#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:18:59 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/79/2017922.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017922_Fobs loop_ _publ_author_name 'Tutughamiarso, Maya' 'Bolte, Michael' 'Wagner, Guido' 'Egert, Ernst' _publ_section_title ; Five pseudopolymorphs and a cocrystal of nitrofurantoin ; _journal_coeditor_code EG3064 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o18 _journal_page_last o25 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.347 _cell_angle_gamma 90.000 _cell_length_a 6.6257 _cell_length_b 26.4880 _cell_length_c 8.0032 _exptl_crystal_F_000 656.00 _reflns_d_resolution_high 0.8401 _cod_data_source_file eg3064Iasup2.hkl _cod_data_source_block Ia #BEGIN Tags that were not found in dictionaries: _shelx_title ' mt48-12 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 213.49 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6724.01 7486.47 133.03 o 3 0 0 398.44 386.13 55.53 o 4 0 0 2363.11 2064.72 439.80 o 5 0 0 131.12 180.13 41.82 o 6 0 0 915.05 666.01 119.12 o 7 0 0 376.50 267.91 53.28 o 2 1 0 12.13 13.19 41.61 o 3 1 0 42.27 48.60 32.67 o 4 1 0 81.42 94.62 31.08 o 5 1 0 58.35 44.25 24.85 o 6 1 0 289.33 313.28 25.45 o 7 1 0 164.76 201.05 25.41 o 1 2 0 11616.15 9198.32 602.14 o 2 2 0 578.09 553.52 44.12 o 3 2 0 1315.55 1364.87 55.27 o 4 2 0 1370.99 1585.94 52.78 o 5 2 0 4161.39 4357.14 195.96 o 6 2 0 338.11 367.23 24.99 o 7 2 0 80.54 56.57 25.46 o 1 3 0 5826.47 5140.75 316.62 o 2 3 0 1652.22 1579.63 98.57 o 3 3 0 2349.08 2499.14 167.79 o 4 3 0 120.91 107.05 27.37 o 5 3 0 442.25 442.82 28.07 o 6 3 0 861.40 869.99 66.28 o 7 3 0 49.75 55.15 23.99 o 1 4 0 15039.43 13388.58 559.39 o 2 4 0 114.20 113.30 38.14 o 3 4 0 4.68 12.04 29.99 o 4 4 0 523.45 538.68 28.31 o 5 4 0 453.24 470.37 42.87 o 6 4 0 9.02 28.86 26.82 o 7 4 0 36.93 42.03 23.70 o 1 5 0 2933.30 3045.79 93.12 o 2 5 0 76.77 80.23 37.22 o 3 5 0 1141.71 1253.18 37.61 o 4 5 0 143.87 120.89 26.53 o 5 5 0 384.03 350.00 26.90 o 6 5 0 667.47 646.82 55.06 o 7 5 0 33.91 27.70 23.79 o 0 6 0 5503.06 4987.44 251.73 o 1 6 0 948.29 953.15 50.51 o 2 6 0 3494.64 3750.05 108.02 o 3 6 0 230.19 258.73 28.41 o 4 6 0 343.67 411.15 28.36 o 5 6 0 4.47 -1.89 22.89 o 6 6 0 1.39 21.77 26.70 o 7 6 0 12.41 57.41 25.78 o 1 7 0 102.73 106.42 42.18 o 2 7 0 64.73 30.21 33.71 o 3 7 0 1147.10 1209.77 47.80 o 4 7 0 7.58 -1.67 26.82 o 5 7 0 55.38 62.14 26.63 o 6 7 0 15.86 6.39 24.10 o 7 7 0 56.44 31.05 25.83 o 0 8 0 34.16 55.55 65.62 o 1 8 0 4272.64 4005.32 189.60 o 2 8 0 6740.66 6583.93 286.75 o 3 8 0 7.72 9.23 27.07 o 4 8 0 87.34 98.83 29.85 o 5 8 0 380.06 419.74 36.02 o 6 8 0 160.89 128.80 24.72 o 7 8 0 361.27 356.90 26.93 o 1 9 0 48.91 40.26 37.76 o 2 9 0 24.78 40.97 30.51 o 3 9 0 0.38 -0.25 26.03 o 4 9 0 11.52 28.16 25.85 o 5 9 0 482.09 520.66 28.50 o 6 9 0 29.63 60.22 24.71 o 7 9 0 22.36 -7.48 23.70 o 0 10 0 247.11 206.36 55.91 o 1 10 0 3585.47 3221.81 136.50 o 2 10 0 55.73 73.47 29.74 o 3 10 0 6617.14 7338.89 255.44 o 4 10 0 282.26 299.67 30.36 o 5 10 0 186.82 201.53 25.41 o 6 10 0 843.95 741.57 64.98 o 7 10 0 45.84 87.59 24.42 o 1 11 0 2057.65 1976.00 54.66 o 2 11 0 73.44 66.66 28.44 o 3 11 0 776.34 849.96 43.54 o 4 11 0 25.65 27.72 25.98 o 5 11 0 41.30 35.45 26.10 o 6 11 0 61.90 76.00 23.80 o 7 11 0 10.95 14.85 24.31 o 0 12 0 853.78 709.75 94.49 o 1 12 0 578.88 570.17 33.91 o 2 12 0 2702.99 2906.48 92.33 o 3 12 0 401.25 344.02 28.72 o 4 12 0 1266.41 1345.59 48.08 o 5 12 0 133.65 106.58 26.12 o 6 12 0 453.84 471.30 26.96 o 7 12 0 41.17 56.98 24.28 o 1 13 0 69.38 68.40 31.74 o 2 13 0 386.54 400.74 32.52 o 3 13 0 1104.32 1223.37 42.59 o 4 13 0 302.77 320.65 26.28 o 5 13 0 0.25 10.40 25.62 o 6 13 0 326.97 323.89 27.21 o 7 13 0 3.92 21.10 25.95 o 0 14 0 39.81 43.66 43.87 o 1 14 0 682.23 670.34 32.43 o 2 14 0 1035.17 1045.60 74.41 o 3 14 0 25.74 31.23 25.68 o 4 14 0 91.64 106.27 25.29 o 5 14 0 114.28 135.93 22.64 o 6 14 0 76.93 80.75 22.42 o 1 15 0 69.32 89.18 27.73 o 2 15 0 129.20 124.17 31.95 o 3 15 0 198.67 210.89 27.92 o 4 15 0 16.44 40.33 25.19 o 5 15 0 198.97 226.81 25.61 o 6 15 0 0.15 12.54 23.52 o 0 16 0 69.72 87.35 46.48 o 1 16 0 102.78 93.97 30.87 o 2 16 0 108.71 91.72 30.04 o 3 16 0 716.69 713.61 32.33 o 4 16 0 72.29 89.91 27.01 o 5 16 0 486.98 472.70 26.28 o 6 16 0 7.02 20.01 23.49 o 1 17 0 319.52 368.26 28.62 o 2 17 0 27.00 46.27 27.68 o 3 17 0 25.92 30.92 27.00 o 4 17 0 34.61 59.36 25.40 o 5 17 0 170.49 168.58 25.13 o 6 17 0 24.01 44.22 25.61 o 0 18 0 5.26 -14.74 43.30 o 1 18 0 29.10 41.85 27.35 o 2 18 0 730.80 830.60 32.63 o 3 18 0 43.45 36.77 27.36 o 4 18 0 62.02 38.66 26.18 o 5 18 0 144.63 112.19 25.07 o 6 18 0 22.82 20.43 26.16 o 1 19 0 166.87 179.42 28.00 o 2 19 0 4.12 -2.68 27.56 o 3 19 0 4.27 9.95 27.02 o 4 19 0 28.63 39.27 26.07 o 5 19 0 72.06 82.49 24.14 o 6 19 0 35.79 11.51 28.29 o 0 20 0 1003.23 1058.11 48.03 o 1 20 0 100.00 126.64 28.44 o 2 20 0 0.09 13.28 27.94 o 3 20 0 13.44 39.98 30.23 o 4 20 0 515.80 556.67 28.84 o 5 20 0 874.12 862.09 53.91 o 1 21 0 90.06 109.33 27.20 o 2 21 0 3.50 18.91 24.71 o 3 21 0 45.50 79.38 27.69 o 4 21 0 291.28 313.69 27.57 o 5 21 0 35.61 25.41 26.63 o 0 22 0 1043.11 854.36 66.43 o 1 22 0 175.38 173.06 28.58 o 2 22 0 10.29 31.73 23.85 o 3 22 0 35.69 15.86 27.80 o 4 22 0 221.86 233.89 29.34 o 5 22 0 60.01 67.43 25.98 o 1 23 0 180.32 160.38 28.65 o 2 23 0 10.01 36.25 24.73 o 3 23 0 110.44 138.01 26.42 o 4 23 0 8.08 32.75 27.41 o 5 23 0 30.39 75.26 25.98 o 0 24 0 494.67 510.34 43.06 o 1 24 0 74.12 69.81 23.62 o 2 24 0 33.94 53.13 24.76 o 3 24 0 34.41 76.88 26.64 o 4 24 0 117.72 132.33 25.48 o 5 24 0 23.57 12.11 26.52 o 1 25 0 27.61 19.91 25.22 o 2 25 0 0.64 15.28 26.82 o 3 25 0 90.49 91.27 26.25 o 4 25 0 34.29 34.49 28.21 o 0 26 0 381.23 389.74 41.42 o 1 26 0 12.60 31.22 23.12 o 2 26 0 395.16 369.22 27.72 o 3 26 0 142.17 196.02 28.05 o 4 26 0 291.33 330.95 29.43 o 1 27 0 23.44 19.00 23.60 o 2 27 0 21.04 45.42 28.23 o 3 27 0 25.85 29.19 26.72 o 4 27 0 46.23 41.23 26.33 o 0 28 0 87.89 97.83 32.61 o 1 28 0 1278.10 1163.55 45.51 o 2 28 0 301.90 277.78 27.69 o 3 28 0 62.47 114.61 29.90 o 1 29 0 10.60 14.73 25.31 o 2 29 0 22.47 32.30 27.21 o 3 29 0 0.64 16.60 29.08 o 0 30 0 416.27 339.67 45.19 o 1 30 0 169.80 143.27 28.48 o 2 30 0 38.48 68.27 30.79 o 1 31 0 158.10 126.37 27.11 o -7 1 1 1.74 12.28 23.41 o -6 1 1 33.08 53.82 25.75 o -5 1 1 484.40 541.06 29.53 o -4 1 1 1944.93 2321.30 81.47 o -3 1 1 983.07 1044.54 74.91 o -2 1 1 350.06 230.54 42.03 o -1 1 1 1095.85 950.88 67.24 o 1 1 1 1673.20 1559.93 63.73 o 2 1 1 75.29 94.46 42.29 o 3 1 1 456.29 526.06 32.69 o 4 1 1 3.44 -16.73 28.08 o 5 1 1 2.93 27.83 23.64 o 6 1 1 1.11 10.42 24.60 o 7 1 1 17.00 51.14 23.04 o -7 2 1 58.45 73.71 23.25 o -6 2 1 467.86 501.40 37.03 o -5 2 1 93.01 124.45 27.91 o -4 2 1 0.77 31.65 27.44 o -3 2 1 3907.28 3890.99 148.34 o -2 2 1 755.48 695.69 47.16 o -1 2 1 876.42 783.28 60.33 o 1 2 1 1325.52 1238.30 76.04 o 2 2 1 2803.98 2835.78 116.74 o 3 2 1 457.57 470.30 33.16 o 4 2 1 2434.90 2475.95 187.89 o 5 2 1 651.24 643.41 35.81 o 6 2 1 70.90 79.14 23.51 o 7 2 1 270.93 238.48 25.65 o -7 3 1 10.76 49.80 24.20 o -6 3 1 16.79 -7.11 26.35 o -5 3 1 234.78 253.78 28.14 o -4 3 1 220.84 233.69 27.84 o -3 3 1 455.39 388.68 32.56 o -2 3 1 1219.16 1130.97 78.64 o -1 3 1 121.99 97.76 47.41 o 0 3 1 2.37 78.18 51.05 o 1 3 1 4187.31 4153.32 80.29 o 2 3 1 1580.11 1570.57 125.47 o 3 3 1 893.69 870.85 90.94 o 4 3 1 47.01 82.63 31.53 o 5 3 1 319.46 336.01 28.17 o 6 3 1 76.36 98.34 23.67 o 7 3 1 100.77 128.72 25.51 o -7 4 1 43.65 34.87 25.46 o -6 4 1 189.57 207.72 26.92 o -5 4 1 418.09 419.45 29.26 o -4 4 1 1954.29 1907.87 118.78 o -3 4 1 292.60 293.82 31.73 o -2 4 1 5667.12 5816.94 131.66 o -1 4 1 582.39 590.92 47.76 o 0 4 1 5797.64 5257.40 411.63 o 1 4 1 2291.80 2059.72 76.19 o 2 4 1 4265.76 4672.35 113.38 o 3 4 1 911.35 1028.01 35.28 o 4 4 1 1474.51 1454.13 82.20 o 5 4 1 38.77 51.36 27.55 o 6 4 1 931.70 947.72 96.04 o 7 4 1 58.99 39.74 23.89 o -7 5 1 240.31 207.93 28.43 o -6 5 1 65.40 65.97 24.97 o -5 5 1 43.86 53.11 25.11 o -4 5 1 19.56 30.94 27.29 o -3 5 1 385.32 400.83 31.54 o -2 5 1 914.43 799.58 40.44 o -1 5 1 713.08 643.38 53.95 o 0 5 1 3.49 -3.11 53.62 o 1 5 1 377.24 364.81 45.21 o 2 5 1 49.29 41.63 31.78 o 3 5 1 144.71 148.83 27.61 o 4 5 1 107.48 125.32 27.22 o 5 5 1 74.32 117.38 28.77 o 6 5 1 640.77 597.97 72.23 o 7 5 1 9.77 20.20 23.49 o -7 6 1 588.51 565.55 54.86 o -6 6 1 24.07 38.45 26.47 o -5 6 1 912.35 767.31 69.44 o -4 6 1 1611.99 1788.75 52.42 o -3 6 1 1996.01 2130.36 45.76 o -2 6 1 668.99 539.17 45.47 o -1 6 1 8947.82 7456.65 529.89 o 0 6 1 2505.60 2421.73 119.00 o 1 6 1 533.45 466.19 43.71 o 2 6 1 3789.61 3912.31 56.09 o 3 6 1 5946.81 6638.12 167.65 o 4 6 1 71.47 53.27 25.47 o 5 6 1 776.20 705.16 87.94 o 6 6 1 195.53 172.46 25.72 o 7 6 1 234.02 234.03 27.70 o -7 7 1 54.35 52.88 23.46 o -6 7 1 105.16 113.66 24.18 o -5 7 1 81.12 73.60 25.25 o -4 7 1 1550.14 1546.58 89.76 o -3 7 1 225.41 227.16 30.84 o -2 7 1 182.55 119.87 32.86 o -1 7 1 847.27 734.97 49.41 o 0 7 1 45.77 42.90 50.86 o 1 7 1 2.57 1.87 37.99 o 2 7 1 249.11 212.10 30.89 o 3 7 1 318.75 366.50 28.74 o 4 7 1 1210.17 1377.94 33.61 o 5 7 1 9.96 19.83 23.63 o 6 7 1 134.61 175.69 27.89 o 7 7 1 0.08 -15.77 24.73 o -7 8 1 0.63 -0.45 24.07 o -6 8 1 1410.14 1265.58 110.30 o -5 8 1 0.76 -6.41 24.44 o -4 8 1 219.11 218.96 27.29 o -3 8 1 1909.45 2029.19 61.47 o -2 8 1 2188.61 2044.43 72.17 o -1 8 1 43.28 23.22 40.70 o 0 8 1 199.49 142.63 46.99 o 1 8 1 950.38 755.31 43.73 o 2 8 1 970.14 961.63 34.18 o 3 8 1 1233.71 1241.28 32.63 o 4 8 1 364.91 356.97 32.43 o 5 8 1 1537.91 1457.82 109.02 o 6 8 1 176.93 157.73 23.81 o 7 8 1 6.07 16.52 25.92 o -7 9 1 10.79 7.54 24.66 o -6 9 1 759.46 812.23 41.77 o -5 9 1 2.78 22.18 26.13 o -4 9 1 334.06 329.45 30.71 o -3 9 1 20.17 23.05 28.31 o -2 9 1 1616.06 1694.47 62.27 o -1 9 1 520.00 511.48 40.29 o 0 9 1 439.00 407.00 42.54 o 1 9 1 4546.45 4240.26 347.82 o 2 9 1 2.84 14.75 27.78 o 3 9 1 31.60 19.53 26.35 o 4 9 1 77.16 111.41 26.63 o 5 9 1 159.86 143.23 26.51 o 6 9 1 4.38 -13.20 24.81 o 7 9 1 3.32 18.55 25.79 o -7 10 1 15.25 31.42 24.28 o -6 10 1 255.28 233.13 25.44 o -5 10 1 316.41 322.07 27.60 o -4 10 1 26.37 27.05 26.28 o -3 10 1 546.81 549.41 32.64 o -2 10 1 687.38 671.76 36.50 o -1 10 1 698.41 675.02 37.06 o 0 10 1 0.16 -15.56 34.71 o 1 10 1 4673.80 4736.70 263.76 o 2 10 1 208.06 223.30 29.94 o 3 10 1 555.92 584.47 28.22 o 4 10 1 244.98 233.10 26.76 o 5 10 1 129.22 147.03 26.21 o 6 10 1 19.84 46.01 23.18 o 7 10 1 301.66 287.13 29.95 o -7 11 1 53.89 62.77 26.06 o -6 11 1 0.82 18.93 23.25 o -5 11 1 57.36 65.86 24.36 o -4 11 1 475.76 473.45 28.58 o -3 11 1 184.14 169.80 28.83 o -2 11 1 609.37 578.11 33.82 o -1 11 1 473.00 481.30 35.89 o 0 11 1 807.82 763.12 48.94 o 1 11 1 305.90 302.93 34.08 o 2 11 1 513.60 547.29 31.87 o 3 11 1 396.20 401.48 27.51 o 4 11 1 1.61 9.11 26.52 o 5 11 1 308.49 310.41 25.40 o 6 11 1 150.39 159.87 24.67 o 7 11 1 17.15 6.92 26.44 o -7 12 1 4.22 5.07 24.59 o -6 12 1 121.56 91.29 24.14 o -5 12 1 0.10 32.31 24.23 o -4 12 1 67.27 79.64 27.09 o -3 12 1 11.34 19.55 26.96 o -2 12 1 16.55 35.99 30.32 o -1 12 1 1994.24 2215.45 45.65 o 0 12 1 106.10 115.85 39.43 o 1 12 1 526.73 525.66 33.26 o 2 12 1 598.87 625.26 30.77 o 3 12 1 119.70 89.34 27.57 o 4 12 1 185.07 153.08 25.45 o 5 12 1 11.04 40.05 23.85 o 6 12 1 108.34 79.64 23.80 o -7 13 1 0.82 19.28 24.26 o -6 13 1 8.62 18.12 23.82 o -5 13 1 637.32 575.34 36.88 o -4 13 1 0.08 17.03 24.87 o -3 13 1 959.17 1091.91 34.53 o -2 13 1 640.86 724.69 44.00 o -1 13 1 1829.62 1851.87 45.82 o 0 13 1 16.29 30.25 33.11 o 1 13 1 42.04 44.27 29.12 o 2 13 1 292.03 279.41 29.35 o 3 13 1 37.99 52.97 25.44 o 4 13 1 56.49 49.69 24.62 o 5 13 1 16.30 32.97 22.35 o 6 13 1 271.14 280.66 24.55 o -7 14 1 3.04 17.71 24.12 o -6 14 1 72.44 50.73 23.47 o -5 14 1 644.90 697.43 41.17 o -4 14 1 65.07 98.70 27.11 o -3 14 1 9.63 19.71 28.56 o -2 14 1 887.64 885.94 48.15 o -1 14 1 1566.65 1698.85 112.08 o 0 14 1 608.32 615.98 37.72 o 1 14 1 1326.73 1373.56 111.63 o 2 14 1 44.00 81.74 28.99 o 3 14 1 65.49 85.56 25.59 o 4 14 1 492.37 466.42 26.73 o 5 14 1 91.83 89.49 23.65 o 6 14 1 95.47 92.53 23.92 o -6 15 1 10.38 33.21 24.26 o -5 15 1 65.24 74.47 23.75 o -4 15 1 150.79 156.21 28.00 o -3 15 1 1.19 7.76 30.52 o -2 15 1 928.30 937.91 43.18 o -1 15 1 75.65 73.29 30.47 o 0 15 1 483.65 440.63 35.29 o 1 15 1 409.00 382.84 34.45 o 2 15 1 639.03 702.56 32.68 o 3 15 1 74.05 90.63 25.73 o 4 15 1 237.56 201.01 24.98 o 5 15 1 265.81 274.42 25.06 o 6 15 1 2.95 15.61 23.21 o -6 16 1 211.78 196.36 25.07 o -5 16 1 35.48 18.15 23.77 o -4 16 1 534.73 580.28 42.06 o -3 16 1 0.65 25.89 27.95 o -2 16 1 0.60 -11.64 31.38 o -1 16 1 1327.35 1343.66 109.18 o 0 16 1 4.01 -20.49 31.17 o 1 16 1 713.45 775.35 34.11 o 2 16 1 31.62 40.65 26.79 o 3 16 1 570.14 573.29 27.24 o 4 16 1 6.39 31.73 24.74 o 5 16 1 1042.21 1074.63 46.16 o 6 16 1 103.68 123.91 26.68 o -6 17 1 152.14 142.17 25.48 o -5 17 1 40.64 58.36 24.38 o -4 17 1 100.73 94.36 27.15 o -3 17 1 91.72 108.55 29.68 o -2 17 1 87.41 88.74 31.37 o -1 17 1 1188.84 1106.12 68.26 o 0 17 1 125.83 116.39 32.46 o 1 17 1 483.33 510.20 33.21 o 2 17 1 130.75 142.66 29.07 o 3 17 1 40.95 95.80 27.44 o 4 17 1 1.14 -22.94 22.94 o 5 17 1 24.52 40.43 23.61 o 6 17 1 39.68 49.40 26.43 o -6 18 1 56.13 45.32 23.99 o -5 18 1 5.47 34.63 23.27 o -4 18 1 21.37 42.72 25.81 o -3 18 1 463.99 465.42 30.83 o -2 18 1 16.54 21.18 28.95 o -1 18 1 2081.87 2062.89 57.22 o 0 18 1 1645.79 1490.65 70.38 o 1 18 1 37.92 57.60 33.07 o 2 18 1 1307.34 1357.48 64.13 o 3 18 1 37.66 32.54 26.45 o 4 18 1 7.60 47.05 24.46 o 5 18 1 37.84 56.48 24.30 o 6 18 1 225.43 189.80 26.23 o -6 19 1 44.26 42.42 24.31 o -5 19 1 5.67 22.45 25.94 o -4 19 1 662.40 657.35 34.71 o -3 19 1 150.07 122.89 26.52 o -2 19 1 386.60 386.92 37.04 o -1 19 1 167.09 157.17 28.64 o 0 19 1 642.37 701.29 50.87 o 1 19 1 603.25 563.24 43.59 o 2 19 1 310.07 313.13 28.43 o 3 19 1 24.23 36.48 26.20 o 4 19 1 244.15 245.29 25.28 o 5 19 1 9.65 9.88 23.23 o -6 20 1 57.25 71.79 28.66 o -5 20 1 1013.63 911.56 56.85 o -4 20 1 189.36 232.49 27.75 o -3 20 1 4.58 36.36 29.40 o -2 20 1 75.26 89.76 25.69 o -1 20 1 1.17 2.93 25.53 o 0 20 1 33.46 10.40 28.51 o 1 20 1 738.99 708.54 36.92 o 2 20 1 361.94 374.67 30.42 o 3 20 1 271.03 302.03 30.14 o 4 20 1 979.82 1057.87 48.54 o 5 20 1 132.25 113.40 24.16 o -5 21 1 617.73 612.51 28.70 o -4 21 1 241.67 246.53 26.49 o -3 21 1 1170.76 1188.06 34.93 o -2 21 1 228.48 240.72 27.05 o -1 21 1 188.17 164.36 27.20 o 0 21 1 0.80 14.83 30.60 o 1 21 1 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