#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/79/2017925.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2017925_Fobs loop_ _publ_author_name 'Tutughamiarso, Maya' 'Bolte, Michael' 'Wagner, Guido' 'Egert, Ernst' _publ_section_title ; Five pseudopolymorphs and a cocrystal of nitrofurantoin ; _journal_coeditor_code EG3064 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o18 _journal_page_last o25 _journal_volume 67 _journal_year 2011 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 111.681 _cell_angle_gamma 90.000 _cell_length_a 16.2038 _cell_length_b 7.4215 _cell_length_c 13.1195 _exptl_crystal_F_000 680.00 _reflns_d_resolution_high 0.8216 _[local]_cod_data_source_file eg3064Idsup5.hkl _[local]_cod_data_source_block Id #BEGIN Tags that were not found in dictionaries: _shelx_title ' mt48-5trans in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 215.39 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 3043.36 2441.75 124.02 o 4 0 0 364.05 307.98 31.05 o 5 0 0 79.37 70.41 30.68 o 6 0 0 258.62 211.64 38.70 o 7 0 0 5094.06 4262.29 280.38 o 8 0 0 170.94 141.29 23.98 o 9 0 0 5064.70 5276.05 295.93 o 10 0 0 310.13 364.71 25.43 o 11 0 0 1139.14 1212.32 31.51 o 12 0 0 53.48 55.39 20.86 o 13 0 0 1667.39 1751.04 32.15 o 14 0 0 43.17 61.43 21.97 o 15 0 0 3.27 14.91 24.75 o 16 0 0 386.44 369.21 27.38 o 17 0 0 18.63 15.08 25.05 o 18 0 0 39.71 45.30 25.59 o 2 1 0 2221.27 1783.04 143.52 o 3 1 0 2367.69 1743.21 209.95 o 4 1 0 1430.84 1279.56 79.07 o 5 1 0 618.09 627.95 22.70 o 6 1 0 1113.87 1055.76 66.07 o 7 1 0 1034.01 978.55 45.33 o 8 1 0 9.97 17.66 15.39 o 9 1 0 2086.74 2098.13 101.83 o 10 1 0 44.25 37.75 16.56 o 11 1 0 486.13 530.68 19.19 o 12 1 0 18.27 18.81 15.46 o 13 1 0 73.18 84.79 15.66 o 14 1 0 65.82 66.84 16.43 o 15 1 0 32.15 25.59 14.73 o 16 1 0 149.95 115.01 17.15 o 17 1 0 1.79 11.04 18.13 o 18 1 0 0.00 17.42 17.99 o 0 2 0 3.70 12.02 31.70 o 1 2 0 791.91 779.17 54.68 o 2 2 0 46393.27 39858.05 2246.55 o 3 2 0 1451.92 1361.85 68.97 o 4 2 0 180.06 185.84 20.31 o 5 2 0 994.34 1060.90 23.67 o 6 2 0 330.02 360.49 18.58 o 7 2 0 2463.95 2775.12 88.23 o 8 2 0 128.29 90.69 16.70 o 9 2 0 23.38 19.70 15.75 o 10 2 0 0.39 19.81 15.75 o 11 2 0 7.75 26.43 15.54 o 12 2 0 36.44 33.79 16.69 o 13 2 0 137.38 131.12 15.80 o 14 2 0 97.86 69.41 15.57 o 15 2 0 331.02 312.06 31.87 o 16 2 0 57.11 59.34 17.30 o 17 2 0 0.54 23.22 15.92 o 1 3 0 78.06 72.66 19.74 o 2 3 0 460.86 434.45 23.34 o 3 3 0 477.12 483.13 21.81 o 4 3 0 747.44 748.49 22.57 o 5 3 0 10.91 25.50 18.35 o 6 3 0 22.14 24.84 16.22 o 7 3 0 1095.88 1004.38 37.17 o 8 3 0 21.20 40.28 17.78 o 9 3 0 21.36 23.75 17.11 o 10 3 0 100.17 79.83 18.18 o 11 3 0 424.06 470.15 18.19 o 12 3 0 18.49 37.24 15.78 o 13 3 0 192.12 152.94 18.01 o 14 3 0 0.05 0.77 15.13 o 15 3 0 10.41 11.51 15.23 o 16 3 0 4.58 23.65 16.64 o 17 3 0 34.42 35.66 16.42 o 0 4 0 30.00 17.36 27.35 o 1 4 0 1077.44 1051.15 27.01 o 2 4 0 26.37 28.17 17.19 o 3 4 0 111.60 100.59 17.75 o 4 4 0 2933.26 3020.08 47.90 o 5 4 0 0.23 12.83 16.31 o 6 4 0 443.65 406.46 23.96 o 7 4 0 90.83 75.03 17.00 o 8 4 0 22.72 26.89 19.43 o 9 4 0 0.79 15.05 16.80 o 10 4 0 87.39 91.65 16.02 o 11 4 0 128.56 118.11 18.01 o 12 4 0 498.76 514.28 18.39 o 13 4 0 62.59 81.82 15.42 o 14 4 0 0.97 10.18 16.36 o 15 4 0 90.39 83.38 18.14 o 16 4 0 60.73 67.87 16.44 o 1 5 0 694.64 788.95 22.71 o 2 5 0 35.28 25.37 15.93 o 3 5 0 443.40 469.38 20.19 o 4 5 0 405.46 443.08 26.85 o 5 5 0 122.06 157.89 17.28 o 6 5 0 2.56 -2.22 17.31 o 7 5 0 21.69 41.51 15.98 o 8 5 0 124.88 133.98 17.46 o 9 5 0 135.79 112.48 17.16 o 10 5 0 6.87 20.64 16.54 o 11 5 0 10.95 10.81 16.18 o 12 5 0 6.41 5.81 15.94 o 13 5 0 1.63 7.42 19.07 o 14 5 0 11.89 22.25 18.35 o 15 5 0 53.20 35.88 18.89 o 0 6 0 3.74 -3.54 34.32 o 1 6 0 3.06 31.71 17.75 o 2 6 0 334.54 292.35 21.12 o 3 6 0 219.21 195.87 18.72 o 4 6 0 243.72 257.90 17.40 o 5 6 0 382.60 395.18 18.71 o 6 6 0 282.96 281.65 17.60 o 7 6 0 153.46 144.67 18.15 o 8 6 0 66.74 68.99 17.04 o 9 6 0 43.44 48.13 17.03 o 10 6 0 232.27 248.84 18.64 o 11 6 0 21.45 40.77 17.89 o 12 6 0 38.70 54.17 18.56 o 13 6 0 0.85 12.41 18.71 o 1 7 0 7.33 8.34 17.64 o 2 7 0 2.22 -1.21 19.92 o 3 7 0 231.16 231.88 19.39 o 4 7 0 4.61 38.87 16.78 o 5 7 0 50.64 50.44 16.50 o 6 7 0 9.39 19.33 17.90 o 7 7 0 0.87 7.98 15.02 o 8 7 0 15.13 30.78 15.55 o 9 7 0 5.94 18.19 16.21 o 10 7 0 1.46 17.11 17.41 o 11 7 0 14.49 22.21 21.67 o 0 8 0 147.04 113.32 26.77 o 1 8 0 15.55 11.79 18.44 o 2 8 0 25.20 44.05 18.50 o 3 8 0 51.57 62.97 17.86 o 4 8 0 145.45 102.82 18.65 o 5 8 0 173.83 141.34 18.83 o 6 8 0 51.49 46.56 16.35 o 7 8 0 2.67 8.01 16.75 o 8 8 0 204.95 183.16 17.94 o -18 1 1 46.49 39.26 17.33 o -17 1 1 43.12 62.06 16.96 o -16 1 1 70.14 46.84 15.57 o -15 1 1 23.23 13.90 15.56 o -14 1 1 9.92 16.97 19.42 o -13 1 1 6.13 -12.31 15.78 o -12 1 1 12.29 26.41 15.59 o -11 1 1 144.93 149.18 17.38 o -10 1 1 214.84 220.24 17.42 o -9 1 1 0.15 7.75 16.12 o -8 1 1 18.29 17.98 16.97 o -7 1 1 25.63 36.56 19.77 o -6 1 1 1421.75 1327.75 28.58 o -5 1 1 550.49 492.08 25.06 o -4 1 1 1936.23 1650.96 106.54 o -3 1 1 265.02 242.94 23.81 o -2 1 1 243.20 211.55 24.82 o -1 1 1 352.57 314.44 69.14 o 1 1 1 423.84 381.16 26.22 o 2 1 1 2828.84 2354.67 174.69 o 3 1 1 348.11 327.57 32.65 o 4 1 1 105.67 67.40 19.13 o 5 1 1 789.98 768.22 22.98 o 6 1 1 59.54 83.93 16.64 o 7 1 1 178.22 171.65 16.73 o 8 1 1 64.64 78.63 16.18 o 9 1 1 47.04 44.46 15.97 o 10 1 1 9.70 5.59 14.96 o 11 1 1 5.96 16.59 15.15 o 12 1 1 2.73 26.66 15.53 o 13 1 1 27.46 37.62 16.83 o 14 1 1 485.42 511.52 19.84 o 15 1 1 134.14 125.28 19.07 o 16 1 1 285.46 268.80 19.40 o 17 1 1 9.34 29.95 17.95 o -18 2 1 91.94 86.90 19.15 o -17 2 1 24.85 50.23 18.28 o -16 2 1 16.62 37.22 18.22 o -15 2 1 71.17 65.16 15.47 o -14 2 1 580.88 560.49 19.05 o -13 2 1 162.64 145.30 15.39 o -12 2 1 10.75 24.88 19.31 o -11 2 1 524.36 514.46 22.33 o -10 2 1 375.59 403.79 18.96 o -9 2 1 828.41 910.92 26.57 o -8 2 1 650.36 699.39 26.53 o -7 2 1 2425.66 2623.70 159.51 o -6 2 1 73.05 104.80 20.03 o -5 2 1 1313.95 1231.16 61.88 o -4 2 1 34.74 18.77 20.94 o -3 2 1 4703.44 4168.52 314.73 o -2 2 1 34610.76 32411.25 417.07 o -1 2 1 12967.13 12563.84 115.76 o 0 2 1 81.28 85.67 22.28 o 1 2 1 25.71 40.40 22.10 o 2 2 1 9815.77 8762.22 526.38 o 3 2 1 1888.68 1842.38 91.87 o 4 2 1 25.86 37.53 19.61 o 5 2 1 603.34 590.85 20.34 o 6 2 1 358.12 285.41 29.08 o 7 2 1 268.55 273.43 16.57 o 8 2 1 82.25 91.26 16.04 o 9 2 1 101.98 111.80 15.20 o 10 2 1 14.59 17.87 15.42 o 11 2 1 2206.05 2124.19 135.00 o 12 2 1 0.39 23.50 17.84 o 13 2 1 79.52 71.64 16.32 o 14 2 1 310.69 284.84 24.97 o 15 2 1 188.04 191.20 17.08 o 16 2 1 6.64 27.23 18.73 o 17 2 1 0.27 9.51 17.63 o -17 3 1 11.58 21.20 18.28 o -16 3 1 99.97 117.73 17.07 o -15 3 1 85.25 97.30 19.19 o -14 3 1 4.47 33.66 15.77 o -13 3 1 51.54 29.56 15.17 o -12 3 1 148.28 142.84 16.31 o -11 3 1 28.37 34.19 16.29 o -10 3 1 14.78 10.20 15.48 o -9 3 1 193.37 156.07 17.16 o -8 3 1 290.63 317.04 18.45 o -7 3 1 113.20 103.42 16.82 o -6 3 1 252.04 264.09 19.95 o -5 3 1 2301.43 2207.11 151.18 o -4 3 1 196.03 186.55 21.39 o -3 3 1 436.93 393.01 21.99 o -2 3 1 1416.64 1379.55 38.52 o -1 3 1 85.22 96.15 19.21 o 0 3 1 929.04 1027.78 24.96 o 1 3 1 56.96 61.25 21.46 o 2 3 1 3299.79 3279.56 96.19 o 3 3 1 164.46 169.88 18.00 o 4 3 1 667.51 620.63 54.94 o 5 3 1 0.30 21.71 17.22 o 6 3 1 1.59 9.96 15.71 o 7 3 1 155.03 186.30 16.31 o 8 3 1 0.78 12.32 15.21 o 9 3 1 113.31 134.89 18.03 o 10 3 1 48.50 52.00 16.08 o 11 3 1 83.61 75.10 17.21 o 12 3 1 556.82 537.33 28.01 o 13 3 1 58.27 55.90 15.00 o 14 3 1 0.09 8.24 14.85 o 15 3 1 16.85 19.54 16.28 o 16 3 1 12.49 12.66 16.05 o -16 4 1 10.01 4.70 17.97 o -15 4 1 5.86 7.52 17.09 o -14 4 1 19.04 32.36 17.38 o -13 4 1 57.10 73.53 15.70 o -12 4 1 57.76 42.24 15.61 o -11 4 1 31.34 20.03 15.81 o -10 4 1 7.12 15.51 17.15 o -9 4 1 40.32 33.98 17.36 o -8 4 1 191.77 185.56 17.32 o -7 4 1 547.37 518.95 35.32 o -6 4 1 120.21 121.34 17.90 o -5 4 1 5293.39 5832.40 69.22 o -4 4 1 7575.87 7299.28 358.67 o -3 4 1 387.41 360.17 21.26 o -2 4 1 0.05 5.03 17.91 o -1 4 1 65.06 99.33 18.80 o 0 4 1 90.50 86.78 20.09 o 1 4 1 5073.89 4862.24 360.21 o 2 4 1 239.20 250.71 19.39 o 3 4 1 125.19 133.37 16.40 o 4 4 1 2860.85 2884.08 205.99 o 5 4 1 1308.42 1457.62 49.51 o 6 4 1 193.43 188.83 16.80 o 7 4 1 0.06 10.28 17.70 o 8 4 1 6.92 14.82 17.20 o 9 4 1 1042.11 1014.98 44.12 o 10 4 1 2.17 0.56 15.08 o 11 4 1 2.55 9.01 15.79 o 12 4 1 213.25 228.32 17.58 o 13 4 1 54.11 57.92 16.38 o 14 4 1 0.23 13.24 15.81 o 15 4 1 15.84 12.06 17.63 o -15 5 1 8.90 9.85 18.07 o -14 5 1 32.89 36.39 18.30 o -13 5 1 210.88 207.33 19.10 o -12 5 1 0.24 0.33 17.87 o -11 5 1 99.69 95.41 17.90 o -10 5 1 299.42 281.41 25.60 o -9 5 1 46.62 31.74 16.54 o -8 5 1 238.96 241.41 17.56 o -7 5 1 60.34 51.43 16.81 o -6 5 1 42.85 47.54 17.04 o -5 5 1 66.61 88.65 15.99 o -4 5 1 180.66 167.19 16.88 o -3 5 1 398.56 393.16 24.94 o -2 5 1 125.57 142.12 18.09 o -1 5 1 5.00 19.63 17.04 o 0 5 1 128.74 139.34 18.42 o 1 5 1 78.21 66.74 17.12 o 2 5 1 116.85 109.43 16.94 o 3 5 1 47.31 78.38 16.27 o 4 5 1 872.41 890.87 47.77 o 5 5 1 234.55 240.83 17.91 o 6 5 1 5.19 5.95 18.00 o 7 5 1 10.61 28.80 17.80 o 8 5 1 1.93 1.97 15.80 o 9 5 1 7.68 24.47 17.18 o 10 5 1 47.07 51.36 16.81 o 11 5 1 209.02 185.78 17.32 o 12 5 1 16.60 10.98 17.15 o 13 5 1 36.56 36.31 17.80 o 14 5 1 33.53 27.57 17.89 o -14 6 1 51.25 54.96 31.28 o -13 6 1 51.11 51.79 19.65 o -12 6 1 21.39 39.66 18.16 o -11 6 1 34.14 40.06 17.80 o -10 6 1 57.97 50.94 17.41 o -9 6 1 6.00 13.65 16.43 o -8 6 1 88.09 81.65 15.62 o -7 6 1 704.16 709.80 25.01 o -6 6 1 1637.01 1722.09 50.49 o -5 6 1 112.54 122.39 16.74 o -4 6 1 69.27 77.05 16.25 o -3 6 1 565.68 582.29 22.26 o -2 6 1 1.72 22.13 18.83 o -1 6 1 34.79 58.88 18.87 o 0 6 1 29.24 41.84 18.48 o 1 6 1 1.16 16.67 16.77 o 2 6 1 73.77 83.96 16.81 o 3 6 1 1384.74 1351.53 42.44 o 4 6 1 0.16 24.19 16.22 o 5 6 1 33.99 50.57 16.86 o 6 6 1 70.18 73.33 16.60 o 7 6 1 85.56 93.42 17.91 o 8 6 1 31.84 26.33 16.70 o 9 6 1 39.16 39.68 16.56 o 10 6 1 237.71 215.94 19.11 o 11 6 1 0.00 25.26 18.15 o 12 6 1 20.70 10.05 19.29 o 13 6 1 6.57 14.30 19.80 o -11 7 1 10.26 6.73 19.15 o -10 7 1 14.80 21.01 16.98 o -9 7 1 135.70 139.55 18.85 o -8 7 1 39.40 48.37 16.28 o -7 7 1 145.77 135.86 16.14 o -6 7 1 291.42 276.40 16.65 o -5 7 1 5.82 13.32 16.58 o -4 7 1 11.94 27.69 16.65 o -3 7 1 60.68 62.06 17.33 o -2 7 1 22.33 25.69 17.37 o -1 7 1 121.00 128.39 20.98 o 0 7 1 52.86 49.75 17.92 o 1 7 1 33.32 44.38 19.04 o 2 7 1 16.88 19.46 17.42 o 3 7 1 0.00 13.56 15.85 o 4 7 1 22.18 33.19 15.69 o 5 7 1 0.35 4.31 14.60 o 6 7 1 291.63 274.22 23.48 o 7 7 1 124.44 105.33 16.60 o 8 7 1 0.37 9.47 15.44 o 9 7 1 12.05 19.19 17.26 o 10 7 1 63.94 53.20 20.55 o 11 7 1 7.57 -2.59 28.72 o -8 8 1 57.44 50.16 18.18 o -7 8 1 128.14 109.00 16.53 o -6 8 1 13.68 23.32 18.86 o -5 8 1 69.34 91.01 19.13 o -4 8 1 0.25 2.84 18.99 o -3 8 1 2.06 -5.43 18.23 o -2 8 1 5.09 11.72 18.67 o -1 8 1 18.16 27.46 17.82 o 0 8 1 43.39 48.10 19.72 o 1 8 1 14.22 21.04 18.84 o 2 8 1 0.34 -0.45 19.36 o 3 8 1 1.01 4.60 16.74 o 4 8 1 5.85 0.47 18.02 o 5 8 1 14.54 16.30 16.29 o 6 8 1 0.37 1.04 17.21 o 7 8 1 106.84 87.99 16.27 o -1 9 1 5.14 13.50 34.93 o 0 9 1 0.80 -29.69 72.77 o -19 0 2 1.52 5.95 29.65 o -18 0 2 179.89 178.64 26.22 o -17 0 2 15.90 17.97 24.24 o -16 0 2 501.28 489.09 26.89 o -15 0 2 32.92 27.78 22.95 o -14 0 2 252.83 277.38 25.79 o -13 0 2 0.75 23.01 22.18 o -12 0 2 218.85 212.37 24.49 o -11 0 2 35.51 16.23 25.45 o -10 0 2 38.59 73.29 23.15 o -9 0 2 5521.03 5893.80 198.72 o -8 0 2 8.30 15.60 27.08 o -7 0 2 0.06 8.90 30.89 o -6 0 2 123.18 131.32 28.50 o -5 0 2 1272.31 1199.23 78.11 o -4 0 2 1587.28 1556.43 138.52 o -3 0 2 25105.64 22764.17 602.79 o -2 0 2 5522.71 4968.00 126.44 o 0 0 2 16489.51 11993.46 250.18 o 1 0 2 5348.20 4581.58 296.40 o 2 0 2 2574.63 2528.40 78.34 o 3 0 2 341.37 328.46 31.23 o 4 0 2 9210.17 7539.59 985.02 o 5 0 2 453.61 405.75 26.81 o 6 0 2 96.32 167.61 22.00 o 7 0 2 38.95 37.19 21.73 o 8 0 2 133.41 143.62 20.72 o 9 0 2 1565.55 1826.14 76.01 o 10 0 2 0.66 -9.26 21.21 o 11 0 2 250.89 241.36 23.85 o 12 0 2 136.05 168.00 21.77 o 13 0 2 1726.06 1790.43 54.61 o 14 0 2 73.77 74.01 21.36 o 15 0 2 20.92 24.51 23.45 o 16 0 2 48.19 57.75 24.87 o 17 0 2 1.75 16.80 27.49 o -18 1 2 54.22 37.28 17.67 o -17 1 2 34.65 26.24 17.32 o -16 1 2 276.70 248.27 19.93 o -15 1 2 231.08 223.54 17.51 o -14 1 2 350.77 326.69 31.01 o -13 1 2 33.63 33.81 16.95 o -12 1 2 396.51 408.60 21.75 o -11 1 2 12.48 13.21 18.54 o -10 1 2 1406.05 1439.11 26.17 o -9 1 2 55.58 38.07 19.12 o -8 1 2 2128.77 2316.67 60.67 o -7 1 2 38.40 51.58 20.11 o -6 1 2 127.34 113.99 20.80 o -5 1 2 368.34 351.37 26.80 o -4 1 2 1001.56 851.63 65.92 o -3 1 2 582.14 548.32 30.35 o -2 1 2 1549.62 1448.23 45.33 o -1 1 2 498.38 417.94 31.13 o 0 1 2 4083.86 3777.73 186.83 o 1 1 2 787.58 773.85 65.62 o 2 1 2 149.21 85.85 22.41 o 3 1 2 2556.41 2274.24 147.16 o 4 1 2 659.82 608.95 21.34 o 5 1 2 13.79 28.26 14.72 o 6 1 2 256.62 228.46 16.02 o 7 1 2 1.23 5.36 15.41 o 8 1 2 177.31 186.69 15.79 o 9 1 2 3.21 20.75 14.71 o 10 1 2 284.65 286.27 21.14 o 11 1 2 313.77 290.91 17.44 o 12 1 2 34.76 38.42 16.00 o 13 1 2 888.22 938.24 21.94 o 14 1 2 0.32 23.96 16.25 o 15 1 2 1.04 21.25 16.52 o 16 1 2 6.48 11.47 17.41 o 17 1 2 1.93 10.06 19.15 o -18 2 2 22.33 26.78 18.24 o -17 2 2 17.91 33.20 18.90 o -16 2 2 7.24 11.77 15.79 o -15 2 2 17.64 45.07 16.25 o -14 2 2 47.58 38.75 15.73 o -13 2 2 27.11 43.82 16.44 o -12 2 2 223.90 242.41 21.31 o -11 2 2 685.77 640.97 50.45 o -10 2 2 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193.36 18.04 o -9 3 2 14.34 22.12 16.39 o -8 3 2 0.03 2.02 17.37 o -7 3 2 20.34 34.42 17.50 o -6 3 2 557.21 592.28 26.96 o -5 3 2 11.89 9.21 17.95 o -4 3 2 403.01 412.79 22.83 o -3 3 2 1055.21 1033.42 38.66 o -2 3 2 297.51 286.39 21.73 o -1 3 2 654.69 598.79 32.40 o 0 3 2 346.47 361.15 22.30 o 1 3 2 0.16 25.71 18.46 o 2 3 2 1429.78 1452.62 130.37 o 3 3 2 88.68 96.66 18.18 o 4 3 2 21.48 19.20 15.56 o 5 3 2 500.81 534.86 19.29 o 6 3 2 99.25 104.48 15.28 o 7 3 2 27.35 40.44 17.25 o 8 3 2 20.61 22.88 15.99 o 9 3 2 246.51 295.18 19.64 o 10 3 2 2.30 10.96 16.01 o 11 3 2 152.85 134.72 17.66 o 12 3 2 6.22 20.96 16.05 o 13 3 2 207.81 216.63 16.22 o 14 3 2 0.49 8.10 16.30 o 15 3 2 138.49 143.98 16.15 o 16 3 2 18.36 12.00 17.33 o -17 4 2 14.33 6.76 17.03 o -16 4 2 73.08 77.01 17.11 o -15 4 2 93.18 71.65 17.78 o -14 4 2 4.76 5.59 15.98 o -13 4 2 127.02 104.62 16.18 o -12 4 2 358.47 369.00 16.58 o -11 4 2 106.98 113.57 15.72 o -10 4 2 81.13 81.03 17.49 o -9 4 2 3.96 13.93 17.80 o -8 4 2 14.37 30.99 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