#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/78/2017847.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2017847_Fobs loop_ _publ_author_name 'Kawano, Tetsuya' 'Yamane, Hisanori' _publ_section_title ; Mg~5~TiO~4~(BO~3~)~2~ ; _journal_coeditor_code KU3033 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i92 _journal_page_last i94 _journal_volume 66 _journal_year 2010 _space_group_IT_number 55 _symmetry_space_group_name_Hall '-P 2 2ab' _symmetry_space_group_name_H-M 'P b a m' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.2636 _cell_length_b 12.2989 _cell_length_c 3.0131 _exptl_crystal_F_000 344.00 _reflns_d_resolution_high 0.7703 _[local]_cod_data_source_file ku3033Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Mg5TiB2O10' _shelx_refln_list_code 4 _shelx_f_calc_maximum 166.52 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x, y, -z' '-x-1/2, y-1/2, z' 'x-1/2, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1.54 3.39 1.06 o 4 0 0 675.82 425.25 7.77 o 6 0 0 688.72 750.71 14.80 o 8 0 0 10722.09 10147.43 183.15 o 10 0 0 49.19 42.95 30.44 o 12 0 0 648.04 628.09 22.62 o 2 1 0 0.16 0.63 0.60 o 3 1 0 680.51 684.66 7.37 o 4 1 0 254.18 282.15 4.21 o 5 1 0 372.26 386.84 6.12 o 6 1 0 20.77 18.23 2.40 o 7 1 0 325.41 316.62 7.05 o 8 1 0 432.33 439.36 8.88 o 9 1 0 6.16 5.28 3.52 o 10 1 0 200.09 205.04 7.92 o 11 1 0 213.14 207.96 9.64 o 12 1 0 13.66 0.04 3.39 o 0 2 0 53.91 56.37 0.87 o 1 2 0 1778.49 2000.88 71.65 o 2 2 0 0.13 0.30 0.47 o 3 2 0 666.47 650.55 7.09 o 4 2 0 28.28 28.08 2.19 o 5 2 0 1918.89 1922.85 21.21 o 6 2 0 10.39 9.60 2.22 o 7 2 0 1767.02 1754.19 22.60 o 8 2 0 23.75 24.11 3.30 o 9 2 0 133.06 136.37 6.09 o 10 2 0 0.10 1.48 2.96 o 11 2 0 41.70 37.18 8.21 o 1 3 0 425.87 442.41 3.48 o 2 3 0 41.22 43.94 0.96 o 3 3 0 306.84 271.42 4.00 o 4 3 0 135.25 143.77 2.98 o 5 3 0 91.10 96.83 2.72 o 6 3 0 83.82 86.81 3.55 o 7 3 0 1480.65 1459.48 18.89 o 8 3 0 84.05 92.11 4.98 o 9 3 0 75.74 68.59 5.66 o 10 3 0 58.18 56.27 5.58 o 11 3 0 207.49 203.43 9.16 o 0 4 0 349.35 374.49 6.67 o 1 4 0 447.26 460.85 3.41 o 2 4 0 10483.82 10791.46 172.36 o 3 4 0 10.97 8.86 1.17 o 4 4 0 430.77 412.10 15.59 o 5 4 0 83.22 79.63 2.53 o 6 4 0 9834.77 9474.12 139.97 o 7 4 0 243.55 237.28 6.58 o 8 4 0 32.51 29.43 3.23 o 9 4 0 72.76 66.70 4.66 o 10 4 0 722.07 672.27 28.32 o 11 4 0 27.25 24.42 4.97 o 1 5 0 157.49 131.20 1.47 o 2 5 0 7804.87 9094.47 242.20 o 3 5 0 1341.99 1427.67 19.39 o 4 5 0 141.16 152.50 2.85 o 5 5 0 1850.06 1826.98 20.59 o 6 5 0 1637.26 1613.65 19.20 o 7 5 0 66.13 63.58 3.20 o 8 5 0 20.59 14.18 3.00 o 9 5 0 679.01 669.10 12.13 o 10 5 0 300.40 291.93 13.02 o 11 5 0 0.41 3.74 3.90 o 0 6 0 3.99 6.30 1.05 o 1 6 0 2815.34 2853.49 37.39 o 2 6 0 1244.90 1245.71 9.19 o 3 6 0 608.13 604.16 4.89 o 4 6 0 230.79 235.80 3.57 o 5 6 0 266.22 275.27 4.29 o 6 6 0 178.45 184.19 3.67 o 7 6 0 279.03 275.94 5.96 o 8 6 0 8.47 6.29 2.70 o 9 6 0 510.08 511.19 10.02 o 10 6 0 427.66 450.84 11.43 o 11 6 0 389.02 373.84 13.35 o 1 7 0 1359.87 1314.58 11.07 o 2 7 0 9.95 10.24 0.80 o 3 7 0 713.90 726.08 10.44 o 4 7 0 104.48 104.88 4.08 o 5 7 0 401.29 404.64 5.91 o 6 7 0 159.16 160.89 3.22 o 7 7 0 1.46 1.49 1.13 o 8 7 0 115.75 121.26 3.94 o 9 7 0 1496.78 1446.00 19.39 o 10 7 0 123.35 131.82 10.92 o 0 8 0 5866.15 5630.84 88.87 o 1 8 0 919.07 933.64 8.63 o 2 8 0 159.47 172.18 3.38 o 3 8 0 219.69 220.76 5.51 o 4 8 0 2291.99 2305.88 33.41 o 5 8 0 31.63 34.10 4.02 o 6 8 0 44.90 51.23 6.14 o 7 8 0 216.01 207.43 4.48 o 8 8 0 1445.22 1432.89 16.63 o 9 8 0 231.24 239.87 12.38 o 10 8 0 8.21 10.83 7.54 o 1 9 0 382.38 374.47 4.38 o 2 9 0 302.70 293.08 3.08 o 3 9 0 950.60 955.09 13.59 o 4 9 0 204.29 172.33 6.02 o 5 9 0 137.41 144.64 6.64 o 6 9 0 306.60 292.13 9.17 o 7 9 0 645.96 647.10 16.44 o 8 9 0 250.50 257.46 12.03 o 9 9 0 2.40 -0.17 4.27 o 0 10 0 80.22 81.00 3.23 o 1 10 0 26.29 25.31 2.24 o 2 10 0 515.84 517.94 5.02 o 3 10 0 1086.83 1088.75 16.29 o 4 10 0 4428.08 4330.18 55.21 o 5 10 0 1173.35 1166.24 19.07 o 6 10 0 65.08 79.57 6.87 o 7 10 0 201.19 193.88 9.26 o 8 10 0 246.53 235.92 12.93 o 9 10 0 4.17 2.96 5.23 o 1 11 0 0.81 0.34 1.10 o 2 11 0 67.65 64.75 2.13 o 3 11 0 1268.90 1169.88 17.34 o 4 11 0 93.63 101.43 6.54 o 5 11 0 227.29 214.74 7.74 o 6 11 0 86.87 89.90 6.39 o 7 11 0 82.19 66.69 14.69 o 8 11 0 77.17 73.77 14.89 o 0 12 0 349.38 347.25 7.39 o 1 12 0 613.37 631.43 8.24 o 2 12 0 802.79 788.67 12.15 o 3 12 0 529.89 527.82 11.32 o 4 12 0 279.86 285.46 8.96 o 5 12 0 103.46 102.34 6.47 o 6 12 0 297.72 293.78 11.86 o 7 12 0 43.73 28.10 17.58 o 1 13 0 213.58 228.26 4.78 o 2 13 0 136.01 138.48 5.84 o 3 13 0 4.38 2.44 3.08 o 4 13 0 16.32 9.19 3.84 o 5 13 0 86.84 71.76 29.96 o 6 13 0 124.02 130.53 10.95 o 0 14 0 902.11 898.77 14.65 o 1 14 0 197.48 196.11 6.08 o 2 14 0 1986.30 1998.78 36.74 o 3 14 0 245.20 239.49 8.43 o 4 14 0 14.28 8.54 4.65 o 5 14 0 151.94 150.42 9.74 o 1 15 0 30.21 0.15 3.77 o 2 15 0 63.50 67.61 19.93 o 3 15 0 158.16 175.84 10.02 o 4 15 0 23.11 18.48 8.22 o 0 0 1 2917.19 3152.96 150.41 o 2 0 1 12960.07 13167.39 152.92 o 4 0 1 23.12 24.92 2.20 o 6 0 1 1020.65 1015.50 13.99 o 8 0 1 33.50 37.53 4.27 o 10 0 1 3243.98 3189.91 47.89 o 1 1 1 268.78 251.09 3.20 o 2 1 1 196.16 221.51 2.73 o 3 1 1 2624.89 2613.23 20.05 o 4 1 1 9.01 12.47 1.35 o 5 1 1 18.94 16.42 1.70 o 6 1 1 42.37 40.79 2.36 o 7 1 1 516.40 499.41 6.58 o 8 1 1 215.66 208.89 4.95 o 9 1 1 20.51 23.88 3.14 o 10 1 1 112.31 119.73 4.99 o 11 1 1 780.70 779.49 12.73 o 0 2 1 410.93 372.67 3.48 o 1 2 1 215.76 328.60 2.71 o 2 2 1 781.31 781.15 6.29 o 3 2 1 6534.36 6652.53 57.24 o 4 2 1 1730.01 1659.39 24.46 o 5 2 1 3768.29 3653.31 29.74 o 6 2 1 328.98 324.21 4.92 o 7 2 1 4.27 7.58 1.85 o 8 2 1 189.10 188.36 4.49 o 9 2 1 73.54 78.53 4.05 o 10 2 1 128.71 134.33 5.44 o 11 2 1 708.30 725.18 11.85 o 1 3 1 423.56 347.92 2.57 o 2 3 1 849.70 910.36 7.97 o 3 3 1 4559.08 4594.29 35.54 o 4 3 1 73.51 72.95 1.86 o 5 3 1 5545.89 5411.32 44.27 o 6 3 1 14.20 12.61 1.66 o 7 3 1 53.60 60.63 3.17 o 8 3 1 46.53 50.78 3.25 o 9 3 1 813.73 805.24 11.36 o 10 3 1 360.00 362.92 7.69 o 11 3 1 121.47 123.97 5.80 o 0 4 1 1769.39 1638.12 13.63 o 1 4 1 13.31 12.67 1.14 o 2 4 1 599.05 613.65 4.20 o 3 4 1 267.52 273.13 3.52 o 4 4 1 6821.95 6612.41 53.66 o 5 4 1 273.44 267.95 4.00 o 6 4 1 496.68 504.32 5.63 o 7 4 1 75.22 75.32 3.28 o 8 4 1 1116.23 1118.58 12.05 o 9 4 1 0.11 1.03 1.74 o 10 4 1 8.84 7.35 2.56 o 11 4 1 8.62 5.48 2.81 o 1 5 1 25.67 26.32 1.13 o 2 5 1 399.17 434.74 3.31 o 3 5 1 3.75 4.38 0.64 o 4 5 1 522.72 523.65 6.06 o 5 5 1 153.25 151.89 2.91 o 6 5 1 18.54 19.69 1.52 o 7 5 1 226.07 223.18 3.96 o 8 5 1 406.49 402.33 6.18 o 9 5 1 438.75 433.84 7.36 o 10 5 1 4.07 2.85 2.13 o 11 5 1 132.57 140.37 7.49 o 0 6 1 1.03 1.55 0.71 o 1 6 1 1328.87 1332.82 8.48 o 2 6 1 509.87 483.91 3.56 o 3 6 1 1433.52 1380.34 10.88 o 4 6 1 7.45 6.62 0.93 o 5 6 1 232.36 228.17 3.88 o 6 6 1 74.88 77.42 2.63 o 7 6 1 78.52 84.00 2.70 o 8 6 1 25.66 21.32 2.75 o 9 6 1 447.24 463.59 7.00 o 10 6 1 198.74 197.92 7.52 o 1 7 1 7798.11 7541.06 49.10 o 2 7 1 84.33 85.90 1.53 o 3 7 1 554.68 540.91 5.62 o 4 7 1 72.83 73.83 2.48 o 5 7 1 85.28 95.26 4.25 o 6 7 1 54.86 57.68 1.73 o 7 7 1 3858.04 3793.62 36.63 o 8 7 1 135.28 136.79 4.23 o 9 7 1 1025.16 1066.83 15.18 o 10 7 1 173.66 181.08 7.70 o 0 8 1 2492.28 2561.52 21.78 o 1 8 1 884.76 899.12 6.71 o 2 8 1 1277.96 1251.54 8.43 o 3 8 1 69.28 71.84 2.31 o 4 8 1 418.85 417.86 5.06 o 5 8 1 90.73 89.02 2.95 o 6 8 1 464.47 455.58 6.87 o 7 8 1 240.03 248.67 7.25 o 8 8 1 660.22 683.59 11.34 o 9 8 1 148.66 154.55 7.10 o 1 9 1 3.02 3.08 0.84 o 2 9 1 581.71 540.64 5.38 o 3 9 1 36.15 36.65 3.58 o 4 9 1 16.06 15.22 1.65 o 5 9 1 70.57 71.09 2.75 o 6 9 1 151.47 152.23 3.94 o 7 9 1 128.23 127.60 4.47 o 8 9 1 0.06 0.46 2.33 o 9 9 1 151.82 160.16 10.46 o 0 10 1 185.24 189.22 3.58 o 1 10 1 179.64 186.73 2.75 o 2 10 1 189.69 189.43 3.41 o 3 10 1 489.51 477.20 5.62 o 4 10 1 191.01 200.51 3.75 o 5 10 1 725.57 715.52 7.96 o 6 10 1 894.44 888.53 9.89 o 7 10 1 327.97 326.05 6.82 o 8 10 1 7.61 6.48 3.40 o 1 11 1 874.26 890.18 6.92 o 2 11 1 0.78 1.28 1.11 o 3 11 1 710.44 704.83 7.62 o 4 11 1 88.72 86.74 4.93 o 5 11 1 2277.87 2185.83 19.37 o 6 11 1 184.56 192.19 6.42 o 7 11 1 508.38 537.40 10.73 o 8 11 1 108.53 118.14 7.07 o 0 12 1 398.57 376.39 6.51 o 1 12 1 1522.10 1569.02 12.64 o 2 12 1 1185.48 1205.27 11.04 o 3 12 1 7.18 5.07 1.66 o 4 12 1 1.43 2.19 1.41 o 5 12 1 2.95 1.25 2.07 o 6 12 1 592.23 622.72 12.10 o 7 12 1 607.58 639.36 12.26 o 1 13 1 113.88 123.20 3.81 o 2 13 1 0.24 0.89 1.24 o 3 13 1 3.42 2.09 1.62 o 4 13 1 1.89 1.71 2.52 o 5 13 1 123.81 133.06 6.17 o 6 13 1 21.57 9.61 5.73 o 0 14 1 1581.67 1531.23 67.49 o 1 14 1 308.80 313.66 7.16 o 2 14 1 4.98 2.79 2.15 o 3 14 1 107.78 99.86 5.40 o 4 14 1 125.56 117.30 5.64 o 1 15 1 497.92 519.09 13.44 o 2 15 1 42.37 32.24 11.37 o 0 0 2 27729.01 26721.19 911.10 o 2 0 2 14.84 10.17 2.75 o 4 0 2 1131.52 1246.14 16.14 o 6 0 2 294.99 279.98 6.67 o 8 0 2 5977.06 5913.00 80.55 o 10 0 2 10.95 8.52 5.95 o 1 1 2 7.76 6.56 1.59 o 2 1 2 0.15 0.21 0.67 o 3 1 2 248.43 253.47 3.35 o 4 1 2 57.37 65.82 2.55 o 5 1 2 163.06 166.16 3.42 o 6 1 2 14.21 13.28 2.19 o 7 1 2 198.36 200.40 5.58 o 8 1 2 227.71 227.86 5.82 o 9 1 2 7.10 4.26 2.62 o 10 1 2 131.42 134.22 5.70 o 0 2 2 21.18 10.47 7.91 o 1 2 2 777.12 732.73 7.69 o 2 2 2 0.27 0.55 1.02 o 3 2 2 498.37 489.84 6.96 o 4 2 2 15.17 15.30 1.43 o 5 2 2 947.72 939.68 10.74 o 6 2 2 6.02 4.92 2.18 o 7 2 2 898.63 902.81 10.56 o 8 2 2 12.13 9.36 2.83 o 9 2 2 94.29 89.18 6.62 o 10 2 2 0.14 -0.34 2.19 o 1 3 2 201.85 203.66 3.15 o 2 3 2 18.87 22.25 1.79 o 3 3 2 171.98 174.49 3.92 o 4 3 2 63.33 62.26 3.00 o 5 3 2 24.11 28.98 2.62 o 6 3 2 42.27 38.54 4.54 o 7 3 2 838.72 848.69 11.00 o 8 3 2 51.38 49.91 5.76 o 9 3 2 52.09 40.13 7.62 o 10 3 2 44.88 29.07 6.67 o 0 4 2 39.71 44.61 3.28 o 1 4 2 161.81 162.44 2.33 o 2 4 2 5105.37 5026.08 36.83 o 3 4 2 12.97 15.73 1.75 o 4 4 2 123.53 107.76 2.32 o 5 4 2 50.82 51.88 3.29 o 6 4 2 5153.31 5109.18 47.00 o 7 4 2 136.67 130.08 4.63 o 8 4 2 29.49 21.93 3.78 o 9 4 2 46.52 34.38 6.80 o 1 5 2 142.62 145.55 2.63 o 2 5 2 2239.57 2151.20 15.97 o 3 5 2 531.45 530.35 5.48 o 4 5 2 59.77 59.82 2.18 o 5 5 2 949.58 947.41 10.51 o 6 5 2 738.70 737.60 10.28 o 7 5 2 42.75 41.00 4.32 o 8 5 2 17.37 13.12 3.11 o 9 5 2 448.41 427.56 10.54 o 0 6 2 0.06 -1.15 2.14 o 1 6 2 1203.96 1163.40 9.78 o 2 6 2 580.11 585.96 5.84 o 3 6 2 368.06 361.96 3.87 o 4 6 2 101.97 107.74 3.01 o 5 6 2 180.01 188.33 3.72 o 6 6 2 107.18 112.69 3.55 o 7 6 2 171.50 169.76 5.63 o 8 6 2 3.32 2.49 2.75 o 9 6 2 354.56 338.13 14.28 o 1 7 2 600.65 579.37 7.24 o 2 7 2 6.76 6.71 1.46 o 3 7 2 367.06 368.47 4.25 o 4 7 2 56.87 58.57 2.07 o 5 7 2 287.58 288.68 4.38 o 6 7 2 95.99 97.92 3.50 o 7 7 2 0.10 0.41 1.33 o 8 7 2 81.44 86.24 6.27 o 0 8 2 3047.14 2965.37 43.02 o 1 8 2 488.42 496.05 6.06 o 2 8 2 114.09 118.16 2.91 o 3 8 2 134.81 142.64 2.85 o 4 8 2 1361.66 1367.38 11.00 o 5 8 2 27.50 28.47 2.07 o 6 8 2 42.52 41.10 4.32 o 7 8 2 153.38 154.62 5.46 o 8 8 2 952.08 953.25 14.17 o 1 9 2 204.48 206.36 3.79 o 2 9 2 114.27 105.58 2.99 o 3 9 2 528.67 536.84 5.62 o 4 9 2 106.62 105.15 2.76 o 5 9 2 70.68 75.57 3.35 o 6 9 2 170.75 173.76 5.57 o 7 9 2 412.41 419.67 8.45 o 0 10 2 69.03 67.08 5.14 o 1 10 2 26.02 19.21 2.33 o 2 10 2 274.27 293.36 4.72 o 3 10 2 642.84 647.09 6.86 o 4 10 2 2498.84 2566.61 22.90 o 5 10 2 741.18 743.79 9.95 o 6 10 2 26.01 26.63 3.32 o 7 10 2 144.03 137.90 6.45 o 1 11 2 1.55 0.90 1.33 o 2 11 2 41.42 40.94 3.12 o 3 11 2 728.96 702.96 9.10 o 4 11 2 62.22 60.59 5.25 o 5 11 2 112.42 110.82 5.72 o 6 11 2 63.38 63.84 5.25 o 0 12 2 255.23 254.58 9.53 o 1 12 2 440.38 456.10 8.84 o 2 12 2 528.97 524.09 8.18 o 3 12 2 340.01 345.08 6.87 o 4 12 2 202.68 209.05 7.37 o 5 12 2 73.12 73.83 5.63 o 1 13 2 135.45 143.45 5.72 o 2 13 2 80.93 79.74 4.80 o 3 13 2 4.22 4.57 3.07 o 0 0 3 646.01 658.82 19.52 o 2 0 3 3050.42 3120.68 40.62 o 4 0 3 17.48 16.51 8.28 o 6 0 3 498.60 516.05 16.61 o 1 1 3 82.17 87.35 3.32 o 2 1 3 16.10 13.10 2.08 o 3 1 3 600.21 632.36 9.11 o 4 1 3 1.21 0.05 1.53 o 5 1 3 2.19 7.05 5.14 o 6 1 3 9.65 3.34 3.58 o 7 1 3 212.88 226.12 10.99 o 0 2 3 163.56 168.06 5.89 o 1 2 3 9.20 8.43 2.49 o 2 2 3 199.57 202.52 3.74 o 3 2 3 1311.38 1285.92 14.85 o 4 2 3 446.05 435.23 9.52 o 5 2 3 1049.18 1025.87 21.10 o 6 2 3 101.16 95.80 9.69 o 7 2 3 18.14 9.28 6.06 o 1 3 3 259.30 281.25 6.33 o 2 3 3 142.60 140.65 4.66 o 3 3 3 967.92 999.83 15.23 o 4 3 3 20.94 17.68 2.77 o 5 3 3 1564.72 1588.64 18.19 o 6 3 3 1.63 0.69 2.25 o 7 3 3 5.78 4.16 3.42 o 0 4 3 860.08 897.85 16.11 o 1 4 3 14.36 14.63 2.64 o 2 4 3 232.30 247.03 6.09 o 3 4 3 78.97 77.03 8.53 o 4 4 3 1991.36 2024.47 21.05 o 5 4 3 87.30 83.10 7.94 o 6 4 3 262.59 263.11 7.09 o 7 4 3 34.60 22.52 5.07 o 1 5 3 6.74 8.37 2.42 o 2 5 3 112.46 108.74 4.94 o 3 5 3 0.02 0.31 1.36 o 4 5 3 113.94 110.20 3.92 o 5 5 3 64.07 60.61 4.50 o 6 5 3 17.14 9.64 3.45 o 0 6 3 0.30 2.41 3.47 o 1 6 3 427.14 428.55 7.53 o 2 6 3 152.10 146.92 5.68 o 3 6 3 442.39 435.47 9.27 o 4 6 3 3.17 5.22 2.35 o 5 6 3 106.48 103.85 9.22 o 6 6 3 27.65 15.61 4.65 o 1 7 3 1967.67 2002.02 20.48 o 2 7 3 23.71 26.13 3.62 o 3 7 3 235.64 259.42 7.48 o 4 7 3 29.29 18.03 4.38 o 5 7 3 27.06 18.54 4.54 o 0 8 3 943.63 976.39 18.76 o 1 8 3 318.00 328.03 7.21 o 2 8 3 524.12 520.80 9.83 o 3 8 3 47.83 33.51 7.71 o 4 8 3 207.94 216.02 6.36 o 1 9 3 1.91 1.71 2.44 o 2 9 3 154.98 154.78 6.00 o 3 9 3 15.18 7.85 2.91 o 0 10 3 73.35 64.38 24.87 o 1 10 3 83.76 86.13 7.84 o