#------------------------------------------------------------------------------ #$Date: 2011-02-15 17:23:33 +0200 (Tue, 15 Feb 2011) $ #$Revision: 11387 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2017916.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2017916_Fobs loop_ _publ_author_name 'Jiang, Li-Fang' _publ_section_title ; catena-Poly[copper(II)-di-\m-acetylacetonato-copper(II)-bis(\m-4-hydroxy-3-methoxybenzaldehyde picoloylhydrazonato)] and (acetylacetonato)(4-methoxybenzaldehyde picoloylhydrazonato)copper(II) ; _journal_coeditor_code MX3036 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m375 _journal_page_last m378 _journal_volume 66 _journal_year 2010 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.683 _cell_angle_gamma 90.000 _cell_length_a 8.4719 _cell_length_b 23.5863 _cell_length_c 9.8635 _exptl_crystal_F_000 892.00 _reflns_d_resolution_high 0.7704 _[local]_cod_data_source_file mx3036Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' d in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 215.04 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 24581.65 25502.46 908.04 o 3 0 0 750.41 701.35 46.16 o 4 0 0 129.20 72.95 54.95 o 5 0 0 5401.90 5914.40 184.94 o 6 0 0 957.10 1092.75 108.47 o 7 0 0 2069.27 2264.10 109.90 o 8 0 0 50.55 -8.10 40.94 o 9 0 0 1117.73 1271.60 117.89 o 10 0 0 23.76 -71.43 89.51 o 2 1 0 5455.56 5861.52 114.94 o 3 1 0 100.18 110.00 19.97 o 4 1 0 32.05 34.89 16.07 o 5 1 0 173.60 168.00 21.54 o 6 1 0 6.29 44.37 20.68 o 7 1 0 24.85 26.79 26.45 o 8 1 0 7.55 3.95 22.88 o 9 1 0 8.70 26.54 40.17 o 10 1 0 13.15 40.05 37.24 o 1 2 0 8098.22 8549.00 134.55 o 2 2 0 15256.97 16212.01 368.68 o 3 2 0 2193.84 2223.52 60.62 o 4 2 0 6654.37 6649.19 147.22 o 5 2 0 137.60 94.40 19.27 o 6 2 0 489.08 482.76 32.43 o 7 2 0 2138.04 2272.20 83.72 o 8 2 0 112.81 135.21 33.64 o 9 2 0 259.19 281.23 49.04 o 10 2 0 40.71 45.62 40.27 o 1 3 0 2094.23 2266.69 40.66 o 2 3 0 807.53 873.64 33.00 o 3 3 0 1455.26 1592.59 52.39 o 4 3 0 2098.75 2216.80 58.47 o 5 3 0 503.69 457.88 41.44 o 6 3 0 202.63 242.39 29.31 o 7 3 0 53.88 82.10 27.64 o 8 3 0 12.08 0.00 24.58 o 9 3 0 4.33 46.64 36.83 o 10 3 0 59.27 31.30 41.76 o 0 4 0 27517.82 26819.62 924.86 o 1 4 0 62.71 63.16 10.51 o 2 4 0 7048.27 7024.61 145.67 o 3 4 0 4535.93 4508.93 95.97 o 4 4 0 970.99 854.54 47.32 o 5 4 0 1278.43 1295.28 49.54 o 6 4 0 947.68 995.21 51.80 o 7 4 0 1740.99 1719.99 99.11 o 8 4 0 4.47 -1.84 28.04 o 9 4 0 578.06 776.57 65.73 o 10 4 0 16.00 82.57 45.03 o 1 5 0 873.63 927.11 18.91 o 2 5 0 2015.69 2071.89 43.67 o 3 5 0 4244.29 4444.09 98.25 o 4 5 0 933.67 1046.77 35.47 o 5 5 0 61.29 67.39 19.17 o 6 5 0 519.37 477.61 39.44 o 7 5 0 22.35 18.33 25.70 o 8 5 0 0.61 -11.54 30.29 o 9 5 0 6.79 23.43 33.80 o 10 5 0 7.98 -33.79 40.14 o 0 6 0 318.10 364.75 27.19 o 1 6 0 1.36 0.40 7.13 o 2 6 0 2877.00 2791.78 61.29 o 3 6 0 1502.57 1358.69 33.88 o 4 6 0 603.50 554.01 29.09 o 5 6 0 1206.15 1235.66 42.69 o 6 6 0 512.32 487.13 34.56 o 7 6 0 831.13 842.04 46.97 o 8 6 0 17.83 89.30 36.82 o 9 6 0 267.62 337.48 81.10 o 10 6 0 22.42 -15.19 34.17 o 1 7 0 2476.69 2449.50 33.39 o 2 7 0 523.69 482.30 21.10 o 3 7 0 2841.63 2688.13 59.98 o 4 7 0 2497.05 2519.26 63.10 o 5 7 0 23.70 55.79 18.33 o 6 7 0 451.78 475.87 37.03 o 7 7 0 55.69 51.28 24.92 o 8 7 0 27.50 3.95 24.17 o 9 7 0 25.63 -31.11 38.22 o 10 7 0 6.26 -36.55 36.55 o 0 8 0 2031.58 1718.29 59.99 o 1 8 0 2331.38 2486.39 33.14 o 2 8 0 6346.63 6220.09 94.72 o 3 8 0 402.69 369.05 34.23 o 4 8 0 6.75 3.43 14.35 o 5 8 0 944.22 865.42 35.97 o 6 8 0 35.12 47.76 22.74 o 7 8 0 101.44 89.56 28.14 o 8 8 0 19.95 9.07 30.29 o 9 8 0 99.75 124.89 40.47 o 10 8 0 0.94 -6.34 31.61 o 1 9 0 81.22 63.22 6.02 o 2 9 0 70.32 55.94 9.11 o 3 9 0 2758.76 2573.33 49.80 o 4 9 0 2155.26 2092.42 46.04 o 5 9 0 356.29 435.17 46.87 o 6 9 0 607.07 631.41 42.83 o 7 9 0 4.24 24.62 25.89 o 8 9 0 60.20 22.55 28.77 o 9 9 0 0.08 67.47 32.93 o 10 9 0 37.09 4.29 38.58 o 0 10 0 175.51 157.96 28.23 o 1 10 0 432.07 463.94 14.22 o 2 10 0 847.41 683.74 17.05 o 3 10 0 2766.22 2905.19 52.59 o 4 10 0 2360.71 2210.25 80.58 o 5 10 0 2452.71 2303.42 65.20 o 6 10 0 724.22 818.09 42.45 o 7 10 0 632.41 630.56 49.78 o 8 10 0 86.82 70.26 28.14 o 9 10 0 77.56 62.94 30.99 o 10 10 0 23.68 0.61 33.34 o 1 11 0 24.38 106.42 14.21 o 2 11 0 91.11 79.97 8.26 o 3 11 0 55.14 115.39 21.77 o 4 11 0 2211.95 2027.73 52.03 o 5 11 0 544.06 557.13 34.19 o 6 11 0 194.59 249.15 32.64 o 7 11 0 124.49 114.62 25.78 o 8 11 0 8.03 -23.87 25.68 o 9 11 0 50.25 5.34 27.20 o 0 12 0 2699.56 3131.06 87.36 o 1 12 0 2486.37 2578.13 70.74 o 2 12 0 2622.78 2593.27 36.98 o 3 12 0 1.47 0.86 8.20 o 4 12 0 304.03 255.08 16.11 o 5 12 0 2.16 1.76 13.06 o 6 12 0 352.18 371.70 31.50 o 7 12 0 4.44 13.10 20.44 o 8 12 0 163.19 157.03 31.23 o 9 12 0 21.65 3.50 28.36 o 1 13 0 2132.76 1934.92 53.58 o 2 13 0 127.47 141.46 13.74 o 3 13 0 1028.60 954.16 28.46 o 4 13 0 572.59 574.68 26.08 o 5 13 0 413.31 452.58 29.41 o 6 13 0 1260.45 1215.76 45.91 o 7 13 0 7.87 14.85 20.57 o 8 13 0 419.01 401.97 72.24 o 9 13 0 7.68 7.11 25.63 o 0 14 0 347.51 313.10 29.95 o 1 14 0 222.74 261.61 24.34 o 2 14 0 1865.81 1789.29 30.15 o 3 14 0 8.09 19.27 9.96 o 4 14 0 160.03 165.45 13.96 o 5 14 0 549.14 533.14 24.58 o 6 14 0 9.75 -17.72 17.72 o 7 14 0 243.17 251.29 26.29 o 8 14 0 14.21 39.29 27.11 o 9 14 0 62.41 52.55 30.11 o 1 15 0 1648.17 1619.23 46.74 o 2 15 0 1349.77 1296.62 45.12 o 3 15 0 859.96 798.36 30.12 o 4 15 0 279.30 270.88 18.12 o 5 15 0 635.05 612.24 27.50 o 6 15 0 277.11 297.67 25.38 o 7 15 0 100.38 77.36 22.51 o 8 15 0 161.71 257.48 91.57 o 9 15 0 0.57 24.12 25.38 o 0 16 0 235.90 174.04 47.15 o 1 16 0 62.49 93.38 24.35 o 2 16 0 442.72 397.25 30.85 o 3 16 0 238.70 205.60 14.53 o 4 16 0 89.04 97.93 14.74 o 5 16 0 9.19 36.83 15.27 o 6 16 0 6.99 7.94 17.42 o 7 16 0 74.02 33.70 19.22 o 8 16 0 19.96 37.10 20.62 o 9 16 0 11.30 -8.95 25.62 o 1 17 0 3556.21 3858.15 91.73 o 2 17 0 497.78 450.72 17.78 o 3 17 0 1463.86 1349.47 24.97 o 4 17 0 171.34 153.17 15.84 o 5 17 0 759.96 690.70 22.71 o 6 17 0 613.55 606.51 32.71 o 7 17 0 103.09 71.84 18.33 o 8 17 0 450.11 403.22 77.47 o 0 18 0 557.04 596.64 52.89 o 1 18 0 24.22 42.04 18.18 o 2 18 0 128.57 162.96 37.80 o 3 18 0 149.72 144.58 13.06 o 4 18 0 441.95 382.28 30.94 o 5 18 0 21.26 35.29 15.35 o 6 18 0 44.36 53.29 17.29 o 7 18 0 95.71 164.54 45.62 o 8 18 0 12.24 23.76 21.40 o 1 19 0 2415.92 2606.45 76.55 o 2 19 0 1017.55 1045.34 70.75 o 3 19 0 1002.40 913.99 43.97 o 4 19 0 246.73 215.08 17.93 o 5 19 0 513.47 477.71 23.22 o 6 19 0 254.45 270.84 23.00 o 7 19 0 104.14 88.78 22.02 o 8 19 0 303.72 306.78 37.28 o 0 20 0 1750.36 1888.86 85.80 o 1 20 0 22.54 56.39 22.34 o 2 20 0 4.48 9.58 26.32 o 3 20 0 5.63 10.24 14.47 o 4 20 0 37.60 29.76 9.86 o 5 20 0 2.60 2.28 13.24 o 6 20 0 12.35 28.52 15.84 o 7 20 0 39.84 43.76 17.36 o 8 20 0 41.75 81.02 24.34 o 1 21 0 3038.51 3465.68 107.66 o 2 21 0 11.62 34.55 36.88 o 3 21 0 107.83 109.09 13.30 o 4 21 0 496.54 385.25 29.39 o 5 21 0 230.73 226.55 28.43 o 6 21 0 433.11 407.84 35.62 o 7 21 0 23.67 24.43 20.26 o 0 22 0 24.77 54.93 44.84 o 1 22 0 88.80 112.76 26.01 o 2 22 0 18.04 66.96 40.22 o 3 22 0 5.41 -30.70 30.70 o 4 22 0 5.98 12.14 11.63 o 5 22 0 19.68 15.08 10.69 o 6 22 0 2.88 -3.42 16.98 o 7 22 0 55.28 72.74 19.45 o 1 23 0 628.41 848.48 49.83 o 2 23 0 1327.82 1385.77 81.30 o 3 23 0 1860.07 2121.80 122.16 o 4 23 0 84.39 47.05 19.20 o 5 23 0 146.24 101.39 16.24 o 6 23 0 195.65 209.08 24.41 o 7 23 0 10.62 35.67 27.03 o 0 24 0 3.05 9.17 38.49 o 1 24 0 252.32 339.47 35.40 o 2 24 0 36.98 100.15 48.52 o 3 24 0 419.91 516.77 69.73 o 4 24 0 0.52 35.25 40.76 o 5 24 0 6.48 -36.30 36.30 o 6 24 0 77.15 31.61 45.08 o 1 25 0 286.69 408.78 60.09 o 2 25 0 2.99 -37.75 37.75 o 3 25 0 382.52 565.68 104.57 o 4 25 0 57.26 87.26 39.35 o 5 25 0 202.99 238.22 69.83 o 6 25 0 68.75 120.67 53.44 o 0 26 0 104.15 205.96 60.85 o 1 26 0 1.60 21.67 31.49 o 2 26 0 168.91 425.91 66.68 o 3 26 0 0.81 113.66 52.12 o 4 26 0 28.95 46.81 48.39 o 5 26 0 1.06 103.96 53.02 o 1 27 0 197.09 259.64 53.18 o 2 27 0 46.29 77.60 47.50 o 3 27 0 437.06 598.17 82.06 o 4 27 0 70.01 28.57 46.60 o 5 27 0 88.36 121.59 64.87 o 0 28 0 49.80 62.03 49.81 o 1 28 0 0.12 -53.10 54.86 o 2 28 0 25.70 34.41 53.47 o 3 28 0 19.38 12.37 79.76 o 4 28 0 16.94 5.23 36.97 o 1 29 0 94.79 150.74 70.19 o 2 29 0 0.42 42.41 70.19 o 3 29 0 108.52 215.81 65.46 o 0 30 0 193.23 157.24 56.37 o 1 30 0 0.54 47.40 118.58 o 2 30 0 30.17 -8.86 109.54 o -10 1 1 0.97 64.37 34.87 o -9 1 1 496.02 654.16 57.20 o -8 1 1 286.97 183.18 62.93 o -7 1 1 2983.94 3106.93 94.86 o -6 1 1 252.41 305.92 27.59 o -5 1 1 6674.37 7336.34 168.72 o -4 1 1 631.11 631.45 35.77 o -3 1 1 2956.86 2914.74 68.94 o -2 1 1 14.05 31.50 15.42 o 1 1 1 2765.94 3057.37 65.60 o 2 1 1 15305.21 16075.06 363.77 o 3 1 1 456.74 406.97 25.24 o 4 1 1 1151.72 1109.10 37.14 o 5 1 1 136.18 95.30 20.20 o 6 1 1 1522.87 1463.22 63.92 o 7 1 1 541.61 667.99 74.77 o 8 1 1 280.31 276.21 35.99 o 9 1 1 383.43 449.78 154.16 o 10 1 1 0.66 30.03 41.01 o -10 2 1 70.37 47.23 34.27 o -9 2 1 6.54 -14.96 28.09 o -8 2 1 35.88 -0.15 38.76 o -7 2 1 28.84 23.16 22.77 o -6 2 1 335.68 361.83 29.25 o -5 2 1 17.64 -5.52 16.96 o -4 2 1 1124.17 1157.04 36.63 o -3 2 1 2167.85 2380.24 58.86 o -2 2 1 2256.93 2446.06 58.39 o -1 2 1 457.14 505.49 23.64 o 1 2 1 4940.73 5333.67 104.04 o 2 2 1 32345.01 36140.37 1082.34 o 3 2 1 246.39 237.03 25.60 o 4 2 1 17.56 36.93 16.01 o 5 2 1 0.19 17.89 16.99 o 6 2 1 123.13 163.62 30.44 o 7 2 1 6.70 -26.64 26.64 o 8 2 1 49.40 30.95 27.27 o 9 2 1 0.33 -39.29 39.29 o 10 2 1 0.45 -1.55 39.50 o -10 3 1 19.32 47.53 42.02 o -9 3 1 250.55 252.46 39.17 o -8 3 1 21.83 -8.24 39.92 o -7 3 1 2948.22 2971.66 92.09 o -6 3 1 665.88 756.39 37.06 o -5 3 1 4836.00 4781.99 112.21 o -4 3 1 2303.74 2535.95 62.48 o -3 3 1 3366.72 3183.66 69.99 o -2 3 1 109.04 180.54 19.86 o -1 3 1 2987.59 2964.06 46.59 o 0 3 1 16961.47 15782.79 233.32 o 1 3 1 54.40 104.95 16.03 o 2 3 1 46240.63 49975.33 1763.88 o 3 3 1 64.77 67.86 20.21 o 4 3 1 6547.99 6672.91 140.69 o 5 3 1 134.71 133.15 22.96 o 6 3 1 520.55 546.19 41.67 o 7 3 1 890.13 963.89 57.05 o 8 3 1 52.92 40.12 29.47 o 9 3 1 337.33 455.30 84.41 o 10 3 1 27.99 0.54 39.25 o -10 4 1 77.81 83.83 39.61 o -9 4 1 76.43 63.28 31.11 o -8 4 1 1.41 42.23 37.20 o -7 4 1 0.01 38.12 22.87 o -6 4 1 149.68 133.63 22.91 o -5 4 1 1034.58 1142.17 41.89 o -4 4 1 548.20 498.31 29.84 o -3 4 1 0.76 -3.62 17.34 o -2 4 1 8343.99 8812.46 183.00 o -1 4 1 15.32 9.94 9.81 o 0 4 1 4021.99 3927.20 46.11 o 1 4 1 3623.06 3858.59 70.98 o 2 4 1 20913.35 23366.79 634.15 o 3 4 1 31.08 18.96 17.83 o 4 4 1 22.01 51.78 19.85 o 5 4 1 585.74 594.25 38.59 o 6 4 1 1.55 -4.68 20.77 o 7 4 1 21.90 12.72 35.87 o 8 4 1 0.48 -0.18 26.17 o 9 4 1 63.17 104.58 36.68 o 10 4 1 15.63 20.90 36.88 o -10 5 1 31.93 35.59 38.39 o -9 5 1 347.98 396.25 47.32 o -8 5 1 6.50 60.23 29.17 o -7 5 1 581.43 652.40 64.26 o -6 5 1 469.03 487.08 33.82 o -5 5 1 1064.53 1056.34 43.35 o -4 5 1 1299.62 1143.69 36.61 o -3 5 1 387.99 330.01 23.54 o -2 5 1 130.04 128.61 14.93 o -1 5 1 4812.28 5003.82 71.44 o 0 5 1 6507.39 6048.26 69.15 o 1 5 1 3934.12 3983.04 60.20 o 2 5 1 16612.77 17743.13 414.40 o 3 5 1 126.18 124.09 17.94 o 4 5 1 6660.64 6555.81 177.93 o 5 5 1 372.84 383.22 36.61 o 6 5 1 876.01 889.99 44.68 o 7 5 1 467.03 469.91 36.90 o 8 5 1 64.89 41.58 31.93 o 9 5 1 106.15 111.54 43.34 o 10 5 1 13.60 39.18 37.63 o -10 6 1 55.22 102.86 49.07 o -9 6 1 121.95 107.32 39.07 o -8 6 1 163.36 162.74 33.45 o -7 6 1 35.03 26.28 24.46 o -6 6 1 327.54 307.38 48.00 o -5 6 1 761.50 849.06 34.99 o -4 6 1 1852.70 1868.41 52.24 o -3 6 1 6350.43 6870.47 141.79 o -2 6 1 5074.95 5129.48 102.02 o -1 6 1 1561.81 1516.85 37.94 o 0 6 1 516.76 504.16 11.81 o 1 6 1 1233.44 1267.45 23.54 o 2 6 1 3125.02 3551.35 71.10 o 3 6 1 31.59 35.41 14.89 o 4 6 1 12.70 8.09 16.41 o 5 6 1 213.38 194.04 31.20 o 6 6 1 715.05 741.13 38.91 o 7 6 1 57.11 49.15 31.52 o 8 6 1 5.64 19.84 33.22 o 9 6 1 223.53 229.59 59.88 o 10 6 1 2.17 61.87 43.80 o -10 7 1 55.97 105.31 53.77 o -9 7 1 470.60 511.18 54.82 o -8 7 1 0.34 -23.67 23.98 o -7 7 1 1257.80 1261.45 71.75 o -6 7 1 41.89 46.16 23.70 o -5 7 1 573.79 567.33 29.96 o -4 7 1 2847.05 2819.50 62.79 o -3 7 1 10.87 8.89 11.78 o -2 7 1 12754.13 13008.88 242.77 o -1 7 1 1150.42 1102.96 23.34 o 0 7 1 5971.08 5523.57 62.22 o 1 7 1 13.52 12.04 10.54 o 2 7 1 5446.35 5343.29 96.77 o 3 7 1 860.97 847.79 55.00 o 4 7 1 3335.79 3156.75 84.72 o 5 7 1 2359.95 2427.53 68.44 o 6 7 1 410.19 355.27 32.95 o 7 7 1 703.42 724.73 41.26 o 8 7 1 47.06 44.83 35.70 o 9 7 1 90.17 116.17 36.81 o 10 7 1 0.07 -24.34 32.37 o -10 8 1 8.85 50.37 37.67 o -9 8 1 127.91 145.58 44.51 o -8 8 1 8.89 15.15 23.12 o -7 8 1 17.28 16.62 24.06 o -6 8 1 15.65 -21.09 21.91 o -5 8 1 893.99 918.66 36.79 o -4 8 1 2149.67 2136.67 53.88 o -3 8 1 622.89 595.68 24.29 o -2 8 1 892.55 880.81 26.26 o -1 8 1 284.50 307.93 16.37 o 0 8 1 16.61 22.10 5.73 o 1 8 1 1315.78 1255.55 20.51 o 2 8 1 1722.55 1617.66 31.43 o 3 8 1 53.87 34.25 16.18 o 4 8 1 124.41 113.75 15.98 o 5 8 1 705.60 646.48 39.55 o 6 8 1 254.53 296.97 29.86 o 7 8 1 93.00 45.33 24.38 o 8 8 1 2.92 -26.65 26.65 o 9 8 1 186.33 89.71 41.11 o 10 8 1 10.34 62.33 41.81 o -10 9 1 62.30 11.94 53.70 o -9 9 1 348.31 527.56 115.32 o -8 9 1 284.18 299.71 46.30 o -7 9 1 10.56 -20.26 21.74 o -6 9 1 105.10 109.26 23.49 o -5 9 1 348.83 391.04 27.23 o -4 9 1 594.17 579.49 24.97 o -3 9 1 2351.44 2327.06 45.44 o -2 9 1 1536.44 1353.41 28.22 o -1 9 1 142.97 201.03 16.30 o 0 9 1 316.37 264.05 9.02 o 1 9 1 238.69 261.13 9.42 o 2 9 1 29.14 57.47 9.40 o 3 9 1 686.41 716.43 39.50 o 4 9 1 1500.98 1367.68 43.92 o 5 9 1 1995.53 2045.25 56.06 o 6 9 1 1300.33 1277.92 57.45 o 7 9 1 1.98 -25.12 28.65 o 8 9 1 0.54 14.81 39.76 o 9 9 1 41.33 27.63 34.84 o -10 10 1 42.39 105.42 47.57 o -9 10 1 40.47 42.92 38.86 o -8 10 1 9.07 2.80 26.28 o -7 10 1 52.31 57.66 23.40 o -6 10 1 272.97 310.31 25.45 o -5 10 1 22.61 37.56 18.16 o -4 10 1 2843.74 2759.71 64.53 o -3 10 1 620.35 529.20 19.10 o -2 10 1 775.74 768.25 18.36 o -1 10 1 4761.56 5105.42 58.22 o 0 10 1 109.91 97.32 7.74 o 1 10 1 3652.57 3600.70 44.63 o 2 10 1 93.58 115.31 12.37 o 3 10 1 1759.10 1457.89 41.85 o 4 10 1 102.44 82.18 18.98 o 5 10 1 352.89 361.85 29.51 o 6 10 1 819.96 852.24 45.43 o 7 10 1 69.07 28.91 25.55 o 8 10 1 148.91 171.15 29.61 o 9 10 1 39.22 56.20 36.22 o -10 11 1 70.85 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