 1 5.53 -16.31 28.76 o -18 2 1 0.60 29.62 26.18 o -17 2 1 90.52 69.97 13.74 o -16 2 1 0.50 14.59 11.16 o -15 2 1 150.42 144.66 12.45 o -14 2 1 418.11 405.21 14.17 o -13 2 1 0.73 9.87 9.01 o -12 2 1 110.92 80.27 9.87 o -11 2 1 69.99 58.81 8.58 o -10 2 1 64.09 45.50 8.16 o -9 2 1 229.64 189.73 10.30 o -8 2 1 112.24 115.04 4.72 o -7 2 1 75.42 100.44 6.01 o -6 2 1 369.00 341.68 9.01 o -5 2 1 315.13 330.95 7.73 o -4 2 1 423.63 373.44 9.87 o -3 2 1 5.24 9.01 3.86 o -2 2 1 14408.17 14328.68 282.87 o -1 2 1 1457.08 1319.08 33.91 o 0 2 1 805.21 667.05 32.62 o 1 2 1 319.27 345.11 11.59 o 2 2 1 11245.58 10306.21 205.61 o 3 2 1 6834.96 6339.54 131.35 o 4 2 1 36.27 48.93 4.72 o 5 2 1 2037.19 2083.13 35.20 o 6 2 1 6100.49 6327.53 113.75 o 7 2 1 79.11 85.85 5.58 o 8 2 1 98.71 96.15 6.44 o 9 2 1 1567.51 1678.35 28.76 o 10 2 1 306.76 276.86 11.16 o 11 2 1 102.70 111.17 8.58 o 12 2 1 198.64 188.44 11.59 o 13 2 1 1.07 -5.58 8.16 o 14 2 1 914.04 1071.83 36.06 o 15 2 1 251.30 239.52 20.60 o 16 2 1 21.93 12.88 18.89 o 17 2 1 50.39 21.89 22.32 o 18 2 1 2.04 -4.72 32.19 o 19 2 1 9.48 -4.72 53.23 o 20 2 1 5.00 -18.46 58.81 o -20 3 1 8.11 -10.30 46.36 o -19 3 1 38.02 29.19 57.95 o -18 3 1 459.22 407.78 30.91 o -17 3 1 865.36 860.21 31.76 o -16 3 1 1204.38 1312.64 38.20 o -15 3 1 486.98 489.34 17.17 o -14 3 1 103.37 67.82 10.73 o -13 3 1 739.32 749.46 22.75 o -12 3 1 2638.79 2785.81 63.53 o -11 3 1 4251.08 4578.77 64.39 o -10 3 1 1787.37 1960.80 31.34 o -9 3 1 1583.04 1604.09 30.48 o -8 3 1 42.85 39.49 7.30 o -7 3 1 3980.93 3771.79 69.97 o -6 3 1 7404.23 6871.38 123.19 o -5 3 1 2457.22 2091.29 44.21 o -4 3 1 471.25 372.59 10.30 o -3 3 1 316.91 315.50 8.16 o -2 3 1 6756.77 6612.12 149.81 o -1 3 1 2940.99 2702.54 65.67 o 0 3 1 1287.33 1045.22 35.63 o 1 3 1 653.88 583.78 14.59 o 2 3 1 6139.21 5685.80 103.02 o 3 3 1 3774.57 3540.00 65.67 o 4 3 1 151.35 114.61 5.58 o 5 3 1 2282.10 2106.74 48.93 o 6 3 1 10293.31 10367.60 213.34 o 7 3 1 3015.53 3030.05 54.94 o 8 3 1 4967.21 5179.29 90.57 o 9 3 1 84.47 97.44 10.30 o 10 3 1 147.53 127.92 9.44 o 11 3 1 4844.63 5536.42 101.73 o 12 3 1 1772.06 1903.71 38.20 o 13 3 1 2798.29 3123.63 63.10 o 14 3 1 89.59 91.86 7.73 o 15 3 1 183.18 158.82 18.03 o 16 3 1 803.04 877.81 35.63 o 17 3 1 354.97 371.30 28.76 o 18 3 1 592.41 631.85 65.67 o 19 3 1 244.13 160.97 58.38 o -20 4 1 0.21 106.88 61.81 o -19 4 1 12.41 -11.59 48.08 o -18 4 1 69.71 64.39 24.47 o -17 4 1 94.34 66.10 23.61 o -16 4 1 36.50 16.31 19.32 o -15 4 1 360.77 324.51 19.32 o -14 4 1 297.04 229.65 21.03 o -13 4 1 336.18 306.05 19.75 o -12 4 1 233.26 185.86 9.44 o -11 4 1 679.66 702.25 18.03 o -10 4 1 588.46 636.57 17.17 o -9 4 1 851.96 869.22 19.75 o -8 4 1 46.65 41.64 7.73 o -7 4 1 125.24 140.79 8.16 o -6 4 1 495.85 500.07 13.74 o -5 4 1 3421.64 3568.33 66.10 o -4 4 1 231.08 233.94 6.87 o -3 4 1 929.54 1071.83 21.89 o -2 4 1 146.20 180.71 7.30 o -1 4 1 197.28 185.01 7.73 o 0 4 1 226.67 262.70 7.73 o 1 4 1 2400.06 2681.07 50.22 o 2 4 1 5303.76 5749.33 128.77 o 3 4 1 22.58 34.34 6.44 o 4 4 1 572.83 571.33 15.45 o 5 4 1 46.42 43.35 5.58 o 6 4 1 608.43 667.48 18.89 o 7 4 1 549.12 524.54 15.02 o 8 4 1 511.48 528.40 18.46 o 9 4 1 9.48 8.58 9.87 o 10 4 1 1.63 -2.15 10.30 o 11 4 1 17.02 16.74 10.30 o 12 4 1 706.84 726.71 21.03 o 13 4 1 21.41 11.59 12.02 o 14 4 1 139.89 120.62 11.59 o 15 4 1 79.68 63.53 21.03 o 16 4 1 104.38 85.85 25.75 o 17 4 1 57.69 75.12 26.18 o 18 4 1 0.26 -36.06 36.06 o 19 4 1 28.06 -36.49 52.37 o -19 5 1 7.38 -50.65 55.37 o -18 5 1 366.66 361.00 45.50 o -17 5 1 707.72 804.84 61.38 o -16 5 1 493.43 480.33 31.76 o -15 5 1 60.50 21.46 24.47 o -14 5 1 3.66 8.16 16.31 o -13 5 1 11.46 1.29 8.58 o -12 5 1 1442.78 1613.54 37.34 o -11 5 1 674.02 690.23 22.32 o -10 5 1 1244.25 1267.57 29.62 o -9 5 1 23.24 33.48 9.44 o -8 5 1 1717.24 1813.14 36.49 o -7 5 1 2525.41 2580.20 53.23 o -6 5 1 11679.99 12176.87 228.36 o -5 5 1 12294.80 13090.31 203.03 o -4 5 1 846.87 715.12 15.88 o -3 5 1 395.70 466.59 10.73 o -2 5 1 645.57 658.89 15.02 o -1 5 1 6726.79 6484.20 201.32 o 0 5 1 9428.98 9188.46 282.87 o 1 5 1 648.54 541.28 16.74 o 2 5 1 118.04 78.55 11.59 o 3 5 1 40.33 64.82 8.16 o 4 5 1 2168.38 2132.50 49.79 o 5 5 1 1854.95 2097.73 58.81 o 6 5 1 6940.08 7231.09 144.66 o 7 5 1 6281.31 6494.50 142.08 o 8 5 1 1587.36 1565.03 43.35 o 9 5 1 1205.98 1337.10 37.34 o 10 5 1 94.02 83.70 12.88 o 11 5 1 1867.41 2071.12 57.52 o 12 5 1 2591.34 2926.17 79.41 o 13 5 1 710.43 725.00 27.04 o 14 5 1 1249.72 1332.38 36.49 o 15 5 1 291.64 281.16 16.74 o 16 5 1 8.73 10.73 30.48 o 17 5 1 69.65 27.04 28.76 o 18 5 1 138.20 81.56 36.92 o 19 5 1 276.98 228.36 74.26 o -19 6 1 10.08 -55.80 55.80 o -18 6 1 47.43 31.76 33.48 o -17 6 1 203.97 131.78 28.33 o -16 6 1 158.00 149.81 27.90 o -15 6 1 12.04 -8.58 9.01 o -14 6 1 148.50 120.62 16.31 o -13 6 1 25.88 22.32 21.46 o -12 6 1 828.21 897.13 29.19 o -11 6 1 399.00 410.79 18.46 o -10 6 1 380.39 386.32 16.31 o -9 6 1 17.21 30.91 9.87 o -8 6 1 152.48 123.62 11.16 o -7 6 1 442.14 482.04 17.17 o -6 6 1 170.27 149.81 7.30 o -5 6 1 499.53 473.03 12.02 o -4 6 1 1.83 0.86 4.72 o -3 6 1 389.55 392.33 24.04 o -2 6 1 35.49 72.11 24.04 o -1 6 1 205.25 197.02 20.60 o 0 6 1 139.21 129.63 21.46 o 1 6 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