#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:18:35 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180847 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/78/2017886.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2017886_Fobs loop_ _publ_author_name 'Gutierrez, Julio' 'Eisenberg, Rodney' 'Herrensmith, Gabrielle' 'Tobin, Thomas' 'Li, Tonglei' 'Long, Sihui' _publ_section_title ; Polymorphism in 2-(4-hydroxy-2,6-dimethylanilino)-5,6-dihydro-4H-1,3-thiazin-3-ium chloride ; _journal_coeditor_code FG3203 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o593 _journal_page_last o595 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.024 _cell_angle_gamma 90.000 _cell_length_a 11.8877 _cell_length_b 9.2120 _cell_length_c 12.6673 _exptl_crystal_F_000 576.00 _reflns_d_resolution_high 0.7700 _cod_data_source_file fg3203IIsup3.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' II P 21/c R = New: P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 163.08 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 67.93 77.79 1.08 o 2 0 0 135.20 121.32 2.07 o 3 0 0 4.37 21.56 2.07 o 4 0 0 2.29 -0.98 0.98 o 5 0 0 114.88 86.85 2.95 o 6 0 0 4649.89 4826.96 69.72 o 7 0 0 0.28 -1.97 1.97 o 8 0 0 881.08 810.04 19.69 o 9 0 0 1434.44 1509.20 31.71 o 10 0 0 239.90 231.61 11.42 o 11 0 0 861.47 898.07 35.74 o 12 0 0 36.59 19.59 16.64 o 13 0 0 17.58 12.81 19.80 o 14 0 0 218.42 246.18 48.25 o 15 0 0 1437.72 2093.34 137.86 o 1 1 0 2719.79 2507.81 29.93 o 2 1 0 645.30 674.27 10.37 o 3 1 0 2287.39 2225.07 28.20 o 4 1 0 2471.41 2481.67 30.95 o 5 1 0 1447.44 1485.48 16.16 o 6 1 0 5366.44 5618.43 62.93 o 7 1 0 3.96 5.51 1.76 o 8 1 0 133.16 128.66 5.48 o 9 1 0 195.77 169.63 6.61 o 10 1 0 182.90 175.38 21.02 o 11 1 0 1766.87 1867.93 54.05 o 12 1 0 1000.72 1086.26 45.42 o 13 1 0 16.20 18.71 12.76 o 14 1 0 131.68 117.88 22.20 o 15 1 0 30.50 -9.38 20.79 o 0 2 0 6.47 5.14 0.93 o 1 2 0 97.52 98.37 2.23 o 2 2 0 435.91 415.11 10.19 o 3 2 0 1065.81 1038.72 24.27 o 4 2 0 482.31 484.59 7.83 o 5 2 0 958.84 985.38 11.30 o 6 2 0 650.30 710.64 10.66 o 7 2 0 0.14 -2.34 3.44 o 8 2 0 519.50 534.41 11.50 o 9 2 0 142.20 127.09 6.65 o 10 2 0 500.15 466.21 14.84 o 11 2 0 426.67 392.33 23.48 o 12 2 0 134.38 142.00 29.59 o 13 2 0 3.76 -0.39 8.23 o 14 2 0 7.02 7.66 15.41 o 15 2 0 32.05 39.94 21.66 o 1 3 0 946.34 949.67 17.42 o 2 3 0 402.69 446.23 6.05 o 3 3 0 4292.27 4264.55 65.53 o 4 3 0 1503.86 1416.10 16.46 o 5 3 0 180.33 159.51 4.40 o 6 3 0 2468.74 2546.04 77.40 o 7 3 0 843.84 883.24 16.11 o 8 3 0 847.42 845.04 17.10 o 9 3 0 1803.50 1982.52 38.47 o 10 3 0 74.91 51.29 15.76 o 11 3 0 188.54 181.00 13.15 o 12 3 0 140.85 121.07 18.64 o 13 3 0 18.87 8.00 16.23 o 14 3 0 157.12 149.48 20.89 o 0 4 0 3000.32 2941.46 80.05 o 1 4 0 146.16 111.94 4.63 o 2 4 0 5034.61 5308.64 66.33 o 3 4 0 7.26 18.66 3.44 o 4 4 0 243.84 280.83 5.27 o 5 4 0 28.23 34.00 3.16 o 6 4 0 1653.26 1666.52 33.23 o 7 4 0 89.75 61.55 4.09 o 8 4 0 2219.22 2406.68 42.42 o 9 4 0 3449.25 3696.25 67.29 o 10 4 0 3.38 5.17 5.92 o 11 4 0 113.59 90.33 9.67 o 12 4 0 3.24 -10.93 10.93 o 13 4 0 58.93 52.09 15.69 o 14 4 0 43.20 35.67 19.87 o 1 5 0 112.38 100.65 4.09 o 2 5 0 2309.91 2384.35 39.88 o 3 5 0 7250.28 7919.36 181.68 o 4 5 0 49.82 29.35 7.92 o 5 5 0 380.98 358.16 7.94 o 6 5 0 243.55 225.36 15.17 o 7 5 0 18.89 14.50 4.03 o 8 5 0 130.53 134.59 6.58 o 9 5 0 186.49 164.59 11.72 o 10 5 0 80.82 62.04 8.54 o 11 5 0 291.55 294.11 13.44 o 12 5 0 844.43 968.87 32.80 o 13 5 0 138.46 104.04 18.11 o 0 6 0 585.83 555.02 13.91 o 1 6 0 462.76 471.18 8.50 o 2 6 0 806.81 792.99 11.78 o 3 6 0 258.74 243.30 5.61 o 4 6 0 8.67 5.89 2.75 o 5 6 0 111.86 120.38 6.07 o 6 6 0 56.77 43.75 8.72 o 7 6 0 17.65 1.02 5.46 o 8 6 0 1186.54 1247.51 25.85 o 9 6 0 901.79 943.84 24.43 o 10 6 0 1.52 2.44 7.32 o 11 6 0 1.13 -0.20 9.18 o 12 6 0 213.40 193.00 16.31 o 13 6 0 385.95 386.65 46.19 o 1 7 0 743.37 762.69 17.89 o 2 7 0 819.20 869.67 16.02 o 3 7 0 287.68 293.30 13.88 o 4 7 0 13.79 16.26 3.84 o 5 7 0 175.51 176.81 12.90 o 6 7 0 47.53 32.28 6.23 o 7 7 0 20.52 9.96 5.86 o 8 7 0 415.21 439.33 17.08 o 9 7 0 286.61 302.03 16.93 o 10 7 0 18.50 20.69 11.33 o 11 7 0 95.28 94.52 13.30 o 12 7 0 31.37 41.63 14.47 o 0 8 0 3359.86 3629.04 97.05 o 1 8 0 1825.07 1849.50 49.82 o 2 8 0 469.56 497.15 16.81 o 3 8 0 106.51 104.76 5.85 o 4 8 0 44.51 34.55 12.75 o 5 8 0 5.35 -2.43 6.45 o 6 8 0 322.28 342.12 21.96 o 7 8 0 935.84 993.69 29.64 o 8 8 0 1009.43 1117.34 34.57 o 9 8 0 244.98 214.68 14.79 o 10 8 0 34.37 37.02 64.99 o 11 8 0 111.12 114.70 27.57 o 1 9 0 381.92 407.85 16.75 o 2 9 0 413.99 431.35 18.34 o 3 9 0 1114.31 1134.48 83.95 o 4 9 0 171.53 155.55 14.07 o 5 9 0 243.53 244.75 16.46 o 6 9 0 1010.64 1052.37 66.72 o 7 9 0 20.51 15.64 13.52 o 8 9 0 7.14 -17.23 17.23 o 9 9 0 10.23 0.83 22.60 o 10 9 0 109.74 139.99 25.25 o 0 10 0 268.09 262.24 28.46 o 1 10 0 650.24 683.30 31.21 o 2 10 0 75.82 64.31 15.27 o 3 10 0 19.64 0.97 11.42 o 4 10 0 88.22 85.88 15.79 o 5 10 0 174.56 187.48 21.78 o 6 10 0 6.16 -4.66 19.20 o 7 10 0 165.06 91.18 24.72 o 8 10 0 278.86 306.91 27.03 o 1 11 0 159.76 139.93 20.78 o 2 11 0 24.58 9.84 16.74 o 3 11 0 20.77 19.59 15.86 o 4 11 0 20.15 24.62 21.76 o 5 11 0 26.85 42.15 20.78 o -15 1 1 7.63 -19.72 19.80 o -14 1 1 10.71 12.74 16.29 o -13 1 1 88.69 65.97 16.35 o -12 1 1 358.52 333.00 18.38 o -11 1 1 4.49 11.26 6.18 o -10 1 1 1393.52 1459.75 32.09 o -9 1 1 298.58 290.31 8.71 o -8 1 1 9.13 7.43 3.03 o -7 1 1 55.53 54.01 7.38 o -6 1 1 468.28 564.72 8.96 o -5 1 1 23.44 7.57 1.53 o -4 1 1 2652.44 2695.61 32.27 o -3 1 1 1090.63 1141.26 14.18 o -2 1 1 809.91 834.05 10.74 o -1 1 1 243.78 209.77 3.20 o 0 1 1 6057.61 6029.85 72.61 o 1 1 1 3201.21 3040.88 35.42 o 2 1 1 2626.90 2459.86 30.81 o 3 1 1 8.07 8.70 0.80 o 4 1 1 412.50 448.64 6.05 o 5 1 1 3396.15 3483.45 39.03 o 6 1 1 179.08 144.70 3.17 o 7 1 1 59.96 40.17 2.38 o 8 1 1 390.30 375.32 8.75 o 9 1 1 29.97 28.80 3.29 o 10 1 1 64.38 55.90 4.85 o 11 1 1 110.63 91.33 12.17 o 12 1 1 112.61 75.36 16.79 o 13 1 1 53.24 45.41 16.74 o 14 1 1 43.84 26.83 18.71 o 15 1 1 83.42 91.82 42.05 o -15 2 1 400.25 397.68 35.60 o -14 2 1 101.51 93.77 22.13 o -13 2 1 363.93 399.33 28.59 o -12 2 1 10.34 1.97 10.14 o -11 2 1 104.67 67.39 7.99 o -10 2 1 309.66 308.81 13.24 o -9 2 1 187.42 170.24 8.28 o -8 2 1 91.65 72.81 4.65 o -7 2 1 2585.29 2488.21 36.08 o -6 2 1 3989.49 4075.95 77.95 o -5 2 1 7.55 6.40 2.46 o -4 2 1 1592.80 1578.30 20.74 o -3 2 1 705.28 726.08 9.71 o -2 2 1 0.51 1.32 0.88 o -1 2 1 11665.63 11911.84 140.44 o 0 2 1 26.54 28.31 2.02 o 1 2 1 749.44 752.42 9.07 o 2 2 1 3303.45 3418.70 42.73 o 3 2 1 3058.44 3048.92 37.92 o 4 2 1 1458.37 1575.85 19.95 o 5 2 1 130.45 103.72 4.78 o 6 2 1 872.93 1013.74 12.96 o 7 2 1 129.03 107.83 5.80 o 8 2 1 948.54 971.42 16.94 o 9 2 1 2830.75 3011.29 55.34 o 10 2 1 734.65 773.11 22.21 o 11 2 1 1071.43 1152.09 79.96 o 12 2 1 20.28 14.54 12.43 o 13 2 1 43.03 18.08 13.39 o 14 2 1 3.84 5.90 32.84 o -14 3 1 3.67 11.24 17.70 o -13 3 1 561.43 670.99 35.25 o -12 3 1 1808.52 1968.36 69.69 o -11 3 1 3.73 -3.39 6.63 o -10 3 1 20.47 6.98 5.59 o -9 3 1 248.86 229.91 13.15 o -8 3 1 0.12 0.72 4.78 o -7 3 1 0.02 2.84 3.07 o -6 3 1 141.59 158.39 5.86 o -5 3 1 551.56 552.04 16.15 o -4 3 1 3692.71 3908.52 84.19 o -3 3 1 6195.09 6383.22 70.92 o -2 3 1 989.45 1009.49 12.67 o -1 3 1 1160.85 1070.28 21.56 o 0 3 1 5507.89 5711.41 99.46 o 1 3 1 194.11 180.80 2.99 o 2 3 1 2500.97 2632.37 30.53 o 3 3 1 1526.38 1562.74 17.38 o 4 3 1 14.88 3.15 1.64 o 5 3 1 1770.47 1694.49 22.80 o 6 3 1 1155.19 1252.51 19.99 o 7 3 1 477.35 466.66 9.24 o 8 3 1 194.22 200.77 6.06 o 9 3 1 1737.47 1795.99 36.34 o 10 3 1 25.56 14.38 6.86 o 11 3 1 601.81 630.35 20.97 o 12 3 1 142.43 132.16 32.99 o 13 3 1 139.64 124.15 19.74 o 14 3 1 659.81 765.44 44.80 o -14 4 1 96.04 78.74 16.45 o -13 4 1 2.69 -17.14 17.14 o -12 4 1 16.65 -0.18 14.72 o -11 4 1 0.32 3.33 9.43 o -10 4 1 381.89 385.40 14.35 o -9 4 1 10.13 7.04 5.21 o -8 4 1 42.24 32.22 5.21 o -7 4 1 472.33 455.01 8.90 o -6 4 1 14.91 11.06 2.63 o -5 4 1 119.64 127.76 4.21 o -4 4 1 277.46 282.50 10.64 o -3 4 1 923.32 938.56 12.45 o -2 4 1 549.55 555.43 10.38 o -1 4 1 100.74 79.46 2.51 o 0 4 1 721.86 781.02 25.41 o 1 4 1 7.69 14.12 1.92 o 2 4 1 0.83 2.95 1.40 o 3 4 1 523.83 562.66 29.64 o 4 4 1 28.32 18.07 2.33 o 5 4 1 64.01 80.23 3.75 o 6 4 1 118.64 106.99 5.46 o 7 4 1 352.70 322.87 8.09 o 8 4 1 399.86 419.49 8.96 o 9 4 1 10.47 13.46 5.19 o 10 4 1 52.72 38.71 10.88 o 11 4 1 244.14 215.93 12.86 o 12 4 1 44.95 41.45 11.12 o 13 4 1 15.65 13.67 22.21 o 14 4 1 22.36 16.11 16.49 o -13 5 1 49.34 55.23 15.25 o -12 5 1 393.51 414.73 19.84 o -11 5 1 211.11 222.35 34.17 o -10 5 1 594.19 574.15 28.85 o -9 5 1 519.39 569.43 17.33 o -8 5 1 56.88 54.78 8.91 o -7 5 1 40.20 46.47 5.02 o -6 5 1 7.63 3.91 3.53 o -5 5 1 122.08 125.73 5.73 o -4 5 1 900.00 980.20 17.41 o -3 5 1 44.39 24.62 2.85 o -2 5 1 874.60 902.38 13.20 o -1 5 1 1382.42 1493.60 25.50 o 0 5 1 203.05 176.34 4.39 o 1 5 1 318.50 315.99 6.30 o 2 5 1 109.04 115.08 3.04 o 3 5 1 2336.16 2501.66 58.00 o 4 5 1 0.40 -0.70 3.66 o 5 5 1 425.48 417.24 8.56 o 6 5 1 77.73 64.27 7.92 o 7 5 1 151.57 134.69 6.21 o 8 5 1 42.68 30.76 4.23 o 9 5 1 24.29 16.12 5.26 o 10 5 1 91.82 76.14 8.19 o 11 5 1 1.77 5.18 7.85 o 12 5 1 557.68 568.64 23.66 o 13 5 1 101.97 70.52 17.80 o -13 6 1 110.87 112.18 37.52 o -12 6 1 48.09 23.52 11.82 o -11 6 1 27.36 23.39 9.28 o -10 6 1 116.05 81.11 10.03 o -9 6 1 78.24 68.34 8.47 o -8 6 1 110.80 90.71 7.43 o -7 6 1 1180.27 1252.27 24.28 o -6 6 1 1281.68 1338.92 24.20 o -5 6 1 184.45 166.54 10.49 o -4 6 1 473.09 471.28 9.46 o -3 6 1 47.88 40.77 3.37 o -2 6 1 849.23 857.15 14.56 o -1 6 1 626.28 600.05 12.80 o 0 6 1 2082.60 2108.51 41.75 o 1 6 1 33.54 30.72 2.98 o 2 6 1 877.50 846.68 19.10 o 3 6 1 1531.15 1654.20 40.82 o 4 6 1 189.25 191.21 8.28 o 5 6 1 227.15 201.40 7.49 o 6 6 1 5.39 5.80 4.18 o 7 6 1 0.22 -3.38 5.46 o 8 6 1 1185.09 1288.51 27.85 o 9 6 1 570.44 625.73 18.30 o 10 6 1 72.52 57.52 11.96 o 11 6 1 811.81 902.47 32.84 o 12 6 1 0.13 9.92 12.56 o 13 6 1 32.17 50.01 16.11 o -12 7 1 174.49 169.52 18.46 o -11 7 1 3.22 1.51 10.40 o -10 7 1 558.36 610.14 26.34 o -9 7 1 223.15 221.18 19.15 o -8 7 1 462.93 467.64 42.73 o -7 7 1 124.74 126.08 18.56 o -6 7 1 0.53 4.09 5.70 o -5 7 1 32.73 20.25 9.31 o -4 7 1 2051.72 2067.68 32.89 o -3 7 1 469.91 450.09 10.80 o -2 7 1 19.29 7.09 2.31 o -1 7 1 574.44 538.50 13.37 o 0 7 1 107.56 108.63 6.15 o 1 7 1 3.17 3.95 2.82 o 2 7 1 215.22 215.63 12.01 o 3 7 1 8.06 9.39 4.97 o 4 7 1 345.78 339.79 10.82 o 5 7 1 1243.01 1304.48 33.98 o 6 7 1 765.60 782.75 22.32 o 7 7 1 0.03 -4.02 5.92 o 8 7 1 1031.81 1238.96 31.03 o 9 7 1 25.64 33.17 8.79 o 10 7 1 14.36 25.91 18.12 o 11 7 1 47.43 45.62 13.48 o 12 7 1 204.25 183.34 57.61 o -11 8 1 46.60 68.05 18.73 o -10 8 1 86.26 68.57 14.85 o -9 8 1 120.28 85.47 13.61 o -8 8 1 1059.46 1239.70 75.88 o -7 8 1 71.69 51.27 13.84 o -6 8 1 383.90 419.97 16.64 o -5 8 1 111.14 112.21 7.72 o -4 8 1 1.80 1.69 4.56 o -3 8 1 537.53 594.71 16.43 o -2 8 1 520.78 589.93 16.81 o -1 8 1 91.55 81.27 5.03 o 0 8 1 150.38 155.20 7.87 o 1 8 1 67.14 59.90 5.96 o 2 8 1 976.74 1071.77 25.16 o 3 8 1 7.27 2.95 5.36 o 4 8 1 6.08 5.30 7.67 o 5 8 1 35.13 23.09 8.86 o 6 8 1 285.65 284.20 19.30 o 7 8 1 435.67 429.98 19.93 o 8 8 1 8.25 9.50 11.75 o 9 8 1 22.84 15.94 13.74 o 10 8 1 15.31 -3.37 12.48 o 11 8 1 15.88 0.00 6.96 o -10 9 1 236.13 177.23 31.96 o -9 9 1 0.41 -7.78 15.52 o -8 9 1 47.40 52.98 14.16 o -7 9 1 136.73 116.21 18.86 o -6 9 1 95.43 102.62 27.97 o -5 9 1 194.12 230.57 23.48 o -4 9 1 1.15 -8.97 9.35 o -3 9 1 0.01 0.31 10.84 o -2 9 1 47.64 42.42 8.59 o -1 9 1 199.55 204.52 12.99 o 0 9 1 31.34 14.34 13.25 o 1 9 1 755.29 802.55 36.29 o 2 9 1 8.48 19.81 10.88 o 3 9 1 51.31 40.19 27.03 o 4 9 1 0.17 13.09 10.04 o 5 9 1 108.68 83.23 13.30 o 6 9 1 0.32 -4.81 10.24 o 7 9 1 96.71 63.59 16.33 o 8 9 1 82.40 64.04 16.09 o 9 9 1 104.64 98.80 20.67 o -8 10 1 57.70 28.77 21.31 o -7 10 1 148.71 159.33 36.68 o -6 10 1 189.01 227.52 25.55 o -5 10 1 28.68 12.87 14.79 o -4 10 1 310.77 321.23 25.11 o -3 10 1 0.01 -5.61 12.67 o -2 10 1 112.51 123.39 16.74 o -1 10 1 15.89 8.86 11.82 o 0 10 1 50.26 29.45 12.90 o 1 10 1 50.70 63.31 12.58 o 2 10 1 1021.95 1140.54 34.62 o 3 10 1 0.51 -9.46 10.74 o 4 10 1 320.01 317.17 21.22 o 5 10 1 12.07 13.25 14.20 o 6 10 1 112.56 95.62 16.44 o 7 10 1 94.53 85.98 17.95 o 8 10 1 6.62 -20.65 29.04 o -6 11 1 6.82 -7.78 21.56 o -5 11 1 14.90 11.91 21.66 o -4 11 1 679.53 767.79 43.43 o -3 11 1 569.48 548.01 35.25 o -2 11 1 21.96 7.78 15.56 o -1 11 1 37.70 31.52 16.93 o 0 11 1 192.25 173.71 24.02 o 1 11 1 479.32 571.73 36.05 o 2 11 1 5.15 29.45 15.66 o 3 11 1 265.25 245.20 24.52 o 4 11 1 4.77 16.64 24.62 o 5 11 1 310.62 301.33 24.98 o -15 0 2 762.26 844.40 62.04 o -14 0 2 257.00 226.89 30.23 o -13 0 2 756.67 899.94 50.81 o -12 0 2 10.75 1.97 9.94 o -11 0 2 2136.51 2053.27 68.24 o -10 0 2 0.60 -1.97 4.92 o -9 0 2 222.37 215.66 10.14 o -8 0 2 671.12 681.63 16.35 o -7 0 2 4069.96 4438.29 75.23 o -6 0 2 5085.13 6139.80 98.37 o -5 0 2 426.32 348.59 9.35 o -4 0 2 6516.81 6641.42 138.06 o -3 0 2 836.69 824.42 18.02 o -2 0 2 1515.38 1439.38 28.55 o -1 0 2 8111.06 7709.27 132.25 o 0 0 2 579.44 458.00 8.07 o 1 0 2 4279.29 4438.29 75.23 o 2 0 2 26594.87 26514.60 889.12 o 3 0 2 304.28 271.39 5.22 o 4 0 2 5638.12 5915.68 82.03 o 5 0 2 22.84 19.59 1.97 o 6 0 2 131.92 154.40 4.73 o 7 0 2 187.24 163.07 5.61 o 8 0 2 2382.53 2439.67 43.43 o 9 0 2 2354.40 2505.16 59.68 o 10 0 2 2.36 -1.97 6.89 o 11 0 2 497.61 534.90 46.48 o 12 0 2 15.58 15.66 13.69 o 13 0 2 720.42 855.34 56.91 o 14 0 2 6.67 -5.80 21.56 o -15 1 2 1.24 11.62 30.43 o -14 1 2 6.98 -7.75 12.75 o -13 1 2 326.88 315.29 26.00 o -12 1 2 96.75 70.31 10.03 o -11 1 2 223.42 233.08 10.87 o -10 1 2 1600.97 1612.88 34.72 o -9 1 2 260.10 260.36 12.16 o -8 1 2 233.44 218.02 11.08 o -7 1 2 474.33 421.82 8.22 o -6 1 2 3.35 2.27 2.83 o -5 1 2 981.28 1087.44 13.84 o -4 1 2 2729.06 2713.56 35.78 o -3 1 2 643.55 585.33 7.52 o -2 1 2 6131.01 6079.50 80.75 o -1 1 2 619.53 719.38 10.98 o 0 1 2 15912.92 15203.83 194.20 o 1 1 2 752.29 688.01 8.68 o 2 1 2 1125.27 1210.52 15.27 o 3 1 2 141.22 167.43 3.27 o 4 1 2 1291.89 1214.21 18.56 o 5 1 2 742.49 713.14 9.47 o 6 1 2 267.73 248.15 6.94 o 7 1 2 2033.26 2102.12 37.32 o 8 1 2 2045.55 2228.99 38.51 o 9 1 2 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